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ARQ 6 - ISOC FEBRUARY 2003 SURFACE WATER MONITORING REPORT FOR WASHINGTON WORKS FACILITY AND LOCAL, LETART AND DRY RUN LANDFILLS WASHINGTON, WV ! Date: April 2003 Project No.: D6WW7423.01 19803400026 18983632.00028 CORPORATE REMEDIATION GROUP An Alliance between DuPont and URS Diamond Barley Mill Plaza, Building 27 Wilmington, Delaware 19805 000383 CONTAIN NO CBI WVDEP 17572 SutacaWate Monitoring Report Table of Contents TABLE OF CONTENTS 10 IMEOGUEHON. rrr mmr] 20 C8 Analytical REDOING... mm--_ 3.0 Washington WOrkS FACHY c.crmrnrnnsd 4.0 Loa! LAM wml} 5.0 LMI LANG cor 60 Dry RUN LANs] ET mms TABLES Table 10 Table2.0 C-8 in Surface Water-Washington Works Facility C-8 in Surface Wate--r Local Landfill | Table3.0 C-8 in Surface Water-- Letart Landfill Table40 C8 in Surface Water~ Dry Run Landfill Figure 1.0 Figure 11 Figure 12 Figure20 Figure2.1 Figure2.2 Figure3.0 Figure 3.1A Figure 3.1B Figure 40 Figure 4.1 FIGURES Site Location Map -- Washington Works Facility Surface Water Sample Location Map ~ Washington Works Facility C-8 Concentration Map February 2003 - Washington Works Facility Surface Water Site Location Map ~ Local Landfill Surface Water Sample Location Map ~ Local Landfill C-8 Concentration Map February 2003 ~ Local Landfill Outfalls Site Location Map~ Letart Landfill Surface Water Sample Location Map - Letart Landfill RL. 33 Stream and Brinker's Run Surface Water Sampling Locations -- Letart Landfill Site Location Map - Dry Run Surface Water Sample Location Map ~ Dry Run Landfill | TWEioRmSo 15.08 i 000384 `Surtace Water Monitoring Report Table of Contents Figure42 C-8 Concentration Map February 2003 ~ Dry Run Landfill Outclass Appendix A Appendix B Appendix C Appendix D Appendix E Appendix F APPENDICES Laboratory Analytical Data Reports ~ Washington Works Facility Chain-of-Custody Records ~ Washington Works Facility Laboratory Analytical Data Reports ~ Local Landfill Chain-of-Custody Records ~ Local Landfill Laboratory Analytical Data Reports ~ Dry Run Landfill Chain-of-Custody Records ~ Dry Run Landfill Wikninglon, DE 000385 `Suraca Wate Mondor Report. Introduction 1.0 INTRODUCTION A multi-media consent order (Order No. GWR-2001-019) was entered into between the West Virginia Department of Environmental Protection (WVDEP), the West Virginia DepartmentofHealth and Human Resources -- Bureau for Public Health (WVDHHRBPH) and DuPont on November 15, 2001 (Consent Order). The Consent Order identified a seriesof requirements and tasks to be performed by the parties to determine `whether there has been an impact on human health and the environment as a result of releasesofammonium perfluorooctanoate (C-), CAS Number 3825-26-1, to the environment from DuPont operations at the Washington Works facility and the associated landfills (Local, Letart and Dry Run). `The Consent Order established the C-8 Groundwater Investigation Steering Team (GIST) to oversee investigations and activities that will be conducted to assess the presence and