Document LpQGdKq5mODmQmaBXd3GLnVdX

(conoco) Interoffice Communication i. * i\ / to . J. W. Leigh From T. J. Mihalcik Date May 18, 1981 Subject NPSES PERMIT APPLICATION A111 fen _____ j. Attached is a copy of the NPDES Permit application filled out by Anne Daubney. Would you please review the attached application and phone any comments to me by May 22, 1981. Tom Mihalcik jw Encs CC! IFW AJN DTE Brad Raffle, Houston K. Cj/flunt, Ponca City C. R. Hampton, Denver 000002606 MCD Please print or type in the unshaded areas only. ERA l.o. NUMBER (copy from item L of Form l) LAD990683716 Form Approved OMB No. 158-R0173 FORM ZC vvEPA NPDES O.S. ENVIRONMENTAL. PROTECTION AGENCY APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURAL OPERATIONS Consolidated Permits Program I. OUTFALL LOCATION For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. X.GUTFAlL NUMBER (list) p. LATITUDE 1. Bit. X. MIN. i. sec. C. LONGITUDE t. DBG. 2. MIN. 3. SEC. ---------- D. receiving water (name; ............. 001 '30 14 18 93 16 40 Bayou Verdine | 002 30 14 25 93 16 40 Bayou Verdine 003 30 14 23 93 15 26 Unnamed Ditch to Calcasieu River II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flowt between intakes, operations, treatment units, and outfalls. If a water balance cannot be determined te.g., ior certain mining activities), provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures. B. For each outfall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if necessary. I.OUT* FALL NO flirt) 2. OPERATIONIS) CONTRIBUTING FLOW I. OPERATION (list) unitt)b. AVERAGE FLOW finciude 3. TREATMENT a. DESCRIPTION b. LIST COOES FROM TABLE 2C*1 Desalters 138,000 lb/hr 001 Coker Blowdown Pond 25,000 lb/hr See Attachment C Ballast and Crude Tank Draw } 15,000 lb/hr 1 / Misc. Users (See Attach. B) 48,000 lb/hr Cooling Twr Filter Backwash 18,500 lb/hr 1j 001 Boiler Blowdown Water 105F Pit Overflow 102,100 lb/hr 169,800 lb/hr See Attachment C I : Cooling Twr Blowdown Water 181,500 lb/hr 001 Sanitary Sewer 10,000 lb/hr See Attachment C Stormwater Runoff 002 From Process Area 1 42,800 lb/hr Sedimentation 1-V 002 37 Stormwater Runoff From Tank Farm Area 102,000 lb/hr None - _ OFFICIAL. USE ONLY (effluent guidelines tub-categonei/ EPA Form 3510-2C (6-801 PAGE 1 OF 4 lO00267 r\C tfCD ov- ^ / C ----r' | ! 1 CONTINUE ON REVERSE CON": VxJUED f ROM THE FRONT C. Except for storm runoff, leeks, or spills, are any of the discharges described in Items ll-A or 8 intermittent or seasonal? Q^yes (complete the following table) 2}no (go to Section III) ! 3. FREQUENCY 4. FLOW 1. OUTFALL NUMBER (list) 2. OPERATION^ CONTRIBUTING FLOW (list) a. DAYS PER WEEK (specify average) b. MONTHS PER YEAR (specify average) a. FLOW RATE (in mgdi b. TOTAL. VOLUME (specify with unite) *. MAXIMUM DAILY C DUR ATION (in dayi) III. MAXIMUM PRODUCTION. A. Ooes an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility? [X] yes (complete Item HLB) []no (to to Section IV) 8. