Document LKpkwXmL1eZwGr9O0LKQ7xe2w
> Jr---------* ----------
Q.V '^9^903
CG &2
CODE RT-870-D PKG ___
mi a p M { DATE ) '
QZJbO ("l o t -)
2579* EST UGT )
D.V 902,9M04E PRINTED;
PROCESSES
APPROVED BY '
< JRT-870-D <H) EUK 1-11-82
COMTYP JOB NAME; 32RT870DMH
TYPED BY: JMH
>n
STANDARD HRS,___________ TIME.
PREPARATION NOTES;
{
NON-BLEEDINC'
EQUIP i MENT I
I I I i ( 1 i I I I
i I USE
I NAME: WATCHUNG RED B
1 LBS
| --J >-----------------------------------------------------:------------------ | ____
I NOTE; DO'NOT START IF PRESS WILL NOT BE
I
I AVAILABLE WITHIN 3 HRS AFTER MAKING, SUPV |
! TO REVIEW WITH P.R. SUPV & RECORD:
i
I PRESS WILL BE_READY_^>^M ^JL/fA.__PR SUPV.l
1 START MAKING_?L^_M^2&A./fi.-^M5fMAKING SUPV.l
I NOTE; NOTIFY PRESS ROOM BEFORE ROPING OFF I
i AREA UNDER V-922
|
I NOTE; RUN 15' WATER INTO V-904. PUMP WATER i
I FROM V-904 THRU DISTRIBUTOR, IF WATER DOES I
I NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH I
I `FULL FORCE, NOTIFY SUPERVISOR.
|
) N-CODE | ACCT ! 1 LBS I----------- - ,---------
I1 I I' I I >' 1I I1 i r ir ii ii
ii i -i
PREP 1 ..
921/ 931
2
1
RECORD
___ .'BATCHES SINCE SPARKLER LAST
CLEANED, AFTER 4 BATCHES, CLEAN, DRESS
SPARKLER & PRE-COAT WITH 151= DICALITE,
FILTER AID.
OBTAIN FOR S11 2-CHLORO-4-AMINOTQLUENE-5-
I J"~ SULFONIC ACID.
! i/OBTAIN FOR S27 3-HYDR0XY-2-HAPHTH0IC ACID
| y'l INSTALL DV & DV RECORDER & CONTROLLER CHART
| RUN 11s (10OG) WATER INTO V-/?_/___a, ADJ TO
| i 80-100 DEG F
I ADD' IN 2-3 MIN DRESINATE X
\/T\ STIR 5 MIN & RECORD
(9.5-10,5)
f 8^r STIR 20 MIN OR LONGER TO DISSOLVE FOR S49
! I 1 ____1
1 i I
i
I I I 777-A I _____
i. 740--Ci S2-C I
I'
.I I
108 |
I
I 530--A | 1^8
I '
922 3
r RUN 35" <722G) WATER INTO V-922
!
WEIGH SODIUM HYDROXIDE IN V-926.J5. RUN IN
.A JT
M _____
? -D
TURN ON AGITATOR & STEAM G DUMP IN FROM S2
740' -C i 1086
2-c h l o r o 4-AMINOTOLUENE
L-OJ . 9i9.0V/ /U
i i
5-SULFONIC
i
ACID DUMP IN ACTIVATED CARBON
i 113-B f
25
DUMP IN FILTER AID
777-A j
10
i \jr\ HEAT TO 212-214 DEG F WATCH FOAM!!
i
m: RECORD: BY__Tl-<+> IF NECESSARY ADJ TO +BY
f
SODIUM HYDROXIDE
ASSUME 50%
7-D
11 STIR 30 MIN AT 212-214 DEG F, THEN SHUT OFF I
STEAM W__A__T_C_H FOAM! NOTE: RECORD SPARKLER |
PRESSURE t2. SUPERVISOR*
_PSI. IF NOT ZERO NOTIFY
JULi261982
I
N32900
!
!
DUP050464645
LOT= _________ COMTYP JOB NAME = 32RT370DHH PAGE 02
EQUIP NENT
9'?'?
