Document LJkBJa4apoQMQGxg8pBa5yZv5

Data Package Contract Lab Program Data Package for DuPont Env. Remediation Svc. TYPE IV INORGANICS DATA PACKAGE DuPont Fort Madison GW Monitoring -- 1996 Annual Water Samples Collected on 09/17/96 - 09/18/96 Sample No. 2583222-2583227, 2583830-2583834 PA Cert. # 36-037 NY Cert. # 10670 NJ Cert. # 77011 J(Prepared by jf/J dALcf 1/L Quality Assurance Review Arvwi Date ipfqjqfe Delivery Date /6fn!%> Lancaster Laboratories A Thermo Analytical Laboratory N36819 Lancaster Laboratories 2425 New Holland Pike, P0 Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681 DUP050307241 dkLancaster Laboratories ^ division of Thermo Analytical Inc. When* quality <s a science Sample Reference List for SD6 # FMD02 with a Package Type of IV-I Lab Sample Number 2583222 2583223 2583224 2583225 2583226 2583227 2583830 2583831 2583832 2583833 2583834 sample Code RS5SF RS4DF 4DDPF RA4SF RD3DF RA3SF 2DDIS 2SDXS 1DDIS 1SDIS FB1DS Client Sample Description FMN-BRA-5S-DIS Filtered Water Sample FMN-BRA-4D-DXS Filtered Water sample FMN-BRA-4D-DIS-DUP Filtered Water Sample FMN-BRA-4S-DIS Filtered Water Sample FMN-BRA-3D-DIS Unspiked Filtered Water Sample FMN-BRA-3S-DIS Filtered Water Sample FMN-BRA-2D-DIS Filtered Water Sample FMN-BRA-2S-DIS Filtered Water Sample FMN-BRA-1D-DIS Filtered Water Sample FMN-BRA-1S-DIS Filtered water sample FMN-BRA-FBLK-1-DIS Filtered Water Sample Lancaster Uborau-.ni'c*:-. 2425 New Holland Pike PO Box 12*325 lancastei. PA 17005-2425 717-656-2.3C0 71 7-650-2631 Shipping Address-. Lancaster Laboratories 2425 New Holland Pike Lancaster. PA 17601 717-656-2300 fax. 717-656-268' M I- M B t- H Environmental Foods Pharmaceuticals ESS! A subsidiary of Thermo ff-t'rviTerh iru. . a Thermo Electron cornnany DU PO50307242 TABLE OF CONTENTS A. Case Narrative-Conformance/Nonconfonnance Summary.................. 1 B. Sample Data................................... ........................................................ ............................. 4 C. Quality Control Data......................................................................................................16 D. Verification of Instrument Parameters........................................................... 37 E. Preparation and Run Logs........................................................................................... 48 F. Raw Data...................................................................................................... ...75 ' Data................................ 76 2. Furnace Data................................................................................................... 167 3. Mercury Data................................................................................................... 251 4. Extraction/Distillation/Digestion Logs................................ 260 G. Chain-of-Custody Record. ....................................................................................... 270 DUP050307243 Case Narrative Conformance/Nonconformance Summary 1 DUP050307244 #Lancaster Laboratories A Thermo Analytical Laboratory_____ DUP050307245 U.S. EPA - CLP COVER PAGE - INORGANIC ANALYSES DATA PACKAGE Lab Name: LANCASTER_LABORATORIES_ Lab Code: Case No.: SOW No.: ILM04.0 EPA SAMPLE No. 1DDIS 1SDIS ~2DDIS 2SDIS ~4DDPF-- FB1DS RA3SF "RA4SF" "RD3DF" "RS4DF" "RS5SF" Contract: SAS No.: SDG No. FMD02 Lab Sample ID. _2583832 2583833 2583830 2583831 2583224 2583834 2583227 2583225 2583226 2583223 2583222 Were ICP interelement corrections applied ? Were ICP background corrections applied ? If yes - were raw data generated before application of background corrections ? Comments: Yes/No Yes/No Yes/No YES YES NO I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package and in the computer-readable data submitted on diskette has been authorized by the Laboratory Manager or the Manager's designee, as verified by^tlje fallowing signature. Signature: Name: _Betty L. Omble Date: Title: _Administrator III "Inorganic Data Packages COVER PAGE - IN ILM04.0 3 rV DUP050307246 Sample Data 4 DU P05 0307247 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER_LABORATORIES Contract 1DDIS Lab Code: ________ Case No.: SAS No.: _____ SDG No.: FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583832 Level (low/med): LOW Date Received: 09/19/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS NO. 7429-90-5 "7440-36-0 "7440-38-2 "7440-39-3 "7440-41-7 7440-43-9 "7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 "7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Analyte Concentration C Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 27.2 U 2.8 U 1.3 B 124 B 0.99 U 0.50 U 103000 0.86 U 1.2 B 0.98 U 329 0.84 U 31800 762 0.0090 U 1.6 U 3130 B 0.70 U 0.30 u 49500 1.1 u 0.44 u 9.5 B Q w N M P P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS Color After: COLORLESS Comments: Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 5 DU P050307248 U.S. EPA CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER_LABORATORIES____ Contract: ___ 1SDIS Lab Code: ________ Case No.: ____________ SAS No ________ SDG No.: FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583833 Level (low/med): LOW Date Received: 09/19/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS NO. 7429-90-5 7440-36-0 7440-38-2 "7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Analyte Concentration C Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 4477 5 2.8 U 1.3 u 74.9 B 0.99 U 0.50 u 166000 1.1 B 0.92 U 0.98 u 19.0 u 0.84 u 60100 6.9 B 0.0090 u 1.7 B 1680 B 163 0.30 TJ 12000 1.1 U 0.77 B 12.0 B Q w SN M P" P F P P P P P P P P F P P CV P P F P P F P P" Color Before: COLORLESS Color After: COLORLESS Comments: Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 6 DUP050307249 ..... - tJ.S. EFA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name LANCASTER LABORATORIES Lab Code: ________ Case No Contract: ___________ SAS No.: - 2DDIS SDG No.: FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583830 Level (low/med): LOW Date Received: 09/19/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. 7429-90-5 "7440-36-0 "7440-38-2 "7440-39-3 "7440-41-7 "7440-43-9 "7440-70-2 "7440-47-3 "7440-48-4 7440-50-8 7439-89-6 "7439-92-1 7439-95-4 "7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 "7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Analyte Concentration C Q Aluminum Antimony Arsenic Barium Beryllium cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 27.2 U 2.8 u 1.3 u 113 B 0.99 U 0.50 U 73300 0.86 U 0.92 u 0.98 u 207 0.84 u 31500 245 0.0090 u 1.6 u 5790 0.70 u 0.30 u 46100 B 2.1 B 0.44 U 9.2 B W N M P P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS_ Color After: COLORLESS Comments: Clarity Before:- CLEAR_ Clarity After: CLEAR_ Texture: Artifacts: FORM I - IN ILM04.0 7 DUP050307250 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. ____________________ Lab Name: LANCASTER LABORATORIES Contract: Lab Code: Case No.: SAS No.: SDG No.: FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583831 Level (low/med): LOW Date Received: 09/19/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C 7429-96-$ Aluminum "7440-36-0" Antimony "7440-38-2 Arsenic "7440-39-3 Barium "7440-41-7 Beryllium 7440-43-9 Cadmium "7440-70-2 Calcium "7440-47-3 Chromium "7440-48-4" Cobalt "7440-50-8 Copper 7439-89-6 Iron 7439-92-1 Lead 7439-95-4 Magnesium "7439-96-5 Manganese 7439-97-6 Mercury 7440-02-0 Nickel "7440-09-7 Potassium 7782-49-2 Selenium "7440-22-4 silver 7440-23-5 Sodium 7440-28-0 Thallium 7440-62-2 Vanadium 7440-66-6 Zinc ' 3B7l S 2.8 u 1.3 u 73.4 B 0.99 U 0.50 u 153000 1.0 B 0.92 U 0.98 u 19.0 u 0.84 u 80100 266 0.0090 u 3.1 B 6340 18.4 0.30 B 52800 1.1 TT 0.69 B 10.0 B Q S N M R P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS Color After: COLORLESS Comments: Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 8 DUP050307251 U.S. EPA CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER LABORATORIES____ Contract: 4DDPF Lab Code: _________ Case No SAS No.: ________ SDG No.: FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583224 Level (low/med): LOW Date Received: 09/18/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q 7429-90-5 "7440-36-0 7440-38-2 "7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 27.2 U 2.8 u 1.3 u 49.5 B 0.99 U 0.50 U 211000 0.86 u 4.5 B 0.98 U 33.6 B 0.84 U 84800 715 0.0090 u 5.2 B 5060 B 0.70 U 0.30 U 54300 1.1 u 0.44 U 14.2 B w WN M P P F P P P P P P P P F P P CV P P F P" P F P P Color Before: COLORLESS A Color After: COLORLESS Comments: Clarity Before: CLEAR_______ Texture: Clarity After: CLEAR_______ Artifacts: FORM I - IN ILM04.0 A 9 DUP0503 07252 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER LABORATORIES____ Contract: FB1DS Lab code: ________ Case No SAS No.: ________ SDG No.: FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583834 Level (low/med): LOW 1 % Solids 0.0 Date Received: 09/19/96 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Analyte Concentration C Aluminum Antimony__ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 27.2 U 2.8 u 1.3 u 1.7 B S'.99 u 0.50 u 17.6 u 0.86 u 0.92 u 0.98 u 26.3 B 0.84 U 19.3 U 1.4 B 0.0090 U 1.6 U 114 B 0.70 U 0.40 B 210 B 1.1 U 0.44 u 11.7 B Q N M P P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS color After: COLORLESS Comments: Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 10 DUPO50307253 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. ____________________ Lab Name: LANCASTER LABORATORIES Contract: Lab Code: Case No.: SAS No. : SDG No. : FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583227 Level (low/med): LOW Date Received: 09/18/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q 7429--90--5 "7440-36-0 "7440-38-2 "7440-39-3 "7440-41-7 7440-43-9 "7440-70-2 7440-47-3 "7440-48-4 7440-50-8 "7439-89-6 7439-92-1 "7439-95-4 7439-96-5 "7439-97-6 7440-02-0 7440-09-7 7782-49-2 "7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 145 B 9.2 B 3.5 B 73.0 B 0.99 U 0.50 U 224000 0.86 U 0.92 U 0.98 U 102 0.84 U 90700 197 0.0090 U 9.9 B 2950 B 20.2 0.30 U 54900 1.1 U 3.3 B 16.8 B W N M P P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS Color After: COLORLESS Comments: Clarity Before: CLOUDY Clarity After: CLEAR_ Texture: Artifacts: FORM I - IN ILM04.0 11 DU PO 50307254 am f. -ij.jitrfAh-v U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name LANCASTER LABORATORIES____ Contract: ____________ Lab Code: ________ Case No SAS No.: ________ RA4SF SDG No.: FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583225 Level (low/med): LOW Date Received: 09/18/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. 7429-90-5 "7440-36-0 7440-38-2 "7440-39-3 "7440-41-7 7440-43-9 "7440-70-2 "7440-47-3 "7440-48-4 7440-50-8 7439-89-6 "7439-92-1 "7439-95-4 7439-96-5 7439-97-6 7440-02-0 "7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Analyte Concentration c Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 27.2 u 2.8 u 1.3 u 110 B 0.99 U 0.50 u TS'eooo 0.86 u 4.5 B 5.98 U 19.0 U 0.84 U 50700 675 0.047 B 13.3 B 2120 B 0.70 U 0.30 U 36300 1.1 U 1.1 B ii.2 B Q N M P P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS Color After: COLORLESS Comments: Clarity Before: CLEAR_ Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 12 DUP050307255 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER LABORATORIES____ Contract: RD3DF Lab Code: ________ Case No. : _____________ SAS No.: SDG No.: FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583226 Level (low/med): LOW Date Received: 09/18/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS NO. Analyte Concentration C Q 7429-90-5 "7440--36--0 7440-38-2 "7440-39-3 "7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 "7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 "7439-97-6 7440-02-0 7440-09-7 7782-49-2 "7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 27.2 U 2.8 U 1.9 B 153 B 0.99 U 0.50 U 69400 0.86 U 2.9 B 0.98 U 28.4 B 0.84 U 28800 791 0.0090 U 5.1 B 2960 B 0.70 U 0.30 U 49100 B 1.1 U 0.87 B 11.8 B W WN M P P F P P P P P P P P F P P CV P P F P P F" P P Color Before: COLORLESS Color After: COLORLESS Comments: Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 13 DUP050307256 U.S. EPA - CLP INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER_LABORATORIES_ Contract: RS4DF Lab Code: Case No.: SAS No.: SDG No.: FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583223 Level (low/med): LOW Date Received: 09/18/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q 7429-90-5 "7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 "7440-48-4 7440-50-8 "7439-89-6 "7439-92-1 7439-95-4 7439-96-5 7439-97-6 "7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium-1 Zinc 40.2 B 2.8 U 1.3 U 50.7 B 0.99 U 0.50 U 210000 0.86 U 4.9 B 0.98 U 117 5.84 u 84100 733 0.0090 u 5.4 B 4260 B 15.8 0.30 U 59500 1.1 T3 0.67 B 10.0 B W N M P P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS Color After: COLORLESS Comments: Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 DU P050307257 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER LABORATORIES____ Contract: ____________ RS5SF Lab Code: ________ Case No SAS No.: ________ SDG No.: FMD02 Matrix (soil/water): WATER Lab Sample ID: 2583222 Level (low/med): LOW Date Received: 09/18/96 % Solids 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS NO. 7429-90-5 "7440-36-0 "7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 "7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Analyte Concentration C Aluminum 27.2 U Antimony ...................... 