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)? yes (complete Item III C) NO (go to Section IV) C. If you answered "Yes" to Item lll-B, list the quantity which represents an actual measurement of your maximum level of production, expressed in the terms and units used in the applicable effluent guideline, and indicate the affected outfalls. a. QUANTITY PCN DAY 161.8 b. UNITS 0^ MIklUl 1,000 BBL 1. MAXIMUM QUANTITY C. OICRATION, NODUCT, MATERIAL, ETC, (Specify) Refining Crude Oil 2. AFFECTED OUTFALLS (list &utfoil numbers) 001, 002,,003 / Fee IV. IMPROVEMENTS . A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operation of wastewater treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions. Q yes (complete the following table) j ^O (go to Item IV-B) 1. IDENTIFICATION OF CONDITION, 2. AFFECTED OUTFALLS AGREEMENT, ETC. a. no. b. SOURCE or DISCHARGE 3. BRIEF DESCRIPTION OF PROJECT 4. FINAL COM PLIANCE DATE 6. RE QUIRED b. PRO JECTED T- ooooo. 608 B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your discharges/ you now have underway or wnicn you plan. Indicate wnetner each program'is now underway or planned, and indicate your actual or fanned schedules for construction. ` X"Jmark if description of additional control programs is attached EPA Form 3510-2C (6-80) PAGE 2 OF 4 CONTINUE ON PAGE 3 era i.o. number (copy from item i of Form h | CONTINUED FROM PAGE 2 LAD990683716 j V. INTAKE ANO EFFLUENT CHARACTERISTICS_ Form ADoroved OMB No. 158-R0173 A, B,&C: See instructions before proceeding -- Complete one set of tables for each outfall -- Annotate the outfall number in the space provided. NOTE: Tables V-A, V-B, and V-C are included on separate sheets numbered V-1 through V-9. D. Use the space below to list any of the pollutants listed in/Table 2c-3/of the instructions, which you know or have reason to believe is discharged or may be ; discharged from any outfall. For every pollutant you listTuriefly describe the reasons you believe it to be present and report any analytical data in vcur . possession. 1 . POLLUTENT 2. SOURCE t . POLLUTANT 2. SOURCE Cyclohexane Xylene Napthenic Acid j, ' ^ * ' All three of these substances are present in the products from the reformer unit. It is therefore possible that at times, these may be found in the process wastewaters as a result . of upsets. Jr-- i \ VI. POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS A. Is any pollutant listed in Item V*C a substance or a component of a substance which you do or expect that you will over the next 5 years use or manufacture as an intermediate or final product or byproduct? *- Qyes (list all such pollutants below) 3 NO (go to Item VIB) B. Are your operations such that your raw materials, processes, or products can reasonably be expected to vary so that your discharges of pollutants may during the next 5 years exceed two times the maximum values reported in Item V? QYES (complete Item VI-C below) [3NO (go to Section VII) C. If you answered "Yes" to Item Vl-B, explain below and describe in detail the sources and expected levels of such pollutants which you