Document LKd170qK1r39pdpnqyV14kdQg
stAmerica
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ANALYTICAL REPORT
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PROAIFOSAnalysis
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Lot, orsoio20r
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Laura VancholJane Hanuszczyk
ESpAamnsoan eer
--
aromahnys October 22,2007
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ss eronsn in ORE ASSEN MASA
nc
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Table Of Contents
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Standard Deliverables
Report Contents
Total Number ofPages
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rSTheteeaoanvfedhaiLreSdatnrDdceadlniDhveeeRerplaobritlCepssarclkeagpee.eTahri rcepoornt siincdomeplret]e []
es pegs sed nh oleofCoinsre nde
TaobfColnteents
+ CaseNamative
+ ExecutiveSummary Detection Highlights
+ Methods Summary
i
Metbod/AnalystSummary
+ LotSampleSummary
+ Analytical Results
+ QCDataAssocation Summary,
+ Chain-ofCustody
NOAHO00! -------
Cas7e04Na0r2r0a7tive
TlheyresMuasraInlc.luAded1I0n t5iss rheapvoerbteheavnefbouenenfroevmieeswtedalforrecqoumiprlieamnecneotwsfitNhEtLheACLaabonrdaatnoryy
exceptons are noted below.
i:
Tis report shBalloont bo reproaducled exnceptvnfel,bwitahount thde wioenn aepprdovaslofttholasborattory rs rerprtatonofth resus.
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`oJSaaebmoprBlareteAterywrtiivalaeltaesmnapmdepRrleaectsourlpeporetfse4n6tedCionntiOscteopboerrt4w,e2r0e07r.eceived a tha TostAmerica Denver
S(tPaFndOa.rdPsFtaOnSda5rds cwoemrmeerpcriepaalrperdepusairnegdtahnedaccarftoedmsolfutlhoonc.ompound peruorooctandic acd
i
peruoro-n1,2,34-Coctancic acd was introduced at he extraction step and vas used t`an iunternnalastannedaerxdtffoarcqiuoanntsitteaptiaonnowfaPsFOuAs.edPaesrfalnuoirnot-e1m-a1l,2s,t3a,n4d-a"rCduJfoorctqaunaatneisuflaiotnoantfe
as
was
POS.
`ESamxpletracatndiAnaolysnis TDhorevsera'msplSeOsFprDeEsNeAnCte-d0I0n1t2h.is report
were
an
aly
ze
d
for
the
target
analytesb
y
Tes
t
A
me
r
i
c
a
FeForoeatnerwsasrasoamscpceleheddsstu8hsa2rimon5ugp0gshm1i6hLdseaphicklasetdeqiwdguioefexht,oerhaahetccethinsaoanenmatapbelltcheenissisaaqnruadeecaewdriudfti,ehedpmdrweiwiotirhhtohar44emlxmitcLr.aoocnoftfdiiom6inNe.otHnhACeadnIfosCrlo1.lt8uhTieohne
eorees brought 1.8 mL. using methanl and the extroct i analyzedby LCIMSIMS.
e EMetehoo odtQ30CsSSaamimpnlpkelssesopfrohceesssaemdermeaagrexn.t wTahleermseptihkeoddbwlialhnkssuwrreorgeatneoann-ddeptreecptatre1d wiftepcaarcthng
mifor tth target analytes.
eEavcehsbwaotcrh wIsipiinepeasrteadblwiisthhedLacboornattoormyiCo,ntrxocleSpatmapslensot(eLdCSb)e.lowT:he LCS recovefroriboetsh
!
AA nalviecrfaolnCweaoimsoarmmespTanlamtecpssolvweaesrrybefyoetrh-oPxlFraOabcoAriIaotdoQriynCfQbrCattbhciahsl7cmh2et67h22o18d16.015wT6ahaseftbLeerCltSohweret7choedveoarwyieehrsofcnoorgnbotttrihmolelevt,ehlast:
re Goirl 1 th re-exaction batch. Both sets of results are reported.
Jtshovid be noted that there i no pomugaled holding tme for tis method.
TThereewasaivnsulfafbiodreanttorsyamcpalnetvoslaummpel0espwrroveidperMepSa/rMedSDinaenaaclhysbeaticnhhteo prroavniadlyetdicaanlibnadcicha,tion
ht tho analyica system was in contol
1 -
NaARO00!