extent of C-8 in drinking water, groundwater, and surface water at and around the Washington Works facility and the Local, Letart and Dry Run Landfills. An additional component of the Consent Order relates to the West Virginia National Pollutant Discharge Elimination System (WV NPDES) permit sampling requirements. In this portionof the Consent Order, specific outfalls and outlets (outfalls) are to be sampled monthly for C-8 by DuPont. Pursuant to Attachment Aof the Consent Order, three tasks were performed by DuPont | and evaluated by the GIST, Tasks A, B, and C. Task A: Groundwater Use and Well Survey/Groundwater Monitoring was completed (DuPont, 2002a; 2002b). Task B: AssessmentofExisting Groundwater and Surface Water Monitoring Data included compiling of historical C-8 data, monitoring all wells at the landfills and developing a Groundwater Monitoring Plan (GMP) for the Washington Works facility. The first part of the task, the historical C-8 data compilation report was submitted to the GIST for evaluation (DuPont, 2002). The second part of this task, monitoring C-8 in groundwater atthe landills, began in December 2001, and was performed monthly for four months and quarterly thereafier. The third partofthe task, developing a GMP for the Washington Works facility, was submitted to the GIST (DuPont, 2002d). Groundwater sampling at the Washington Works facility began in January 2002, and was conducted monthly for four months and quarterly thereafler. Task C: Plume Identification/Groundwater Assessment was also completed (DuPont 2003). This report presents the resultsofthe monthly C-8 surface water sampling that was performed in February 2003 at the Washington Works facility, and the Local, and Dry Run Landfills. Monthly C- surface water sampling at the Letart Landfill was not conducted in February 2003 because an ice storm downed trees, blocking the access road to the landfill VimroonRo0s8oc Aor 15.00 000356 7 S Surtacu eWatelr Moo ntornc g Repoort WalerMontCoC88gAAnnaaR llyyttie iccaallpRReeppo oorrttn iinngg 2.0 C-8 ANALYTICAL REPORTING hTahveeacnhalayntgiecadlomveetrhtoidm,e.mePtrhioordtdoet1e9c9t1i,onDuliPmoitn,tapnedrflaobromreadtoCr-y8utainlailzyesdisfoartCt-h8e DanuaPloynsits IEnxvpeesrtiimgeantitoanlwSatastcioonndiuncWtield,mitnhgetaonna,lyDseilsawwaarse.conItnra1c9t9e1d,twohtehne CthHe;RMHCiRllALVaebroifriactaotriyonin DMeotnetcgtoomre(rGyC,-AElCaDba)mbaa.seBdoatnhallyatbiscaulsmeedtahoGdaswiCthhrodmeatetcotgiroanphliym/iEtlsefcotrrCo-n8Cathpatturraenged from0.1 0 1.0 ug/L cCeHa;seMdHiolpelractoinodn.uctTehdeCC--88anaanlaylsytiiscfaolrwDourPkownatsinttroantshfeerfraleldotfo 1L9a9nc8awshteernLtahbeorlaatboorriaetso,ry uLsaincnagsGteCr-, EPCA,DifnorMaDrucPhon1t99u9n.tilLOacntcaosbteerr2L0a0b1o,rawthoerinedsecvoenltoipnmueednttoacnodntdeuscttinCg-w8asanalysis lcoocmaptleedtiendSotnatae Cnoelwleagnea,lyPtAic)althmaettuhtioldizdeesvLeilqoupieddCbhyroEmxaytgoegnrRaepsheya/rTcah,ndIencm.M(aEsxsygen; | aSnpaelcytsriosmientwrayt(eLrCi/nMNSo/MvSe)m.berDu2P0o01ntaanddopEtxeydgetnhewraesgucloanrtursaectoefdLtoC/peMrSf/orMmStfhoeraCn-a8lyses