anticipate will be discharged from each outfall over the next 5 years, to the best of your ability at this time. Continue on additional sheets if you need more space. MCD 000002609 EPA Form 3510-2C 16-801 PAGE 3 OF 4 CONTINUE ON REVERSE ONTINUED cROM THE FRONT /II. BIOLOGICAL TOXICITY TESTING DATA Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on < receiving water in relation to your discharge within the iBst 3 years? yes (iden tify the testfs) and describe their purposes below) Xno (go to Section VII!) - r. / / '> 'jo rill.CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? yes (list the name, address, and telephone number of, and pollutants analyzed by, each such laboratory or firm below) A. NAME a. ADDRESS rXiMQ (go to Section IX) c:telephbwe (area code & no ) D. PbLLClYANTS ANALYZED __________ Ml__________ MCD 000002610 X.certification a f certify under penalty of law that i have personally examined and am familiar with the information submitted in this application and all attachments and that, based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the information is true, accurate and complete, i am aware that there are significant penalties for submitting false information, including the oossibiiity of fine and imprisonment. \. name & OFFICIAL title (type or print) B. PHONE NO. (area code & no.) C.JIGNATURE D. DATE SIGNED fH . 'I 1 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS O N LY . You may report some or all of this inform ation on separate sheets {use the same form at) instead o f com pleting these pages. SEE INSTRUCTIO NS. EPA I.D . n u m b e r (copy fro m Item 1 o f Form I) i AnQQOfsft 17 1fi Form Approved OMB No. 158 R0173 EPA Form 3510-2C (6-80) PAGE V -t CONTINUE ON REVERSE (o p tio n a l) j lx N O . O F A N A L YSES fTT CONCENTRATION , 5. IN T A K E o o U< g |S> S e> < a .t cr oa nt icoenn b . M A S S 4. U N IT S ! --------------------------------1 ppm d. N O . O F A N A L YSES V A LU E Y ) 3. E F F L U E N T A le D o 30 a tla i fU aMv hi 3 J < > mw < I eU CtS S i! 0Z Ss 0 z 0J u --"o0uK<CHZazi 1 0ts<f1i 0bz 130 CM CM On CO vO O CM CO XXX 9 zr 20 O CO ITEM V-B CON JED FROM FRONT 232 8 .5 2.15 37 ppm lb s / d i ppm ! j i i jj i j ! i i | i i : i i i i j j 1 PPm ppm ppm mdd mdd mdd mdd & & i CL a OJ a i i - T--1 pH -H -1 -1 p-H - - 38 ppm lb s / d .. i 0.286 CM O o vO O. 1 i-- 026^2 OOOO tfCD O On Q CO o V0 CM X -4 0 1 XX XXXX HX X CO 6 _ e_ 3 o i _n H*,,co 5* C Wl CD a cc --<--r c<(Nw0 c/i cc 30 <C <0V) CN <s ok! i- o o CO S* c CT --2 c<ot 1 2 *n o 5 * rj o? O-- C 25' Ec i-2 SC EPA Form 3510 2C 16-80) PAGE V-2 CONTINUE ON PAGE V - 3.S-S c 4> > t"i *o* .2 m o. C ^co - 2 g oo. oSS 8SS = 75 *4 aai S| c 3 go. S ^ g i o2 s o t; J3 s . -o cm " q. EScoE )r P co O 101 8 g > 2vci U^, .> s_o| 0==) ^CO NTINUED FROM PAGE 3 OF FORM Z - C LAD9906837 16 1Form Approved OMB No. 158-80173 PART C - If you for. M colum to bel suits c See in TM <3 C,*;" <0; _ -- -m ^ CN " <3 2 || s i *2 S3 o w 1 oZE o2 i*- j = V c a j _ 0 c 2 o gL |o? 2= 8 is -- 2 Z 1.e'S . w0> 5 <o :ewater, refer to Table 2c-2 in the instructio ly to your industry and for A L L toxic metals nd non--requiredGC/MS fractions), mark " > >u believe to be absent. If you mark either c seven pages to this part; please review each c. = "&Q*?