Document LKYKn1KyvV9O8Kk8a1MOEgzNz
QUIPMENT
NAMEsWATCHUNG" r ed b
USE N ACCT
UB$
CODE
LBS .
NOTE: DO NOT START IF PRESS WIEL NOT BE AVAILABLE
'
WITHIN 3 HRS. AFTER MAKING. MAKING SOPV TO REVIEW
WITH P.R. SOPV & RECORD:
\
Press will be ready
Start Making
M
M/
P.R. Sup' r
/ . Making Supv
'>
/
Prep
1 Record:
Batches since Sparkler last cleaned.
1 : JAfter 5 batches, clean , dress Sparkler & pre-coat with 15#
777-A
2* J3btain for S 12 (2 Qhlorp-4 amino Toluene 5 sulfuric acid)
740-C
3 * *jQbtain for S 51 (Beta pxy Naphthoic Acid ) | ^l L Install by a CV Recorder & Controller charts
253-C
-.... ..........-- lCr...*..... ..... ......... ...... ... ; 5* tcaa*#?" (120G) water into VCf#f & adj to 80-10QF
--2 1 "$
' 'f^V' * }` . ; 922
$*# ^ddin 1-2 min (Sodium Dr^sxnate)
J0tSt
7, ^ad in 1-2 min (Sodium Pre&Lnate)
.
8,r>
& Record: pH / *9 (9.5-10.5)
9., min or longer to dislplve for S 29
ipr
........
-...-... -- ....... ..... -----....... ..... `
water into V-922 ...... ______________ * .
99~A ijfcrr
5 30-A
...
.. ....... ./ '
! : 3-
V-926 & run in (Caustic Soda Sol.Hi /,!/, 4faf&k.. VP" : 7-D '
!
urn on i's- i:
agitator &
steam, &
dump
in
from
S 2......... . *
r . ; _>i4 ..............m<A? ::::.......
74Q-C . .
i; . . jit;*
13 in
::.:.::rv ............................ '... --................... (activate carbon)
14* (filter aid)
V
15* to 212-214F
Watch Foam
1,jB* rR^^fd: By *f*'. must be +,, Adj if needed 17* ^Stir/15 min at 212-214F , then shut off steam
Assume 50% Watch foam
iajj gHecptd: HT/T* F & Rec j-fQ F
Circulate 15 min or longer thru Sparkler until soi*n is Clear- Maintain at l9d*-19$0F for S 24
Record: Startff/ld Total IlinClaritvL,^
25 10
..
Hisc ^3
ji wasurell units in V-928 for S-42 M jt $
iliUi:;^aciS) ...Mm.
4L -Weigh in PT for S 45 . .. M
... , .
'........... *....-..........
Weigh in drum for S 53
(sodium nitrate sol)
r
\
. . ;--
... ........;--
'S*fr---
d Run 1"
g water into V- $ b "3
Note:.. Use GV if MTY. If CV is hot MTY. use V-904
When S 19 complete ^ pump _ in Vi~922 thru ..parkier.-., .Maintain
V-922 at 190~195F Record*
Total Min
av, A 13* BEV.
___
4*. / *
113-A T.; .2.5'!.' 777-A
1:
2SrD 725-A 7 25-A
f
^^, -----
N35111
DU P050107708
s.v,
CO 32 CO0E MW
PKG.
_ TwF21 SO 3tn0T7-- '
ESTc WGT.
2669
LBS.
STD. HRS.
TIME
c.v. 901(903
MAKING INSTRUCTIONS: BATC^ UNIT
o.y. 902,904
PROCESSES
APPROVED BY
{ ) RT-761-D
(J) JOG 4-4-78
("TKT-838-D "7TT OCG 4-5,78
( ) ( ) MTW 4-13-78 () ()
TYPED BY
NSA 4-19-78 :
EQUIPMENT
n ame; WATCHUNG RED B
NOTE:
Do not start if press will not be available within
3 Hrs after making. Making Suov to review with P.R.
Suov. & Record:
Press will be ready
M_____ /
P.R. Sunv
Start Makino..........M ____L__ Makina Snpv_ ____........
