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PLAINTIFF'S EXHIBIT November 30, 1977 Formula V-970 NEW MILFORD, VIRGINIA PLANT FORMULA READY MIX TOPPING COMPOUND V-970 (HAND TOOLS) DESCRIPTION OF PRODUCT - White Ready Mix-Topping Joint Compound used for finishing joint and spotting nail heads. FORMULA Raw Material Function RM Spec Percent Lbs/Batch Limestone Mica Natrosol 250 HXR Troysan PMA 10-SEP Minugel FG Magnesium Oxide (heavy) Prophylitte SK Sorbitol (Powdered) Elvace EP-200 Nalco 71D-5 Acrysol ASE-60 Water Filler Anti-cracking Water Retention Preservative Bulking Agent pH Stabilizer Bulking Agent Borax Stabilizer Adhesive Defoamer Thickener Solvent 13 11 163 - 8 - - 185 147 - - 78.595 7.39 .625 .20 1.72 .12 4.93 .12 6.0 .10 .20 - 100.00 1599.7 150.0 12.7 4.0 35.0 2.5 100.0 2.5 122.1 (13.72 gals 2.0 4.0 996.0 (120 gals.) 3030.5** *Approximately 56.5 lbs/100 lbs of active ingredients (this may vary + 8 gallons per batch.) **0ne batch yields 49 five gallon pails Ready Mix joint compound at 62 lbs/pail. SPECIAL MIXING INSTRUCTIONS - Blend ingredients in following order: 1) Water 2) Elvace EP-200 3) Nalco 4) Filler 5) Mix until filler is dispersed 6) Add Acrysol ASE-60 7) Mix until Ready Mix is smooth - pumping viscosity should be 380 + 20 to al?ow for 24 hour viscosity build of 200 pts. WORKING CONSISTENCY Specifications for Paste Refer to Plant Testing Procedure No. 32. If paste is not proper working consistency, a maximum of 5 cc water per 150 grams of paste may be added to adjust. Brabender: (580 + 20)For machine tools add 7 gallons 1^0 (400 + 20) pH Minimum - 9.0 Maximum - 10.0 (24 hrs.) HCF:jr Continued on Page 2 . . . SGP 0017380 WORKING PROPERTIES Specifications BONDING PROPERTIES Specifications CRACK RESISTANCE Specifications COLOR Specifications November 30, 1977 Formula V-970 NEW Page 2 - Refer to Plant Testing Procedure No. 33. Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. - Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall show at least 90% fiber tear when delaminated. - Refer to Plant Testing Procedure No. 37. Rating shall be 4 or better. - White Dried compound shall match color of standard sample. HCF:j r SGP 0017381 November 30, 1977 Formula V-970 NEW MILFORD, VIRGINIA PLANT FORMULA READY MIX TOPPING COMPOUND V-970 (HAND TOOLS) DESCRIPTION OF PRODUCT - White Ready Mix-Topping Joint Compound used for finishing joint and spotting nail heads. FORMULA Raw Material Function RM Spec Percent Lbs/Batch Limestone Mica Natrosol 25'. HXR Troysan PMA 10-SEP Minugel FG Magnesium Oxide (heavy) Prophylitte SK Sorbitol (Powdered) Elvace EP-200 Nalco 71D-5 Acrysol ASE-60 Water Filler Anti-cracking Water Retention Preservative Bulking Agent pH Stabilizer Bulking Agent Borax Stabilizer Adhesive Defoamer Thickener Solvent 13 11 163 - 8 - - - 185 147 - - 78.595 7.39 .625 .20 1.72 .12 4.93 .12 6.0 .10 .20 - 100.00 1599.7 150.0 12.7 4.0 35.0 2.5 100.0 2.5 122.1 (13.72 gals. 2.0 4.0 996.0 (120 gals.) 3030.5** *Approximately 56.5 lbs/100 lbs of active ingredients (this may vary + 8 gallons per batch.) **One batch yields 49 five gallon pails Ready Mix joint compound at 62 lbs/pail. SPECIAL MIXING INSTRUCTIONS Blend ingredients in following order: 1) Water 2) Elvace EP-200 3) Nalco 4) Filler 5) Mix until filler is dispersed 6) Add Acrysol ASE-60 7) Mix until Ready Mix is smooth - pumping viscosity should be 380 + 20 to allow for 24 hour viscosity build of 200 pts. WORKING CONSISTENCY Specifications for Paste Refer to Plant Testing Procedure No. 32. If paste is not proper working consistency, a maximum of 5 cc water per 150 grams of paste may be added to adjust. Brabender: (580 + 20)For machine tools add 7 gallons HgO (400 + 20) pH Minimum - 9.0 Maximum - 10.0 (24 hrs.) HCF:jr Continued on Page 2 . . . SGP 0017382 WORKING PROPERTIES Specifications BONDING PROPERTIES Specifications CRACK RESISTANCE Specifications COLOR Specifications November 30, 1977 Formula V-970 NEW Page 2 - Refer to Plant Testing Procedure No. 33. Compound shall be plastic, buttery working