Document LKwkj2mNjnbGRwLjbdNKvJwKd
.* CO * 01 CODE YE-698-I)
( DATE ) BLENDED
L2H26 (~LOT )
5527* LBS< EST WT )
PROCESSES ( > YE-698-D (T)
APPROVED BY: FWP 10/15/82'
COMTYP JOB NAME; 01YE698DMT *
EQUIP I MENT
NAME: MOLYBDATE ORANGE
1 USE 1 LBS
I ACCT N-CDDE | LBS
PREP 1
351 *9
359 3
r\ OBTAIN SODIUM SULFATE FOR S-13
1 84
I 2 I CALCULATE & SET ON BADGER METER FOR. ! j/tNITRIC ACID WEAK)
16
LJ.1
I 3/1/OBTAIN SODIUM CHLORIDE FOR S-33
1 734
I 4 *|L/0ETAIN. SODA ASH FOR S-37
1 146
I 5 #1>OBTAIN SODIUM SILICATE FOR S-39
I 237
I 6 /jvfjBTAIN SODA ASH FOR S-43
I 350
I 7 if OBTAIN ANTIMONY TRIOXIDE FOR S-46
i 70
----- |------ -------------------------------- ------------ -----------------
I ~-+''WEIGH SODIUM CHROMATE INTO V-351
1 I*
o pt r
mite
I OPTR _____, MK _
.Sfk\ |i ........... .
S-'TWEIGH IN SODIUM MOLYBDATE SOLUTION
T-M&.S.L-IA-/.I*1
OPTR______ MK
I
I
OPTR_____, MK
T~______ _________%7.\\
108-A
33-D 4-A 3-A
32-D 3-A
711-B
10-D
423-D
1 84 1 ^7 1 1 734 1 146 1 237 1 350 1 7
I 1885
1 303
358 4
UN 10* (500 G) WATER INTO V-358
| RUN V-359 INTO V-351 6 PUMP IN V-351
ia-^.-A35J'.tO 55* (2600 G)
Ijrf SIFT IN N-108-A FROM S 1,
>4"T STIR 5 MIN & RECORD: PHZ^1_%.<9/0-10*0)
1>H"''ADJ TO PH 9*8-9*9 6 RECORD: Ph JLi Jl
I (CAUSTIC SODA SOLUTION)
ASSUME 50%
L. '
ASSUME 667.
ADD N-33-D FROM S 2 USING BADGER METER
ADJ TO 66* (31,21 G> AT A^-69*F
L-RECORD: VOLj&^L* & __J?Z_*P
%Sr\ STIR 5 MIN Jv RECORD: PHX'-3<7.4-7*6) 6
I G/ML L`J?Jl 7<1 *080-1 *083)
i NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK
I LIST 6 ATTACH. TAKE 1 QT SAMPLE
7-D 33-D
SV RUN 20* (996 G) WATER INTO V~_j2 5 DRD N-41-D STORAGE TANK TO PUMP FROM* CIRCLE ONE: 402 410 411 420 424 425 20 I CHECK WITH CO SUPV; *STORAGE TANK MUST CONTAIN AT LEAST 2376 GAL: 402=49", 410=25", 411=48", 420=25*, 424=25* 425=31* *STORAGE"TANK MUST HAVE STIRRED AT LEAST
20 MIN SINCE LAST ADDITION OR ADJUSTMENT *STORAGE TANK MUST BE ISOLATED UNTIL ALL
PUMPING FOR THIS BATCH IS COMPLETE
V: SET METER FOR 300 G 6 PUMP TO SV _*.7
NO.VS 1982
M40882
-tor* EQUII MEN! SV~~ 5 CONT
23
24
CGMTYP JOB NAME: 01YE698DMT PAGE 02
DATE PRINTED:i0/15/82
USE LBS
N- ACCT CODE LBS
AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH 6 DENSITY, RECORD BELOW. IF NOT IN RANGE, STOP PUMPING & SEE SUPV.
* PH:______ <2-2-3,7)
* DENSITY: ------------- ,, G/ML (1.270-1.328) IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD
DENSITY ______ _ G/ML ON TRAPPED SAMPLE FROM END OF S-21 PUMPING.