> 1. P O LLU TA N T AND CAS NUMBER SjiiSo N M ARK k -5 2 a i 'i11CONCENTRATION1 3J< < >2 >J < 0 u J3 Hi u z < 2 5 _z s< at? r k. si lil rto ''Z m 2i :o lb <* J D * < 2 3 J < > H Z Id u (J u y z 0 0 J --'Z u 0z tN i K z 0 St 0-s It* M < 2 J < > 3 LJ V) H D ct N O .O F ANAL YSES a. C O N C E N TR A TIO N b MASS 1 1 A Va.E LROANGCI i E TVEARLMU E --> SU Ki oZu zc 2 in 2 ft. m< id 2 < 32 E^|3-g s *= S -g 5 73 m t w O co c w ts -g c &s b. N O .O F 1 ANAL YSES X< V) Ufcl ,K z > 0. LB------ 1 WW.'.t jJS <tf 0 UJ* -i O z _i H o H z < X 1M. A n tim o n y , T o ta l <7440-36-0) X ppm 23 'w' 2 a nT Q Q Z < 2> _5 u S CO 8 < H UJ 2 o2 o o " o 1- i'f? o co CO < 5^ CN C- X r 5 .2 6 =^ 0^ CD --aj 5o OH (hJA (3A Id C Id & o(A Id Q X to Al i co hIc <0 0 C 'n-.O-5S CN u c -- 5 <0 ^.9m 0^ 6 0 CO 4M . C adm ium , T o ta l (7440 43-9) 5M . C hrom ium , T otal (7440-47-3) 7M. Lead, Total (7439-97 6) 8M . M ercury, Total (7439-97-d) 9M . N ickel. Total (7440 02 0) 10M . Selenium , Total (7782-49-2) 11M. S ilver, T otal (7440-22 4) 12M. T hallium , Total (7440 28 0) 13M. Z inc, T o ta l (7440-66-6) 14M . C yanide, Total (57-12-5) 15M . Phenol*, T o ta l | DIOXIN EPA Form 3510-2C (6-80) "o ~ H0 _ X X X X X X XX X X X X r> O O O vf Q 2 7S"| Q 2 N D (4) 0.57 8 .6 0.061 0 .1 0.25 ! 3 .7 L i ______ 0.173 2.654 N D (4) r-H c0n0 - - - ppm lb s /d ppm ppm ppm 90*0 oooVJ CD J02e 13 *--4 *--4 m A s-/ Q Z 0 .3 6 0 .0 5 8 ^--4 0.025 0.031 0 .4 7 1 0 .0 2 3 0.025 0.382 38 ppm ppm ppm lb s /d PAGE V-3 CONTINUE ON REVERSE ft 0 r ft o 0 2 i ij X X X X |X I X X X fC O N H N U E D ,F P Q M THE1 RONT 1. P O L L U T A N T j AND CAS NUMBER 2. M A R K *X ` sd J a. M A X IM U M D A IL Y V A L U E s VI> n 0 f2t 22H_--. > 0 2 {? r ejj;; Dvr: tj-CT (if available) -|G C /M S FR AC TIO N V O L A T IL E COMPOUNDS IV . A crolein (107 0 2 8 ) 1 ft 0 f2t "! 2 X<_ >H 0W 2 1b. 1 M A X IM(Uif Ma v a3i0la Db lAe )Y VALUE m n ** r s c m M z -i 2V. A crylo n itrile (107-13-1) X zz2 oo 4> 4>s-/ V--* 3< 5? F.J = A 3 O 4 V . Ris (C h lo ro m cth vl) Ether (542-88 1) X 1 | ND(4) ND(4) !s-<| a< itO 95 n K3 CD |Uft b! w " ; Cl -- S NJ 9 "! "i O 3 7V. C hlorobenzene (108 90 7) ND(4) 2z a x--\ /-N 1 ~ U CD S3 O ^ ^3 o CD 3 -2 $ ''So to3 9. Os o> *m If aa 3AN 39 Xx XXX XX X X i1 1 zz a /--s /-N P- P* V_f 1 0) ^ 1 01 ! ?O co y .0 _0 3 9V . C hloroethane (75 00-3) 10V . 2 C hloroe th ylvin yl Ether (110 75 8) 12V. D ichlorobro m o m ethane (75-27-4) 13V. D lchlorod if luorom ethane (75-71-8) 1 4 V . 1,1 D ic h lo ro ethane (75-34-3) 15 V . 1,2 -D ich lo ro ethane (107-06-2) 16V . 1,1 -D ic h lo ro ethylene (75-35-4) 17V . 