for DuPont. i EarxeyegveanluraetpeodrtfsoCr-p8rerceissuilotns bfoyrctohmeplaarbionrgattohrey frieeplldicsaatmeoplfeeraecshulftiteoldtshaemcpolrer.esTphoensdeinrgesults laboratory replicate result. | Q sIafmboptlherfeosrultthsataraenalleystsetihsacnotnhseidperarcetdictaolhqauvaentpiatsastieodntlhiemiptre(cPiQsLi)o,n ctrhieterreipalicate. Q cIfoonnseideorrebdottoh hreasvueltmseatrethbeeptrweeceinsioonnecraintderifaiivfe tthiemetswtohreePsuQlLts,dtihfeferrepblyiclaetses itshan the PQL. Q dIiffofneererdesbuyltaivsalleuses tlehsasntthhaenPtQheLPaQnLd,tthheeortehpelriciastneoti,s saanidd itfothheavtewmo erestuhlets acceptance criteria. Q I`fmebtotthhercersiutletrsiaairfetahteleraesltatfiivveepteirmceesntthdeifPfQeLre,nctehe(RrePpDl)icabteetiwseceonnstihedetrweod to have results is mleesasstuhraenmoerntesqudailvitode2d0%b.y tThehier aRvPerDageis.the absolute valueofthe differenceoftwo f`iWehlednsatmheplpereacnidsiloanbcrreitpelriicaatoeutrleisunletdsarbeopvoretaerdebmyett,heElxaybgoreantorreyp.orItfsctrhiteearivaerfaogreporfectihseion `awreheenxcoeneedereds,ulEtx(yfgreonm rtehpeosrtasmptlhee/hliagbhereroplfitchatee spaaimrp)lies aabnodvleabthreepPliQcLateanrdesuolntse.beFlionwal,lyt,he ErensvuilrtotnhmatenitsaalboDvaetatbhaesPeQ(LCSEDis)raenpodrtaerde.reCp-o8rtreedsualslsFCar-e14re3coforrdecdonisnitshteenCcoyrpwoirtahte historical results. MAnSaalniaqluyostiosf aeraechusefdietlod sasasmepslseaciscuarlascoya.naTlhyezeMdSasraecmoavterriyx vsapliukee (mMuSs)t. falRlesbuelttwsoeefnt7h0e to WE-iB_m--aStHonR5do8cAer 15.03 000387 2 . S Surfau ce Watler Mo onincg Reo port WelrMovtogCR C--88AeAnnaalp lyyttiio ccaallt RReepp_ oorrtti_ inngg . m13a0x%i,muunmleasmsotuhnetsaumsepdletocosnpcieknetrfiaetlidosnaimspaltelseaisst5f0o0urugt/iLm.es the amount spiked. The AllalbodraattaorpyacSktaangdeasrgdeOnpeerraatetdinbgyPErxocyegdeunreasre(rSeOvPi)ewaendd idna-thaouussaebifloirtyc,oumspilniganthceecwhietchkltihset pErxoyvgiednedhainvethbeeQenAPgPen.erRaetseudlitnsocfotmhpeliiann-cheouwsiethretvhieelwabionrdaitcoartye SthOaPt,dawtiathrefpeorwteexdcbeyptions jausdngoetdedusianbtlheefionrdtihveidpuuarlproesveisoefwtshuemmparroijeesct.. All data reported by Exygen have been `FWEiBmiSngiHonR,dDoEc Ap. 15.03 -- - 5 3 000358 `S Surfacu e Wateb r Monitc oring Roeportwstrlooto WaWsahswhiinngagttoonR nWWoore rkkssFpaFcaciilt liittyy 3.0 WASHINGTON WORKS FACILITY Figure 1.0 shows the locationof the Washington Works facility. OnFebruary 27, 2003, six outfalls were sampled for outfalls collect process water C-8 and (001, 002, 003, 005, 007, and 105). stormwater runoff. No changes to Allofthese. routine sampling protocols or other observations were recorded in the field notes during this sampling event. Monthly samplingofthese outfalls is required by the Consent Order and WV NPDES permit No. WV0001279. The locations ofthese outfalls are shown in Figure 1.1 i `Table 1.0 provides the C-8 analytical results for surface water. For each sampling point listed in the table, historical Figure 