5*"
CONT
t
! PAGE 2 OF 4 CG 32 CODE RT-870-D (H)
CIRCULATE 15 MIN OR LONGER THRU SP&FfKLER ' iI uUrNTIL S__O__L_1_N___IS_ JJL__E_A_R_* _M__A__I_N_TAIN^jl ?0~1 95 I DEG F FOR S22/REC0RD: START
TOTAJk MEN___ kL___ CUAam*J_____IrfEZ" 1 HT_yjf_H__ F '& REC
DATE PRINTED: 7/19/82 USE N-CODE i ACCT LBS 1 LBS
t. .
MISC 4
MEASUR3E LZJS UNITS IN V-928 FOR $39
:
I LH4YDRQCHLOQRIC ACID
M__J_____ , JsSlEJ-Z
11^1 WEIGH SODIUM NITRITE IN PT FOR S42
M.
WEIGH. SODIUM NITRITE IN DRUM FOR S50
l/f&fj
\USB-- i '
28-D
725-A 725-A
I. I
i I
I j
438 397 -43
\28T
2' <58G>-WATER INTO V-904/CV
|
WHEN SI 7 :IS COMPLETE*? PUMP IN V-922 THRU \
SPARKLER, HA I NTA^ ..V-922 AT 190-195DEG F* I
RECORD: START__^____ TOTAL MIN__*L?L_ 1
I
922 I WHEN S2'2 COMPLETE, SHUT OFF PUMP AND INSERT 1
6 22 FOOT PLUG
I
i RUN IN 10" C209G) WATER & HEAT TO 190-195 F
I
! CIRCULATE 15- MIN THRU SPARKLER -
!
I
SSS^CVIS-f^l AND PUMP V-922 THRU SPARKLER INTO V-904/CV 7
902 . l3rjLUN 65' <16960 WATER INTO V-902 8 i^'TwE.IGH SODIUM HYDROXIDE^IN V-92^^JL^IN
IJgasn DUMP IN FROM S3 i 3-HYDROXY-
I -t 2-NAPHTHOIC ACID
____________ (JgJLJT ___________________
! ADJ TO 70-90 DEG F $, STIR TO DISSOLVE
i
! 7-D I 82-C I
399 994
922 I3m\ RUN IN 5* <1040 WATER & HEAT TO 190-195 F J
9 I I CIRCULATE 15 MIN THRU SPARKLER
*j
iI
,I
P V-922 THRU SPARKLER INTO V-904/CV
I
WHEN MTY BLOW OUT SPARKLER INTO V-904/CV. |
SSOLVE ALKANOL XC IN 20G WATER AT 150-160]
U^Hfe AARTOMTQ HO1T65W-1A7T0ER
MIXER F FOR
IN S38
DRUM
&
PGURIN.
I I
I
932. 11
RUN 16" <3280 WATER INTO V-932 & AD.J TO
i 8B00--110OO0 DEECG Fl F ADD IN 6-17 MIN DRESINATE X I STIR 5 MMIINf & RECORD PH.________<9*5-10-5)
\y6 | STIR 20 MIN OR. LONGER TO DISSOLVE FOR S59
I I
| 1
1 33--B*
378 r 53300-A I
32 378
DUP050464646
LOT=_________ COMTYP JOB NAME - 32RT870DMH PAGE 03
BATE PRINTED: 7/19/82
CG 32 CODE -870-D <H)
USE LBS
N-CODE
ACCT LBS
N-74f-C SDL. WA PUMfED DIRECTLY
KLERlTO Cl S2i 1B,2| OMli S3l &3S
(5G> w a t e r iin t o
\'-?m AT 65-1W0 DEG! F THRU UreDERSuR-
HSTlfelBUTSR INFO CV &FAP K12-145 HIH>
N IN N-28-D HYDROCHLORIC ACID FROM SI 8 IN
12-15 MIN. MAINTAIN' 165~17*F IN CV. STIR 15 MIN AT 165-170 DEG F
no i
ADJ TO 46" (4347G) AT 32-38'DEG F
PS4.X330 |
RECORD: TEMPDEG F, VOLUME_____
RUN IN N-725-A SODIUM NITRITE FROM SI 9 AFAP
(5-1 MIN) & RINSE IN F'T
NOTE: PROCESS HAS A VERY LOW N-23-D EXCESS
CHECK CR VERY CAREFULLY
STIR 20 MIN AT 32-38 DEG F MAINTAINING
+CR, +KI FOR S44. RECORD: TIME START______
CR___-l__, KI,,__rkr___ NOTE:
1)' IF CR-, KI--ADD 2v "AS IS" INCREMENTS
RECORD CR'(+) KI( + )
HYDROCHLORIC ACID
ASSUME 32%
2) IF CR+, KI- ADD 204 "AS IS" INCREMENTS
RECORD CR______( + ) KI< + >
SODIUM NITRITE
ASSUME 33%
DUMP IN CALCIUM CHLORIDE
ADD FOR MAINTAINING 32-38 DEG F THRU. S55
7-A i'3l3>l&
1026 L&sjoo
FILL PT APPROXIMATELY 1/2 FULL WITH 90-110*1
WATER FROM HOT WATER MIXER
j
IN STRONTIUM NITRATE
i
STIR 30'MIN OR LONGER WITH LIGHTNIN MIXER I
TO SOLUTION FOR S58
|
-------------------------------------------------- :---------------------*-------------------- !