2.8 U Arsenic 1.3 U Barium 28.3 B Beryllium 0.99 U Cadmium 0.50 U Calcium 219000 Chromium 0.86 u Cobalt 0.97 B Copper 0.98 U Iron 19.0 U Lead 0.84 U Magnesium 99600 Manganese 347 Mercury 0.0090 u Nickel 9.4 B Potassium 3650 B Selenium 0.70 U silver 0.30 U Sodium 46100 Thallium 1.1 U Vanadium 0.62 B Zinc 8.9 B Q W WN M P P F P P P P P P P P F P P CV P P F P P F P P color Before: COLORLESS Color After: COLORLESS Comments: Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 15 DUP050307258 Quality Control Data DUP05 03072 59 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: LANCASTER_LABORATORIES____ Lab Code: ________ Case No.: _____________ Initial Calibration Source: LLI Continuing Calibration Source: LLI Contract: SAS No.: ________ SDG No.: FMD02 Concentration Units: ug/L Analyte Initial Calibration True Found %R(1) True Continuing calibration Found %R(l) Found %R( 1) Aluminum 30000.0 30147.18 100.5 25000.0 25441.28 101.8 25702.91 102.8 Antimony " 600.0 588.92 98.2 " 500.0 471.18 94.2 481.68 96.3 Arsenic 50.0 53.47 106.9 40.0 42.39 106.0 41.90 104.8 Barium 600.0 602.03 100.3 00.0 89.93 98.0 494.46 98.9 Beryllium 600.0 614.65 102.4 500.0 498.53 --99.7 519.89 104.0 Cadmium 600.0 632.31 105.4 500.0 510.41 102.1 513.69 102.7 Calcium 30000.0 29493.75 98.3 "25000.0 25060.71 100.2 25171.61 100.7 Chromium 600.0 602.67 100.4 500.0 495.13 99.0 516.60 103.3 Cobalt 600.0 596.18 99.4 500.0 488.93 "97.8 506.67 101.3 Copper 600.0 615.39 102.6 500.0 501.61 100.3 505.91 101.2 Iron 1RJ000.0 29795.76 99.3 25000.0 25039.39 100.2 26158.78 104.6 Lead 20.0 19.93 99.6 25.0 23.92 95.7 24.99 100.0 Magnesium 30000.0 30024.36 100.1 25000.0 25191.80 100.8 25887.75 103.6 Manganese 600.0 596.42 99.4 500.0 493.10 98.6 510.56 102.1 Mercury 2.0 2.04 102.0 1.0 1.04 104.0 1.05 105.0 Nickel STFO.O 595.57 99.3 500.0 492.08 98.4 09.41 101.9 Potassium "lUOOO.O 30379.39 101.3 25000.0 26338.93 105.4 26186.62 104.7 Selenium 20.0 19.22 96.1 25.0 24.24 97.0 22.82 91.3 Silver 600.0 606.33 101.1 500.0 93.83 98.8 06.49 101.3 Sodium 30000.0 30599.42 102.0 25000.0 25979.78 103.9 25986.76 103.9 Thallium 50.0 49.34 98.7 40.0 41.00 102.5 44.00 110.0 Vanadium 600.0 602.86 100.5 500.0 500.91 100.2 517.59 103.5 Zinc 600.0 579.86 96.6 500.0 485.78 97.2 514.54 102.9 (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 17 DUPO50307260 U.S. EFA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: LANCASTER_LABORATORIES____ Lab Code: ________ Case No-: ____________ Initial calibration source: LLI Continuing Calibration Source: LLI Contract: SAS No.: ________ SDG No.: FMD02 Concentration Units: ug/L Analyte Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Initial Calibration True Found %R(l) True Continuing Calibration Found %R(1) Found %R(1) 20.0 18.54 25000.0 500.0 40.0 500.0 500.0 500.0 25000.0 500.0 500.0 500.0 "51000.0 25.0 ,25000.0 500.0 1.0 50o.o 25000.0 92.7 25.0 500.0 25000.0 40.0 500.0 500.0 26142.43 497.65 41.77 103.25 535.24 516.20 25314.66 531.37 520.70 513.46 26819.42 26.02 26440.93 525.10 0.97 126.00 51405.22 24.37 116.08 26327.98 42.30 530.35 535.94 104.6 99.5 104.4 100.6 107.0 103.2 101.3 106.3 104.1 102.7 107.3 104.1 105.8 105.0 97.0 105.2 105.6 97.5 103.2 105.3 105.8 106.1 107.2 42.63 534.86 26243.89 26.16 1.03 23.48 43.55 106.6 107.0 105.0 104.6 103.0 93.9 108.9 M P~ P F P P P P P P" P P F P P CV P P" F P P F P P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 18 DUPO 50307261 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: LANCASTERJLABORATORIES____ Lab Code: ________ Case No.: ' Initial Calibration Source: LLI Continuing Calibration Source: LLI Contract: SAS No.: ________ SDG No.: FMD02 Concentration Units: ug/L aaia tit aait taaa tataaai t aa aa aaaai t it a a t aa Analyte Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Initial Calibration True Found %R(l) True Continuing calibration Found %R(1) Found %R(1) 40.0 42.49 106.2 500.0 530.42 106.1 "25000.0 25987.42 103.9 43.43 108.6 25.0 26.01 104.0 25.10 100.4 30000.0 29565.49 98.6 25.0 24.41 97.6 25000.0 24911.96 99.6 25091.76 100.4 40.0 42.30 105.S 42.80 107.0 M NR (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 19 DUP050307262 U.S. EPA CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: LANCASTER_LABORATORIES____ ah code: ________ Case No.: ____________ Initial Calibration source: LLI Continuing Calibration Source: LLI_________ . Contract: __________ ' SAS No.: ________ SDG No.: FMD02 Concentration Units: ug/L Analyte Initial Calibration True Found %R(1) True Continuing Calibration Found %R(1) Found %R(1) M Aluminum NR Antimony_ NR Arsenic 40.0 43.56 108.9 F Barium NS Beryllium NR Cadmium NR Calcium NR Chromium NR Cobalt NR Copper NR Iron NR Lead 25.0 25.53 102.1 25.69 102.8 F Magnesium NR Manganese NR Mercury NR Nickel NR Potassium NR Selenium 20.0 19.01 95 0 25.0 24.62 98.5 24.55 98.2 F Silver NR A Sodium 25000.0 25049.85 100.2 25376.81 101.5 P Thallium 50.0 46.71 93.4 40.0 42.15 105.4 40.61 101.5 F Vanadium NR Zinc NR (1) Control Limits: Mercury 80-120? Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 20 DUP050307263 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: LANCASTER_LABORATORIES____ Lab Code: ________ Case No.: ____________ Initial Calibration Source: LLI Continuing Calibration Source: LLI Contract: SAS No.: ________ SDG No.: FMD02 Concentration Units: ug/L Analyte Initial Calibration True Found %R(1) Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium ** silver Sodium Thallium Vanadium Zinc 2d.b IS. 69 94.5 True Continuing Calibration Found %R(1) Found %R(1) 25.0 24.14 96.6 24.96 99.8 25000.0 25039.48 100.2 40.0 40.55 101.4 M NR NR (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 21 DU P050307264 U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: LANCASTER_LABORATORIES___ . Lab Code: ________ Case No.: ____________ AA CRDL Standard Source: LLI ICP CRDL Standard Source: LLI Contract: SAS No.: ________ SDG No.: FMD02 Concentration Units: ug/L Analyte Aluminum Antimony Arsenic Barium Beryllium Cadmium calcium Chromium Cobalt copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc CRDL Standard for AA True Found %R 10.0 12.41 124.1 3.0 0.2 3.0 10.0 4.29 143.0 0.19 5.5 4.12 82.4 12.38 123.8 True CRDL Standard for ICP Initial Final Found %R Found %R 120.0 117.73 98.1 118.87 99.1 10.0 10.0 20.0 100.0 50.0 9.93 99.3 10.02 100.2 20.68 103.4 101.45 101.4 51.34 102.7 10.62 106.2 10.13 101.3 21.70 108.5 106.18 106.2 51.14 102.3 30.0 S7T7TT 20.0 100.o 40.0 30.52 101.7 80.90 loi.i 20.77 103.8 104.58 104.6 40.50 101.2 31. 97 106.6 85.92 107.4 21.19 106.0 108.55 108.5 43.75 109.4 FORM II (PART 2) - IN ILM04.0 22 DU P050307265 U.S. EFA CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: LANCASTER_LABORATORIES____ T-ah Code: ________ Case No.: ____________ AA CRDL Standard Source: LLI ICP CRDL Standard Source: LLI Contract: SAS No.: ________ SDG No.: FMD02 Concentration Units: ug/L Analyte Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc CRDL Standard for AA True Found %R 3.0 3.55 101.7 5.0 10.0 2.35 47.0 9.64 96.4 True CRDL Standard for ICP Initial Final Found %R Found %R 10.0 10.52 105.2 FORM II (PART 2) - IN ILM04.0 23 DUP050307266 U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: IANCASTER_LABORATORIES____ Lab Code: ________ Case No.: ____________ AA CRDL Standard Source: LLI____________ ICP CRDL Standard Source: LLI Contract: SAS No.: ________ SDG No.: FMD02 Concentration Units: ug/L Analyte Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc CRDL Standard for AA True Found %R 5.0 4.54 90.8 True CRDL Standard for ICP Initial Final Found %R Found %R FORM II (PART 2) - IN ILM04.0 24 DU P05 0307267 U.S. EPA - CLP 3 BLANKS Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code; ________ Case No.: ____________ SAS No.: ________ Preparation Blank Matrix (soil/water): WATER_ Preparation Blank Concentration Units (ug/L or mg/kg); UG/L_ SDG No.: FMD02 Analyte Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Initial Calib. Blank (ug/L) C 27.2 tj 2.8 U 1.6 B 0.14 B 0.99 U 0.50 U 17.6 U 0.86 U 0.92 U 0.98 U 28.0 B 0.84 U 19.3 u 0.18 B -0.017 B 1.6 U 113 B -0.82 B 0.30 U 161 U 1.1 U (!) .44 U 4.1 U _ Continuing Calibration Blank (ug/L) 1C2 C 3 C 43.2 B 6.1 B 1.3 U 0.13 B 0.99 U 0.50 U 21.5 B 0.86 U 0.92 u 0.98 u 42.6 B 0.84 u 39.3 B 0.30 B -0.020 B 1.6 U 118 B -1.4 B 0.30 U 198 B 1.1 U S'.47 B 4.1 U 27.2 U 5.1 B 1.3 U 0.10 U 0.99 U 0.50 u 17.6 u 0.86 u 0.92 u 0.98 u 20.8 B 0.89 B 19.3 U 0.24 B -0.028 B 1.6 U 109 B -1.2 B 0.30 U 181 B 1.1 U 0.44 U 4.1 U 41.5 B 5.4 B 1.7 B 0.14 B 0.99 U 0.50 U 17.6 U 0.86 U 0.92 u 0.98 u 40.9 B 1.0 B 49.3 B 0.26 B -0.031 B 1.6 U 114 B 0.30 U 172 B 1.1 U 0.44 U 4.1 u Prepa ration Blank C M 27.200 u 2.800 u 1.930 B 0.100 U 0.990 U 0.500 U -32.040 B 0.860 U 0.920 U 0.980 U 33.900 B 0.850 B 19.300 U 0.860 B 0.009 U 1.600 u 107.510 B -1.410 B 0.300 U 227.360 B -1.720 B 0.440 U 8.740 B P P F~ P" P P P P" P P~ P F P~ P CV P P F~ Pp- F F" P- FORM III - IN ILM04.0 25 DUP050307268 U.S. EPA - CLP 3 BLANKS Lab Name: LANCASTERLABORATORIES____ Contract: I,ah Code: ________ Case No.: ____________ SAS No.: ________ SDG No.: FMD02 Preparation Blank Matrix (soil/water): _____________ Preparation Blank Concentration Units (ug/L or mg/kg): ______________ Analyte Initial Calib. Blank (ug/L) C Continuing Calibration Blank (ug/L) 1C2 C 3 Prepa ration C Blank C M Aluminum Antimony Arsenic 2.0 s 1.0 a 1.5 1 Barium Beryllium Cadmium o.SO u 0.50 11 calcium -21.6 B 17.6 U Chromium Cobalt Copper Iron Lead 0.84 u 1.0 B 0.84 u Magnesium Manganese Mercury -0.029 B Nickel Potassium Selenium -2.& B -3.0 B 0.70 U -2.8 B Silver A Sodium Thallium 192 B 161 U 1.1 u 161 U 1.1 U 161 TJ 1.1 U Vanadium Zinc NR NR F NS NR P P NR NR NR NR F NR NR CV NR NR F NR P F NR NR FORM III - IN ILM04.0 26 DUP050307269 U.S. EPA - CLP 3 BLANKS Lab Name: LANCASTERJ^ABORATORIES____ Contract: Lab Code: ________ Case No.: ____________ SAS No.: ________ SDG No.: FMD02 Preparation Blank Matrix (soil/water): _____________ Preparation Blank Concentration Units (ug/L or mg/kg): ______________ Analyte Initial Calib. Blank (ug/L) C Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc =07TS I i.i u Continuing Calibration Blank (ug/L) 1C 2 C 3 1.8 s C 0.84 u 0.84 U 0775 5 161 TT 1.1 u 0.70 5 161 5 1.1 u 1.1 u Prepa ration Blank C M NR NR F NK NR NR NR NR NR NR NR F NR NR NR NR NR F NR P F NR NR FORM III - IN ILM04.0 27 DUP050307270 U.S. EPA - CLP 3 BLANKS Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: ____________ SAS No.: ________ SDG No.: FMD02 Preparation Blank Matrix (soil/water): _____________ Preparation Blank Concentration Units (ug/L or mg/kg): ______________ Analyte Initial Calib. Blank (ug/L) c Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 0.84 u Continuing Calibration Blank (ug/L) 1C2 C 3 0.84 u 0.84 u Prepa ration C Blank C M NR NR NR NR NR NR NR NR NR NR NR F NS NR NR NR NR NR NR NR NR NR NR FORM III - IN ILM04.0 28 DUP050307271 U,S. EPA - CLP 4 ICP INTERFERENCE CHECK SAMPLE Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: ____________ SAS No.: ________ ICP ID Number: 05936_________ ICS Source: LLI SDG No.: FMD02 Concentration Units: ug/L Analyte True Sol. Sol. A AB Initial Found Sol. Sol. A AB %R Final Found Sol. Sol. A AB %R Aluminum 500000 500000 Antimony_ 0 600 Arsenic Barium 0 500 Beryllium 0 500 Cadmium Calcium 500000 500000 Chromium 0 500 Cobalt 0 500 Copper 0 500 Iron 200000 __ 200000 Lead Magnesium 500000 500000 Manganese 0~ 500 Mercury Nickel 0 1000 Potassium 0 0 Selenium Silver 0 200 Sodium 00 Thallium Vanadium 0 500 Zinc 0 1000 525760 524021.1 104.8 12 620.5 103.4 536675 533192.3 106.6 12 643.4 107.2 0 530.1 106.0 0 ____489.0 _97.8 8 535.2 107.0 0 ____520.6 104.1 507611 2 1 -1 __ 203541 508732.9 101.7 498.8 99.8 491.8 98.4 553.6 XlO.7 203410.4 