Document LgRG5gyyLw1ogK8QEDOBe1ma5
CQ 40
/04 J Sawn**1#
C.V* 260
CODE RT-531-D PKG ___
mfjm < DATE )
F<ZT01 < LOT >
DATE PRINTED*. ~ 4/3 D. V.*` 303, 315, 317/^322,(3^
PROCESSES
APPROVED BY
< 5RT-.531-D < N > EWK 11-24-81
CDMTYP JOB NAME: 40RT531DMN
TYPED BY: JMH
EST. UT. 642* LBS.
entr-M^TTMTM HRS\,----- TIME _____M
PREPARATION NOTES; SUPV'R NOTE: DDO NOT USE V-303 FOR NAAPPHHTT1HANILS WHEN
CAMPAIGNING DALAMARS YC-39-A, YC--440-A, YT-839-P, YT-S840-P, YT-858-D, AND
YT-863--D,
jgL_0-_ t/'JM TWa*.
SEMI-BLEEDING
DV n^
NAME: NAPHTHANIL RED LIGHT
OBTAIN 4-NITR0-2-AMINQT0LUENE FOR S6
It AIN 3-HYDR0XY-2-NAPTHYLAMIDE FOR SIS I CLEAN, DRESS, CLOSE 24* CLARIF PRESS -
15 FRAMES
ijm^486 G) WATER INTO V-__3J&3*L-_
RUN IN HYDROCHLORIC ACID FROM V-324
-
ML
, 2 %%%.
j DUMP IN FROM SI
LOT^
I 4-NITR0-2-AMIN0T0LUENE
I USE t N-CODE | ACCT
i LBS |
I LBS
I-*------- 1--------------- 1----------
I I 504-C |
I I 150-C |
I
X&l Q.
28-D | 126504-C J
n*//
& STIR A 3 MIN TO WET
LOT___
| ^>ADJ TO &1Z?J <1020 G> AT 40-45 DEG F
1/M SIPHON IN SODIUM NITRITE IN 7-10 MIN
1 M__ f.___JE3L3E6u--% I-TO | STIR 5 MIN 6 RECORD:' CR Jr__< + ), KI2f!!__< + >
I I NOTE: (1) IF CR-, KI- ADD 204 *AS IS*
[ | INCREMENTS HYDROCHLORIC ACID ASSUME 32%
I | RECORD: CR( + ) KI__< + >
i | (2) IF CR+, KI- ADD 101 AS IS* INCREMENTS
I. S..O__D_I_U_M N___I_T_R7ITE ASSUME 33%
I L^RECORD: CR_jf___<+> KIi__.!L_< + >
J STIR 10 MIN AT 40-45F MAINTA^Ili^+CR, +KI
I I FOR SI3 RECORD; TIME STARTs
5X330
57-A rrjcps
I 725-A I ?5
'I
1 28-D I --L--
i I 725-A l_____
I
** t SLURRY DICALITE FILTER AID IN 40 GAL WATER I 5 1 777-A 1
IN DRUM 6 PRECOAT CL ARIF PRESS
l' 1
i
5
WHEN S11 STIR COMPLETE DUMP IN ACTIVATED I
CARBON
I
IN DICALITE FILTER AID
I
| STIR 30 MIN AT 40-45 DEG F
ASSUME 33% I
MAINTAINING +KI FOR.^23.
,
I
I RECORD: START
KI __
___< + >
I
15. t1 10 1 _____ 1
i
11 3-B 11 15
777-A 1 10 725-A 1
57-A 1 iM, 1
RUN 13" <1770 WATER INTO V-330
SLURRY TRISULPHOIL SOAP D IN 25G WATER &
L-'POUR IN
lT| DUMP IN 3-HYDR0XY-2-NAPTHYLAMIDE FROM S2 &
1 I STIR 30 MIN OR LONGER TO WET.
LOT
I I RECORD: STARTJeT
| 1 | |
$<Le.
-VVJmS'-'C
16
I 39-A | 1 6
I 150-C | 370
N38974
EQUIP MENT
2 OF 3 CG 40 CODE RT-531-D <N>
USE N-CODE i ACCT LBS I LBS
RUN 12* <1^440 WATER INTO V-302
UR IN SODIUM HYDROXIDE
ASSUME 50%
I 50
SIPHON IN ACETIC ACID & STIR 3 MIN ,,
I ,..
m
,
% I -JL.&Z,
RECORD PHJS^(6.7-7 *5 ) IF
6.7-7.5.
, ACETIC
NECESSARY ADJ TO ACID ASSUME 70%
IJ
S;*s?;- ' '
RECORD PHJZ|c SODIUM HYDROXIDE ASSUME 50% }ZZIIZI
7-D | 29
30-D 7-D
23KT TURN ON
AGITATOR i, ADD ICE, THEN )12X330
J^SHUT OFF AGITATOR
I
2&AI PUMP DV THRU CLARIF PRESS INTO DV.USED IN i
I S 23, MAINIAININ& TfeMP AT 40-45*F* RECORD: I
I START:jmM&.