USE LBS.
NON-BLEEDING
N
CODE
ACCT.
LBS,
Prep '1
1 Record:
Batches since Sparkler last cleaned.
After 5 batches, clean, dress Sparkler & pre-coat with 15#
2 Obtain for S 12
3 Obtain for S 27
4 Install BV & CV Recorder & Controller charts
777-A . 740-C
82-C
921/ 931
5 Run 16" (160 G) water into V- __ A adi t.n 80-100F
6 Add In 2-3 min 7 Add in 1-2 min
8 Stir 5 min & Record: pH
(9.5-10.5)
9 Stir 20 min or longer to dissolve for S 30
... .110. .... 50
QQ^A _ i in 530-A ...... 50
922 10 Run 35" (722 G) water into V-922
3 11 Weigh in V-926 & run in
M ......... .................... %
12 Turn on .agitator & steam & dump in from 5 2
Lot
#100%
,%
7-D 216 .. 740-C.. nos
T3~ Dump in
14 Dump in
15 Heat to 2l2-214F
Watch foam
16 Record: RV
.muct he +.' Adi if needed
Assume 50%
17, Stir 15 min at 212-214F, then shut off steam,.Watch Foam
18 Record: HT IL_ ..... F & Ree----------F
19 Circulate 15 mTh or longer thru Sparkler until sol'n is
clear. Maintain at 190-195F for S 24 ......
____
Mi sc . 20 Measure ,
units in V-928 for S 39
4 21 Weigh In PfTor S 42-------------- ------
22 Weigh in drum for S 48
*L. .........______ ___% M.r
904/CV 23 5
24
Run 1" L - Gl water into V- __ .... . Note: Use CV if MTY. If CV is not MTY, use.V-9Q4..
When S 19 complete, pump ip V-922 thru Sparkler. Maintain V-922 at 190-195F. Record: Start. ._Jotal Min
25 10
113-A 777-A
7-fl
25 10
28-D 725-A 725-A
533 40l
40
DUP050107709
EQUIPMENT
902 25 6 26 27
PAGE 2 CC 32 CODE RT-761-D (J), RT-838-D (H)
Run 56" (1566 G) water into V-902 Weigh in V-926 & run in Dump in from S 3
Lot
LBS.
USE LBS.
N CODE
ACCT. LBS.
_Z=EL SSSL 82-C 1012.
28 Adj to 70-90F & stir 10 min to dissolve 29 Slurry in 30 Sal water & pour Into V-902~ 30 Steam elect tn V~921~931 from S 9
m
39 A m
922 & M. When S 24 complete., stop _pump & insert V-922 foot plug
904/CV 32 RunJrt.121.1242.. .g.)-WAt^ J;.heat, to 18Q-19QF
7 33 Pump V-922 thru sparkler into V-9Q4/OV
When V-922 MTV hlnw out-sparklep-mto-V--;904/CV
45. Weigh ft add to, V
36 Heat V-904/CV to 165-170P for S 39
.Lot,,
wnTF; If N-740-C solution was pumped directly from sparkler
23 & 24 omit S'.s 42..&..38..
,18...oz 749r.C.
JZ. Run.JPx.1",-OS 61.water into 48. Tf V-904 ts used, pump V-904 at 165-170F thru undersurface
distributor into CV AFAP (i2->15 min) maintain CV at 165-170F
42. Run in N-28-D from S 21 In 12-15 min
40 Stir 5 min
41. Adl_ta.431.C408Q G) at 32-_3.8P.F-
45.x 330
42_ Run In N-725-A from S 21 AFAP (5-10 min)
Stir 10 min at 32-38F maintaining
57-A
DUP050107710
EQUIPMENT
fealT fa 6
PAGE 2 CO 32 COPERT~76j-D(K)^ > EeSsxX. WWOOTT.
LBS,
nan 45" (1250 G) water into V-90
Weigh in V-926 & run in
M
Adj to 70^90QF & stir 10 min to dissolve
lurry in 30 gal water & pony into V-9Q2(Trisulphoil Soap D)
Steam eject in V-Sj&%/93! from S 9
USE LBS,
75^r
ACC UBS
Too* 3 9-A
922 &_
aen S 24 complete, stop pump & insert V-922 foot plug
904/CV
Run in 12" (247 G) water & heat to 190-195gF
'circulate 15 min or longer thru Sparkler until solution is clear.