101.7 552591 1 1 -2 __ 218028 550367.6 529.0 516.7 554.4 216338.2 110.1 105.8 103.3 110.9 108.2 532064 529026.2 105.8 6 ____501.0 100.2 556438 551692.3 110.3 6 ____527.6 105.5 0 954. S _95.4 107 101.4 0 1008.4 160.8 103 107.9 0 217.2 108.6 177 217.0 0 223.1 111.6 185 194.3 -2 513.7 102.7 4 916.2 91.6 0 540.0 108.0 4 1011.4 101.1 FORM IV - IN ILM04.0 29 DUP050307272 U.S. EPA - CLP ^4 ICP INTERFERENCE CHECK SAMPLE Lab Name: LANCASTERJLABORATORIES____ Contract: T.gb Code: ________ Case No.: ____________ SAS No.: ________ SDG No.: FMDG2 ICP ID Number: 05936_________ ICS Source: LLI Concentration Units: ug/L Analyte True Sol. Sol. A AB Initial Found Sol. Sol. A AB %R Final Found Sol. Sol. A AB %R Aluminum 500000 __ 500000 Antimony_ Arsenic Barium Beryllium Cadmium 0 1000 Calcium 500000 500000 Chromium Cobalt Copper Iron 200000 200000 Lead Magnesium 500000 __ 500000 Manganese Mercury Nickel Potassium Selenium Silver Sodium 00 Thallium Vanadium Zinc __ 515741 528366.2 105.7 __ 526696 522991.1 104.6 -2 1000.0 100.0 -3 998.6 99.9 ___506855 319084.3 103.8 __ 520723 518008.7 103.6 __ 202271 206537.3 103.3 __ 207481 305958.0 103.0 __ 520596 530856.3 106.2 __ 530875 525886.2 105.2 168 ____230.8 117 ____225.8 FORM IV - IN ILM04.0 30 DUP050307273 U.S. EPA - CLP 4 XCP INTERFERENCE CHECK SAMPLE Lab Name: LANCASTER LABORATORIES____ Contract: Lab Code: ________ Case No.: ____________ SAS No.: ________ ICP ID Number: 05936 ICS Source: LLI. SDG No.: FMD02 Concentration Units: ug/L Analyte True Sol. Sol. A AB Aluminum 500000 __ 500000 Antimony Arsenic Barium Beryllium Cadmium 1000 Calcium 50t>000 __ 500000 Chromium Cobalt Copper Iron 200000 __ 2 DO000 Lead Magnesium 500000 __ 500000 Manganese Mercury Nickel Potassium Selenium Silver Sodium 00 Thallium Vanadium Zinc Initial Found Sol. Sol. A AB %R Final Found Sol. Sol. A AB %R __ 526432 529259.7 105.9 -3 1022.9 102.3 __ 531199 529330.5 105.9 __ 210581 210094.3 105.0 532149 S31J754.8 106.4 257 246.9 FORM IV - IN ILM04.0 31 DUP050307274 U.S. EPA - CLP 5A SPIKE SAMPLE RECOVERY EPA SAMPLE NO. Lab Name: LANCASTERJLABORATORIES____ Contract: RD3DFS Lab Code: ________ Case No.: ____________ SAS No.: SDG No.: FMD02 Matrix (soil/water) s WATER________ . Level (low/med): LOW % Solids for Sample: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L Control Analyte Limit %R Aluminum 75-125 Antimony_ 75-125 Arsenic 75-125 Barium 75-125 Beryllium 75-125 Cadmium 75-125 Calcium Chromium 75-125 Cobalt 75-125 Copper 75-125 Iron 75-125 Lead 75-125 Magnesium Manganese 75-125 Mercury 75-125 Nickel 75-125 Potassium Selenium 75-125 Silver 75-125 Sodium Thallium 75-125 Vanadium 75-125 Zinc 75-125 Spiked Sample Result (SSR) C 2145.8200 523.6200 42.4900 2165.2300 51.2200 52.4700 207.0500 511.3200 259.3800 1072.1300 18.5500 1299.9600 1.0600 515.7600 6.6800 52.2100 45.7100 518.1900 510.2000 Sample Spike Result (SR) C Added (SA) 27.2000 U 2.8000 U 1.9300 B 153.3800 B 0.9900 U 0.5000 U 2000.00 500.00 40.00 2000.00 50.00 50.00 0.8^00 u 2.9000 B 0.9800 U 28.4500 B 0.8400 U 200.00 500.00 250.00 looo.oo 20.00 791.1500 0.0090 U 5.0600 B 500.00 1.00 500.00 0.7000 U 0.3000 U 10.00 50.00 1.1000 U 0.8700 B 11.7900 B 50.00 500.00 500.00 %R Q M 107.3 P 104.7 P 101.4 F 100.6 P 102.4 P 104.9 P NR 103.5 P 101.7 P 103.8 P 104.4 P 92.8 F NR 101.8 P 106.0 CV 102.1 P NR 66.8 N F 104.4 P NR 91.4 F 103.5 P 99.7 P~ Comments: FORM V (PART 1) - IN ILM04.0 32 DUP050307275 U.S. EPA - CLP 6 DUPLICATES EPA SAMPLE NO. Lab Name: LANCASTER_LABORATORIES Contract RD3DFD Lab Code: ________ Case No. : ____________ SAS No.: ________ SDG No.: FMD02 Matrix (soil/water) : WATER______ _ Level (low/med): LOW % Solids for Sample: 0.0 % Solids for Duplicate : 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L____ Control Analyte Limit Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium_ Vanadium Zinc Sample (S) C 27.2000 U 2.8000 U 1.9300 B 153.3800 B 0.9900 U 0.5000 U 69418.4900 0.8600 tr 2.9000 B 0.9800 U 28.4500 B 0.8400 U 28777.0900 791.1500 0.0090 u 5.0600 B 2861.5000 B 0.7000 U 0.3000 U 49149.4000 B 1.1000 U 0.8700 B 11.7900 B _ Duplicate (D) C 27.2000 U 2.8000 U 1.3900 B 149.4900 B 0.9900 U 0.5000 U 70170.5000 0.8600 U 1.9000 B 0.9800 U 22.0600 B 0.8400 U 26183.7900 770.6700 0.0090 U 5.8100 B 25^0.4700 B 0.7000 U 0.3000 U 49255.0000 B 1.1000 U 0.8600 B 9.1700 B RPD JT75 2.6 1.1 41.7 25.3 2.1 2.6 13.8 1.4 0.2 1.2 25.0 QM P P F~ P P P -- P P~ P _ P~ * " P -- F- _ P~ P CV * P P" -- F P" _ P~ F -- "" P" P FORM VI - IN ILM04.0 33 DUP050307276 U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE Lab Name: LANCASTERJABORATORIES____ Lab Code: ________ Case No.: ____________ Solid LCS Source: ________________ Aqueous LCS. Source: LLI Contract: SAS No.: ________ SDG No.: FMD02 Analyte Aqueous (ug/L) True Found %R Aluminum 2000.0 2163.48 108.2 Antimony ~ 500.0 " 535.43 107.1 Arsenic__ 40.0 42.82 107.0 Barium "2000.0 ` 2056.73 102.8 Beryllium " 50.0 " 51.82 103.6 Cadmium 50.0 54.64 109.3 Calcium "4000.0 "4268.33 106.7 Chromium " 200.0 " 210.49 105.2 Cobalt 500.0 ` 511.23 102.2 Copper 250.0 257.82 103.1 Iron 1000.0 " 1088.89 108.9 Lead " 20.0 21.81 109.0 Magnesium Tooo.o 2063.02 103.2 Manganese 500.0 " 518.04 103.6 Mercury 1.0 1.07 107.0 Nickel^___ 500.0 521.13 104.2 Potassium 4000.0 '1964.98 99.1 Selenium " 10.0 8.63 "86.3 Silver 50.0 51.69 T03.4 Sodium 4000.0 '1025.15 100.6 Thallium 50.0 47.85 95.7 Vanadium 500.0 527.17 105.4 Zinc 500.0 ' 525.15 105.0 True Solid (mg/kg) Found C Limits -- %R FORM VII - IN ILM04.0 34 DUP050307277 U.S. EPA - CLP 8 STANDARD ADDITION RESULTS Lab Name: LANCASTERJLABORATORIES Lab Code Case No Contract: SAS No.: ________ Concentration Units: ug/L SDG No.: FMD02 EPA Sample No. 1SDIS 2SDIS 0 ADD An ABS 1 ADD CON ABS 2 ADD CON ABS SE 0.034 5.00 0.046 10.00 0.056 PB 0.003 -- 5.00 0.046 "10.00 0.084 3 ADD CON ABS 15.00 0.066 15.00 0.122 Final Cone. rQ 16.3 0.9989 0.6 0.9995 A FORM VIII - IN ILM04.0 35 DUP050307278 U.S. EPA - CLP 9 ICP SERIAL DILUTIONS Lab Name: LANCASTERJLABORATORIES____ Contract: ____ Lab Code: ________ Case No.: ____________ SAS No Matrix (soil/water): WATER EPA SAMPLE NO. RD3DF L ____ SDG No.: FMD02 Level (low/med): LOW_ Concentration Units: ug/L Analyte Initial Sample Result (I) C Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 27.20 13 2.80 U 153.38 I 0.99 u 0.50 u 69418.49 0.86 u 2.90 B 0.98 U : 28.45 B 28777.09 791.15 5.06 B 2961.50 B 0.30 tJ 4914.94 B 0.87 B 11.79 B Serial Dilution Result (S) C iSS.do u 17.20 B i------- Differ ence QM P P 153.25 5 4.95 U 2.50 u 68253.40 4.30 u 4.60 u 4.90 u 146.65 B 0.1 177 Ido.o 415.5 P P P P~ P P P P 27504.05 789.75 4.4 P 0.2 P~ 9.65 5 3147.80 B 9077 6.3 F~ P 1750 U 4503.35 B P 8.4 P 3.00 B 25.55 B 244.8 116.7 P P- FORM IX - IN ILM04.0 36 DUP050307279 Verification of Instrument Parameters 37 DUP050307280 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: _________ SDG No.: FMD02 ICP ID Number: _________________ Date: 07/15/96 Flame AA ID Number: __________________ Furnace AA ID Number: ____ 02803 Analyte Wave length (nm) Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium'. Cobalt Copper Iron Lead Magnesium Manganese Mercury__ Nickel Potassium Selenium Silver Sodium Thallium 276.80 Vanadium Zinc Back ground BD CRDL (ug/L) 10 IDL (ug/L) M NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 1.1 F NS NR Comments: FORM X - IN ILM04.0 38 DUP050307281 D.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: _________ SAS No.: ________ SDG No.: FMD02 ICP ID Number: ____________ _ Date: 07/15/96 Flame AA ID Number: ___ _____________ Furnace AA ID Number: ____ 03812 Analyte Wave length Back CRDL (nm) ground (ug/L) IDL (ug/L) M Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium_ Cobalt____ Copper Iron Lead 283.30___ BZ Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thalli'um_ Vanadium Zinc NR NR NR NR NR NR NR NR NR NR NR 3 ____ 0.84 F NR NR NR NR NR NR NR NR NR NR NR Comments: FORM X - IN ILM04.0 39 DUP050307282 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER_LABORATORIES____ Contract: Code: ________ Case No.: _____________ SAS No.: ________ SDG No.: FMD02 ICP ID Number: _________________ Date: 07/15/96 Flame AA ID Number: _________________ Furnace AA ID Number: ____ 04724 Analyte Wave length fnm) Back ground CRDL (ug/L) Aluminum Antimony Arsenic 193.70 Barium Beryllium Cadmium Calcium Chromium_ Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel_.___ Potassium Selenium_ Silver sodium Thallium Vanadium Zinc B2 10 IDL (ug/L) M NR NR 1.3 F NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR Comments: FORM X - IN ILM04.0 40 DUP050307283 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER_LABORATORIES_ Contract: Lab Code: ________ Case No.: _____________ SAS No.: ________ SDG No.: FMD02 ICP ID Number: _________________ Date: 07/15/96 Flame AA ID Number: _________________ Furnace AA ID Number: ____ 04725______ Analyte Wave length Back CRDL (run) ground (ug/L) Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium 196.00 Silver Sodium Thallium Vanadium Zinc 5 IDL (ug/L) M NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 377o F NR NR NR NR NR Comments: FORM X - IN ILM04.0 41 DUP050307284 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER LABORATORIES____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: _________ SDG No.: FMD02 ICP ID Number: _________________ Date: 07/15/96 Flame AA ID Number: ____ 05220 Furnace AA ID Number: _ Analyte Wave length Back (nm) ground Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury 254.00___ Nickel Potassium Selenium Silver Sodium Thallium Vanadium_ Zinc CRDL IDL (ug/L) (ug/L) M UK NR NR NR NR NR NR NR NR NR NR NR NR NR 0.2 _0.0090 CV NR NR NR NR NR NR NR NR Comments: A FORM X - IN ILM04.0 42 DUP050307285 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No. : _____________ SAS No. : ________ SDG No. : FMD02 ICP ID Number: ____ 05936_____ Date: 07/15/96 Flame AA ID Number: _________________ Furnace AA ID Number: Analyte Wave length (nm) Aluminum 308.21 Antimony- 206.83 Arsenic Barium 493.40 Beryllium 313.04 Cadmium 226.50 Calcium 317.93 Chromium 267.71 Cobalt 228.61 Copper 324.75 Iron 271.44 Lead Magnesium 279.07 Manganese 257.61 Mercury Nickel 231.60 Potassium 766.49 Selenium Silver 328.06 Sodium 330.23 Thallium Vanadium 292.40 Zinc 206.20 Back ground CRDL (ug/L) 775 60 200 5 5 5000 10 50 25 loo 5000 15 40 5000 10 5000 TO 20 IDL (ug/L) M 2777 P" 2.8 P NR 0.10 P 0.99 P 0.50 P 17.6 P 0.86 P 0.92 P 0.98 P 19.0 P NR 19.3 P 0.17 P NR 1.6 P 53.4 P NR 0.30 P 161 P NR 0.44 P 4.1 P Comments: FORM X - IN ILM04.0 43 DUP050307286 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: _________ Case No.: _________ SAS No.: _________ SDG No.: FMD02 ICP ID Number: ____ 05936 ____ Date: 09/12/96 Analyte Wave length (nm) Interelement Correction Factors for: A1 Ca Fe Mg CO Aluminum --303721 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Antimony_ "206.83 "0.0000000 "0.0000000 "0.0000000 _o.ooooooo _o.ooooooo Arsenic Barium 493.40' 0.0000006 6.ooooooo o.oooooOO 0.0000000 0.0000000 Beryllium 313.04 -0.0000020 0.0000000 -0.0000010 0.0000000 0.0000000 Cadmium 226.50 0.0000020 0.0000000 0.0001110 0.0000000 -0.0001580 Calcium 317.93 0.0000000 "0.0000000 -0.0002340 0.0000000 0.0000000 Chromium 267.71 0.0000000 0.0000000 0.0000040 0.0000000 0.0000000 Cobalt 228.61 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Copper 324.75 0.0000060 "0.0000000 "0.0000000 0.0000000 0.0000000 Iron __ 271.44 _0.0000000 "0.0000000 _o.ooooooo _o.ooooooo _0.0717430 Leadl Lead2 Magnesium 279.07 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Manganese __ 257.61 _0.0000000 _o.ooooooo _o.ooooooo _o.ooooooo _o.ooooooo Mercury___ Nickel 231.60 0.0000000 0.0000000 0.0000000 0.0000000 -0.0006820 Potassium 766.49 "0.0000000 "0.0000000 "0.0000000 "0.0000000 _o.ooooooo Seleniuml Selenium2 Silver 328.06 0.0000000 0.ooooooo 0.0000000 0.0000000 0.ooooooo Sodium __ 330.23 -0.0000620 _o.ooooooo _o.ooooooo _o.ooooooo _o.ooooooo Thallium_ Vanadium 292.40 0.0000000 0.0000000 -0.0003270 0.0000000 0.0000000 Zinc ___206.20 _0.0000290 __o. ooooooo -0.0000860 _o.ooooooo _o.ooooooo Comments: FORM XI (PART 1) - IN ILM04.Q 44 DUP0503 07287 U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: _________ Case No.: _____________ SAS No.: ________ SDG No.: FMD02 ICP ID Number: ____ 05936 ____ Date: 09/12/96 Analyte Wave length (nm) Interelement Correction Factors for: CR MN MO NI TI Aluminum 308.21 0.0000000 0.0000000 -0.0043470 0.0000000 -0.0062140 Antimony_ ___206.83 -0.0033330 "0.0000000 _0.0000000 _0.0000000 -0.0020410 Arsenic Barium 493.40 0.0000000 0.00O0000 0.0000000 0.0000000 0.0000000 Beryllium 313.04 0.0000000 "0.0000000 0.0000000 0.0000000 0.0000000 Cadmium 226.50 ~0.0000000 "0.0000000 0.0000000 0.0000000 0.0000000 Calcium 317.93 0.0000000 "0.0000000 "0.0000000 "0.0000000 0.0000000 Chromium 267.71 0.0000000 0.0000620 "0.0000000 0.0000000 0.0000000 Cobalt 228.61 -0.0004150 "0.0000000 "0.0000000 0.0002200 0.0014390 Copper 324.75 0.0000000 "0.0000000 0.0000000 0.0000000 0.0000000 Iron ___271.44 _0.0014000 "0.0000000 _0.0000000 _0.0000000 _0.0000000 Leadl Lead2 Magnesium 279.07 0.0006000 0.0000000 0.0000000 0.0000000 0.0000000 Manganese __ 257.61 _0.0000000 "0.0000000 "0.0000000 _0.0000000 _0.0000000 Mercury Nickel 231.60 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Potassium ___766.49 _0.0000000 "0.0000000 _0.0000000 _0.0000000 _0.0000000 Seleniuml Selenium2 Silver 328.06 0.0000136 -0.6001320 0.0000000 "oToo'ooooo 0.0000000 Sodium ___330.23 -0.0060000 _0.0000000 _0.0000000 _0.0000000 -0.0498100 Thallium_ Vanadium 292.40 -0.0008170 0.0000000 0.0000000 0.0000000 0.0005900 zinc ___206.20 _0.0007900 _0.0000000 _0.0003360 _0.0000000 _o.6000000 Comments: A ___________ A FORM XI (PART 2) - IN ILM04.0 DUP050307288 U.s. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: LANCASTER^LABORATORIES____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: ________ SDG No.: FMD02 ICP ID Number: ____ 05936 ____ Date: 09/12/96 Analyte Wave length (nm) Interelement Correction Factors for: v ___ ___ ___ ___ Aluminum 308.21 0.0219600 0.0000000 0.0000000 0.6000000 0.0000000 Antimony "206.83 "0.0000000 "0.0000000 "0.0000000 30.0000000 _0.0000000 Arsenic Barium 493.40 o.ooooooO o.ooOoooo 0.0000000 0.0000000 0.0000000 Beryllium 313.04 0.0011680 0.0000000 0.0000000 0.0000000 0.0000000 Cadmium 226.50 "0.0000000 0.0000000 0.0000000 "0.0000000 0.0000000 Calcium 317.93 0.0000000 0.0000000 "0.0000000 0.0000000 0.0000000 Chromium 267.71 "0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Cobalt 228.61 "0.0000330 0.0000000 0.0000000 "0.0000000 0.0000600 Copper 324.75 -0.0001130 0.0000000 0.0000000 0.0000000 0.0000000 Iron ___271.44 _0.0095260 _0.0000000 _o.ooooooo _0.0000000 _0.0000000 Leadl Lead2 Magnesium 279.07 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Manganese ___257.61 _0.0000000 _0.0000000 _0.0000000 JO.0000000 _0.0000000 Mercury Nickel 231.60 o.Ooooooo 6.0000000 0.0000000 0.6666006 6.0000000 Potassium "766.49 "0.0000000 _0.0000000 _0.0000000 30.0000000 _0.0000000 Seleniuml Selenium2 Silver 328.06 O.ooOoooo 6.0000000 0.0000006 0.0000000 O.0000000 Sodium "330.23 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000 Thallium Vanadium 292.40 o.oooooo6 6.0000000 0.6600000 0.0000000 0.0000000 Zinc "206.20 _0.0000000 _0.0000000 _0.0000060 30.0000000 _0.0000000 Comments: FORM XI (PART 2} - IN i-5u.. ILM04.0 46 DUP050307289 U.S. EPA - CLP 12 ICP LINEAR RANGES (QUARTERLY) Lab Name: LANCASTEK_LABORATORIES____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: ________ SDG No.: FMD02 ICP ID Number: ____ 0593 6______ Date: 07/15/96 Analyte Sluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Integ. Time (Sec.) Concentration (ug/L) M 10.00 10.00 ib.flfl -- 10.00 10.00 10.00 10.00 10.00 10.00 10.00 io.oo 10.00 10.00 10.00 io.Oo 10.00 10.00 10.00 600000.0 W 50000.0 P NR SOoo.O P 5000.0 P 20000.0 P Sooooo.o P 100000.0 P 50000.0 P 50000.0 P 200000.0 P NR 60006O.6 P 50000.0 P NR 50000.0 P 50000.0 P NR SObo.o P 50000.0 P NS 50000.0 P 5000.0 P Comments: FORK XII - IN ILM04.0 47 DUP050307290 Preparation and Run Logs 48 DUP050307291 U.S. EPA - CLP 13 PREPARATION LOG Lab Name: LANCASTER-LABORATORIES____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: Method: P SDG No.: FMD02 EPA Sample No. 1DDIS 1SDIS 2DDIS 2SDIS 4DDPF FB1DS LCSW PBW RA3SF RA4SF RD3DF RD3DFD RD3DFS RS4DF RS5SF Preparation Date 09724796 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 " 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 Weight (gram) Volume (ml) 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 FORM XIII - IN ILM04.0 49 DUP050307292 U.S. EPA - CLP 13 PREPARATION LOG Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: ________ Method: F SDG No.: FMD02 EPA Sample No. 1DDIS 1SDIS 2DDIS 2SDIS 4DDPF FB1DS LCSW PBW RA3SF RA4SF RD3DF RD3DFD RD3DFM RD3DFS RS4DF RS5SF Preparation Date 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 Weight (gram) Volume (ml) 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 FORM XIII - IN ILM04.0 50 DUP050307293 U.S. EPA - CLP 13 PREPARATION LOG Lab Name: LANCASTER_LABORATORlES_____ Lab Code: ________ Case No.: _____________ Contract: SAS No.: _________ Method: CV SDG No.: FMD02 EPA Sample No. 1DDIS 1SDIS 2DDIS 2SDIS 4DDPF FB1DS LCSW PBW RA3SF RA4SF RD3DF RD3DFD RD3DFS RS4DF RS5SF Preparation Date 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 Weight (gram) Volume (ml) 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 FORM XIII - IN ILM04.0 51 DUP050307294 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD02 instrument ID Number: 05936_ Method: P_ Start Date: 09/24/96 End Date: 09/25/96 EPA Sample No. SO S S S ICV ICB CRI ICSA ICSAB CCV CCB PBW LCSW RD3DF RD3DFA RD3DFD RD3DFS RD3DFL RS5SF RS4DF 4DDPF CCV CCB RA4SF RA3SF 2DDIS 2SDIS 1DDIS 1SDIS FB1DS CRI ICSA D/F Time i.00 TZTZ 1.00 2218 1.00 2222 1.00 2226 1.00 2229 1.00 2234 1.00 2238 1.00 2242 1.00 2247 1.00 2251 1.00 2255 1.00 2300 1.00 2304 1.00 2309 1.00 2313 1.00 2317 1.00 2322 5.00 2326 1.00 2331 1.00 2335 1.00 2339 1. 00 2344 1.00 2348 1.00 2353 1.00 2357 1.00 0001 1.00 0006 1.00 0010 1.00 0015 1.00 0019 1.00 0023 1.00 0028 %R Analytes X s A B B c C e 6 F p M M N X s A N IT z LB s AEDAR0uE B GN G I E GA L N XX X X XX XX X XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX X XX XX XX XX XX X XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX X XX .. X XXX X XX X XXXX XXXX XXX X X XX XXXX XXXX XXXX XXXX XXXX XXXX XX X X XX XX X XX XX XX XX XX XX XX XX XX XX X X XX XX X XX XX X X XMM MM -- X X X -- X X MM -M XX XX MM. MM X X X MM X X X X "" MM XX XX XX XX XX X X "" X X MM X X MM XX X X MM X X MM X X X X MM X X X MM -- X X X X MM M. mm X XXX X x" X X XX X MM MM. MM *-- XXXX XXXX X XX XX X MM. M. M. X X MM MM X X X X XXXX XXXX XXXX XX XX XX XX XX XX XX X X X X X X X mmm mm mm *" X X X X X MM MM " MM X X X X X X X X M. -- " MM XX XX X X ' X X MM. X X MM X X MM XXXX XX --M XX XX MM XX X X X X X X X X X X X X X X X X X X X X X X X X -- -- X X X X X X X X X X X X -- mmm mmm X X X X X X X X X X X X MM. MM MM * *-- X X X X X X MM -- -- X X MM MM MM -- MM MM X X X X X X X X X X X X -- -M -- -- -- -- XX X X XXX _ _mm X X X """ X X X MM MM X X X -- -- -M X X X X -- -- MM. FORM XIV - IN ILM04.0 52 DUP050307295 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTERJ^ORATORIES Lab Code: ________ Case No.: Instrument ID Number: 05936_ Start Date: 09/24/96 Contract: SAS No.: ________ SDG No.: FMD02 Method: P_ End Date: 09/25/96 FORM XIV - IN ILM04.0 53 DUP050307296 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTERJLABORATORIES. Contract: ____________ Lab Code: ________ Case No.: SAS No. : ________ SDG No. FMD02 Instrument ID Number: 05936_ Method: P_ Start Date: 09/26/95 End Date: 09/26/96 EPA Sample No. SO S s s let? ICB CRI ICSA ICSAB CCV CCB PBW LCSW RD3DF RD3DFA RD3DFD RD3DFS RD3DFL RS5SF RS4DF 4DDPF CCV CCB RD3DF RD3DFA RD3DFD RD3DFS RD3DFL RA3SF 2DDIS CRI ICSA D/F Time 1.00 0911 1.00 0916 1.00 0921 1.00 0925 1.00 0929 1.00 0934 1.00 0939 1.00 0944 1.00 0949 1.00 0954 1.00 0959 1.00 1004 1.00 1009 10.00 1014 10.00 1019 10.00 1024 10.00 1028 50.00 1033 1.00 1038 10.00 1043 10.00 1048 1.00 1053 1.00 1058 1.00 1103 1.00 1108 1.00 1113 1.00 1118 5.00 1123 10.00 1128 10.00 1133 1.00 1138 1.00 1143 %R Analytes ASAB B C C C c C F PMMHN K S AN TV z LB S AEDAR0UEBGN G I EGAL N XX X X -- X X XX XX X XX XX XX XX XX XX X X "" X X -- mmm " -- -- ~~ X X "-- -- """ "" "" "~ X X XX X X-- -- XX XX X X * ** ~ -- -- X X X *-- "" --"" -- --* XX XX X XX _ _ ___ mmm ~---- _ X X "" "" " "" X -- -- -- -- FORM XIV - IN ILM04.0 54 DUP050307297 U.s. ERA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTERJLABORATORIES Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No. FMD02 Instrument ID Number: 05936_ Method: P_ Start Date: 09/26/96 End Date: 09/26/96 EPA Sample No. ICSAB CCV CCB 2SDIS 1DDIS RS4DF 4DDPF RA4SF RA3SF 2DDIS 2SDIS 1DDIS 1SDIS CCV CCB FB1DS CRI ICSA ICSAB CCV CCB D/F Time ITTO 1148 1.00 1152 1.00 1157 10.00 1202 10.00 1207 1.00 1212 1.00 1217 1.00 1222 1.00 1227 1.00 1232 1.00 1237 1.00 1242 1.00 1247 1.00 1252 1.00 1257 1.00 1302 1.00 1307 1.00 1312 1.00 1317 1.00 1321 1.00 1326 %R Analytes A s A B B C C C C P M M H N K s A N T "V 2 LB SAEDARoUE B GNG I EG AL N XX XX XX X -- X _---- X X ""mmt mmm mmm XX XX XX XX XX XX XX XX XX XX X XX XX XX XX _ _ _mmm mmm _ ~_ _ -- -- -- "" mmm "" "" X~---- M mmm _ "" X X ~~ "" """ _" _ "" *" X M. mm X -- M. "_ < X M. X --'" "" ~ __ FORM XIV - IN ILM04.0 55 DUP050307298 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTERJLABORATORIES____ Contract: Lab Code: ________ Case No.: SAS No.: ______________________ SDG No. : FMD02 Instrument ID Number: 04724_ Method: F_ Start Date: 09/24/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Analytes A S A B C C C C C F P M M H NX S A N i V z LB SAEDAR0UEBGNG I EGAL N 5T5------------S10 S20 S40 S60 S80 ICV ICB CRA CCV CCB zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz CCV CCB zzz^Z! zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz 2109 1.00 2113 1.00 2117 1.00 2121 1.00 2125 1.00 2129 1.00 2134 1.00 2138 1.00 2142 1.00 2146 1.00 2150 1.00 2154 1.00 2159 1.00 2203 1.00 2207 1.00 2212 1.00 2216 1.00 2220 1.00 2225 1.00 2229 1.00 2233 1. 00 2238 1. 00 2242 1. 00 2246 1. 00 2250 1.00 2254 1. 00 2258 1. 00 2303 1.00 2307 1.00 2311 1.00 2315 1.00 2319 X X X X X X X X X ---- mmm FORM XIV - IN ILM04.0 56 DUP050307299 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTERJ^ORATORIES Contract: ________________ Lab Code: _________ Case No.: SAS NO.: ________ SDG NO.: FMD02 Instrument ID Number: 04724_ Method: F_ Start Date: 09/24/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Analytes ASABB CCC CC F PMMHN K S ANTV z LB S A E DAR0 U E B G N G I E G AL N ZZZZZZ ccv CCB ZZZZZZ zzzzzz ZZZZZZ zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz CCV CCB PBW PBWS LCSW LCSWA RS5SF RS5SFA RS4DF RS4DFS 4DDPF 4DDPFA CCV CCB RA4SF RA4SFA RD3DF RD3DFA RD3DFD 1.00 2321 1.00 2328 X 1.00 2332 X 1.00 2336 1.00 2340 1.00 2344 1.00 2348 1.00 2352 1.00 2356 1.00 0000 1.00 0004 1.00 0008 1.00 0013 1.00 0017 X 1.00 0021 X 1.00 0025 X 1.00 0029 104.6 1.00 0033 X 1.00 0037 __ 108.8 X 1.00 0041 1.00 0046 93.3 X 1.00 0050 X 1.00 0054 92.7 X 1.00 0059 X 1.00 0103 91.9 X 1.00 0107 X 1.00 0111 X 1.00 0115 X 1.00 0120 108.4 X 1.00 0124 X 1.00 0128 9572 X 1.00 0133 mmm __ _ _ _ -- " -- -- """ FORM XIV - IN ILM04.0 57 DUPO 503 07300 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD02 Instrument ID Number: 04724_ Method: F_ Start Date: 09/24/96 End Date: 09/25/96 EPA Sample No. ? SDF? $ RD3DFS ZZZZZZ RA3SF RA3SFA CCV CCB 2DDlS 2DDIS5 2SDIS 2SDISA 1DDIS 1DDISA 1SDIS 1SDISA FB1DS FB1DSA CCV CCB D/F Time 1.00 0137 1.00 0141 1.00 0146 1.00 0150 1.00 0154 1.00 0159 1.00 0203 1.00 0207 1.00 0211 1.00 0215 1.00 0219 1.00 0223 1.00 0227 1.00 0231 1.00 0235 1.00 0240 1.00 0244 1.00 0248 1.00 0252 Analytes %R AS AB B C CC C c F PMMHNK S ANTV Z LB SAEDAROUEBGNG I E GAL N 102.2 X X 102.4 112.0 103.7 100.6 109.0 111.8 X X X X X X X X X X X X X X X FORM XIV - IN ILM04.0 58 DUPO50307301 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: __________ Lab Code: _________ Case No.: SAS No.: ________ SDG No.: FMD02 Instrument ID Number: 03812_ Method: F_ Start Date: 09/24/96 End Date: 09/25/96 EFA Sample No. D/F Time %R Analytes A S ABB C C C C C F PMMHN K S A N T V Z LB SA E DAR0U E B GN G I E G A L N SO S3 S9 S15 S30 S60 ICV ICB CRA zzzzzz ccv CCB ZZZZZZ zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz ccv CCB ZZZX22 zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz l.TO 2048 1.00 2053 1.00 2058 1.00 2103 1.00 2108 1.00 2113 1.00 2117 1.00 2122 1.00 2126 1.00 2131 1.00 2136 1.00 2141 1.00 2145 1.00 2150 1.00 2154 1.00 2159 1.00 2204 1.00 2209 2.00 2213 2.00 2218 1.00 2223 1.00 2227 1.00 2232 1.00 2237 1.00 2241 1.00 2246 1.00 2250 1.00 2255 1.00 2300 1.00 2304 1.00 2309 1.00 2314 X X X X X X X X X X X X X ' FORM XIV - IN ILM04.0 59 DUP050307302 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: Lab Code: ________ Case No.: SAS NO.: ________ SDG No. FMD02 Instrument ID Number: 03812_ Method: F_ Start Date: 09/24/96 End Date: 09/25/96 EPA Sample No. 222ZZB zzzzzz ccv CCB ZZZTSZ zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz ccv CCB ZZZ^ZE zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz ccv CCB PBW PBWA LCSW LCSWl D/F Time 1.00 2318 1.00 2323 1.00 2327 1.00 2332 1.00 2336 1.00 2341 1.00 2346 1.00 2350 1.00 2355 1.00 0000 1.00 0004 1.00 0009 1.00 0013 1.00 0018 1.00 0023 1.00 0027 1.00 0032 1.00 0037 1.00 0041 1.00 0046 1.00 0051 1.00 0056 1. 