1,2 D ic h lo ro propano (78-87 5) 18V. 1,2-D ichlorop ro p y le n e (542 75-6) X X 20V. M ethyl B rom ide (74-83-9) 21V. M ethyl C hloride (74 87 3) EPA Form 3510-2C (6-80) ND(4) ND(4) ND(4) | ND(4) ND(4) ND(4) ND(4) ND(4) ND(4) ND(4) ND(4 ) OOo *'T9Z 00 10W PAGE V-4 n 2-- H" 2X 0 >4 ef 0 2 s 12 j 1 i j H-* M j -- - I--* ! i 1 i I > < wM > r c w *-- >s | d. N O . OF ANAL YSES 4. U N ITS b MASS | i > <9 2r 0? PI**' 5. IN T A K E {o p tio n a l/ | 2 * r> ?S 2o * _ 1 -r 1 an >0 ~rz 1? | i 1 i )-- A i 1 i> ! 1 ! i !1 !j !1 ij !! ii | ji 1 1 i j 1 i !i :1 ! i i i i !! t--* | --* 1-- I--- t-- j ! iJ j ,j i - )--* CONTINUE ON PAGE V-5 I1 >m m o p* o s zp tftp o ' T| * 2 r> < UJ 2 aN < a S o e U. Q cy 2 Z P 2 O o UiCOO b0 6 CN N*OlD . wo X X X X X X XX XX X i>l . t ' 2:5 * oS`. 1. P O L L U T A N T AND CAS NUMBER | | a. M A X IM U M D A IL Y V A L U E | fftt < 2 z 0 < -**C --z u z 0 g jt ;z*jS:uo (if aoatlablf) -[G C/M S FR AC TIO N V O L A T IL E COMPOUNDS (c o n tin u e d ) 1 22V . M ethylene C hloride (75-09-2) ND(4) w o zZ XXX X X X X X X X a 9 b ".c N . >Sd, S5t 24V . T etrachloroethylene (127-18-4) ND(4) 9 c 9_ _2 cn r,~CcQd >8 <inN H-- 26V . 1.2-TransD ichloroethylene (156 60-5) 27V . 1,1,1-T rlc h lo ro e th a n e (71-55-6) 28V . 1,1,2-T rlc h lo ro e th a n e (79-00 5) i , | ! 29V. T rich lo ro ethylene (79-01-6) Q ND(4) ND(4) ND(4) w 'o 1 | 30V . TrichlorO fluorom ethane (75-69 4) ~T <1 z 31V. V in yl C hloride (75-01*4) -|G C/M S F R /^C T ipN A C ID COMPOUNDS 1A. 2 C hloropheno (95 57-8) ND(4) /*--s --\ | 2A. 2,4 D ichloro phenol (120-83 2) ND(4) 3A. 2,4 D im ethylphenol (105-67-9) ND(4) a z 4A . 4,6 D ln itro OC resol (5 3 4 -5 2 1) /--s <r N-/ Q Z 5A. 2,4 D im trophenol (51 28 5) 6A. 2-N itrophenol (8 8 7 5 51 7A. 4-N itrophenol (100-02-7) N D (4 ) 6u oU0 z. in (J ^ a. o 9A. Pentachlorophenol (87-86-5) 10A .P henol (108-95 2) ND(4) ND(4) /-S "-T 'd* V-/ W Oa zz oVooooN B61 MCD au 0 Sz UJ U < * --2 z So 0 3d < Sw a O<o <*S 3. E F F L U E N T PAC. >2 M* < J < 3 u e Ul 3 2 3 Z J _fa-H <o iHk-o' 13 0 i 0 *, v0 E ftp a-1 ?TO 300 OsD jO 'i 1z3^3 d < a. UJ (j u u g z 0 z 0 J 0 --z _K b ff= < z 0 l! c-Jt u >5 < J < 3 - i-H i UJ -- | 1 | j i ! i I 1 i i *--t1 p--i i r--b *--4 ii i i !! i ! -1 j ! ,! 1 ! ;j |i i !j d. N O . O F ANAL* YSES Zz wu0ZH 0< U2 .K 4. U N IT S b. M A S S 1 11 m bi ]5 . I N T A K E (o p tio n a l) ' b. N O . O F ANAL YSES a 2 TJ j` :| - h Z 3* wU C2 Ud *p 0< !ij | i CQ 5 o 'dQSj ! !i :! ! ! * ! !; 1 d ; 1I pb ! !: ! 1 X X X X X X > > > > i i * X X X X X X X 1 X X > /-s /*> <r < ^w< G> a Q P 55 Z 2 z 0 X < __ 2 wZ IV u z 0 u MCD 00(D002!616 00 < 2 C O N T IN U E D FROIV c F R O N T z 0 X < ex --z z 0 u oj SgiiSc "*3t U)K ^ <u 2 urn .2 02 ? Z3 5 <2 5 I8. M A X I M U M D A I L Y V A L U E | ] b. M ____ A X I M OUfMa v a3i0la Do lAe iY VALUE i] c l o n g -|GC/M S FRACTIO N B A S E /N E U T R A L COMPOUNDS | IB . Acenaphthene (83-32-9) o 55 0 C 5 *-> c 4> (0 U Ci -i 3B. A nthracene (120-12-7) ND(4) ND(4) * e v r-s CQ CO d"Sa >w /--< /-- < Qcd G 222 5B. Benzo (a) A n th ra c e n e (56 55-3) 6B . Benzo (a) Pyrene (50-32-8) < 6M 9 c c9 c QQ ^ "Ig c v_ * 2 <* V. G 2 I 8 B . B enzo (g h i) I Perylene 1 (191-24-2) 9B. Benzo (k) F lu o ra n th e n e (207-08-9) 10B. Bis (2-C hloroe th o xy) M ethane (111-911) < . c 2 z 0 < -- z k z J0 m 2 m 2 v a lu e tt N O . O F A N A L YSES a. C O N C E N T R A T IO N 1 b. M A S S j < / v /- \ / \ r ? ? <t v. aa sz 1 r- 4 --< 6s o ~ 5 -c fia o := s 5 u "IS ft3 2uj* S1-1N 'if' CD V |8 CD CO m * gn *5s 9 5e .2 0. J, CO H _ n ^ i-H 9 C >01 uo CD N 14B. 4 Brom ophenyi Phenyl Ether (101-55-3) 15B. B utyl Benzyl P hthalate (85-68-7) 16B. 2-C hloronaphthatene (91-58 7) 17B. 4 C hlorophenyl Phenyl Ether (7005-72-3) 19B. D ibenzo (o.h) A nthracene (53 70 3) 21 B. 1.3 O ichloro benzene (541-73-1] V ND(4) ND(4) ND(4) ND(4) ND(4) -- 6p 56u> .a uS Q ff> CN ' cffl 22 O9 (N J3 - o o w ft < z vZ UC u z; > < * [ ! | h N O .O F ANAL VSES du * k dijS z 0 u < *--s --z j 8. M A X IM U M D A IL Y V A L U E BA SE/NEUTRAL COMPOUNDS (co n tin u e d ) z z c < r -lz z 0 u 00 I 3. E F F L U E N T 1 b. 1 M A X I M(Ui f M a v a3 i0l a DAY b le ) VALUE w < 2 22 B. 1 .4 -D ich lo ro benzene (106-46-7; X ND(4) 1 23B . 3,3' D ichlorob e n z id in e (91-94-1) 24B. D ie th yl P hthalate (84-66 2) ^ j 25B. D im e th yl P hthalate (131-113) 26B. Di N -B utyl P hthalate (84-74-2) X X X X W o ss ND(4) ND(4) 27B. 2,4-D initrotoluene (121-14-2) 28B . 2,G -O initrotoiuene (606-20-2) 29B. Di N O ctyl P hthalate (117-84 0) 30B . 1,2-D iphenylh yd ra zin o (as A zobenzene) (122-66-7 X X X X ND(4) .J ND(4) J ND(4) ND(4) <7 V-- zQ i 2 3 1 B. F luoranthene (206 44 0) *L.. 32B. Fluorone (8 6 -7 3 7) X X 1 i /*> !1 | ND(4) XX 9C o i ?~ $ I "o f* D 0 O O --- 34B. Hexa c h lo ro b u ta d ie n e (87-68-3) 35B. H exachloroc y c lo p e n ta d ie n e (77-47-4) 36B. H exachloroethane (67-72-1) ND(4) ND(4) ND(4) -- XXX X e9c b TS c2 -e^9 2"S r> CC M('D C 3 8 B. laophorone (78-59-1) ND(4) ND(4) ooo 9C 9 .C an 26 CD. 8a C4 ^ 406. N itrobenzene (98-95-3) 41 B. N -N itro sod im e th y lam ina (62-75 9) X X ND(4) ND(4) 026 1 ( ' N /*--v <7 QQ ZZ XX 59 o-H tE2-r' z s! sziS EPA Form 3r510-2C (6-80) PAGE V-7 "-co *<x> Ip z ! 1 1 i ! i ! 1 ! i - w u z 0 z 0 J 0 --z S5 __ <X Z 0 a !i 1 eU CLi ii >2 j ! *A J < 1 1 3 i U j1 jI 1 1 ~| ! > C< 4. U N ITS d NO. OF ANAL YSES a. C O N C E N TR A TIO N b. M ASS 5. IN T A K E (optional) | oi >L VT EARL MU E ____ b N O .O F ANAL M 4s YSES Z iZ v0 < e lZ - || !i Jj 1 ! ii i i i i 1 *--1 "H - - "H J i 1 ij i I - ;; i1 |j ! ! -- COM ( l'; t 'F OM Itr: v'tlU IE C O N TIN U E ON PAGE V 9 0 J*fl n <W 0T y4 <vrt o o >j C , <1 : si 2h 0< OK 0 Jvi A0 2<^W T4> PAG E V -8 MCD 000002618 5 oo Q Z D O c. o2 u _l <tt u* TT" D UJ Z (UAJ ^^-73 0} H Z < WE i H r- <f O -- az za zQ az zQ a z za zo a a O Q Cl Q 2222 2 XX - oo ^ en C flrj ^cn X XX XX a a-- s! l QQ~ . CT * in in 2.: ^r* CO -- O O Q- - co ** Tf If) 2*'CnM C) *~ b a. . in O 610 UO a. Ip. cm . CM w3 --3 o ~ V *r* -to -- a. T5 * S5~ EPA Form 351(F2C (6-80) CONTINUED FROM THE F tloN T . NUMBER ( fU)99068: a te r th C 4J 4J (Q xXJ. XJ 0 co C 0) 03 co (0 3 o 0) 0 T5 EPA Form 3510-2C (6-80) PAGE V-6 CONTINUE ON PAGE V-7 EPA Porm 3510-2C (6 80) PAG E V-7 CON T IH I IF O N R E V /F R ^F CONTINUE ON PAGE V-9 C - wft cv i*S^ CM O 3i o III: j -: v : z; - 2Z C! X h- z <t i: f- < u -J d pj z r 0<2 a. ?o z o o t3 . 