and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. - Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall show at least 907. fiber tear when delaminated. - Refer to Plant Testing Procedure No. 37. Rating shall be 4 or better. - White Dried compound shall match color of standard sample. HCF:jr SGP 0017383 March 30, 1978 Supersedes Formula V-970 Dated: 11/30/77 MILFORD, VIRGINIA PLANT FORMULA READY MIX TOPPING COMPOUND V-970 (HAND TOOLS) DESCRIPTION OF PRODUCT - White Ready Mix Topping Joint Compound used for finishing joint and spotting nail heads. FORMULA Raw Material Function RM Spec Percent Lbs/Batch /Limestone /Mica Natrosol 250 HXR /Proxcel CRL Minugel FG Magnesium Oxide (heavy) /Prophylitte SK Sorbitol (Powdered) Elvace EP-200 Nalco 71D-5 Acrysol ASE-60 Water Filler Anti-cracking Water Retention Preservative Bulking Agent pH Stabilizer Bulking Agent Borax Stabilizer Adhesive Defoamer Thickener Solvent 13 11 163 8 185 147 - " 78.80 7.37 .62 .04 1.72 .12 4.91 .12 6.0 .10 .20 100.00 1602.81 150.0 12.7 .89 35.0 2.5 100.0 2.5 122.1 (13.72 gals 2.0 4.0 996.0 (120 gals.) 3030.5** *Approximately 56.5 lbs/100 lbs of active ingredients (this may vary + 8 gallons per batch.) **0ne batch yields 49 five gallon pails Ready Mix joint compound at 62 lbs/pail. SPECIAL MIXING INSTRUCTIONS - Blend ingredients in following order: 1) Water 2) Elvace EP-200 3) Nalco 4) Filler 5) Mix until filler is dispersed 6) Add Acrysol ASE-60 7) Mix until Ready Mix is smooth - pumping viscosity should be 380 + 20 to allow for 24 hour viscosity build of 200 pts. WORKING CONSISTENCY Specifications for Paste Refer to Plant Testing Procedure No. 32. If paste is not proper working consistency, a maximum of 5 cc water per 150 grams of paste may be added to adjust. Brabender: (580 + 20)For machine tools add 7 gallons l^O (400 + 20) pH Minimum - 9.0 Maximum - 10.0 (24 hrs.) HCF:jr Continued on Page 2 . . . SGP 0017384 October 29, 1981 NEW FORMULA V-970 MILFORD, VIRGINIA, PLANT FORMULA READY MIX FILLER V-970 DESCRIPTION OF PRODUCT - Filler for Ready Mix Joint Compound V-971 and[ Topping Compound V-9 7 5. FORMULA Raw Material Pyrophyllite-SK Aqua-Fil K-8 Methocel Sta-Gel Starch Limestone Function RM Spec Bulking Agent Bulking Agent Water Retention Adhesive/Thickener Filler 1 229 16 3 10 13 Percent 7.627 3.520 .352 .939 87.562 100.000 Lbs/Batch 650.0 300.0 30.0 80.0 7462.0 8522.0 WORKING CONSISTENCY - Refer to Plant Testing Procedure No. 32. Maximum 62 Minimum 58 Average 60 WORKING PROPERTIES - Refer to Plant Testing Procedure No. 33. Specifications Filler shall be heavily bodied and possess fair plasticity. It shall be free of any coarse, gritty or undispersed particles. COLOR Specifications - White Dried sample shall match color of standard sample. NOTE: A wet mix of the filler shall be prepared according to Formula V-971 at least twice a day or with every sixth or seventh batch of filler manufactured. This prepared mix shall be tested and shall meet all the specifications required of Ready Mix Joint Compound - Formula No. V-971. BGR:ps SGP 0017385 October 29, 1980 NEW FORMULA V-971 Page 2 WORKING CONSISTENCY Specifications for Paste Brabender (540 + 20) PH WORKING PROPERTIES BONDING PROPERTIES CRACK RESISTANCE COLOR Specification - Refer to Plant Testing Procedure No. 32. - If paste is not proper working consistency a maximum of 5 cc water per 150 grams of paste may be added to adjust. - For machine tools add 4 gallons H20 (450 + 20). 7.0 - 8.5 - Refer to Plant Testing Procedure No. 3 3. Compound shall be plastic, buttery working, and free of any coarse, gritty or undispersed particles. Material shall be free from lumps due to incomplete mixing. - Refer to Plant Testing Procedure No. 35. After compound has dreid, tape shall show at least 90% fiber tear when delaminated. - Refer to Plant Testing Procedure no. 37. Rating shall be 4 or better. - White Dried compound shall match color of standard sample. BGR:ps SGP 0017386 SGP 0017378 MILFORD FORMULA # 970 ASBESTOS CONTAINING PRODUCTS SGP 0017379