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AttacShtmuednitess atondLeOtttehrertoICn.foArumeatridoanteodn MCearyta1i8n, 2000 Perfluorooctane Sulfonate-Related Compounds 3. PFOSAA | Perfluorooctane sulfonylamido (ethylacetate Acute Toxicity, 1) ANoc.utTe-O1r9a8l3T(oFxCi-c1i2ty8,~pRoattass,sBiiuomsesaalrtch1,00In%c,,sPorliodj)e,ctJaNnou.ar7y7-5,1110987A5, 3M Reference. 2) Acute Oral No. T-2001 Toxicit--y (FC-128), RJaatnsu,arByio6s,ca1r9c7h8, Inc, Project No. 77-1274, 3M Reference. 3) RPerfiemraernycEeyNeo.IrTri-t2a0ti0o1n S(tFuCd-1y2~8)R,abJbaintusa,rByi6o,se1a9rc7h, Inc., Project No. 77-1274, 3M # RPerfiemraernycSekNion.ITi-t2at0i0o1n(SFtC-u1d2-8y),RaJbabnitusa,ryBi6o,s1e9ar7c8h, Inc, Project No. 77-1274, 3M 3) ParnojAecctutNeo.In7h8a-la7t1i8o6n,T3oxMicRietfyerSetnucdey Noof.T-T2-3203707C(oFCC-i1n2t8h)e,RFaerb,rBuiaor/yd8y,na1m9i7c6s, Inc. Additional Acute Toxicity Studies Not Submitted (Bibliography only) 1) ANoc.utTe-2O0ra8l1 T(oFxCi-c1i2t9y,~aRpaptrso,xBiimoasteealrych4,0-In5c0.%PirnojseocltutNioon.),78M-a1r1c9h1A2,, 139M78Reference 2) RPerfiemraernycEeyNeo.IrTi-a2t0i8o1n S(tFuCd-1y2~9)R,abMbaitrsc,hB2i,os1e9a7r8ch, Inc, Project No. 78-1191, 3M 3) RPerfiemraernyceSkNion.ITi-t2at0i8o1n(SFtC-u1d2--9y),RaMbabirtcsh, B2,io1s9e7a8rch, Inc, Project No. 78-1191, 3M 4) 3LAac2bu9otr0ea4tO0orra%yl,TKRoi'xkiPecFritOLyaSbSAocrAraetieonnri3wei%st,hEITnXc-O,3H2,Pr9o10j7Cec%otCNIioPn.AA0lab8ni8dnA4oR00Ra3t6s2,,Sa3fMetyReEfvearleunacteioNno. T- 501), November 5, 1982 % H.0, L-6778, F-6873, Lot 3). L3Par2bi9omr0aa4rty0orS%yk,inKRi'IkiPetrFaOtLiaSboAonrATaetiosnrt3iweis%t,hEInITcO-.,H3,P2r9o10j7Cec%otCNIioPn.AA0al8bn8idEn4oB00R4%a2bb3Hi,yt0s3,,MSLa-Rf6eefteyrEevnacleuaNto,ionT- 501), October 15, 1982 778, F-6873, Lot ) ALacbuotreatOocruyl,arRiIkmeirtaLtaiboonrTaetosrtiweist,hInTc-.,3P2r9o0jeCcotCNion.A0l8b8iEnoB0R4a2b4bi,ts3,MSaRfeefteyrEevnacleuNaot.ion1- "3 600177 -- ee ------------ AttacShtmuednitess atondLeOtttherertoInC.foArumeatridoantoend MCearyta1i8n, 2000 Perfluorooctane Sulfonate-Related Compounds 350219),0O4c0to%beKr'26P,FO19S8A2A in 3% EIOH, 17% IPA and 40 % Ho, L-6778, F-6873, Lot Genotoxieity !). BB1ai8co1tt5ee,rsitRaielnpgoRrCetevneNtroes.re,TMC4uh6te6amt3ii,coan3lsTMeIsRntesofpfeercvte-in1oc,neHaNinotda.TRTee-ss6te6i6an8rgchInsItaibtourtea,toSrtiusd,yCChoedmei:caKlo1- 50% in solutionofwater and organic solvent), .1. October, FC-139 1996 (approximately 40- 2) K3In2'9VP9iFtCtOooCS,MAiAcSrRioInbiI3onlt%eorgEniaIctaOiloHn,Maul1,ta7Pgr%eonjIieccPtiAtNyaonA.ds3s41a04y%5s,o3fM3 RefCeormepnacneyN'os.CTo3m3p0o0u.n(d40T-% November, 1982 Hy0, L678, F-6873, Lot 501), Pharmacokinetic Studies 1) RR2e8efaeDureaertnmicaoelnNPloea.brocTru-at3ta9onr9yc1,o,uRsMiakArebcrshoLrap1b5to,irao1tn9o8rS1iteusd,yIwnict,hPFrCoj-e1c2t8Noi.n A0l9b7i9nAoBR0a6b2bi6t,s,sSnagfety 2) RS2ea8ffDeetrayeynEcDveealrNumoaa.tliTo-Pn3e9rl8scb9uo,traaMntacoorruyc,shRA1ib4ks,eorr1p9Lt8ai1boonraSttoruideys,wiItnhc.F,CP-ro1j2e9ctinNoA,lb0i9n7oR9aAbBb0i6t2s7,, 3M 3) 