1.2 presents the C-8 data is summarized with the most concentration map for the outfalls recent results listed first. sampled in February. Laboratory analytical data reports and the Chain-of-Custody records are included in Appendix A and B, respectively. | WFiemesstwonRe08 me 0--003--289-- `Surface Water Monitoring Report Local Landfill 4.0 LOCAL LANDFILL Figure 2.0 shows the locationofthe Local Landfill. Monthly sampling of five outfalls is required by the Consent Order and the WV NPDES permit No. WV0076538. These five outfalls collect stormwater runoff. Outfall 101 was sampled for C-8 on February 26, 2003. During the monthof February, outfalls 004(Old), 004(New), 005(01d)/SS1, and 005(New) were not sampled due to no-flow conditions. No changes to routine sampling protocols or other observations were recorded in the field notes during this sampling. event. The locationsof these five outfalls are shown in Figure 2.1. Table 2.0 presents the C-8 analytical results for the February surface water sample. The table includes the historic data available for each location sampled. The data are presented with the most recent data first. Figure 2.2 presents the C-8 concentration map for the outfalls sampled in February. Laboratory analytical data reports and Chain-of- Custody records are provided in Appendices C and D, respectively. i | Wimogo08n 000390 . Surtace Water Monitoring Report Letart Landfill 5.0 LETART LANDFILL Figure 3.0 presents the Letart Landfill location map. Monthly sampling of Outfalls 002 and 003 (both containing stormwater runoff) and Cap Runoff (which collects leachate and stormwater runoff) is required by the Consent Order. On February 28, 2003 an attempt to sample was made. However an ice storm downed trees that blocked the access road to the landfill. Therefore samples were not collected at any locations at the Letart Landfill. The location of Outfall 002, Outfall 003, and the Cap Runoff samples are shown in Figure 3.1. In Table 3.0 historical data is summarized with the most recent results listed first for each sampling point sted in the table. The locationof the Brinker's Run and the Rt. 33 Stream surface water sampling points are shown in Figure 3.1B for reference. i FWEirBigSioRn,dOoEc Agr. 15.03 000391 | `Stace Wate Moning Report Dry Run Landfill 6.0 DRY RUN LANDFILL F0i0g1u,r0e034,.0asnhdo0w0s4tihserleoqcuaitrieodnobfy tthhee DCronysRenutnOLradndefrilaln.dMWoVnthNlPyDsEaSmppleirnmgiotfNOou.tfalls NWVP0D0E7S62p4e4r.mit(NOou.tfaWlVl0000726i2s4a4r.eqHuiorweedvoeurt,falitlwsaasmpaltienmgploorcaartyiornealsocsattaitoendoifnOWutVfall 001 0a0nd4 ncoollleocntgesrtoerximswtsa)t.erOountlfya.llO0n01Fecoblrlueacrtys s26t,or2m0w0a3t,erOuatnfadllle0a0c1hatwea.sOsuatmfpallelsd.00D3uarnidng tNhoe mchoanntghesoftoFerboruutairnye,sOaumtpflailnlgs 0pr0o3toacnodls00or4owtehreer onbostesravmatpiloendsdwueeretorneoc-ofrldoewd icnontdhietifoinesl.d notes during this sampling shown in Figure 4.1. event. The locationsofthe surface water sampling points arc `Table 4.0 presents the C-8 `cach sampling point listed analytical results for the February surface water samples. in the table, historical data are summarized with the most For recent outfall results presented first. sampled in February. LFaibgourraet4o.r2yparneasleynttiscatlhdeaCt-a8recpoonrctesnatrnadtiCohnaimna-poff-oCrutshteody records are provided in Appendices E and F, respectively. { I ES T B E WaR R Ar115A 5.030 - 000. 