V 922 thru Sparkler into V 904/CV
in 8" (165G) water into V922) & heat to 190-195F
iirculate 15 min or longer thru Sparkler until solution is d.ea:r.
V922 thru Sparkler into V9P4/CV Hhm wcm Mrnblow out Sparkler into V904/CV
Heat V-904 to 165-170F for S 42
HCXTE: If N-740-C solution was pumped directly from Sparkler
to cy atS's 23 & 24 omit S's 40-41
.^L-A
Ar/ird-ZCOMm 4 Pauli tei JJQ
cv -4P- Run 1" (95 G) water into V-
8 4i- If V 904 is used, pump V-904 at 165-170 F thru under-surface
3S|istributor into CV AFAP (12-15 min) Maintain CV at 165-170 F
iun in N-28-D from S 20 in 12-15 min
S:Sitir 5 min
|2:ij to 25" (3300G) at 32-38F
(Ice)
in N-725-A from S 21 AFAP (5-10 min)
X330
Stir 30 min at 32-38 F maintaining -fCR, -KKi CR. Hi* (+) KI-t '
HQTfc:.
JuL
(1) If CR-KI- add 20# "As Xs" increments
Record CR
(+), Kl
(L
(2) If CR t KI-- # add 201) "As Is" increments
Assume 32% Assume 33%
CR (+.) t KI JL
(Calc1urn chloride)
iimp-jajgu
(Strontium nitrate) (Blanc Fixe)
-for jniaiiLtainin.g^3 2-38F ..dvring..jcoupllng.
Dump in from S~3
LOT
seta.
z&B m.
57-A
28-D
7 25-A
20-A 246-P
6.5-A 57-A 253-C
mk VIZI
lof
9
Weigh on postal balance and dump in and stir 10 min
-a,---- -------------- ,-----:-----------J^pUr^r:--------- (iHydroxy 2Naphthoic acid)
5>* J^tfr N-725-D from
kju f W
JyK* Duiuu "in
TO* Y
(ammonium'chloride)
cv Tfe** irmnimt ediately couple V-902 thru undersurface distributor into.
10 min. Maintain DV at 32__3__8__F______ Records Star^^33^Total tlin
Stir 30 min & record; Base
(+),Diazo
PEI 4. I (9.5-10.0)
1f necessary, adi to pH 9.5-10.0 & Record
igh in drum & pour in (ISo Octanol)
l L
pH M Assume 50%
Assume 32%
to 184-186UF in 70-75 min
cord; Stir 30
min
HT at
j18m4-1.86OeFp-
& Rec m.
ter 10 min S 61 stir, record; ?A&. (9,5-10.0)
If necessary, adj to pH 9.5-10.
Assume 50%
Record: p H |IL*|if pH above 10.0- do not adjust
a o n e,v
m
180--C
m.
V
W
W=SL
28-D 588--D
22 ytt-p m
DUP050107711
DUP050107712
EQUIPMENT
PAGE 3 c g 32 CODE RT~761~D (J)s RT-838-D (H)
When Instructed by Processing Area half-waythru pressing
1. Dump In -2o Stir 5 min 3 Advise processing to resume Dressing
USE LBS*
CODE
ACCT. LBS.
in SftfUA ?n
START
~
FIR ~ _
---------------
V
A ..
f
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,*
> DUP050107713
Tn^e. OP PKD4- o n STUDY-
fitmiffer __l . *
cwGimcemNG
COMPUTATION SHE'ST
Sms err Mo.
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o * STur>r :M. , WO.Si<S-- --------------
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st> iZU/M i $i P&0 a / J AS is a J '&Pr'
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AFrSfc Sj > 3 64
>
mz siAMOxms yc/t
e$$s#T->x .i^s t /u .u v ^o ^s
DUP050107714
DU P050107715
l oot -
DUP050107716
DUP050107717