00 0100 1.00 0105 1.00 0110 1.00 0114 1. 00 0119 1.00 0124 1. 00 0128 1.00 0133 1.00 0138 1.00 0143 %R Analytes A S ABBC C C Cc FPMMHNK SAN TV LB S A EDAR0 U E B GN G I E GAL N X X iii.o 115.3 X X --' X X X mmm "" ---- ***" "" "" X X X FORM XIV - IN ILM04.0 60 DUP050307303 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTERJUVBORATORIES Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD02 Instrument ID Number: 03812_ Method: F_ Start Date: 09/24/96 End Date: 09/25/96 EPA Sample No. D/F Time RS5SF RS5SFA RS4DF RS4DFA 4DDPF 4DDPFS CCV CCB RA4SF RA4SFA RD3DF RD3DFA RD3DFD RD3DFDA RD3DFS ZZZZZZ RA3SF RA3SF5 CCV CCB 2DDIS 2DDISA 2SDIS 2SDISA 1DDIS 1DDISA 1SDIS 1SDISA FB1DS FB1DSS CCV CCB 1.00 0147 1.00 0152 1.00 0157 1.00 0202 1.00 0206 1.00 0211 1.00 0216 1.00 0220 1.00 0225 1.00 0230 1.00 0234 1.00 0239 1.00 0244 1.00 0248 1.00 0253 1.00 0258 1.00 0302 1.00 0307 1.00 0312 1.00 0316 1.00 0321 1.00 0326 1.00 0330 1.00 0335 1.00 0339 1.00 0344 1.00 0349 1.00 0353 1.00 0358 1.00 0403 1.00 0407 _____ 1.00 0412 Analytes %R A S A B c c c c C t P to a N K s k N T V z LB SAEDAR0U EB GNG I EGAL N 68.4 3.4 6.0 106.4 5970 71.7 61.6 72.0 66.8 71.2 7174 110.4 _ ___ - X X X X X X ~ ~~ MM MM MM> MM X X " " "M_ MM MM MM X _~ X X X X X --X "*M_ MM MM t " M-- "*** MM MM. X -- MM MMM. MM MM. X MM MM. MM -M MM MM. X MM MM MM MM MM X MM -M MM X MM MM MM MM MM -- ~ -- MM MM MM MM MMM MM MM MM MM --MM M MM ~ MM MM X """ -- **" --> PM> MM. MM. MM MM XXMM MM MM MM MM MM MM ' MM MM MM M MM M. -- MM "" MM -- -- M. -- -- MM MM. -- -- -M MM -M M. " X __. . --M. MM MM. X _ M. -- FORM XIV - IN ILM04.0 61 DUP050307304 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: SAS No.; ______________________ SDG No.: FMD02 Instrument ID Number: 03812_ Method: F_ Start Date: 09/24/96 EPA Sample No. D/F Time %R End Date: 09/25/96 Analytes -------- A S A B B C C C C CT P M M H N K S A N T V Z L B S A E D A R O IT E B G N G I E G A L N SO S3 S9 S15 S30 S60 ICV ICB CRA CCV CCB ZZZZZZO ZZZZZZ1 ZZZZZZ2 ZZZZZZ3 ZZZZZZO ZZZZZZ1 ZZZZZZ2 ZZZZZZ3 ZZZZZZO ZZZZZZ1 ZZZZZZ2 ZZZZZZ3 ZZZZZZO ZZZZZZ1 ZZZZZZ2 ZZZZZZ3 2SDIS0 2SDIS1 2SDIS2 2SDIS3 CCV CCB 1.00 053T 1.00 0550 1.00 0552 1.00 0555 1.00 0558 1.00 0600 1.00 0603 1.00 0605 1.00 0608 1.00 0610 1.00 0613 1.00 0615 1.00 0618 1.00 0620 1.00 0623 1.00 0625 1.00 0628 1.00 0630 1.00 0632 1.00 0635 1.00 0637 1.00 0640 1.00 0642 1.00 0645 1.00 0647 1.00 0649 1.00 0652 1.00 0654 1.00 0657 1.00 0659 1.00 0702 1.00 0704 1.00 0707 X X X X X X X X X X X X X X X FORM XIV - IN ILM04.0 62 DUP050307305 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD02 Instrument ID Number: 04725_ Method: F_ Start Date: 09/25/96 End Date: 09/25/96 Analytes Sample No. D/F Time %R A S A F B C 6 rc F F TT TT N K A N T V z LB SAEDARouE B GNG I E GAL N SO S5 S15 S25 S40 S50 ICV ICB CRA CCV CCB PBW PBWA LCSW LCSWA RS5SF RS5SFA RS4DF RS4DFA 4DDPF 4DDPFA CCV CCB RA4SF RA4SFS RD3DF RD3DFA RD3DFD RD3DFDA RD3DFS ZZZZZZ RA3SF RA3SFA I77HJ 0123 1.00 0127 1.00 0131 1.00 0135 1.00 0139 1.00 0143 1.00 0147 1.00 0151 1.00 0155 1.00 0159 1.00 0203 1.00 0207 1.00 0211 104.0 1.00 0216 1.00 0220 __ llB.4 1.00 0224 1.00 0228 7577 1.00 0232 1.00 0237 93.9 1.00 0241 1.00 0245 73.7 1.00 0249 1.00 0253 1.00 0257 1.00 0301 101.5 1.00 0305 1.00 0309 97.6 1.00 0313 1.00 0317 98.8 1.00 0321 1.00 0325 1.00 0329 1.00 0333 8870 X X X X X X X X X X X X X X X X X X X X X X X-- "" -- "" -- _ " -- -- "" "" "" FORM XIV - IN ILM04.0 63 DUP050307306 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No. FMD02 Instrument ID Number: 04725_ Method: F_ Start Date: 09/25/9(5 End Date: 09/25/96 EPA Sample NO. D/F Time %R Analytes AsABBCC CCCF PMMHNK SANTV Z LBSAEDAROUE BGNG I E GAL N CCV CCB 2DDTS 2DDISA 2SDIS 2SDISA 1DDIS 1DDIS5 1SDIS 1SDISA FB1DS FB1DSA CCV CCB T7W (5337 1.00 0341 1.00 0345 1.00 0349 94.2 1.00 0353 1.00 0357 110.6 1.00 0401 1.00 0405 lie. h 1.00 0409 1.00 0413 -9.959$ 1.00 0417 1.00 0421 124.0 1.00 0426 1.00 0429 FORM XIV - IN ILM04.0 64 DUPO 50307307 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: Lab Code: _________ Case No.: SAS No.: ________ SDG No.: FMD02 Instrument ID Number: 04725_ Method: F_ Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. D/F Time 0% R Analytes AS ABB C C C C c P MMH N LBSAEDARouEB GNG I ! SANTV z EGAL N SO S5 SI'S S25 S40 S50 ICV ICB CRA CCV CCB RA4SF RA4SFA RD3DF RD3DFA RD3DFD RD3DFDSRD3DFS ZZZZZZ RA3SF RA3SFA CCV CCB 2DDIS 2DDISA 2SDIS 2SDISA 1DDIS 1DDISA 1SDIS 1SDISA FB1DS 1.00 0905 X 1.00 0909 X 1.00 0913 X 1.00 0917 X 1.00 0921 X 1.00 0925 X 1.00 0929 X 1.00 0933 X 1.00 0937 1.00 0941 X X - 1.00 0945 X 1.00 0949 X _1.00 1.00 0953 0957 .... .9~6~15 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- X X -- ------- 1.00 1001 7178 X 1.00 1006 X 1.00 1010 1.00 1014 1.00 1018 72.9 ---- -- -- -- -- -- - -- -- -- -- -- -- -- -- -- X X -- -- -- -- -- -- 1.00 1.00 1022 1026 ____ 91.3 -- X X 1.00 1030 X 1.00 1034 1.00 1038 1.00 1042 1.00 1046 X X 86.9 -- -- -- -- -- -- -- -- -- -- -- ---- -- -- -- -- X X -- -- -- -- -- - 1.00 1050 __ 102.4 1.00 1055 1.00 1059 __ 100.8 5.00 1103 X X X 5.00 1107 __ 137.2 1.00 1111 X FORM XIV - IN ILM04.0 65 DUP050307308 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: Lab Code: _________ Case No.: SAS No.: ________ SDG No.: FMD02 Instrument ID Number: 04725_ Method: F Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Analytes AS ABBC C C CCFPMMHNK SANTV Z LB SAEDAROUEB GNG I EGAL N FB1DSA CCV CCB rros 1115 __10S.6 1.00 1119 1.00 1123 X - X FORM XIV - IN ILM04.0 66 DUP050 307309 U.S. EPA - CLP 14 ANALYSIS RON LOG Lab Name: LANCASTERJ^ABORATORIES Contract: _____________ Lab Code: ________ Instrument ID Number: Case No.: 04725_ SAS No.: ________ Method: F_ SDG No. FMD02 Start Date: 09/27/96 End Date: 09/27/96 EPA Sample No. SO S5 SI5 S25 S40 S50 ICV ICB CRA CCV CCB 1SDIS0 1SDIS1 1SDIS2 1SDIS3 ZZZZZZO ZZZZZZ1- ZZZZZZ2 ZZZZZZ3 ZZZZZZO- ZZZZZZ1 ZZZZZZ2- ZZZZZZ3 zzzzzzo- zzzzzzi ZZZZZZ2 ZZZZZZ3- zzzzzzo ZZZZZZ1- ZZZZZZ2- ZZZZZZ3 CCV - D/F Time i.Od 0112 1.00 0114 1.00 0116 1.00 0118 1.00 0120 1.00 0122 1.00 0125 1.00 0127 1.00 0129 1.00 0131 1.00 0133 10.00 0135 10.00 0137 10.00 0139 10.00 0141 5.00 0143 5.00 0145 5.00 0147 5.00 0149 5.00 0151 5.00 0153 5.00 0155 5.00 0157 5.00 0159 5.00 0200 5.00 0202 5.00 0204 10.00 0206 10.00 0208 10.00 0211 10.00 0213 1.00 0215 %R ASAB W LB SAE Analytes c C C c T1 -p- M IT H N K S A If i V 2 ARouE BGN G I EGAL N I on * X X -- X X X X X X X X X X -- -- -- -- -- -- -- -- -- -- -- _ -- -- -- -- -- X X -- -- -- -- -- -- X -- -- "" -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --- -- FORM XIV - IN ILM04.0 67 DUP050307310 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANGASTERJLABORATORIES____ Contract: Lab Code: ___ Case No.: SAS No. : ________ SDG No. : FMD02 Instrument ID Number: 04725_ Method: F_ Start Date: 09/27/96 End Date: 09/27/96 1 OO EPA Sample No. D/F Time %R ASABBCCC LB SAEDAR Analytes C FPMMHN K S AN TV Z UEBGNGI EGAL N CCB 1.00 0217 X FORM XIV - IN ILM04.0 68 DUP05030731 1 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name : LANCASTER_LABORATORIES Contract: _ Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD02 Instrument ID Number: 02803_ Method: F_ Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Analytes A S A B B C C c C cF P M M H NX s A N T V z LB SAEDARouEBGNGI EGAL N SO S10 S20 S40 S60 S80 ICV ICB CRA ZZZZZZ CCV CCB ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ A ZZZZZZ CCV CCB ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ TTcR) 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1. 00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1. 00 1. 00 1.00 1. 00 1.00 1.00 0523 0527 0530 0534 0538 0541 0545 0548 0551 0555 0558 0602 0605 0609 0612 0615 0619 0622 0626 0629 0633 0636 0640 0643 0646 0650 0653 0657 0700 0703 0706 0710 X X - X X X X X -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- X X -- -- - X X -- -- -- -- -- -- -- -- X X -- -- -- -- FORM XIV - IN ILM04.0 69 DUP050307312 TJ.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTERJLABORATORIES Contract: Lab Code: ________ Case No.: SAS No.: ______ _ SDG No.: FMD02 Instrument ID Number: 02803_ Method: F_ Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Inalytes A S B B C C C C c F P M M H N K S A N T 17 z LB SAEDARouEB GN G I EGAL N zzzzzZ ZZZZZZ CCV CCB ZZZX2Z ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV CCB PBW PBWS LCSW LCSWA RS5SF RS5SFA RS4DF RS4DFA 4DDPF 4DDPFA CCV CCB RA4SF RA4SFA RD3DF RD3DFA 1.00 0713 1.00 0717 1.00 0720 1.00 0723 ........ 1.00 0727 .......... 1.00 0730 1.00 0733 1.00 0737 1.00 0740 1.00 0744 1.00 0747 1.00 0751 1.00 0754 1.00 0757 1.00 0801 1.00 0804 1.00 0807 1.00 0811 110.6 1.00 0814 1.00 0818 98.6 1.00 0821 1.00 0825 100.4 1.00 0828 1.00 0832 89.7 1.00 0835 1.00 0839 96.0 1.00 0842 1.00 0845 1.00 0849 1.00 0852 105.2 1.00 0856 1.00 0859 ____ 98.8 X X X X X X X X X X X X X X X X X X X X FORM XIV - IN ILM04.0 70 DUP050307313 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Lab Code: ________ Case No.: Instrument ID Number: 02803_ Start Date: 09/25/96 Contract: SAS No. : ________ SDG No. Method: F_ End Date: 09/25/96 FMD02 EPA Sample No. D/F Time %R S B C C C C C F P M H N K S KN T V z LB SAEDAROUEB GNGI EGAL N 1 RD3DFD 1.6TJ 0903 RD3DFDA 1.00 0906 98.8 RD3DFS 1.00 0910 ZZZZZZ ....... 1.00 0913 RA3SF l.oo 0917 RA3SFA 1.00 0920 89.9 CCV 1.00 0924 CCB 1.00 0927 X X X X X X FORM XIV - IN ILM04.0 71 DUP050307314 U.S. EPA CLP 14 ANALYSIS RON LOG Lab Name: LANCASTERJLABORATORIES Contract: _ Lab Code: ________ case No.: SAS No.: ________ SDG No.: FMD02 instrument ID Number: 02803_ Method: F_ Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. SO S10 S20 S40 S60 S80 ICV ICB CRA ZZZZZZ CCV CCB ZZZX2X ZZZZZZ 2DDIS 2DDISA 2SDIS 2SDISK 1DDIS 1DDISS 1SDIS___ 1SDISA CCV CCB s FB1DSS CCV CCB Analytes D/F Time %R ASABBC C C CC FPMMHNK S ANTV z LB S A EDAROUEB G NG I EG AL N 1.00 TUB 1.00 1228 1.00 1232 1.00 1236 1.00 1239 1.00 1243 1.00 1246 1.00 1250 1.00 1253 1.00 1256 1.00 1300 1.00 1303 1.00 1306 1.00 1310 1.00 1313 1.00 1317 92.3 1.00 1320 1.00 1324 100.6 1.00 1327 1.00 1331 93.6 1.00 1334 1.00 1338 98.6 1. 00 1341 1.00 1344 1. 00 1348 1.00 1351 ___103.2 1. 00 1355 1.00 1358 _~ -- -- M. X " - -- -- -- "" X X X X X--~ X ~X "" X X *-- "_ X X X -- """ -- -- x X -- -- -- X X X X X X-- X X X A FORM XIV - IN ILM04.0 72 DUP050307315 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: IANCASTERJLABORATORIES Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD02 Instrument ID Number: 05220_ Method: CV Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Analytes A S A B B C C C C F P M U N TC s A N ijr V z LB S AEDAR0 U EB GN G I EGAL N SO SO. 2 SO. 5 S1.0 S2.5 S5.0 ICV ICB CRA CCV CCB zziZzz ZZZZZZ zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz CCV CCB zzzzzz zzzzzz zzzzzz ZZZZZZ zzzzzz PBW LCSW RS5SF A RS4DF 1.00 1714 1.00 1716 1.00 1718 1.00 1721 1.00 1723 1.00 1726 1.00 1728 1.00 1731 1.00 1733 1.00 1735 1.00 1738 1.00 1740 1.00 1742 1.00 1745 1.00 1747 1.00 1749 1.00 1751 1.00 1754 1.00 1756 1.00 1758 1.00 1800 1.00 1803 1.00 1805 1.00 1807 1.00 1809 1.00 1812 1.00 1814 1.00 1816 1.00 1818 1.00 1821 1.00 1823 1.00 1825 -- -- __ -- X X ~ ~ * "" m-- X X X mmm X X X X X X ""mm mmm "-- mm "mmm ~ ~ "" mm -- X X "" ~- mm ------ *--* "" -- ---- - . ... --X X X _ X _ " "" -- "- -- *--* -- -- FORM XIV - IN ILM04.0 73 DUP050307316 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: Lab Code: _________ Instrument ID Number: Case No.: 05220 SAS No.: ________ Method: CV SDG No.: FMD02 Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. 4DDPF CCV CCB RA4SF RD3DF RD3DFD RD3DFS RA3SF 2DDIS 2SDIS 1DDIS 1SDIS FB1DS CCV CCB D/F Time 1.00 1827 1.00 1830 1.00 1832 1.00 1834 1.00 1837 1.00 1839 1.00 1841 1.00 1844 1.00 1846 1.00 1848 1.00 1850 1.00 1853 1. 00 1855 1.00 1857 1.00 1859 %R Analytes A L S B A S B A b E C D C A C R C o C U F E P B M G M N H G N I K s E A G N A * L V i N ~ ~ "* ** X X X ~-- "" X X X X X "" X-- ------------ -- X X X X X FORM XIV - IN ILM04.0 74 A DUP050307317 Raw Data 75 DUP050307318 ICP Data 76 DUP050307319 I ~ or s ;.:riew*c c-> q. ^hotA sr-f'ep -5v: lata rile Name : .26-50 r i d 2 . OAT ku" Name: 9 6 ? 6'8 0 7 7 6 2 strument Parameters: Rinse "1me: Individual Integration 7 i ms: Total Integration Time: SO s @c 1 u s sc 30 rgc L 'ierrienz Symool \a A'i t- Co l ?> ur f .< ivtf >10 WC:V * IV' i- D PlT\0 ?.