USING DENSITY FROM S-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21* CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
*** t a b l e #***
G/ML 1.270 1 .271 1.272 1.273 1 .274 1.275 1.276 1 .277 1 .278 1 .279 1 .280 1 .281 1.282 1 .283 1 .284
1 .285 1 .286 1 .286 1.287 1 .288 1.289 1 .290
SETTING 1 G/ML SETTING i G/ML
1678 1 1.291 1534 1 1 .312
1670 1 1.292 1527 1 1 .313
1 663 1 1.293 1521
1 1 .314
1656 1 1.294 1515 1 1 .315
1649 1 1.295 1509 1 1 .316
1641 1 1.296 1503 1 1 .317
1634 1 1.297 1497 1 1 .318
1 627 . 1 1.298 1 490 1 1 .319
1620 1 1.299 . 1484 I 1 .320
1614 1 1.300 1478 1 1 .321
1607 1 1.301 1473 1 1 .322
1600 i 1.302 1467 1 1 .323
1 593 1 1.303 1461 - 1 1 .324
1586 j 1.304 1455 1 1 .325
1580 1 1,305 1449 1 1 .326
1573 1 1.306 1 444 1 1 .327
1566 1 1.307 1438 I 1 .328
1566 i 1.307 1438 1 1 .328
1 559 1 1.308 1432 1 1 . 329
1553 I 1 .309 1427 1 1 .330
1 546 1 1.310 1 421
1 1 .331
1540 1 1 .311 1415 1 1 .332
SETTING 1410
1404 1399
1394 1388 1383 1378 1372 1367 1362 1 357 1351 1346 1 341 1336
1 331 1326 1326 1543
1537 1532
1 526
25 SET METER 6 PUMP ___ ___G (RECORD FROM. TABLE)
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY 30 SECONDS 26 ADJ LEAD NITRATE TO 76 (3625 G) AT 67-69*F.
RECORD: ___ ______F
STIR 5 MIN & RECORD PH: ____ (2.2-3.7)
28 IF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 667.
6 RECORD PH: _____
ASSUME 50%
NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING
RECORD: ____ __ G/ML (1,143-1.144) IF OUT OF SPEC
FILL OUT CHECK LIST & ATTACH.
.
30 STIR AT 67-69*F FOR S-31. TAKE 1 QT SAMPLE.
*
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41-D 57-A
33-D 7-0
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COMTYP JOB NAME: 01YE698DMT PAGE 02
Erw?2
LBS | CODE I LBS
AT APPROX 100..G WHILE CONTINUING TO PUMP, CHECK PH & DENSITY. PECORD -BELOW. IF NOT
IN RANGE. STOP PUMPING 6 ste&UPV. * FH:_g^ (2.2-3.?) ' 'Sir;.
DENSITY: JJZJLfk. G/ML < 1 JZZfrr*-.328>
IF S-22 OK 6 WHEN 5-21 COMPLETE.,-..,RECORD
NSITY LxJrJZt G/ML. ON TRAPPED iSAMPLE
FROM END OF S-21 PUMPING.
ir
USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21.
CIRCLE DENSITY A SETTING IN TABLE BELOW.
*.**.* TABLE ****
~ I --~,
;
I i G/ML SETTING 1 G/ML SETTING I G/ML SETTING ! j 1.270 1644 i 1.291 1504 I 1.312 1382 I 11.271 1637 1 1.292 1487 1 1.313 1376
i i 1.272 1630 1 1 .293 1491
1 1.314 1371
I 1 1.273 I i 1.274
1623 1616
i 1.294 | 1 .295
1485 1479
1 1.315 1 1.316
1367 1361
1 11.275 1 1 1.276
1609 1602
1 1jl?6 ___i 472L 1 1.317 | 1 1.318
1 356 1351
1 1 1.277 1595 1 1 .298 1461
1 1.319 1345
1 i 1.278 1 1 1.279
1588 1582
i 1.299 I 1 .300
1455 1448
1 1.320 1 1.321
1 340 1335
i ! 1.280 1575 J 1 .301 1444 I 1.322 1 330
1 J 1,281 1568 | 1 .302 1438 1 1.323 1324
i 1 1.282 1562 1 1 .303 1432 1 1.324 1319
1 ! 1.283 1555 1 1 .304 1426 1 1..325 1315
1 1 1.284 J i 1.285
1549 1542
1 1 .305 1 1 .306
142 1416
1 1.326 1 1-.327
1310 1305
I ! 1,286 1535 1 1-307 1 410 1 1.328 1 300
! 1 1.287 1528 1 1 .308 1404 1 1.329 1295
I J 1.288 1522 | 1 .309 1399 1 1.330 1 290
1 i 1.289 1515 | 1 .31 1393 1 1.331 1 285
1i( 1 1 .29
1510
I 1 .31 1
1387
I 1.332
1280
3t3S"METER & PUMP
.G (RECORD FROM TABLE)
1 FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY
! [3 SECONDS
DJ LEAD NITRATE TO 3625 G (76"-242/245 6 74-5"
2D AT 6,-7j 69mF
. i FrECORI):
___ *F 6 ICE CONSUMED (3304/BL0CK)
27T STIR 3 MIN. 6 RECORD PH: itcjL (2.2-3.?)