77 Stace Wate Montarng Report References 7.0 REFERENCES DuPont. 2002a. One-Mile Radius Survey and C-8 Sampling Report and Ohio River Public Water Supply Sampling, DuPont Washington Works (December 2001- February 2002) January 2002. DuPont Corporate Remediation Group and URS Diamond. DuPont. 2002b. Two-Mile Radius Survey and C-8 Sampling, DuPont Washington Works Facility/Local Landfill, West Virginia (March-May 2002) August 2002. DuPont Corporate Remediation Group and URS Diamond. DuPont. 2002c. Compilationof Historical C-8 Data, DuPont Washington Works Main Plant and Landfills January 2002. DuPont Corporate Remediation Group and URS Diamond. DuPont. 2002d. Proposed Groundwater Monitoring Plan for Washington Works Facility Plant and Landfills January 2002. DuPont Corporate Remediation Group and URS Diamond. DuPont. 2003. C-8 Data Summary Report, Consent Order GWR-2001-019, DuPont i Washington Works Facility, and Local, Letart, and Dry Run Landfills January 2003. DuPont Corporate Remediation Group and URS Diamond. SmToEs go0nF ns 000393 7% Ne g5z 000394 TABLES 000395 - Table 1.0 `SummCa8ryionfSAunraflaycteicWaaltReersults: 4 DuPont W`aWsahsihnigntgtoonn,WoWrVks Facility SGUTwiETe607 T Zam w Gwcesegn || mmee eaes | 2 ome -- wes -- | ommwe [Com a wsem]|| [ww ee Te wa r| oe ss | CTRL omeemrTaam s ]| 7---- -- [ ossees Te a ass e m y||| oomw7ee--s7-- %e-- || | [epC wwee ema m aeesem|| | I7 ae -- -- p-- e -- -- | 7 Amme-- Te-- a s-- || 7 romeoser-- r a-- 2ms i-- || m eeeaem os ooswss||| [e1 mm m-- Toa -- ee-- | CIETS [ms semsses To e om se s||| wm om | 2 o7ne-- ---- -- we|n-- -- | [ ommee T m e ooe mmm||| a1 veee--a a-- s|-- || C [ ome erm T e atw emsm|| 1 -- E-- 000396 0415/03 1013 Table 1_0.doc `Summary ofTaAbnlaley1t.i0cal Results: C8 in Surface Water DuPont WWaasshhiinnggttoonn,WoWrVks Facility [sam CUTPe ALL O35 To [m Cm zaes [C e odw ee -- on --| [me7 m-- Tm -- -- ] [o7 [ nen-- am er-- e [Cwm 7eg----0] -- I [ ommr e-- a -- w epey--; r [ mees e m r we e ] [oam on a ae [7m -- em C-- S-- o [ [mm [ en ez r | on es s se s is ] ]| | [[aesee eTp I -- -- mem| eae SOTETo7 [T Coomw T m m [ ommes [ rTm--a -- re --s [one ozr | [ [m e TTi a woo c wsrm e| [I rves T -- o-- s I ease-- --T---- --o -- m| [ eee7 C --T Io -- o a w m-- e ]| [oC mo eT mo mm ie w r 0403 2013 000397 Table 1_0.doc Table 1.0 `SummCa8ryionfSAunraflaycteicWaaltReersults: DuPont Washington Works Facility Washington, WV [samp COTe E 05 Tomae ms ET T -- comwoe-- n-- ------1] [ eem Te e Jos r r|| [ 7o ---- n sts-- e [emme ----em [e I s ----s&s --] [ Trmewm -- e--e [a[ see T w u es ] [ [m m 1o e o 9e;m g r | NNoQte=: ANnoatlQyulacnatlifmiaeblne.oDectheacnigeeddaatsacoofncNeonvtermabteiron20a0b1ov(eseteheSeLcOtiDonan2d.0boelroGweltahles)l.imi of | quantification (LOQ). | oartsi03 3013 000328 Table 1_0.doc ji Table 2.0 SummCar8yionfSAunraflaycteicWaaltReersults: Local Landfill Washington, WV CUTFsALmL Goe8 TonT 200o 3 T gm 7 [s -- e eTr r r-- -- --71-- -- -- Nor fo-- -- wconT dli--ons-- -- e 77-- ---- e r -- -- r-- CUTPRLCOH O [ I 7--a -- wTw eTTr-- -- | 7 7 se ---- 2r asr-- -- | >--r -- r-- I 7 ee-- -- r n-- e-- r-- | amme AE im ) i e is7e ----e Wofowxc-- ongo | [ eem ra -- io -- a--e [ F 1g --e --ie -- r s SUTFALL 005 ew [ Tzo m e mce at s ] 0 7 wer -- -- 7 r ege Trr---- [7a 027-- T ---- fT roo -- wrconT aion-- s-- | -- > -7------ -- -- r rx-- r r-- -- [ww wow 0415/03 000329 toi2 Table 2_0.doc. Table 2.0 SumomfAanalrytiycal Results: C8 in Surface Water WaLsohcianlgLtaonndf,ilWlV CUTPAsLL0m06e(OVST T |__b | 22Wo8 fce oiwceon0 dmoms 3| eT -- Lr-- e I-- T w-- r-- 7 ---- -- -- --Tr-- ooerm-- s -- e-- } mre TT -- s ere -- . Tommees --T ws----| [CToommmeeT 1%s -- | | I 7 -- -- I -- -- -- CUTE To Ceme e Taw y | [remeerm masms} [rise er) | emom --------wmo| eommeerTw mo o --7-- ---- -- -- -- Com 7-- ------@7w-- Co romer e m ee a]| C -- er om -- m 2-- o| COTLET THT C2EACHATETRIET erm Tm Eve mee | Note: Analytical method changed as ofNovember 2001 (sce Section 2.0fo details). 045/03 000400 2012 Table 2_0.doc Table 3.0 Summary of Analytical Results: C8 in Surface Water LeLteatratrtL,anWdfVill TOATEsACHmATeE BAST T o | w 22803Ta Tio Sompem gTM | 7 ams 1 ---- Fo1 n-- | [[mrsoesseTee ws) } [esoomome ---- ammw0----) [eaet7e---- Worm-- e-- r | ooomme mar m ) --ate>-- ms -- --) [t7r 77 -- s-- er] 7 7---- -- -- -- I I -- 10 ---- -- a-- [7 03| 1 NoPlow Conditi-- ons | 1 7-- ---- -- TTrr---- [ 7Jo -- m "2 om e r-- | | -- 7-- --ir -- -- T-- -- --7-- --L-- -- T---- -- [ eT-- me o-- mem -- [ 7-- ms r -- owT ee -- | FSET To1 omer--T-- ------7&-- [ 7-- mm 7-- 2a s -- | --e1-- ---- -- -- -- --7 ---- -- --7 7-- ---- -- |-- -- [i m-- or -- 7 e-- s --ememmn[m 1 eowse 1 Tp owe] 0415/03 000401 tof2 Table 3_0.doc Table 3.0 `SummCa8ryoinfSAunraflaycteicWaaltReersults: Letart Landfill Letart, WV CsP RwUeNG Towais cFeonn | [ 7 roso e-- T mae -- e s--r| eae7----T wsr -- | [eaa7 mme-- 1 to -- r am-- i. es|| 1---- rT-- N=otSeampAnlaelsytwiecrael tmaektehnoadttchheanrgeespdecstsiovfeNsourvfeamcebew7rat2e0r--0l1oc(ast-- cioensS,ecHtoiwoenve2.0r-- f,orduGeeltaoia)n. error by th courier, i t=hTehessaempsluersfaacreriwvaetdeatlhoceatliaobnswwaerrmeannodt wsearmeplneodtdaunaeltyozeddo.wned tres from an ice storm that prokibited access to the landfill oarts03 000402 2012 Table 3_0.doc . Table 4.0 SummCar8yionfSAunraflaycteicWaaltReersults: Dry Run Landfill Lubeck, WV OsTmEeGar Tow mseTc ese mmeees w se e e] ] [ree ee eer e] 7 [o 1 Rofowcn ondtons 7 1--| w sme ae] e I C-- o -- m a-- ee 1 ees T -- e a-- CoE i mee---- coTonond-- os] [ [7 i 2t 8NNoo0 ffe oowwccoonn6 ddittoonns ss 7| | [arivt 0z |oNNooffm loowwccoonnddittoions nss | o mS2e5e0 r Notow] conatons eT er | COTETo [t[ io z {o