*fr :# 5-r ;.r T* n V / 7 r. Element Name Silver Aluminum A.r sen i c boron bar i urn Beryllium Calcium Cadmiurn Coca 11 Cnromium Copper Iron Potassium Magnesium; manganese lio'i yb ci enu It 'S od i um 1M 1 C K fe : Lead L ?. 9 CAntlmony Se`t eni um elenvjm 7 i r. jti'ontium 7i*?.n *i j rr Thallium V 9 i*i3Ql u n*. r'ttri um 2 \ n : (Navel enstn s nm 323.06 3 06.2 f 189.04 249.67. 493.40 3 13;. 0 4 317.93 226.50. 228.si . 267 .7 ", 324.75 21 1 . 44 765.49 279.07 2 57.5 1 2 0 2.0 3- 330.23 23 1 . 60 220.35/1 220.35/2 2 0 6.8 3/1 196.02/2 ; 9 6.0 2 /1 189.96 4 2 1 .55 334 ci i, 190.06 2 9 2.4 C 7 1.03 206 . 2C :he dlE TRACE ICP uses a Or swf ord-.Kunse 1 man Noise Reduction Technique for `lead ana seTemum. Tins requires the utilization of tne first and second oraer wavelengths in the calculation of each of these metals 77 determinations. The 5'lc. TRACE ICP' also uti lizes Yttrium as an interna"! standard to compensate for fluctuation' in neou1ization and olasma conditions. DU P050307320 r rmn r.r~ . .-..rrO ; Ttv' 'if. n aas LANCASTER LABORATORIES kun Name-,: 9 6 26 so? re-: I#S$Ru '( N1 ID; 950 Tube: 1 SO 09/24/96 22; 14 ELE'M CONC i o? m ; AvC- In n SI0 RATIO %R50 It '! 2 In t ; r $t o n s it 2 T* C' __ Afl __ A1 As Zj' __ 3a Be __ Ca __ Cd Co Cr __ Cu Fe K __ lvig __ i*l n __ Mc> Na NT __ Pb __ Sb Se __ Sn Sr Ti T1 __ S y __ 2 r< . 0 : 000 0.000 0.000 0.000 0.000 0.000 . o. ooo 0.000 U .000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 . ooo 0.0 0 0 , 0.000 0.000 0.000 0.000 0.000 0.0 00 N/A 0 . ooo -0.00265 0.01376 -0.00008 0.00003 0.00017 -0.02449 -0.00160 0.001 15 -0.00034 -0.00026 -0.00528 -0.00140 0.00310 0.001 16 0.00273 -0.00109 0.00029 0.00067 0.00082 0.00211 --0.01296 -0.00279 0.00196 -0.00368 -0.00061 0.00021 52809.66796 Q . 000 1 0 6.239 0.590 327.2 125.1 18.94 0.101 9.936 41.40 36.50 14.09 1.161 20.27 28.41' 9.646 10.89 26.06 16 5.1 65.72 187.1 24.15 6.379 26.8$ 4.877 6.890 21 .80 100. ( 0.312 11.10 -0.00256 0.01385 0.00024 0.00001 0.00020 -0.02446 ' -0.00147 0.00083 -0.00022 -0.00030 -0.00524 -0..00145 0.00213 0.00128 0.00247 -0.00100 -0.00026 0.00028 -0.00043 0.00167 -0.01359 -0.00207 0.00200 -0.00341 -0.00049 0.00045 52980.00Q00 0.00009 -0-00255 0.01375 -0.00028 0.00000 0.00015 -0.02450 -0.00157 0.00170 -0.00047 -0.00022 -0.00535 ! - 0.0 01 6 c 0.00331 0.00113 0.00267 -O'. 00142 0.00056 0.00058 0.00255 0.00198 -0.01202 -0 . D0272 0.00204 -0.00392 -0.00060 0.00 0 1 5 52799.00000 0.00009 -0.00284 0.01369 -0.00022 0.00007 0.00015 -0.02450 -0.00178 0.00093 -0.00032 -0.00026 -0.00526 -0.00110 0.00385 0.00106 0.00305 -0.00087 0.00056 0.00115 0.00036 0.00267 -0.01327 .-0.00357 0.00186 - 0.0 037 2 -0.00075 0.00003 52650.00000 0.0001 1 78 DUP050307321 _ANCASTER l ABOftATOR IES ivt'i'i N sms : 952680 77 61' : ube : : t. F h 2 S1*5> CONC ( p pun AV'3 INTENSITY RATIO __Al __Ca __f e ,HK __ Ma Na Y 50 .000 5 u .000 50 . 000 50 . 000 50 . 000 50 . 000 N/A 2.62627 2.90745 3.09015 3.88840 2.88370 0.46207 52159.33203 09/24/96 22: 18 iNSTRljnEN" H> n c,o %RSD 0.913 0.660 0.672 1.039 0.739 0.92 8 0.941 #1 2.65220 2.92 590 3.10909 3.93296 2.90864 0.46685 51 599 ..00000 INTEGRATIONS #2 2.62177 .2.90886 3.09344 3.87815 2.87844 0.46 0 8 2 52363.00000 #: 2 . 60484 2.887 57 3.06792 3.85408 2.86402 0.45854 52516.00000 79 DUPO 50307322 I *10? : LANCASTER LABORATORIES j.'un Nams : 9 6 2 6 8 0 7 T 6 2 I NSTRUF:ENT I r, - 059 Tube: U. E T> 3 "t S CONC ( ppm ; A V& INTENSITY RATIO 09/24/96 %RS0 #1 22:22 INTEGRATIONS #2 4*3 __Aa As & __ B.a ___Be __ Cd Co __Cu _rln ~JT __ Pb . __ Se Sr ___T1 Y ' Zn 1 .000 1 .000 1 .000 1.000 . 1 .000 1 .000 1.000 1 .000 1 .000 1.000 1 .000 1.000 1 .000 1 ' 000 N/A 1.000 0.61604 0.24353 0.07480 1.05727 1.48756 3.13216 0.32844 0.62087 7.337 13 0.67080 0.58800 0.90521 28.99900 ' 0.06758 52005.00000 . 0 - 14054 0.251 0.452 0.545 0.204 0.498 0.565 0.401 0.415 0 .'347 0.780 1.146 0.521 0.049' 1 .375 0.431 0.834 0.61436 ' 0.24233 0.07434 1 . 05535 1.48396 3.13019 0.32782 0.61842 7.33229 0.67160 0.59495 0.91002 29.01424 0.06656 52068.00000 0.14045 0.61743 0.24450 .0^0751 1 1.05686 1.49610 3.15078 0.32996 0.62064 7.36473 0.67559 0.58757 0.90506 28.98539 0.06781 52318.00000 0.14175 0.61632 0.24376 0.074.95 1 . 059 8'' 1.48263 3.11552 0.32755 0.62357 7.3143 8 0.66521 0.58148 0.90057 28.99735. 0.06838 51869.00000 0.13942 80 DUP050307323 _ A N C A 5 T E R L .43 OR A T OR I E S ;un Name 95 2 6807762 ' RUmF NT I IT 05 Q lube:. 4 S3 09/24/96 22:25 t EM AVG CONC - INTENSITY (ppm) RATIO %R$0 #1 INTEGRATIONS #2 _Or __Mo __S b Sn __n V __r i . 000 i . 000 i . ooo' i .000 i .000 i . 000 N./A 0.62434 0.92905 0.44899 0.79624 3.72417 1.05483 51638-.33203 0 . 141 0.594 0.375 0.058 0.3 0*3 0.205 0.844 0.62428 0.92337 0 .'45089 0.79570 3.73639 1.05733 51156.00000 0.62349 0.92939 0.44769 0.79647 3.71404 1.05351 52004.00000 0.62525 0.93440 0.44838 0.79654 3.72209 1.05365 51755.00000 81 DU P05 0307324 I n a : LANCASTER LABORATORIES r; n Name: utae:. 5 9626807T62 ICV 09/24/96 2 2:29 INSTRUMENT IL: 0 593c t LEM Aa _Al As __ 8 Ba Ss __Ca __ Cd Co Or __ Cu fe __ K Ma _Mn ...Mo __ Na Ni ,,_Pb __ Sb Sn _Sr Ti . ___i't __ V r __ Zn A VO (ppm)' RSD 0.60633 30.14718 0.60588 0.62077 0.60203 . 0.61465 29.62161 0.58424 0.59618 0.60267 0.61539 29.79576 30.37939 30.02436 0.59642 0 ..60867 30.59942 0.59557 0.59554 0.58892 0.60581 0.60350 0.59975 0.61546 0.60029 0.60286 ' 50933.66796 0.57986 0.236 0.423 1 .357 0.652 0.414 0.442 0.613. 0.540 0.404 0.503 0.287 0.. 5 28 0.568 0.388 0.416 0.302 0.394 0.131 0.306 0.722 1 ..178 0.770 0.348 0.407 1 .355 0.482 0.334 0.802 *1 0.60521 29.99975 0.59742 0.61609 0.59916 0.61282 29.54345 0.58319 0.59419 0.60103 0.61359 ` 29.72206 30.23456 29.92606 0.59492 0.60677 30.46132 0.59646 0.59357 0:58413 0.60019 0.59948 0.59735 0.51302 0.59608 0.60078 50973.00000 0.57638 INTEGRATIONS 42 43 REREAD RED IG 0.60795 30.21740 0.61384 0.62305 0.60325 0.61777 29.82928 0.58779 0-. 59887 0.6061? 0.61547 29.97664 30.33303 30.15318 0.59929 0.61044 30.65144 0.59521 O'. 59717 0.59019 0.6 1-384 0 : 60859 0.60079 0.61803 0.. 60967 0.60618 50747.00000 0.58521 0.60584 30.22441 0.60638 0.62316 0.60369 0.61335 29.49209 0.58174 0.5S549 0.60080 0.61712 29.68857 30.57058 29.99384 0.59505 0.60880 30.68548 0.59502 0.59587 0.59240 0.60340 0.60243 0.6011? 0.61533 0.59518 0.60163 51081.00000 0.57747 DUP050307325 LANCASTER LABORATORIES air- Name: I iiDa : 9526807T62 IC8 09/24/96 22:34 in s t r u m; n t iu: 05935 u N Aa "'$ T '"'.As lTM'6 __8e _C a _`^Cd __ Co "M_Cr __.Cir __/ e __K Mg __,Mn __ Mo Na __.NT __Pb 7.Z-b ___ Se ____ Sn C>- __ T i _TT " ,y _r Zn Ave (ppm) %RSD #1 0.00020 97 .38 0.00042 0.00428 13.26 . 0.00475 -0.00057 290.6 -0.00239 0.00406 26.39 0.00526 0.00014 47.99 0.00022 -0.00033 31.57 -0.00024 -0.04501. 3.249 -0.04333 0.000 IS 187.3 -0.00017 0.00033 106.5 0.00068 . 0.00035 62.54 0.00054 -0.00005 164.4 0.00005 0.02802 26.02 0.03328 0.11317 0.481 0.11265 0.00531 32.48 0.00-575 0.00018 36.87 0.00024 0.00149 98.21 . 0.00319 0.13790 19.58 0.13217 -0.00090 41.71 -0.00077 -0.00010 457.4 -0.00063 0.00271 46.10 0.00333 -0.00017 668. 1 0.00066 0.00010 218.3 0 .0034 0.00011 27.09 0.00014 0.. 0001 6 54.85 0.00024 0.00520 8.288 0.00483 -0.00009 156.6 0.00006 51687.66796 0.153 51738.00000 0.00056 74.41 0.00010 INTEGRATIONS 42 0.00001 0.00443 -0.00026 0.00371 0.00009 -0.00032 -0.04565 0.00028 -0.00002 0.00039 -0.00013 0.01970 0.11314 0/00340 0.00011 0.00072 0.11422 -0.00060 0.00009 0.00.127 0.00034 0.00005 0.00009 0.00006 0.00567 -0.00023 51729.00000 0.00065 43 Rr ; r ; $? 0.00019 0.00365 0.00092 0.00320 0.00011 -0.00045 -0.04604 0.00034 0.00032 0.0001 1 . -0.00009 0.03110 0 . 11373 0.00579 0.00018 0.00057 0.16732 -0.00132 0.00023 . 0.00353' ; -0.00154 .-0.00009 0.00009 0.00018 0.0-0509 -0.00011 51596.00000 0.00093 RED If? 83 DUP050307326 LANCASTER LABORATORIES |. ijri Nsms: Tub*: 7 9626307T52 CRI 09/24/9-6 22 :38 INSTRUMENT IE1:' 0 5 936 ri i M An Al As , 0 Ba tie Ga Cd Co Cr Cu f e. K Mg Mn Mo __ Na NT Pb __ Sb Se Sn Sr Ti __ IT V -2n AV6 (ppm) SRSD 0.02077 0.800 -0.00600 39.46 0.01986 18.83 0.00197 38.32 0.00019 13.83 0.00993 1 .008 -0.05881 0.636 0.00988 1.347 0.10145 0.587 0.02068 1.355 0.05134 0.466 0.01675 57.81 0.10651 2.551 -0.00222 40.09 0.03052 0.834 0.00052 115.7 0.10308 80.26 0.08090' 1.218 0.00624 15.11 0.11773 1 .224 0.00788 3.919 -0.00012 781.8 .0.00004 25.98 0.00009 107.8 0.02010 5.212 0.10458 0.891 51909.00000 0.520 0.04050 1.450 41 0.02062 -0.00707 0.01988 0.00153 0.00021 0.00992 -0.05851 0.00990 0.10076 0.02052 0.05109 0.00796 0.10408 -0.00305 0.03028 0.00122 0.10606 0.08037 0.00521 0.11608 0.00754 -0.00005 . 0.00004 0.00015 0.01911 0.10354 52175.00000 0.04020 INTEGRATIONS 42 . 0.02073 -0.00764 0.01610 0.00154 0.00016 0.01003 -0.05869 0.00973 0. 10178 0.02052 0.05137 0.01515 0 . 10601 -0.00234 0.03050 0.00016 0.01889 .0.08204 0.00706 0.11874 0.00794 -0.00115 0.00003 -0.00002 0.02000 0.10484 51917.00000 0.04013 43 REREAD RED 1(3 0.020 95 -0.00328 0.02358 0.00284 0.00020 0.00983 -0.05923 0.01000 0.10180 0.02101 0.05157 0.02714 0. 10 945 -0.00128 0.03079 0.00018 0.18429 0.08029 0.00646 0.11838 0.00815 0.00082 0.00005 0 ..0001 5 0.0 21 2 0 0. 10535 51635.00000 0.04 VI 8 84 DUP050307327 c l A N C A S T R . L A B 0 R A TOR I E S Run Name: Tube : 8 9S26807T62 ICSA 09/24/96 22:42 INSTRUMENT ! n ; 05 9''f. ELEM Aq AT As s Ba Be Ca d Co Cr Cu F& K Mo Mn Mo Na N1 __ Pb Sb Se Sn Sr Ti __ T'l V __ Y __ Zn AVG uppm) 35RSO 0.00023 525.76043 b.00300 0.04673 0.00858 -0.00006 507.61065 -0.00695 0.00095 0.00161 -0.00098 203.54052 0.10682 532.06390 0.00594 -0.00017 0.17668 0.00021 *-0.00260 0.01165 -0.00923 0.00670 0.02060 -0.00093 -0.00119 -0.00208 48213.00000 0.00398 127.0 1.281 22.28 1 . 186 1.484 276.5 0.96.5 4.184 46.98 24.83 39.04 1 .024 1.822 0.999 1.114 414.2 78.34 390.7 75.60 33.45 11.28 34.04 1.192 9.730 12 1.7 13.46 1 . 042 3 2.61 #1 0.00058 518.00402 0.00323 0.04617 0.00844 0.00012501 . 96990 -0.00668 0.00135 0.001-60 -0.00055 201.13175 0.10904 525.93115 0.00594 0.00003 0.01748 0.00015 -0.00045 0.00834 -0.01039 0.00800 0.02032 -0.00085 -0.00177 -0.00181 48793.00000 0.00484 INTEGRATIONS #2 0.00007 529.14843 0.00353 0.04675 0.00860 -0.00009 510.02285 -0.00726 0.00103 0.00202 -0.00129 204.77078 0.10598 535.37274 0.00601 -0.00097 0.26859 0.001 10 -0.00432 0.01067 -0.00893 0.00406 0.02073 -0.00103 0.00046 -0.00206 47906.00000 0.00460 #3 REREAD'REDIG 0.00004 _______ 530.12890 0.00225 0.04727 _ 0.00869 -0.00022 510.83923____________ ___ -0.00692 0.00046 0.00122 ______________ ; -0.00109 204.71903 0.10543 534.88775 0.00587 0.00041 0.24396 -0.00060 -0.00305 0.01595 -0.00837 0.00803 _______ j 0.02075 ________________ -0.00090 -0.00226 _______ _______ -0.00237 47940.00000 0.00248 85 DUP050307328 LANCASTER LABORATORIES JL i j i f f'J ^ n Ki?: lube : 9 9626o0/ T? 2 ICSAB El. EM A ci ___ A 1 -A-'- __ Re C (Id __ C o Cr __ Cu __ r < __ K __ MCI __j'in Mo Na N1 __ P b Sb ___So* __ 'Sri Sr r-i __ T I __ V Y 2n AV6 (ppm.) 5SRSD 0.21717 0.512 524.02111 0.517 0.09779 2.022 . 0.02636 4.590 0.53013 0.417 0.48895 0.497 508.73291 0.567 0.93317 0.334 0.49185 0.349 0.49883 0.505 0.55362 0.392 203.41040 0.492 0.10137 3.491 529.02618 0.445 0.50096 0.419 0.00047 576.9 0.21701 22.47 0.95453 0.459 0.04941 3.582 0.62054 0.935 0.03812 5.541 0.00482 136.4 0.02055 0.516 -0.00086 10.86 0.09129 8.44:3 0.51368 0.455 48434.66795 0.351 0.91623 0.854 09/24/96 22:47 INS TRIJMENT ] [i Q 5 9r, #1 0.21652 522.63897 0.09564 0.02525 0.52909 0.48736 506.87170 0;93096 0.49076 0.49694 0.55292 202.78616 0.09742 527.97576 0.49982 -O '. 00125 0.18404 0-. 95346 0.04937 0.61385 0.03679 0.01224 0.02051 -0.00096 0.09101 0.51300 60?.00000 0.91115 INTEGRATIONS #2 0.21845 527.14782 0.09819 0.02765 0.53267 0.49175 51 2.06097 0.93674 0.49383 '0.50169 0.55606 204.56604 0.10244 531.72381 0.50339 -0.00093 0.19396 0.95935 0.05120 0.62365 0.04055 0.00253 0.02067 -0.00078 0.08372 0.51620 48262.00000 0 .'92525 #3 REREAD RED 16 0.21653 _______ 522.27648 0.09953 0.02617 ________________ 0.52862 0.48773 507.. 26602 _ 0.931 82 ____________ ___ 0.49096 0.49787 0.55189 202.87899 0.10425 527.37896 0.49969 _______ 0.00359 0.27303 ________________ 0.95077 0.04766 ________________ 0.62414 ____ : 0.03701 -0.00030 0.02047 -0.00083 ________________ 0.09913 0.51175 48440.00000 0.91230 86 L DUP050307329 PX ' *1 : L ANCASTER L A80RATOR IE Run Name: 9626807T62 Tube : 10 CCV 09/24/96 22:51 I N S TRI IM F !\|T ID; f) 5 9 3 r. ELEM AVG (ppm). %RSD .m INTEGRATION 5 #2 43 REREAD REDIG Aa 0.49383 0 . 132 . 0.49309 0.49433 0.49408. __ A1 25.44128 0.070 25.45718 25.42186 25.44478 As 0.4974.9 0.628 0.49428 0.50053 0.49767 8 0.50418 0.463 0.50151 0.50589 ' 0.50513 Ba 0.48993 0 . 