TOTAL MIN_^L___
I
OTE: DO NOT USE V-303 - TOO SMALL
I
WHEN S23A CLARIF COMPLETE WASH DV <S4>
|
I LINES PUMP 6 PRESS FOR 20 MIN OR TO A -CR I
I TEST ON A SAMPLE OF TOTAL PRESS EFFLUENT I
I WHICHEVER COMES FIRST. COLLECT WASHINGS IN I
I LM <S23) RECORD; START^^Jfep_.j^ < ^0R+> I
uasnwrwHHEEKN S24 I_S___C__O_M.P_L_E__T_E__T_E_S_T DV^23) ASSUME 33%
I l>*RECORD: KI,,.gKL< + > TEMP_Js L_-J{40-45* F)
U6-TWEIGH SULFAMIC ACID IN RUBBER BUl CKET AND I -Lo-RINSE IN AND STIR 5 MIN.
i" 1 10
RECORD: KI_a^!l_. MUST BE - i IF NECESSARY
J TO -KI.WJTH SULFAMIC ACID
i ADJ TO
* (1925 G) AT 40-45 DEG F
1 __2k_. |1X330_
/aSRUN 39* <3900 G) WATER INTO V~3tf
1 >i
1 1
725-A 57-A
!mi <
1
395-D i io
395-D J at- 57-A 1 zrrnrzvz.'
! 1
330
WHEN SI 8 STIR COMPLETE, POUR IN SODIUM
1
i
9
YDROXIDE IN 3-4 MIN.
ASSUME 50% I 220
7-D i mo
HEAT TO 128-132 DEG F AFAP. & STIR 5 MIN TO
DISSOLVE. STOP AGITATOR.
10 toS
IMMEDIATELY RUN V-330 AFAP INTO CV^NO
St a t io n in cv. r e c o r d : sTARTjMlir*
TOTAL MIN
___
POUR IN ACETIC ACID *, STAR 5 MIN.
T'J ^
RECORD: PH,,*?!:__< 10.5-11.0) ASSUME 50% IF NECESSARY ADJ TO PH 10.5-11.0
CORD: PASSUME 70% UN IN V-302 AFAP
DUMP IN BARIUM SULFATE
HEAT JO 78-82 DEG F AND RECORD:
1T,,_M,_..,DEG F AND REC__jf____ DEG F
WHEN^28 COMPLETE, COUPLE DV UNDERSURFACE
65-70 MIN. MAmpiN CV AT 78-82 DEG F
ECDRD: START^jR/fei TOTAL MIN _7id____
STIR 5 MIN, DISCONNECT TRANSFER LINE AT CV
& RECORD: DIAZ0_M.\i3i.*ir_ <+/-JL
BAS_rr:.<MUST BE +) PH^JteJL<4.2-4.6)
14.1 IF NECESSARY-STIR TO - DIAZO, RECORD:
START._ifcSbXjfc* TOTAL MIN____________
RECORD: DIAZO
MUST BE -
BASE ___ MUST BE +
PH <4.2-4.6)
35
I
I 30-D | 150
7-D |___
I 30-D i
I 65-A !
35
I. i
DUP050047468
CUMTYt? JOB NAME
*------ >i,--\-- EfllUP I MEi^T !
40RT531PMN
FACE 03
--
3 OF 3 * CG 40 COPE RT-531-D .(N)
PATE PRINTED:MM/PD/YY
j' I N-CODE i ACCT
I LBS I
) LBS
.411 SC 142/ 1 ABB* )G WATER AT 130-140* TO DRUM FROM HOT | #'11 i I JOT MIXER APP BLANCOL N ASTIR. FOR S43 |
30 I- 567-B | 30 II
sm 143/ KFOUJ IN N-567-B SOLUTION FROM S42
12 14-$/ 1 BPa T TO 194-196 PEG F IN 55-60 MIN AND
foS j /r ec 145/ 1 WHJ2
HTA%^___ DEG F AND RECjsHfl__DEG F 4 HEATING COMPLETE, RUN IN ALUMINUM
SOLUTION THRU BADGER METER, NOTE; i 120
N LINE AFTER N-115-D SOL'N.RUN IN, r
STIR 30 MIN AT 194-196 DEG F
FLOOD TO 80' (7928G) AND STOP AGITATOR
115-D
60
VAT | V-303|V-315IV-317|V-322|V-323 S4 (436G) 1 20"I 14" | 14* I 14* | 14* SB (10200)1 43*| 30* | 30* I 30* I 30*
START f,*tvw
"FIN
if.
OPTR .&2.
II
-jm--____
DUP050047469
DUP050047470