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No other anomalies were noted.
i
NIAWO00! ------
EXECUTIVE SUMMARY - Detection Highlights rana0zer
wvTeR.
mor smepaorRTING pwns Avemmiorpo.
BXRCR CREEK 5OB 10/02/07 03:15 092
:
Psroonx
coooe 0o0ss wvain oomm --cc--00001122
DRRNTE FOB 10/02/07 13:15 003
rroosn ros
0lo0r4e33 00..01050 vvaa/nL oooss 3 0010 wall
DoEmX --1ice--0a0m122 Dm -rc-0012
|
son
cloves 3 olois val mv -1c-0012
i NIAWO00058
METHODS SUMMARY
:
rasa0z07
H eawversm
me wrTmIoeL r u eRapAm RATIOd N
: Les us, Bron
om 1-002
References:
oe oSpeevreartniTnrgenPtrocLeadbuorrea.tores, Denver, Facility Standard
i ---
NIAWO00S ess.
A O------
i
METHOD / ANALYST SUMMARY
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orsoasann
i
nEmoonvo
fr
rFyer
om -a-0012
Sacueline Bonnet
onsen
Reterencen:
pm sCoeevrearstTorsenptrocieadbuorrea.toren, Denver, Pactidty Standard
NAN000587
SAMPLESUMMARY Dr0s0207
Wo # Spies CLIENT swpLe 1D | Jo76exT o00n2 BsIeRCcHsCRErEoKr FOF
S76x0 G03 DRRWTR OB
snueLED smwee 1200//0022//0077 0089::2205 10/02/07 13:25
| H-- BAoRmRb(5c) rndeon eg il rf re hn --
eimpotetoth ppormcar,seeelst,re 4w7cgpp ae ph peroet,Fo,i,
crof,hoany.dy, gl, A yr A, oti, KL, pney 0
i '
NIAWO00E ----
marican ates company
Client Semple To: BECKETT 208
me
LTrooettep"-SSDaaaptlemsemrio..e.1..1:+
D20I/T0O2N/007T-900G:L30 20/05/07
WDoartke ORnedceeriv.e.d..+: Nasdyois Dacei.
J10/N04/U01 10/23/01
MaLrix.........: WATER
DTirtopucBioanteac0t1o1r.:1 71282130
Noaiyeis Time: 02141 Mothod........: DEN -10-0032
|TomBaBere
frB=
spprointa mo
ie
Gos wen com
seca
sacovaxr
o SSceiuurpromoxs eoowrs KiE mecoveRyLGGioo m=- 2m_o_0m
J
i
1
NOAH000589
asbeet s nseo comees0
|LetTBeeEiRtmTeieo:o sTaamoeE hrnesRw me Rnme bbai eory nn
ompope
A oz2 r mCTlme m mE nom
|= smomenns
oI m a
:
i
; worwoooss0
American ater Company
Client Sample ID: BIRCH CREEK FOB
we
TDoatt-eSaSmapmlpele#d.....:.t Prep Date.....:
D1I0I/00420/20077-0090:215WoDartke ORredceeriv#.e.d.:.: 10/09/07 Aealysis Date:.
J1I0E/X0T4/I0R7A 20/11/07
.{DilburetpipoantchFac#t.o.r.:: 17282100
AnalysteTime. : 02:57 Method. ......: DEN -1C-0012
Matedx....oooot WATER
| Pmreosne ron
' soRmomTs | T1o3cce4 wperoons
somnso 0.016 `emrBzccovmEnRTY 57
RuevroRTING pars wm Soosw vwoah 00..00603301 Rperceotvyery ((5500 -- 220000))
NIAW000591
i
American Water Company
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Client Sample TD: BIRCH CREEK FOB
me
1
tDa-tseamSepclpele#d......:: rep Date......:
D12I000//001M330//2000777-0090:215WDNoaertakelyOsRniedaceDeriavteed.......:::
J10T/E0X4T/Z0A7A 10/15/01
Matrit.........t WATER
i| opirteupemtoan rpaectser.: 17aaaSe
oalyais Tioe..: 02:21 Method........+ DEN "10-0012
i perrsone
awms
LREproRTING G.o0
wvalou rse0n.0020
vos vai 0.0031
ES
0.018
i sancmeoarrosn.