149 0.43921 0.48991 0.49067 Be 0.49853 0.488 0.49573 0.49969 0.50016 __ Ca 25.41222 0.302 25.32382 25.46367 25.44916 __ Cd 0.485.9 2 0.557 0.48285 0.48693 0.48799 Co 0.48893 0.325 0.48711 0.48964 . 0.49005 Cr 0.49513 0.551 0.49201 0.49627 0.49710 Cu 0.50161 0.205 0.50105 0.50098 0 ..50280 ___Fe 25.03939 0.463 24.90595 25.09465 25.11757 ___K 26.33893 0.077 26.33915 26.31854 26.35910 Ma 25.19180 0.079 25.18878 25.17333 25.21328 ___Mn- 0.49310 0.410 0.49084 0.49374 0.49473 Mo 0.50176 0.708 0.49787 0.50256' 0.50484 __ Na 25.97978 0.238 25.97319 25.92129 .26.04486 ___ Ni 0.49208 0.446 0.48961 0.49280 0.49383 __ Pb 0.48915. 0.463 0.48684 6.49137 ' 0.48924 A __ 5b ___Se 0.47118 1.921 0.49247 1.527 0.46394 0.48411 0.46828 0.49868 0.48133 0.49463 __ Sn 0.49955 0.366 0.49751- 0.50105 0.50008 Sr 0.49192 0 . 173 0.49122 0.49166 0.49287 TT 0.50325 0.344 0.50130 .0.50391. 0.50458 ___ T'l . 0.49270 1 .-920 0.48185 0.49922 0.49704 V 0.50091 0.449 0.49853 0.50118 0.50301 __ Y 51208.66796 0.665 .50816.00000 51380.00000 51430.00000 __ Zn 0.48578 0.455 0.48323 0.48695 0.48716 87 DUP050307330 haoo : LANCASTER LABORATORIES Run Warner Tube: 1 1 9626807T52 CCB 09/24/96 22:5 INSTRUMENT ID: 05936 ELEM Aa __ AT As 0 __ Ba __ Be Ca Cd __ Co Cr Cu __ Fe __ K ' __ Mg __ -Mn __ Mo __ Ns NT __ Pb __ Sb ___Se Sn Sr TT T'l V __ Y Zn ' AV6 (ppm) %RSD ' 0.00023 75.64 0.04316 16.11 0.00035 1 69 . 1 0.00421 0.333 0.00013 21.03 -0.00021 32.23 -0.00569 119.3 0.00005 442.5 0.00004 915.4 0.00074 59.23 -0.00014 151.4 0.04264 30.02 0.11775 5.241 0.03929 22.91 0.00030 10.42 0.00186 49.51 0.19796 36.43 0.00010 814.4 -0.00024 766.5 O.O0614 38.58 -0.00049 458.9 0.00211..35.58 0.00011 30.84 0.00013 53.73 0.00626 34.0 & . ' 0.00047 159.4 51910.66796 0.294 0.00015 320.2 41 INTEGRATIONS #2 0.00029/ 0.0'5 1 07 0.00059 0.00423 0.00016 -0.00017 0.00214 -0.00020 -0.00037 0.00064 -0.00019 0.05628 0.11625 0.04840 0.00032 0.00290 0.17720 -0.00054 0.00164 0.00841 0.00154 0.00172 0.00014 0.00013 0.00852 -0.00012 51735.00000 0.00065 0.00038 0.03800 -0.00033 0.00420 0.00011 -0.00016 -0.00978 0.00023 0.00033 0.00122 0.00009 0.03088 0.12453 0.03906 0.00031 0.001 55. 0.27820 0.00102 -0.00021 0.00633 -0.00292 0.00164 0.00013 0.00021 0.00428 0.00133 52015.00000 -0.00030 #3 REREAD REDIG 0.00003 0.04041 0.00068 0.00420 0.00013 ________________ -0.00029 -0.00944 0.00012 _ 0.00015 0.00036 -0.00033 _______ 0.04076 ________________ 0.11247 0.03040 0.00026 0.00113 0 . 13848- __ -0.00017 _ -0.00217 0.00368 0.0 001 0- _______________ . 0.00298 0.00007 ____________ ___ 0.00006 0.00597 , 0.00023 51982.00000 0.0001 0 ___ 88 DUPO 50307 331 LANCASTER LABORATORIES f^uii Name: 9626807T62 luDe: 12 PBW P&U) 100-100.DFI .962685720002.8. , 09/24/96 23:00 3 NSTKUlviENT 3 0: 05936 H EM i/Aa j^Al AS B / fta Be Ca ___Cd /Co k'.Cr _Cu S'J e /_ng wi-Mn Ho TH _Pb ,tsb ___Se Sn Sr Ti n Y ^-n AV6 (ppm) %RSD 0.00027 0.02260 -0.00104 0.00833 0.00006 -0.00069 -0.03899 -0.00002 0.00010 0.00077 -0.00037 0.03390 0.10751 0.01564 0.00086 -0.00002 0.22736 0.00049 -0.00048 0.00198 -0.00030 0.00301 0.00005 0.. 00007 -0.00009 0.00043 50955.33203 0.00874 125.5 36.44 101.3 10.36 76.74 73.97 2.652 678.3 364.7 32.21 61.73 30.55 7.349 12.51 8.437 2552. 14 . 8 5 107.0 222.6 33.98 1 092. 8 2.76 10.20 121.9 2265 . 61.30 3.065 8.406 #1 -0.00011 0.01874 -0.00223 0.00883 0.00002 -0.00028 -0.03798 0.00003 -0.00024 0.00088 -0.00049 0.02198 Q.09869 0.01669 0.00084 0.00047 0.23988 0.00054 0.00002 0.00175 -0.00290 0.00346 0.00005 0.00000 -0.00051 0.00066 51996.00000 0.00790 INTEGRATIONS #2 #3 ' 1REREAD. RED 1G 0.00041 . 0.01701 -0.00018 0.00733 0.00011 -0.00051 -0.04004 -0.00024 0.00003 0.00095 -0.00010 0.04075 0.10988 0.01584 0.00079 -0.00077 0.18912 -0:00005 0.00024 0.00274 -0.00138 0.00032 0.00005 0.00016 -0.00198 0.00014 51711.00000 0.00905 . 0.00051 0.03206 -0.00071 0.00882 0.00005 -0.00126 -0.03896 0.00011 0.00054 0.00048 -0.00051 0.03896 0.11395 0.01338 0.00093 0.00021 0.25308 0.00099 -0.00173 0.00145 0.00338 0.00524 0.00004 0.00005 0.00221 0.00050 49159.00000 0.00927 c. 89 DUP050307332 P.3ae : LANCASTER LABORATORIES Run Name: 8626807T62 Tube: 13 LCSW L.CJS.L0 X XXX. -J _ 'j DPI,962685720002,8, 09/24/96 23:04 INSTRUMENT ID: 0 5 93~. EL EM >^Aq AT As __ B r 8a >Be Ca Cd i/Co Cr _/Cu j^Fe K Ma Mn Mb Na. */"Ni _Pb 5b ___Se __ Sn ___Sr Ti n _v __ r \/ Zn AV6 (ppm) SKRSD . *n INTEGRATIONS #2 #3 REREAD RED 16 0.0S169 0.557 2.16348 0.161 .2.07037 Q.293 2.10931 0.244 2.05673 0.124 0.05182 0.023 4.19189 0.145 0.05170 0.135 0.51123 0.123 0.21049 0.021 0.25782 0.085 1.08889 0.709 3.96498 0. 135 2.06302 0.362 0.51804 0.123 2.10835 0.656 4.02515 4. 161 0.52113 0.248 0.51889 0.042 0.53543 0.781 2.07232 0.488 4.20968 0.033 1.02592 0.103 1.03188 0.164 2.06717 1.259 0.527 17 0.193 51534.00000 0.142 0.52515 0.268 0.05154 2.16255 2.06961 . 2.10344 2.05385 0.05181 4.18787 0.0.5173 0.51062 0.21045 0.25789 1.08744 3.96334 - 2.05544 0.51741 . . 2.09314 4.11783 . 0.52080 0.51868 0.54013 2.06082 4.20804 1.02470 1.02993 2.03728 0.52638 51521.00000 0.52442 0.05203 , 2. 167352.06471 2.11132 2.05870 0.05183 4 . T8889 0.05174 0.51120 0.21048 0.25800 1.09724 3.96063 2.07040 0.51802 2.11173 3.83179 0.52003 ' 0.51887 0.53407 2.07989 4.21033 1.02656 1.03265 2.08501 0.52681 51468.00000 0.52426 0.05152 2 . 160-53 2.07679 2.11316 2.05765 . 0.05182 4.19889 0.05161 0.51188 0.2105a 0.25757 1.08198 3.97097 2.06320 0.51869 2.12018 4.12583 0.52256 0.5191 1 0.53209 2.07626 4.21066 1.02651 1.03306 2.07921 0.52832 51613.00000 0.52678 e 90 DUP050307333 LANCASTER LABORATORIES Run Name: 962680/T6* Tube: 14 2583226 Dxxx_ t 00-1 00.DF 1.96268 720002,8. , 09/24/96 23:09 ] N 5 T R U KF N T I D ; l; m ^Aa *A1 As __ B j SL3 X Be Ca __ Cd X Co XJ> X_Cu X Fe X_K _X_Mg X Mn __ Mo Na XNi Pb _X_Sb __ Se ___Sn Sr Ti __ TI X-Vy _X_4n Ave (ppm) %RSD 0.00025 67.51 0.01058 24.39 0.00149 107.8 0.44955 0.467 0.15338 0.245 -0.00054 25.99 ' 58.93593 0.657 -0.00020 55.57 0.00290 11.28 0.00030 156.4 -0.000211 -1 63.5 0.02845 20.96 2.96150 0.086 28.77709 0.408 0.79115 0.465 0.01488 14.37 52.88848 0.126 0.00506 23.14 0.00034 368.6 0.00141 210.3 -0.00001 5192. O'.00252 49.24 0.54757 0.284 0.00027 27.65 0.00270 75.86 0.00087 30.11 5 T3 5S.00 00 0 0.43 1 0.0 1 'l 7 9 6.43 '! 4t 1 0.00014 0.01222 -0.00036 0.44871 0.15331 -0.00038 68.41291 . -0.00031 0.00263 -0.00012 0.00018 0.02271 2.96381 28.66698 0.73692 0.01712 52.91938 0.00437 0.00156 -0.00175 0.00053 0.00144 0.54632 0.00035 0.00498 0.00096 51244.00000 0.01122 INTEGRATIONS #2 if 3 REREAD 0.00045 0.01190 0.00243 0.45195 0.15379 -0.00066 69.191 18 -0.00009 " 0.00281 0.00081 -0.00037 0.02801. 2.961 9.5 28.90110 0.79372 0.01465 52.93439 0.00642 0.00043 0.00415 0.00016 0.00224 0.54931 0.00019 0.00210 0.00108 51232.00000 0.01150 . 0.00017 0.00760 0.00240 0.44801 0.15305 -0.00058 69.20369 -0.0001 9 0.00327 0.00022 -0.00046 0.03462 2.95873 28.76318 0.79280 0.01286 52.81 166 0.00439 -0.00095 0.00184 -0.00073 0.003 8 8 0.54709 0.00027 0.00101 0.00057 51 622.00000 0.0126 5 C DUPO 50 307334 LANCASTER LABORATORIES Run Name: 96268Q7T6.2 Tube: 15 2583226 ft UP5** 100-100,DF1,962685720002 ,8,, 09/24/96 23 : 13 INSTRUMENT I[) 0593 EL EM __ Ag __ A'l As __ B __ Ba __ Be Ca '__ Cd Co __ Cr __ Cu __ Fe __ K __ Mg __ Mn __ Mo __ Na __ NT __ Pb __ 3b ___Se __ Sn Sr __ Ti __ Tl __ V __ Y __ 2n AVG , (.ppm) %RSD #1 0.02136 0.43859 0.02103 0.64872 0.55734 0.00996 68.88213 0.00995 0. 10520 0.02085 0.05100 0.25304 5.03544 29.33096 0.80828 0,21052 53.71411. 0.08628 0.01163 0.11423 0.00941 0.56380 0.55691 0 . 10385 0.02234 0.10363 51035.66796 0.05705 1.779 0.632 5.581 0.271 0.317 1.217 0.281 2.229 0.323 3.000 1.103 5.65.5 0.490 0.236 0.270 0.561 0,570 0.843 10.53 1.772 15.39 0.538 0.259 0.248 16.14 0.647 0.114 1.229 0.02100 0.43926 0.02072 0.64748 0.55530 0.00987 68.73272 0.00971 0.10554 0.02068 8.05054 0.24680 ' 5.00823 29.25507 0.80669 0.20919 53.43099 0.08579 0.01 170' .0.11481 0.01108 0.56180 0.55528 0.10356 0.02225 0.10298 50996.00000 0.05672 INTEGRATIONS #2 43 REREAD RED]( 0.02176 0.44096 0.02233 0.65073 0.55825. 0.01009 . 68.75846 0.00997 0.10486 0.02033 0.05163 0.26942 5.04162 . 29.39129 0.80738 0.21144 53.67198 0.08712 0.01282 0.11198 0.00862 0.56231 0.55746 . 0 . 10395 0 . 02599 0.10360 51008.00000 0.05657 0.02132 0.43553 0.02005 0.64795 0.55847 0.00990 69.10520 0.01016 0 . 10520 0.02155 0.05083 0.24292 5.05648 2-9.34653 ' 0.81077 0.21094 54.03935 0.08593 0.01037 0.11591 0.00852 0.56729 0.55801 0.10405 0.01878 0.10432 51103.00000 0.05785 92 DUP050307335 t'ias: LANCASTER LABORATORIES Run Name: 9626807T62 lube:' 16 2583226 > [I***, 1 0 0-1 00 fDF1 ,962685720002,8, 09/24/9-6 23:17 INSTRUMENT ID: 05936 EL Eh . Aa AT As & i/8a /Be Ca __ Cd Co /Cr / Cu / Fe K Ma^ hn __ Mo __ Na / Ni Pb _k_Sb Se __ Sn Sr TT T1 V __ V 2n ' . $v (ppm) ' %RSD 0.00000 2105 . 0.00826 34.34 0.00028 915.6 0.43597 0.378 0.14949 0.303 -0.00039 16.24 67.72151 0.330 -0.00004 251.2 0.00190 36.30 0.00047 17.52 -0.00046 44.37 0.02206 39.74 2.92047 0.114 28.18379 0.129 0.77067 O'. 178 0.01102 9.303 51.70436 0.076 0.00581 12.43 0.00012 677.4 0.00041 455.9 -0-00073 143.1 0.00242 34.47 0.53595 0.191 -0.00007 116.6 0.00535 46.66 0.00086 40.98 51309.33203 0.132 0.00917 0.768 INTEGRATIONS *M #2 #3 1REREAD REDIG -0.00016' .0.00708 -0.00253 0.43539 0.14902 -0.00032 67.69328 0.00005 - 0.00204 0.00043 T0.00063 0.02311 2.92406 28.14248 0.76995 0.01218 51 .70823 0.00663 0.00111 0.00183 -0.00041 0.00334 0.53507 -0.00016 0.00812 0.00128 51368.00000 0.00926 0.00001 . ' 0.01151 0.00088 0.43469 0 . 14992 -0.00042 67.51300 -0.00001 0.00115 0.00040 -0.00052 0.01281 2.91740 28.19722 0.76980 0.01024 ' 51 .74161 0.00525 r0.00031 0.00111 0.00011 0.00171 0.53708 -0.00010 0.00468 0.00067 5 1 235.00000 0 . 00914 0.00017 0.00621 0.00249 0.43784 0 . 14953 -0.00043 - 67.95824 -0.00016 0.00251 0.00056 -0.00023 0.03025 2.91997 28.21165 0.77226 0.01064 - 51.66323 0.00556 -0.00041 -0.00171 -0.00190 0.00222 0.53571 0.00002 0.003 2 S 0.00065 51325.00000 0.00912 c 93 DUP050307336 Page: 1 6 LANCASTER LABORATORIES Run Name: 9626807T62 Tube: 17 2583226 100-100,DF1.962685720002 , 8, , 09/24/96 23:22 INSTRUMENT ID: 0593c EL Eh *^Aa _^A1 As ___B Ba Be Ca Cd ^ Co y_Cr Cu jSjr e j^K Mg ^Mn Ho __ Na u- N i Pb _jr_Sb ___Se __ Sn __ Sr Ti T1 j LS ;__ Y ^/2n AVG (ppm) %RSD #1 0.05221 2.016 . 2.14582 2.769 0.04223 0.766 2.50975 2.132 2.16523 2.475 0.05122 1.341- 72.72531 1.908 0.05054 2.146' 0.51132 2.095 0.20705 1.748 0.25938 2.423 1.07213 1.222 7.25458 2.395 30.60723 2.300 1.29996 2.093 2.07931 1.871 56.47587 1.956 0.51576 1.854 . 0.02084 8.824 0.52362 2.285 0.00934 3.956 4.29438 1.949 1.59645 2.429 1.05570 2.210 0.05552 2.023 0.51819 2.033 51025.00000 1.727 0.51020 1.857 0.05342 2.2.0191 0.04205 2.55413 2.21357 0.05179 74.17394 0.05160 0.52161 0.21104 0.26472 1.08300 7 -. 3-8560 31.27621 1.32679 2.11416 57.38246 0.52622 0.01912 0.53609 . 0.00911 4.38060 1.63226 1.07785 0.05434 0.52848 50080.00000 0.52063 INTEGRATIONS #2 #3 1REREAD REOIG 0.05161 2.08355 0.04260 2.45031 2.10758 0.05046 71.40739 0.04943 0.50023 0.20398 0.25245 1 .07582 7.05747 29.87265 1.27238 2.03733 55.24474 0.50745 0.02278 0.51223 0.00977 4.21339 1.55526 1.03133 0.05566 0.50742 51825.00000 0.50212 0.05159 2.15199 0.04203 2.52480 2.17453 0.05141 72.59459 r. '0.05058 . .t=. 0.51212 0.20612 0.26098 1.05758 7.32066 30.67282 1.30071 2.08646 56.80042 Crr 0.51362 0.02062 0.52253 0.00915 4.28914 1.60182 1 . 057 90 0.05658 0.51868 5 1 170.00000 0.50785 94 DUP050307337 19 LANCASTER LABORATORIES I-,rn Name: 9626807T6? 18 2583226 [__ (jL 100-100,DF5.962685720002,8. . 09/24/96 '23:26 INSTRUMENT ID: 05938 $v (ppm) %RSD ft '1 INTEGRATIONS #2 #3 REREAD RED I. G Aa 0.00003 1 T06 . 0.00013 0.00030 -0.00035 __Al ' As 0.0001 1 2 218. 0.00001 9696. 0.00031 0.00064 0.00258 0.0014Z -0.00255 -0.00201 __ B 0.09372 2.371 0.09575 0.09407 0.09135 6a 0.03065 0.431 0.03070 0.03074 0.03050 __ Be -0.00037 37.50 -0.00047 -0.00044 -0.00021 Ca 13.58854 0.242 . 13.57057 13.62660 13.56846 __ Gd 0.00010 80.98 ' 0.00020 0.00006 0.00004 ___Co - -0.00042 49.57 -0.00063 -0.00020 -0.00043 __ Cr 0.00030 46.94 0.00044 0.00016 0.00029 Cu -0.00010 91.31 -0.00019 0.00000 -0.00012 __ F<? 0.02933 28.50 0.03762 0.02948 0.02090 __ K 0.62956 0.335 0.62973 0.63158 0.62737 Mg 5.50081 0.312 5.49800 5.51923 .5.48520 __ Mn 0.15795 0.233 0.15776 0.15837 0.15771 ___Mo 0.00492 53.80 0.00775 0.00453 0.00249 Na 10.48541 1.174 10.61211 10.47810 10.36604 __ Ni 0.00193 38 1 99 0.00211 0.00257 -0.00110 __ Pb 0.00000 45112 0.00022 -0.001 14 0.00092 __ Sb 0.00344 35.43 0.00371 0.00450 0.00210 ___Se 0.00016 391 ; 1 -0.00035 . 0.00086 -0.00002 __ Sn 0.00251 46.71 0.00199 0.00168 0.003 8 5 A Sr Ti __ n 0.10863 0.315 -0.00026 72.89 -0.00137 33.57 0.10881 -0.00010 -0.00132 0 . 