00Fi11n35a01l591R5e1ap,nodritnTv--i6Av0no5aSl4ytitunidcRyaalRbebSiftteusrd,eyn:3cMSeiNnEogn.lveiH-rDWoonIsmee6nD3te2ar9lmaLalboArbastoorrpyt,ioSnt/uTyoxNiec.itAyDStLud,y of SNoMveRemfbeerren2c2e, Nos. 1995 T-6051 (FC-129 treated fabric-)1a3n3d (TH-a6z0l3e4to(nFWCi.s1c9o5nssoilnu,tiIonnc).),, R2Foi1nt-ael6re0Rne5cp4eoriNtno,.RAanHbaWbliIyt#ts6i,c33a2lM9R-e1Epn3ov8ri,troSantnmudednSytiNanolg.iTeAe-cMDhDonsToe-l1Io2ngt2yr0ad9v4eSneoruvsicPehsa,rmIancvoikeirnSettuicSdtyudy 129, November 22, 1995 .3, 3M Returns neFC Studies in Progress 1) SCtorraptoergaicteToTxoixciocloolgoygyLaSbtourdaytoOruyt,liJnuel,y,FC1-919829 Preliminary ADME Sercen in Rats, 3M -4- 000178 Attachments Studies atondLeOtttehrertoICn.foArumeatridoanteodn May 18, Certain 2000 Perfluorooctane Sulfonate-Related Compounds Pre-1976 Studies (bibliography only) 1) Skin and Eye Irritation Reference No. FC-128, individual eye scores Assay April Report, WARF Institute, 24, 1962 (plus Decembey Project No. 2031046, 3M 29, 1966 letter containing ) 5. a ---------------- 000179 ` Fe-izp Submitted to: BIOSEARCH. INC. tp.oe.lbeoxph85o9neph:ilade(lp2hi1a5, )penns8yl4v8an.ia441991091 Project Number - 77-1108A 33MM CCoemnptaenry, 5St5.101Paul, Minnesota Material: Sample Received: Date of Report: Test: Object of Test: Procedure: 3M Company - T-1983c0C 11/2/77 Study Initiated: 11/18/77 Study Completed:12/15/77 1/5/78 Acute Oral Toxicity - Rats tTohesstuubdjyectthemaatceurtiealo.ral toxicity in rats of aSFnhodeurrm30ag0nr-ogWumipsswteaorrfeS5etmrmpaaliloneyew&dei5gihnfientmghailsbeetsatwluebdeiynn.o20rT0ahtes of the ma2ranatdteshrdoiowuasrelserdeprbdyieoprdriirvteeocdtdoosfaidnmfgio.nodistEbruaatcthinoaonntimowafaltetrwhaesfeoxwrpeeirgihneedntal and dosinginnteoedtlhee. stomach by means of a syringe The sample was dosed as a 50% w/v suspension in water. The following dosage levels were administered: 1.25 2.50 mmll//kkgg.. 150..00 mmll//kkgg.. Results: Conclusion: pfFeoorolidloodawniddnugrwiaantdgemriwnhiaidscthr1aittbiiiomtenuntthfheoerraanttihsemawl1os4redwaeoyrbesoebarslvelerso.vwaetdion for signs of toxicity and mortalities. See Table 1. 22T1.h8e5innsolu/bkjrgeacttsofmhaaatse5r0ai%nalwac/uvwtheesnuosrpsaetlnusdiiLoe0nd50 iinonfwmaaatpleperroaoxnridma1ft.ee2ml5aylge/kg. of the original sample. 000180 DKiarrelctLo.r Gabriel, V.M.D., Ph.5 --_-- 1 Ket tral Toxicity Material IN Company TISBSEC, 5 o 508 w/e suspension in water. SS[ an -- Si, 15 sms o M5 Sfemls S #0 sms 2B2S0O seme smile 50 stele 00 smile 00 stewie Lessrr8etSao%tirci0es nn nu bThaodle NTa otale diiiel fionmr 000000000 00000 00000000000000 o 5 s 2 we mus 0110000000 0000 020000001 000 00 3 sas : dom so... 40... o us o 50 - soo... soo... LLL, . o zo us - The L950a15msppriateolyt2.a5 alg. of a 502 uv suspension in water a042S8h9che,Ton1c0u1r2aIes5p0psneaksadkrgae.ndG.o1"t4meo(dr(0ro2.it1t631.5ghhaga"iaREn.g3s.r1u)3enruW5tlm:ihua0okrcasy3a"nuSittamh1rgar1slo)3su5hghwposeaurhteaatrtieh)gedhctaulhsyearTenoecrthirermstrohcreiefeohrn,2u4orhootnurr$sa3aenndd 3G5ronsinStaeisimiaonsdiccoemxstnotnreatwihoinninTo3seWtaerss"sothitnhg anil were remarkable. eatery ore