e`nvecaovreRY ig
L`RaecrovseRY (50 - 200)
| 1304 PROS.
a
(50 - 200)
1 NIAHO00592
American Water Company
Client Semple 0: DRRNT? FOB
me
oLrotetep-SaaSmatpmlepelre..d......:.+
D1700/00420/20077-1020:315 10/03/07
WDoartek ROercdeeirved.....:: Baalysin Date..:
1J0I/E0X4O/L0A7A 10/11/07
MALEAX.........: WATER
| prielpuiBoatnchFacdt.o.r.:: 17202120
Analysis Tine:. 03:23 [----
!
eParonsuTER
R0e.s0u0r347 0.0076 3
LREozaorRTING pars bo was
w0.n0630
os van 0.002
ProR.
`SsaucmhsoporTosn
spncraevTy 20
`pRercotvery (so - 200)
Tacs pros
0
(50 - 200)
| om):
; NIAW000593
American Water Company
lent Sample 1: DRIP FOB
me
oDatt-eSaSmapmlpeled4......:+ Prep Date...
D11I00J//0014230//3000777-10301315 WDAonaratkleyORsretdcseeirDvaedt...e...:.:: J21T00//B10O54//T00A77
MALEER.........: WATER
PDrielputBiaotnchFa9ct.o.r.: 71286156
malyots Time:. 02:42 Method...+ DEN +1C-0012
Foronse
r0.e0n00)57 0.0089, 3
iRemvaorRTING wmars bow wat
e0.u0630
os vai 0.0031
Fron
|Po sscmemowmromn
psrEeRca 5
RLuewcrorsv.er so - 2007
|| 1o3cmee5708
es
(50 - 200)
i
NIAWOOOS.
pane QC DATA ASSOCIATION SUMMARY
Sarpie Preparation and Analysis Conceel Wabere
| . sem wm smonuerrions
i.
wn wmmm oomm weoenes
wr nwmm oomm ccooomna
wr wmmm oomneinca
wiees mmaama xem mTaeaansse mTaesessee Tenazso
;
.
|
aAw000 -
somesom
!
||P
tSa Eot T oree s oemesmmnesorer
SrHPLC SeeeRpmEacEe reroos
So H20/E03/07
EE
NealystaThea..: 01153
Co i 5
p2=on sRB CaI c ea umm
|| cmoemam
mm= eon paman
sm u ee
i
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THD Bu RErORT
!
me
Clfens fot #...: D0040207 WorkOnder ...: JUNGSIAA
Marbx...o.... WATER
ToToesemis b1 aslywio Dave..s
R73120000-156 10/15/07
bpereepp DDaavteeh..#.o.o.s1
T1I0R/6113S/607
Aaalysin Tme..s 00:39
Diiurion Factor: 1
:
w Tron era
mwo swr
swEaEev--orr Gos
wuSaRmm
eoowmm
iucoene
ros
| sBummaownwrs
mseomcmarsr wwo
LsGsoocao=mv7r007 Go = 200
13 ros
b mee r EEES
|
|
|
NaAR000! en
LABORATORY COFERGL SAMS SVALGNTION RESORT.
woe
CSeleiseenTptoaeT-tosteumBnp.ti.e.sd:
DR2I7000/005430G/02000707-11|0 WAosraklyOsntdserDate.....::
JIGTIAC 10/11/07
Matrix........os W! ER
| DDiilpucmioenmFaactlolrls a3 mmo Moaayeds Times 02:09
| mroen m
Smsccoamx a
sGsLocpoavr-esRmym
bsonmcooos
5
Gs 220 pan comz
ros
| sSemvsomnomr
smcmao in=
mpaacotvseRy Go0 - 270000)
13a ros
L C|omes f E rim R " msc-- ortren. --
NOAWO0059
--
i
i
| chttoet m#..t.: i 1P0r8epLeoDtaa-tSeeanmp#l.ee.ft.t::: | pidueion racers ToeEY
rFrroons ! sSmamceorarosn
ace pros
ne LABORATORY CCHTROL SNPS DATA RERORT
00080207 WorkOlax $sJIGTEC
RT77o23j00a78s10/1000070-110 AAsnaallyyssiios TDiatmee....:: 1020:/0193/07
3
osomre Poe
smemowo basa
oa oma
ican4nocv
MabriX.oooooot
mize smeecnocveey wwm ns8 mGRoBCm-OVEaR7Y00) 0 - 200)
-ok--b ctrmce ae odetsiir dsclso.m hot
WATER bMeEmo1o6-0017 Dn 1-002
NIAWO005S
LABORNIORY CONTRGL SALE SALINTLON REFORE
me
C5l8ieTnotat1sooateg.ti.e.::
RDN1729o0094o0002o0007-120
Work Onder ...: Aealysis Date.