i ioffoowwccoonnaar o voonnss [t[ omo8{ 3t 0 tiofooi wwcc0 oonndsttoonnsso 2| mrer ---- ronT--| [s7 meTh --o f7 ow conatons-- I ome--q-- rar o-- --1 -- -- 045/03 000403 Tor2 Table 4_0.doc Table 4.0 `Summary of Analytical Results: C-8 in Surface Water Dry Run Landfill Lubeck, WV Swe PROPERTY BOUNDARY. owe [Cie] [omooz 3_ 8 __ 1 [e | mo Wofiowct ondiionsz | [s 1 m eme [Tana 1 ees | [e 1 s 28 e [e 1 s 3e1-- e 1 ewe 1 1 [ma ae o [To| pen 3ses1] [n| ame ossss| [a-- mne 9ss -- s 1 "STREAM SAMPLING PONTH |__ tomoz| tes | [e | mo WNofiowc condions2| [s | eo tes e 1 [wpe om | [meso 116 | [ops 1 o--ss] [wwe Tossa | Co 1 ng 1 e -- r [Joma 1 ors | [zz 1 ene osess| I STREAM SAMPUNG POWNTRZ |___too | -- 282 | [samo 1 si0 [a 1 w 2s e | Teese 1 es | ees 1 a3 | [mmo | ae} [emaor Tas [T 1 om ara e s1 [Tzpenorees 1 [sn 1 one a5 ss DRLEACHATE. ose | ve | [s 1 em ww e 1 [e | pae w e [meso 1 sw [oes | 26 | [meee Tae 1] [enzo ve 1 [Tzpenees [a [snemessIs 77221997 Te 1 POND UNDERDRAIN [o |m era e 1 [epee wma [eso | er | [o | s ax e 1 [mo 23 e oe Area thd chan[ gede sof Nn ovez mbo er 011 ix Sein 203f8orade) 1] 000404 outsis 2012 Tavle 4_0.0c 32$ B 000205 i 4 FIGURES | 000406 | e7s - : B yl et, : ' Pat,Vo Ce : CNT E {L .:P SRY E - Ta an Le TaN AEJieis fo2s Ge # N) BN - = == i = ono Lc ATE - WASHINGTe ONR WOe RKS wali foo le FACILITY _. ----omimes Pf[: iJTr o aa e emu | Em dE -- HS=r ---- Slenn, 257 I Pr maaraoniio F | Loy "J aVa R eopn iei p=re:| SCO : 0of<. 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"NG zi retortFans NER im | [7 fi; hi \ cn ) ANT \ o Ils mf oY | il it 7 Wi ji SUNNA A wm sro | 00015 [ETREB | lett ee| cen EeeTeEd ERT t | : S y (a OSSa be b XODECa or En es) A | N= = do a 0 ANS | i oi VoD Te) a Ke Lh Nia Neer N= I Nayio Pa me= en i rH at von J ESF | il > Lf Neve 15:1 P JENN =il A)i i a } i i2 - Ca oo 000416 | |, E E EEE lEN l ogieiy | iA | {it ede i om As hs VENT L eyeTE WR ESriHi Ey==) \ & l L- A{ het , REPS Ne E ~ 8 | os i 000418 | | | | APPENDICES i | | | 000419 :;i 3 000420 4 | APPENDIX A | LABORATORY ANALYTICAL DATA REPORTS | WASHINGTON WORKS FACILITY 000421 'E en Re i XY8RESEARCH `Proven Results. WdLA Avalytca Resi Washingion Works CO Sampling 203 1 rns arroes) 1 nvwscZzooouuuimato0o0n08 1p0o5i0o0 1ge WWi K-Z-m Outfuantlol. er-ar0o0os5 4- 6np4re0]0 JE J Lr nen 00cm sy ro I Linkotuantaion 100) or prosacurs 50751 A vo:Conpoundrorcowns [7 a+ Compound detected a a aot borwaen ie LOD an LOO. Runottquansta 1 ooovamocco 1 Results are calculated according to the following criteria 1 R E eRIS If the sample and laboratory duplicate are greater than 250 ng/L, Sand tnhe rerlative en percent difference 1 Ba 5If0t,htehseaamvpelreagaendvallabuorfastroerpyordtuepdl.icaIftethaereablseoslsuttheaf2e5r0enngc/Le, iangdrotahteerabtshoalnut5e0,dihfofehreingchearisvalelsuss tihsan 1 : 4 E tai 0007, a Saki \ 000422 X=Rif usa ra) SYgEa 3 g 2g3 000423 APPENDIX B ! CHAIN-OF-CUSTODY RECORDS | WASHINGTON WORKS FACILITY 000424 ------ ee ---- 600-- 0 ------- EsS fIL S RE Gd E sR E A E 5, Erg |[ET --NIET EETEI EEEYSPE[23E30s =e1H I COETxoO R- EENiEaFdRE:E gs HERUeANK RE 3000000 sad vioz :g a +3 IS: MEL | i 2 add 4TH 4AR8E9A95999 ol Hdgl] Sil gn] fn aifl:193]|| 395735 oii ia Eif 2 | Sl CEN Ed li 2 : i| maa SoR ilB edClH es 8 LH omeoLo ITtT 33 8 5 Q O] "BZ oda = Hel? =: WM. $ 33455328 143 249949548 | QL 423949214 P| 327494724 | i{l 412 :E ila ; ScHaAnNdE > olin Br 2h QQ:= Wl 5H 34/44Dr 3 SRELs: =| S eiZ n [82 HHo52e59H: EEs 24344 g z <| Le A 2 wl Egguiudds Of pf 3 S2[8h3 SEREAZ|L3E3 2 3 W$ dSl]i 2y JJ ~=-0004. 3 x 3 8: 000426 APPENDIX C | LABORATORY ANALYTICAL DATA REPORTS | LOCAL LANDFILL i 00042; E n o " a egFoRraRtcEhhSEARCH i Fe Hi If ) ) Analytica Resus Loca Landi C8 Sampling 2123 DuPont Sample ldentiication APFO (rat) ' LCL-Z-Outlet 101 43900 : LLiimitt ooff QDuaatncitiiaotnio(nLOLD0)Gf)orfhorehperopcroecdeudrurseaipsp5o0xinmga.taly 10 nig. | ND Compound not detected | mo<lon<nacion ! NQ - Compound detected at a level between the LOD and LOQ. Result is not quantifiable. Resuls ar calcite accoring to he folowing crria | (v1B1aP10Dl)ssiameepplsoesriatenadsnta20b,orthceorayvecruapgceatvaeluaereisgreepaotreerdr.an 2h5e0 nAPtD, ias ngranteerretlhiave20p, oirthidghieerrnce 5rIfe0tp,hoe1r0seadamvpelreagaendvallabuorsatroroypdeudp.licIate arealbesss tthac2i5e0ranngc/Le, agndrethterabnsonlut5e0.dihffemregnrceerisvliesos t5han 000428 4G!Gy M& onoEnS Rion, usa gAmD, 3 1 8x 000429 APPENDIX D | CHAIN-OF-CUSTODY RECORDS | LOCAL LANDFILL 000430 . ] A. sE----ih BiH aHEH | z := IB STITT || E-- T] RHEE | CITT Hs nik g| 9| s H |=: mHanHnaHn BBEZ H1H2a0i0d000i0 oo 2: 0: : SURE] 3 i aE ille |{ =H] BIER on 154il:BJ, glki shh rem i 5 : 18 2 : saquingy| al2osrhif: 5si3df| yell dEe I = fCee H rn il Ek il ll [4 :i 3 : 4Ay | ET | Oo Hil 15 =|3 lo HIS SER Ey i Z|E -HE | LE ES TE g ara g ] ? :: el] | 1 . 0004 |, &a 33 g2n 000432 ; 4A APPENDIX E | LABORATORY ANALYTICAL DATA REPORTS | DRY RUN LANDFILL 000433 .E 2: en 1T.0eRESEARCH nN . rg Sot rym oC Sgn ro SE ' DuPont Sample Identification APFO (sngo)o |1 roca Limit of Quantitation (LOQ) for the procedure is 50 ng/L 4 Compound toe vl swe LOD rd LOG. Fos not uf 1 raomerice | Results are calculated according to the following orteria bVoopmn If the sample simon meme and laboratory duplicate asare goran 20g, greater than 250 ng/L, av ve re por te and the relative percent difference pofmrhsasmagieraat ong)dfhoe snoesS50th. svatt fiesdlfforroernUCtTER i ~ July 000434 C88h52aRam \. 1: 814.272.1039 x 3 ggx 000435 : y APPENDIX F | CHAIN-OF-CUSTODY RECORDS DRY RUN LANDFILL 000436 sion Ss A FT EIT EE 8 5. S J HF ITOH EL i | | C |B [ITT H, [s8:e: Eos TTITTTTTT ES 3:24:|| 2 SE TTT ME zeit, 2 Hr KIT 2 [fi3s33:] Gs BH 77r=#77 WT] HE 3000000 xz Rs | 8 L1 4] sah: 8 5 = 5d g <: 3 35 Zz :i 2 g A] 2 : os SIE | i= g 3 I 1 3 SHAT `Ooii: 2l=s i: | 1S O Hils WE laagd:Sy Sfs 25E| E ,ER] 4Hg EE . J Sei fe [FF 3) eelLIT ld I Si fisC= :, 3 5 | 2SER |f)og E palI l] A : q 3 [Tz _: GRIEEE Q: wl g : i B Haigld12]| H= ]3 I] H A13= 9 NY: 15 HeNH lBlu2E | Er 23 78d 3 | 333g FE <[E IN : H7il A -; a a : n Fio EHAos 2