Document LKqegKjKB27GNoEOBLVn28QRb

j -'"f A PC8 LITERATURE REFERENCES INFORMATION SOURCE Organochlorine Resi dues, 0.E,C.D. Preliminary Study 1966-1967, Sweden, G. Widmark, Univ. of Stockholm. Chlorinated Hydro carbons in British Wildlife Nature 216, 227 (10/21/67), BTC. Holmes, O.H. Simmons, 4 J. O'G. Tatton. Organochlorine Pesti cides in Seals & Porpoises, Nature 216, 1274 (12/30/67), ATV7 Holden 6 K. Marsden. Chlorinated Biphenyls in Fish, Mussels, 1 Birds from the Rhine & the Netherlands Coastal Area. Nature 221, 1126 (3/22/69), J.H. Koeman, M.C. TenNoluer OeBrauw, & R.H. DeVos. TYPE * LEVEL PCS REPORTED ' Analytical tech . NIQUES REPORTED MATRIX OF SPECIES ANAL. 4 LOCATION Reported as PCB EC/GC on QF-1 4 SF-96 Sea Eagle, Salmon (juv.) (Cl4-Cl8) ppm columns chemical con 4 Pike. Sweden. chromatograms firmation; Nitration similar to Aroclors (mild) 4 Sulfuric acid, 1254-1260. extraction. Some GC/Mass confirmation. Reported as PCB resins. Eludes to highly chlorinated biphenyls and 1ightly chlorin ated terphenyls PPb. Reported as appar ent PCB. No level stated; chromato grams similar to Aroclors 1254 1260. Reported as PCB to Aroclor 1260, Phenchlor DP6 4 Chlophen A60, ppbppm. Also re ported the pres ence of tetra- 6 penta-chlorobenzene 4 of trlchlorobiphenyl In a roach 4 eider sample, mostly Cl4i5-Cl8. EC/GC on SE-52, Aplezon Sparrowhawks, kestrels, L, 4 XE-60. Some T.L.C. giullemots. Also Sample clean up DMF/HEX detected small amounts partition followed by In human 4 animal fats. L.C.C. (Alumina). U. K. EC/GC on XE-60, DC200, 4 QF-1. Sample clean up DMF/HEX par tition saponifica tion. Seal 4 Porpoise Fat. British coastal waters. EC/GC on DC-200. Samp le clean up DMF/HEX partition followed by l.C.C.(Fluorlsll). Confirmed by GC/Mass (CH4). Roach, groundling, nussel, sand eel, sandwich tern, elder. VALIDITY Positive 7 7 Positive HONS 073402 PCB LITERATURE REFERENCES Page 2 INFORMATION SOURCE TYPE & LEVEL PCB REPORTED ANALYTICAL TECH . NIQUES REPORTED MATRIX OF SPECIES ANAL. A LOCATION IALIDITY W. A . R. F. Institute Study of Lake Michigan - unpub1ished 9/69. Progress Report to the Wise. Conservation Di v . , Dept, of Natural Resources for Research Contract on Chlorin ated Organo Contami nants in Milwaukee River, S.F. Lee & G.D. Vei th. Reported as appar ent PCB similar to Aroclors 1254-1260 ppt-ppb. Reported as uni dentified com pounds possibly Aroclor 1248-1254, A 1260. EC/GC on DC-200. Sample clean up, saponifica tion followed by L'.C.C. (Fluorosil). EC/GC on QF-1/0V-17, sample clean up L.C.C. (Fluorosil). Water, Fish A Plankton. Water, Fish A Plankton. S' ? ? Polychlorinated Bi phenyls in the Global Eco System, Nature 220, 1098 (12/14/68), R.ffTRisebrough, P.Rieche, D.B. PeakalT, S.G. Herman, M.N. Kirven. HONS 073403 Reported as PCB type of Aroclor used as standard not stated. Aroclor 1262 mentioned in article ppb-ppm. EC/GC on DC-200, QF-1 & SE-30/qF-l. Some microcoulometric work. Chemical treatments nitration & saponifi cation. 1 Peregrine falcon(adult, juv. A egg). Eared grebe, Black petrel. Least petrel A eggs. Fish bat, Craveri's murrelet A eggs. Elegant tern eggs, Heermann's gull eggs, Adelie penguin ^ggs, Western grebe. Fulmar, Pink-footed shearwater. Ashy petrel. Brown peli can eggs, Frigate A eggs. Brown booby eggs, Brandts cormorant eggs. Pelagic cormorant eggs. Cinnamon teal. White-tailed kiteeggs, Cpopershawk, Golden 'eagle egg. Osprey,Meilin, American kestrel A eggs. Black-crowned night heron A eggs, Western gull eggs, Forster's tern eggs, Caspian tern eggs, Red phalarope. Common murre eggs, Cassin's auklet, ' (Continued) 1 INFORMATION SOURCE DDT & PCB In Marine Animals from Swedish Waters, Nature 224, 247 (11/18/69),'17 Jensen,A.G. Johnels, M. Olsson, G, Otterland. PCB LITERATURE REFERENCES TYPE & LEVEL PCB REPORTED ANALYTICAL TECH . NIQUES REPORTED Reported as PCB (Clg-Cls). low ppb to nigh ppm. EC/GC (2 column) chemical treatment, saponification A extraction with sulfuric acid. Some GC/Ma$s. Page 3 MATRIX OF SPECIES ANAL. & LOCATION . (Continued) Ancient Murrelet, Rhi noceros auklet. Morning dove (N.D.), Barn owl ' eggs. Meadowlark, White crappie, Bluegill. Panama - Isla Pacheca & Isla Pachequilla in Gulf of Panama. - California - Puget Sound, San Diego Bay, San Francisco Bay, Baja. < VALIDITY Mussel, herring, plaice, picked dog fish, cod, salmon, grey'seal, common seal, ringed seal, guillemot, white tailed eagle. Positive 1 MQNS 073404