2 csj.C CN -- LI L) _ ^ 5) ys ! O C3 ft 8- O CO o& .SJ- 'T U s_ o -- " 03 ^C. in "f^coo Ic tr (J r- * min Q r.m e (n 2; O o. z. (V r- Q- -- o M*- t3n *--- , 4, - T3 vf EPA Form 3510-2C (6-80) .Wiiilo r;voM m e r ik in t Form Approved OMB No. 158 R0173 k0. Jt o** *2 *;> 1 4 * u I* ; *< 5 _ H Z li z .r to "u Sf; *> C <J /I lo < 5 4. UNITS 3 EFFLUENT E P A I D . N U M B E R ( c o p y from Item 1 o f Form 1) [ O U T F A L L N U M B E R LAD990683716 002 Zj Z * 0< UK 0 w* j <2 iJy/>l f l> w JD >3 (Lvi >| s! z 0 < 0z 0 J 3s c u z 0 u u 3 >J< < 2 < o2 m0 55 * P X --z <J Iz c 2 | a. MAXIMUM DAILY VALUE | z 4 _a -z 2 Cc S 0 '2 0 X X CO loli c < -s;** u 2 to ;* ,, ''- 1!: aZz - LU a. 1 z< t/> (V T H tCfNt --r- CCNN _CN CD (N cb S COC*TOL 5oC?bN 0 irt cn ^ CcoNl' ^ ,-- 21P. PCB-1232 (11141-16-5) 23P. PCB-1260 (11096-82-5) ?4P. PCB-1016 (12674 11-2) * XX X 3CN _<o CD CaNt 0O* ff<x*0 CN w T3 O J2 LJ V B o> X Li 0 < a. >< X oop ( o ca> fON 6 AO CO * hOx in cJ>. e a.'8 o $2 X CO o 0) 5 ai O T5 pH 44 B 3 03 B H H c 0) H Ue 0) c 0) LJ 4= 4J c a> c -c <0 P*- r-- iJ CP rH>N P 03 0) 0 3 Li Li O CO 3 Qi CUO 4 60 pi U Co oC CL o H e Li a) o CO 0) Li CO L Li 4J 3C 03 <D 03 cd Qi O c cd St 60 ow 03 <D H C JJ H V |4 B 0) T3 LJ 0) cO U 0) LJ CO s u CL 03 0) U LJ CO 7C (8-801 I'A O I >/-l CONTINUE ON REVERSE CONTINUE ON PAGE V OOj 5 . IN T A K E (optional) " j MO. OF ANAL YSES | 1 4. U N IT S V U4 *3 s s z0 Ss p< > < z T.1*- o 0z u VmI < 2 A zz w n$u o- u. Ojw 6<S *.< S a CL y 3 J < < >J & * EE a CL CL CL - CLS a. BEEB cl CL CL EE CL CL E CL a. CL CL CL CL CL CL CL pH pH -1 -- -1 ^h pH pH rTMH H 1 PAGE V-2 J. E F F LU E N T *z 0 <K 0 z 0 J --zWV 0z yu y 3 J m << >s >*_ CO 21 no z 55 0 p r2 CM X < ~z W u 5 z0 au u DJ < mm< >I n&o $*>c iO > J < 0 2 0z 3 2 __ K X C-->i < 2 u 0oz co rH /--s /*--s opH CO CO CO CO <o w V-/ IT) ON Q Z CO CM 00 <* Q in Z o CM h* ON pH a z <r CO a z z Ooo O o o | ; X 5.$ - jis`8 a w Ktt < X X X X XX X X X X X X XX X X X X X X iL > n t i 3 2 * n o n_-|-Ox * 3zOS i 2.Z, m Ui-J<22 u si o? 2- ^5 CD 55 r6 !|S 8^ SCS *-,3 ua a* o a6 a <2 a: -- o 4) U CD 5 E .2 'c3 cl 2 53 E3 6 o hoc , * <N -- (N 5 2 = 08 *5 VJ j -- >2 O If) <* --v ^ tr'in :C u t/>uj n El: C -- e" _ u t 3 E 3 - o </> s? c oKw p2c "o -n 5 2 SJ at- I- CO F-v <N 0* Q "5 3 CO p* * . a S _ 0? o 0n1 i; n . r- -- E^ 5 Jg c o> 2?_do) 5 *r'K^ s B ^ tf> (0 -- o"? E to 2 ? GT> c ^5 - oi 2-6 *0 X - w u. M olybdenum , T o ta l (7439-98-7) EPA Form 3510-2C (6-80) b NO Oh ANAL- ' Y5ES 5M . C hrom ium , T otal {7440 47-3) j 7M. Lend, Total (7439-97 6) 8M . M ercury, Total (7439 97 6) 9M . N ickel. T otal (7440 02-0) 1 10M . S elenium , 1 Total (7782 49 2) 1 1M. S ilver, T o ta l (7 4 4 0 -2 2 -4 ) 12M . T h a llium , T o ta l (7440-28 0) 13M . Zinc, T otal (7 4 4 0 -6 6 -6 ) 1 4 M . C y a n id e , T o ta l (57 12 5) 15M . Phenols, T o ta l | D IO X IN 2 .3 ,7 ,8 -T e tra chlorodibenzo-P D io x in (1 7 6 4 01 G) EPA Form 3510-2C (6-80) 5 v? ^ C QJ -- 0) n O *- re o c t: ct v> <y i t b D O - ~ O c "o o 3 cO <: TM >% O 0) o .S - o | u s 25 S R t5.. 