WHEN S28A COMPLETE, 'STEAM EJECT V-921/9.31 |
FROM SS INTO -V-902. .
|
POUR IN N-725-A SODIUM NITRITE-FROM S2
ADD AMMONIUM CHLORIDE
CV Vfs2 I1 IMMEDIATELY COUPLE V-902 THRU UNDERSURFACE 1
15 i I DISTRIBUTOR INTO CV IN 18-22 MINI RECORD: (
1 1i STARTJ&'dbrTsn.___ TOTAL MlN__SyC______ _
1
| | |
'HITS ! PT 1 DURING S52 WEIGH SODIUM HYDROXIDE' Itf-aPT,***" 1 vjra i
16 iI
m__zlL___ /ttzLvJtz
^54 :I DILUTE TO MAXIMUM VOLUME (+/-100G) FOR S56 [
i |
CV
WHEN S52 COMPLETE, STIR 30 MIN & RECORD:
I
17 DIAZO_j___( + )
BASE____ +1___ ( + )
PH__
(5.0-6.0)
TEMP_3cT (32-38 F) I
| RUN SODIUM HYDROXIDE IN PT FROM S54 THRU I I i UNDERSURFACE LINE, RINSE IN PT i STIR 15 MNI
RECORD: DIAZQ
BASE,.!!___ ( + )
PH___ f
<9. -9.8)
\p8o 1 RUN IN STRONTIUM NITRATE N-246-B,E SOL'N
VK!?9 ! FROM S48 & RINSE IN PT STEAM EJECT IN V-932 FROM S36
.i STIR 5 MIN-&-RECORD;--PH
<9.0-9.8)
1 i i
1 7-D i
i
140
DU P050464647
LU I
UUM5YP JOB NAME 32RT870BHH PAGE 4
iTE PRINTED: 7/19/82
EQUIP | KENT |
PAGE 4 OF 4 CG 32 CODE RT-870-D <H>
USE j N-CQDE I ACCT
LBS 1
I LBS
17 61 I IF PH BELOW 9. ADJ TO PH 9.0-9.8. WITH CONT I . i N-7-D ONLY. RECORD PH_______
I' |
SODIUM HYDROXIDE
ASSUME 50% i.
vj-ssr"i POUR IN I OCTANOL
1
iA&s i HEAT TO. 193-195 DEG F IN _70-75 MIN & RECORD!
' 7-D 38 | 588-A
38
HT_Z&C__DEG F AND REC_/i&S___DEG F
|
1 STIR 60 MIN 'AT J 93-195- DEG F.
j
1 I RECORD: START|
I AFTER 20 MIN S64 STIR
RECORD:
|
Ii
PUjSt-CL < B. 8-9.3) I
1 I pi PH BELOW 8.8, ADJ TO PH. "78-9.3 WITH
I
I D ONLY. RECORD PH.
ASSUME 50%
7-D
\'t> I AFTER S64 STIR, FLOOD TO 180-190*
<+/--1S,00OG) AND STOP AGITATOR
I I WHEN INSTRUCTED BY PROCESSING AREA HALFWAY |
|
|
! I THRU PRESSING, DUMP IN, STIR 5 WIN- & STOP I 10 I 588-A i 10
I ! AGITATOR. RESUME PRESSING.
!]
|
DU P060464648
^32900.01
DUP050464649
N32900.02
DUP050464650
N32900.03
DUP050464651