! Js**** USE TITRIMETER TO ADJUST N-41-D PH ***
!2m IF NECES;SARY ADJ TO PH 3.0-3.1 ! I & RECQOIRD PH: PjJLm
ASSUME 66%I ASSUME 50%J
1/HMOJTfEE: DILUTE N-7-D 10:1 WITH WATER BEEFFO_R..,,E. A__D_D__IN__G_
iCPT RECORD: Lll&y G/ML (1 .143-1.144) IF OUT OF SPEC!
FILL OUT CHECK LIST 6 ATTACH.
j
301 STIR AT 67--69*-F FOR 5-31. TAKE 1 QT SAMPLE.
!
41- 5110
57-
33- D |. 7- D I. !
*
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DUP050059679
LOT: .
jreUip' MENT'I
COMTYP JOB NAME: 01YE698DMT PACE 03
DATE PRINTED : 10/J 5/82
USE N- IACCT LBS CQDE I LBS
OBTAIN 1 QT SAMPLES OF S-18 & S~3 SOLUTIONS
& TITRATE TWICE
NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
7,1-7-4 OR IF THE TWO TITRATIONS DIFFER BY
MORE THAN 0-1 ML N-10-D <IF YES, FLUSH ALL
EQUIPMENT 6 REPEAT TITRATIONS)- DO NOT
PROCEED IF N-10-D TITRATION IS OUT OF RANGE
AD JUST V-358 FOR A TITRATION PH OF
FRO% FINAL IN-LINE TITRATION, .RECORD LOWEST
9* lij:L. 6 ML N-10-D
^>1 ViMf
/,*r-
WHEN S-31-TITRATION~OK~~ STRIKE~V-35i_THRU "
BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
16-18 MIN
, jt
j
RECORD: . START
TOTAL MIN___ /A____
NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
i BUBBLES APPEAR IN SIGHT GLASSES
IMMEDIATELY DUMP IN N-4-A FROM S 3 & SET TIMER
FOR 15 MINUTES
URING S 33, WASH IN V-358
STIR 2 MIN & RECORD PH_._jL.!^< 1 -8-2-5)
f'BXS,__3Z__(MUST BE + )
STIR TOTAL OF 15 MIN FROM S-33 &
RECORD : TEMP__Jj.__ F < 67-?3*F)
DUMP N-3-A FROM S-4
STIR 3 MIN
POUR IN N-32-D FROM S-5
STIR 2 MIN
-RUN IN LIQUID ALUM USING BADGER METERSTIR- 3 MIN & FLUSH ALUM LINE WITH WATER
734
DUMP IN N-3 FROM S-6
STIR 4*MIN FOR S-48
4*r
RUN IN HYDROCHLORIC ACID USING WEIGHT & FLOW., I * -
aiM-% Ji?.CONTROL PANEL
K jL..,
I
MK ,,_______ %1______ _
DURING S-44 SIFT N-711-B FROM S-7 INTO V-390 |
WITH AGITATOR ON IN 1-2 MIN
|
STIR i-2 MIN TO MILKY SOLUTION
33-d 7-D
115-DI 28-D 28-D
367
WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B
SOLUTION GRADUALLY OVER 5.MIN PERIOD INTO SV
WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
UNTIL FOAM SUBSIDES-
DUMP IN BLANC FIXE N
WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
TOP' OF PAGE 1
__
RECORD: CODE
LOT _r=.___ , ___Z_____*
STIR '20 MIN
j
RECORD: PH_JL-Jl-- < 5 - 8-6.0 )
IF NECESSARY, ADJ TO PH 5-8-6-
ASSUME 50%
6 RECORD: PH-jfcn_
ASSUME 66%
FLOOD TO 153" (7298 G) STOP AGITATOR
330 | 128-A 330
7-D 33-D
I
4W4-
3FiI?NIsSH*hr\
F;TR
DUP050059680