2 3 <3 o -23 Ot cl w > > c Cl 5 3 ,, - 2 7 >r C C a, c CJ > UJ re ^ c? r H 3 == .c JC o o - o CL CL^ ^5 c .c >-3 J! o c -- "R 3 2 TM o -= ro o > c ~ . 2 ~ -9 CN . -O (N a E ro 3 O 3 : - P re O ;S=nO -1 8 c > a. C O N C E N T R A T IO N *3 t. U 1LJ X < L.u VI < 2 z o2rjf jZ, z in jcu (C> uc 5: < uc in < <A 2 H D *T d. N O .O F ANAL YSES S 5. . E 3 u u> -- av c .i. o 3 i the instructio . L to x ic metals ions), mark " > u mark either c : review each ce E U a 2 3 Z J CO JO <O L. h 3 0 t rr o trt CN ^ 2 QJ 6 o '** -- o. CN **- </)... 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P O L L U T A N T AND CAS NUMBER O ct LL o UJ hz c O z0 < > c> JnS <r 0 c 0 co` r ^ c -J < <^ H LU 2 c (Q 0 h- U *" ciV-. 0an1 <0 fv E5 .2 6 -- XJ > XT C^ CC --fC` 20 0) Ern7 3? 0xj ^ Xj r<e -- u -0 20 "w o-- y- 4) 5- o o L U Oin <J 2 Csi -- re - 10 "I/- ppm CONTINUE ON REVERSE Ul h J 3 in Li E UJ 0 E O in Ul 0 X PAGE V-3 MCD 000002632 000002634 VIC'D ATTACHMENT B Miscellaneous uses are: Various water washes. Caustic system. Stormwater runoff that goes into the oily-water process sewer. Miscellaneous units contributing process wastewater are: Alkylation Unit P-P Reformer Unit P-F Debutanizer Unit No. 2 Crude Tower No. 3 Crude Tower FCC Unit Thermal Cracker Unit PBC Fractionation Unit Normal Paraffin Unit MCD 000002638 ATTACHMENT C The wastewater streams from the desalters, coker blowdown pond, ballast, crude tank draws, and the miscellaneous users are all receiving the following treatment steps: TREATMENT Description Code 1. API Separator 2. CPI Separator 3. Equalization Basin 4. Activated Sludge Unit 5. Process Lagoon 6. Dissolved Air Flotation XX XX 3-B 3-A 3-B 1-H The cooling tower blowdown water and the sanitary sewer streams both combine with the CPI Separator effluent of Step 2 of above and continues on through the remainder of the treatment steps. The cooling tower filter backwash, boiler blowdown water, and the 105F pit overflow streams all go through a sedimentation pond (1-V) then combine with the Activated Sludge Unit effluent and continues on through the remainder of the treatment steps. The size, flows, retention time, and ultimate disposal of any solids of each of the treatment units are shown in Table I. 000002639 Treatment Unit API Separator CPI Separator Equalization Basin Activated Sludge Unit Reaction Section Clarifier Process Lagoon Fire Water Pond Dissolved Air Flotation ATTACHMENT C (CONTINUED) TABLE I LAKE CHARLES REFINERY WASTEWATER TREATMENT UNITS Size, Gal 113,100 77,800 860,200 994,800 161,600 5,200,000 Flow Rate (Gpm) 452 Retention Time (Hours) 4 452 835 835 835 1,537.8 2.9 17 20 3.2 2.3 Ultimate Disposal of Solids Slop oil emulsion from the separators is removed by a contrac tor. Sludge is removed to a land farm owned by Conoco Inc. 1,600,000 79,100 521 1,537.8 2.1 0.8 Sludge is removed to a land farm owned by Conoco Inc. Mod 00002e40