JIGTID 10/13/07
Matrix... WEE
| ToOiP eeteiitlsl 7+ s Aealyeis mime. 02138
C[LTt HE ros
Sssmceovaerny 05
LmTsacwoonvsemRye Goh roncavr
sooermmawen oeme acoveRy
{dcsyamy ooos m
m&" ov L GGoo --m 7200007)
Nmoirsee):es po
----
|
NOAHOOO! en
C5hSienLtotT-SoatmpBl.e.h.ss urepppBaattech. .o.i.:: Dilution acter: --PanneTEn PBrroons.
`TsaucmsmoaparTosn 1304 B08
LABORATORY CONTROL SAWPLDNTA REFORT
we
DRII3008900200070-110 10/05/07
Work Oxder #...s maalysis Date..:
JIGITID 10/11/07
MaLrx......ot
71202120 Analysis Time..: 02:25
sfenir ome
rEnsuRED 0.0140
oars ReEcRocavNRTy aft 7
loo oo at s6
ssEeRccoEvNrTy &
ReLcuoavseRY (50 - 200)
"
(50 = 200)
WATER jmDwanTnEO11D06--000102
| Cop tuuten per ormtedpnoe eri i es ee ld i.
|
i NIAWO006(
|
sonscoonswveen men tentn 1rr vkor hvHERI Pan OTR
| IAT EERe mpsiRcaNeAr
i m3p=ee
E FB3 oaEmE-- mm em, S mweEoR
FosPnm
Bm=xI em E-- HwEym
E-- Te E E T S
sawaoosez
i
LABORATORY CONTROL SAWPLS DATA REPORT
i
CLlCiSenLtot1-S0akmpl.e.d.:: DeepDate. ...:
DRT0T1030000?0-156 10/13/07
Work Order ...: Asalyels Date..:
JESUS 10/15/07
Mati... WATER
|{| pDirleupcpiaotncFhac#t.o.r.:: 71206156 Aoalysis Time..: 00:35
i PmAmRnETER
mseomeo 0.200
EmAosowRED .209
oaaftis
RsEERcCoEvNeTR.y 108
MDEaTHO-D10-002
at F
bmx "10-0012
| ewes
0.200 0118
sTacmeepraonrs
smmcnocvaevnr y 76
RecovERY L Go -s 200)
} 1304 PROS
(50- 200)
pEomes).
----
[mi--
i
NIAWO00: -- ee ----
|
LABORNTORY CONTROL SNHFLE EVALONTIOH RERORT.
:
Client tot ...: D79040207
me Work Order ...: JBXESIAD
Matrix ences WER
1T0e5pLDoatt-eS.amrpoluets rcp Batch ...:
K1107/11330/00070-156 7206156
AAnnaallyyssiiss
DTaitmee....::
0100/:1551/07
Dilution Factor: 1
sproase
ssesRccomwry 710
RLEaCOtVsERY T(3o9 -2312300)7
eprma1n6-0012 . paw -1e-002
| wes
rescar RecoveRY
r Tacs vron t 1304 208
mapcovmry i
T(s5Lo0 D-- 2u20000m)0
oEresE): | otcto pre
----
| |
NIAW000( es
E LABORATORY CONTRO SELB DATA RAORT.
me
0CelsieeTnopttatTseoraterp4l.oe.ts.:
DRdII0/T0a10200/02000707-156
orkOnder ...5 amalyets Date..:
JOKGSIAD 10/15/07
MatEdx.c..o..t WATER
| Dmiluetioan Falctoir: e1 s eds mess 00s
o sEaover
.
ngew SGoowmne
mmeeoww oowlaas
mSoros namsecnocvaery dDeenm3o5-5013 wm mo oan 16-0012
os
| i
sSeoowmtoeuwnossr
Imnmowsy lTGoopo m> 0201)
r e tm enai rei a
i NIAHO00605
SRLS
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