10885 -0.00020 -0.00186 0.10824 -0.00048 -0.00094 __ V 0.00060 43.42 0.00075 0.00075 0.0 0030 __ Y 51282.66796 0.547 51030.00000 51233.00000 51585.00000 __ In 0.00511 4.839 ' 0.00500 D.00539 0.00494 95 DUP05 0307338 LANCASTER LABORATORIES Run Name: 9626807T62 Tuba- T9 2583222 EJS5SF ***F -100-100,DF1,962685720002,8, . 09/24/96 ' . 23:31 INSTRUMENT ID: 05936 ELEM X Aa V A1 As & X Ba X Be Ca __ Cd -AX-*--Co Cr X Cu X Ffr XK X Mq X Mn __ Mo XNa V Ni Pb X_5b Se __ Sn Sr Ti TT Xv __ Y X-Zn AV6 (ppm) %RSD .0.00029 44.14 0.00430 30.04 -0.00076 279.9 0.05345 1 . 135 0.02826 0.219 -0.00055 11 .34 294.71853 0.501 -0.00001 1113. 0.00097 44.63 0.00032 106. 1 -0.00032 83.98 -0.10746 11.02 3.65219 0.490,, 99.64209 0.428 0.34697 0.420 0.00218 38.50 46.07854 0.404 , 0.00940 9.478 -0.00125 115.2 0.00032 5 2.-65 0.02456 16.43 0.00072 120.6 0.58730 0.246 -0.00046 4.911 -0.00004 2426. 0.00062 63.83 50389.66796 0 . T9 5 0.00887 2.961 #1 0.00021 0.00281 -0.00132 0.05414 0.02832 -0.00048 296.42440 -0.00006 0.00085 0.00000 -0.00063 -0.11586 3.63694 100.13279 0.34864 0.00316 45.87762 0.00969 -0.00236 0.00049 ' 0.02000 0.00041 0.53894 -0.00045 0.00104 0.00017 50483.00000 0.00871 INTEGRATIONS #2 0.00023 0.00512 -0.00255 0.05317 0.02820 -0.00057 293.89859 0.000.14 0.00061 0.00030 -0.00017' -0.11262 3.67191 99.35937 0.34598 0.00164 .46.24588 0.00840 0.00037 0.00014 0.02598 0.00004 0.58619 -0.00 049 -0.00101 0.00092 50399.00000 0.00873 #3 REREAD RED 10 0.00045 0.00497 0.00159 0.05303 0.02828 -0.00059 293.83261 -0.0001 1 0-00145 0.00068 -0.00015 -0.09391 3.64771 99.43412 0.34627 0.00175 46.11213 0.0.TO IT -0.00176 0.00033 0.02769 0.00170 0.53678 -0.00045 -0.00015 0.00078 50287.00000 0.00918 B 96 DUP050307339 ) ' ,*i U 6 ' 21 LANCASTER LABORATORIES |.,,n Name: 9S26807T62 |,,be: 20 2583223 R.S4 CbF 100-1 00,DF1 . 962685720002.8, T 09/24/96 23:35 INSTRUMENT ID: 05936 1 l. E M ^ Aa `^A'l As B ^ Ba iBe Ca Cd X!co X-Cr >j_Cu . XLK V_Ma .XJv'n Mo Na . JS-Nf Pb XSD |n Sr T1 T1 Xv __ V .i-ln AVG (ppm) %RSD 0.00023 0.04021 ' -0.00076 0.36655 0.05073 -0.00055 211.28497 0.00001 0.00486 0.00079 0.00026 0.11725 4.25541 84.14281 0.73258 0.00604 62.90862 0.00536 0.00035 0.00040 -0.00216 0.00184 1.49062 0.00068 0.00657 0.00067 50775.66796 0.01003 122.3 9.286 286.6 0.437 0.. 648 10.79 0.342 770. 1 5.056 41.00 44.3 0 11.80 1 . 508 0.494 0:399 16.35 0.981 10.45 311.6 299.5 84.42 77.87 0.719 1 1 .86 17.71 37.01 0.203 9.990 #1 0.00054 0.03605 -0.00065 . 0.36491 0.05035 -0.00055 21 0-. 64900 0*00008 0.00486 0.00116 0.00040 0-.' 130 19 4.18877 83.66310 0.72935 0.00691 62.25154 0.00597 -0.00071 0.0 0.1 8 1 -0.00419 0.00337 1.47825 0.00077 0.00639 0.00095 50845.00000 0.01119 INTEGRATIONS #2- #3 REREAD REDIG -0.00001 0.04130 0.00136 0.36811 0.05091 -0.00061 211.13452 0.00006 . 0.00511' 0.00053 0.00018 0.10266 4.26058 84.40352 0.73331 0:00625 62.99785. 0:00488 0.00149. -0.00022 -0.00161 0.00052 1.49623 0.00061 0.00782 0.00048 50657.00000 0.00954 0.00016 0.04327 -0.00300 0.36663 0.05093 -0.00049 212.07141 -0.0001 1 0.00462 ' 0.00069 0.00021 0.11890 4.31688 84.36180 0.73507 0.00496 63.47646 0.00521 0.00028 -0.00036 -0.00067 0.00162 1.49737 0.000.66 0.00551 0.00058 50825.00000 0.00937 C E fa 97 DUP050307340 LANCASTER LABORATORIES Run'Name: 9626807T62 Tube: 21 2583224 Hb'CbPP' ****. -| 00-100.0F1 . 9S2&85720002. 8 r f 09/24/96 23:39 INSTRUMENT ID: 05936 ELEh A Aa *Ai As B A-8a A8e Ca Cd < Co X Cr X Cu X Fe XK X Ma X Mn Mo Na x-Ni Pb 2S_Sb Se __ Sn Sr Ti T1 xy __ Y A 2n AVG (ppm) %RSD 0.00026 26.42 0.00288 18.49 0.00038 631.6 0.31673 0.236 0.04947 0.488 -0.00067 5.503 214.06993 0.273 -0.00015 117.9 0.00447 5.917 0.00017 490.8 -0.00037 60.42 0.03359 24.79 4.06072 0.580 84.83772 0.280 0.71531 0.305 0.00649 17.09 62.33151 0.409 0.00521 17.93 0.00044 518.2 0.00000 1 0575 -0.00081 381.3 0.00158 111.6 1.50005 0.372 -0.00030 14.08 0.00165 256.8 0.00024 17 1.3 49882.33203 0.381 0.01422 1.389 INTEGRATIONS #1 42 0.00025 0.00265 0.00309 0.31647 0.04920 -0.00063 213.40110 -0.00021 0.00473 -0.00077 -0.00012 0.04034 4.03462 84.56331 0.71282 0.00710 62.03695 0.00629 -0.00181 -0.00293 0.00072 0.00014 . 1.49362 -0.00025 -0.00241 -0.00019 50092.00000 0.01420 0.00033 0.00250 -0.00166 0.31757 0.04966 -0.00068 214.48423 0.00005 0.00421 0.00095 -0.00042 0.02428 4.08048 84.98316 0.71690 0.00521 62.48110 0.00471 0.00036 0.00127 -0.00440 0.00356 1.50379 -0.00033 0.00604 0.00028 49834.00000 0.01442 43 ' REREAD REDIG 0.0001 9 0.00349 -0.00026 0.31614 0.04955 -0.00070 214.32444 -0.00029 0.00446 0.00034 -0.00057 0.03614 4.06706 84.96667 0.71622 0.00717 62.47647 0.00463 0.00278 0.00164 ' 0.00123 0.00105 1.50274 .-0.00031 0.00132 0.00062 49721 .00000 0.01403 CL & .. **' 98 DUP050307341 a LANCASTER LABORATORIES Run Name: 9526807T62 lube: 22 CCV . 09/24/96 23:44 INSTRUMENT ]0: 05936 EL EM Aa __A1 As __ B __ Ba Be Ca Cd __ Co Cr Cu Fe __ K __ Mg __ Mn . __Mo Na m __ Pb . __ Sb Se Sn Sr Ti T1 V __ Y __ 2n AV6 (ppm) %RSD 0.50649 1.549 25.70291 1 .403 0.51087 2.314 0.51520 1.526 0.49446 1'. 580 0.5.1989 1 .549 26.64335 1.443 0.50685 1.718 0.50667 1 . 568 0.51660 1.511 0.50591 1 . 626 26. 1587 8 1 . 544 26.18662 1.16 5 25.88775 1 .703 0.51056 1 . 563 0.51679 1 .303 25.98676 1.150 0.50941 1.544 0.50449 1.421 0.48168 1.970 0.50127 . i: 81 o 0.51492 1 .852 0.49813 1 . 598 0.51657 1.494 0.50397 1.615 0.51759 1.484 50518.00000 1 . 292 0.51454 1 .384 #1 0.50360 25.63928 0.50241 0.51353 0.49223 0,51615 26.46556 0.50287 O'. 5036 9 0.51306 0.50358 25.98394 26 . 1 8972 25.71452 0.50695 0.51110 25.90622 0.50733 0.49996 0.47251 0.49599 0.50989 0.49566 0.51337 0.49666 0.51473 50537.00000 0.51062 INTEGRATIONS 112 0.51538 26.091 14 0.5 243 9 0.52377 0.50314 0.52914 27.08460 0.51684 0.51567 0.52556 0.51505 26.62075 26.49015 26.38906 0.51971 0.52423 26.31772 0.51811 0.51276 0.49146 0.5.1 17 6 0.52592 0.50704 0.52538 0.5T275 0.52629 49856.00000 0.52276 #3 R.EREAO REDIG 0.50051 25.37832 . 0.50582 0.50831 0.48799 _ 0.51439 26.37989 0.50085 ________________ 0.50065 0.51119 0.49910 25.87163 25.87999 . _______ 25.55968 0.50501 0.51 505 25.73635 0.50279 0.50076 ____ _ _______ 0.48106 0.49608 0.50895 0.49170 0.51096 ____ ; 0.50250 . 0..51174 51 161.00000 _____ ; 0.5 1024 _` 99 DUP050307342 LANCASTER LABORATORIES Run Name: Tube: 23 9626807T62 CCB 09/24/96 23:48 INSTRUMENT ID: 0 593 6 EL EM Ao A1 As B Ba Ca Cd Co Cr Cu F K Ma Mn Mo Na Ni Pb Sb Se Sn " "Sr Ti T'l. V V Zn $v (ppm) %RSD #1 -0.00004 583.4 -0.00012 1683. -0.00200 42,80 0.00358 4.289 0.00009 11.85 -0.00029 41.17 -0.02570 19.49 -0.00002 255.0 -0.00005 341 .7 0.00017 95.39 -0.00020 176.9 0.02079 18.76 0.10873 6.124 . 0.00832 22.64 0.00024 4.805 0.00111 69.12 0.1813-4 18.63 0.00058 147.9 -0.00035 359.1 0.00511 55.97 -0.00112 109.5 -0.00020 767.8 0.00023 24.49 0.00009 50.88 0.00000 55161 -0.00015 177.7 51160.66796 0.084 0.00058 13.73 -0.00028 0.00111 -0.00107 0.00349. 0.00009 -0.00015 -0.01993 . 0.00005 -0.00021 0.00029 -0.00057 0.01632 - 0.10121 0.01036 0.00025 0.00185 0.20585 0.00132 -0.00179 0.00738 -0.00016 0.00072 0.00029 0.00005 0.00134 -0.00040 .51162.00000 0.00053 INTEGRATIONS #2 #3 REREAD REOIG . 0.00021 0.00097 .-0.00219 0.00376 0.00009 -0.00037 -0.02826 -0.00006 0.00014 -0.00001 0.00016 0.02348 0.11112 0.00664 0.00023 0.00115 0/14280 -0.00036 0.00005 0.00604 -0.00069 -0.00206 0.00020 0.00014 0.00248 -0.00019 51117.00000 0.00053 -0.00006 -0.00245 -0.00275 0.00349 0.00007 -0.00034 -0.02892 -0.00006 -0.00009 0.00023 -0.00022 0.02259 0.11387 0.00796 0.000230.00031 0.19538 0.00079 0.00067 0.00189 -0.00250 0.00070 0.00018 0.00009 -0.00380 0.00013 51203.00000 0.00067 100 DUP050307343 LANCASTER.LABORATORIES lain Name: 9626807T62 lube: 24 2583225 ,100-100.DF'1:962685720002.8, , 09/24/96 23:53 INSTRUMENT 3D: 05936 CL. EM X Aa *>i As B X6a X Be ___Ca ___Cd S Co ' XCr X Cu X Fe JLK 2LM9 jL^n- Mo X_Ni Pb Se __ Sn 'Sr Ti T1 SX __ Y 2L2n AVG (ppm) %RSD 0.00007 0.00147 0.00173 0-. 067 53 . 0.10980 -0.00048 128.95361 . 0.00009 0.00446 0.00067 0.00017 -0.03702 2.11816 50.68542 0.67471 0.00238 36.32926 - 0.01330 .-0.00061 0.00125 0.00262! 0.00096 0.34095 -0.00017 0.00047 0.00112 50568.00000 0.01119 220.8 167.1 94.51 0.228 0.577 32.14 0.724 90.78 4.968 51 .62 112.0 28.34 0.438 0.609 0.644 28.73 0.604 1 . 066 .14.69 218.2 16.94 2 57.1 O'. 520 40.37 340.6 21.51 G . 550 5.000 . #1 -0.00009 -0.00135 -0.00002 0.06769 0.10918 -0.00031 128.15255 0.Q0018 0.00468 0.00044 0.00024 -0.04914 2.10833 50.43771 0.67094 0.00236 36.09600 0.01316 -0.00053 0.00041 0.00210 -0.00105 0.33936 -0.00025 0.00235 0.00091 50845.00000 0.01 06.1 INTEGRATIONS #2 #3 REREAD REDIG 0.00020 0.00307 0.00201 0.06738 0.11044 -0.00061 129.97949 0.00000 0.00424 0.00108 0.00031 -0.03069 2.12681 51.03158 0.67947 0.00308 36.53194 0.01329 -0.00071 0.00432 0.00288 0.00371 0.34286 -0.00015 -0.00033 0.00139 50288.00000 0.01173 0.00010 0.00269 0.00321 0.06753 0.10979 -0.00051 _____________ 128.72879 '(1...... ............. 0.00010 _____________ 0.00446 _______ 0.00050 _______ ________ -0.00004 -0.03124 __ 2.1 1 934 _ 50.58698 ______ 0.67373 _____________ 0.00171 36.35983- 0.01345 _______ '_____ __ -0.00059 -0.00096 ______ : 0.00287 _______ ______ 0.00022 ^ 0.34064 -0.00011 -0.00058 0.00106 _ 50571 . 00000 _ 0.01124 _______ ______ 101 DUP050307344 LANCASTER LABORATORIES ft >j n N * me: 9626807T62 rutatf! 25 2583227 r 1 00-100 . OF 1 . 962685720002.8 , , 09/24/96 23 -.57 INSTRUMENT ID: 0 93? EL EM ? __ As EJ Xs * ___Ca Cd 2co JLS>~ X-Cu XMn __ Mo Na Un i __ Pb XSb __ Sis __ 5n __ Sr ___T 1 n Xv Y g> AVG' (ppm) SJRSD '0.00024 99.97 0. 1447 0 8.151 0.00308 61.97 0.06088 1.556 0.07303 0.293 -0.00053 14.74 228.60113 0.432 0.00013 81.25 0.00058 48.19 0.00063 62.78 0.00062 47.03 0.10191 30.53 2.94722 0.331 90.73548 0.286 0.19734 0.379 0.00587 17.27 56.79251 0.241 0.00988 7.450 0.00103 118.2 O'. 00915 17 . 24 0.03086 5.924 0.00199 43.49 0.69788 0.288 0.00405 9.044 0.00050 447.1 0.00327 4.926 50167.33203 0.528 0.01678 1 . 253 #1 -0.00001 0.15790 0.00088 0.06014 0.07316 -0.00055 228.61134 0.00020 0.00041 0.00066 0.00028 0.07465 2.93659 90.85043 0.19751 0.00484 56.75139 0.-00975 0100075 0.00841 0.03253 0.00101 0.69900 0.00447 -0.00188 0.00314 49902.00000 0.01654 INTEGRATIONS \ .#2 0.00028 0.14101` 0.00430 0.06056 0.07278 -0.00044 227.60835 0.00020 0.00090 0.00022 0.00078 0.09526 2.94921 90.43773 0.19651 0.00687 56.68053 0.01067 0.00237 0.01096 0.03114 0.00264 0.69556 0.00379 0.00259 0.00345 50432.00000 0.01693 #3 ' 1REREAD 0.00045 0.13519 0.00407 0.06195 0.07315 -0.00060 229.58369 0.00000 0.00042 0.00101 0.00080 0.13582 2.95585 90.91829 0.19798 0.00591 56.94561 0.00922 -0.00002 0.00807 0.02890 0.00232 0.69909 0.00388 0.00080 0.00322 50168.00000 0.01688 L ___ (-r 102 DUPO 50307345 i' tae : 27 LANCASTER LABORATORIES Run Name: 9626807T62 Tube: 26 2583830 oJOCiX'S .***.100-100fDF1,962685720002,8,, 09/25/96 ' INSTRUMENT 10: 00: 01 05936 F. LEM 2C.A9 X-A1 As Ei XBa V6e 'ca __ Cd JLfio X_Cr X-Cu X/ X_K 2L|V|9 y_Mn __ Mo Na N1 Pb X-Sb ___Se __ Sn Sr Ti T1 X.V __ Y XXn AVG (ppm) ,%RS0 -0 .00040 0 .00004 -0 .00261 ' 0 .31934 0 .11264 -0 .00034 74 .56600 -0 .00032 0 .00037 0 .00007 -0 .00047 0 .20694 5 .78812 31 .47292 0 .24479 0 .00911 .50 .93051 0 .00128 -0 .00071 -0 .00229 -0 .00180 0 .00242 0 .54488 -0 .00008 0 .00532 0 .00039 50799 .00000 0 .00924 97 . 17 2603 . 52 .41 0. 355 0. 666 25 .64 0. 1 66 52 .35 14 . 63 21 7 . 9 47 .78 9. 298 1 . 075 0. 407 0. 259 4. 949 0. 559 59 .62 22 9.7 83 .28 96 .96 27 . 05 0 . 653 104.4 50 .23 70 . 39 0. 950 3 . 148 INTEGRATIONS #1 #2 -0.00085 ' -0.00081 -0,00327 0.31816 0.11343 -0.00043 74.69541 -0.00049 0.00043 '0.00024 -0.00070 0.18578 5.85269 31.61358 0.24553 0.00860 51.23508 0.00065 -0.00179 -0.00435 -0.00363 0.00197 0.54835 -0.00016 0.00373 0.COO 23 50247.00000 0.00949 -0.00010 -0.00028 -0.00353 0.31944 0.11254 -0.00026 74.44797 -0.00031 0.00032 -0.00006 -0.00025 0.21163 5.78315 31.44233 0.24438 0.00946 50.88600 0-. 00106 0.001-16 -0.00195 -0.00015 0.00211 0.54385 -0.00007 0.00841 0.00023 51007.00000 0.00892 #3 REREAD RE0IG -0.00025 0.00122 -0.00104 0.32042 0.11194________________ -0.00031 74.55464 C _______ -0.0001 5 _____________ 0.00038 0.00003 -0.00045. 0.22340 5.72852 31.36285 0.24447 ; 0.00927 _____________ 50.67045 fx _______ 0.00214 -0.001 50 _ -0.00057 -0.00161____________ ___ 0.00317 _____________ 0.54195 Q. 00000 _________ _ 0.00383 0.00072 51 143.00000 :: 0.00932 _ 103 DUP050307346 LANCASTER LABORATORIES . Run Name: 9626807T62 Tube: 2T 2583831 <^tsXS *:**, 100-100.DF1,962685720002.8, t 09/25/96 ' 00:06 INSTRUMENT ID: 05936 EL EM AV'G (ppm) %RSD #1 INTEGRATIONS 42 43 ' REREAD REDIG X Aa 0. 00030 184.9 -0.00025 0.00030 0-00087 2LA1 As 0. 03609 1 1 .33 0. 00030 327.5 0.03826 -0.00059 0.03137 0.00013 0.03864 0.00-136 __ B ' 0. 13435 0 . 938 0.13351 0.13580 0 . 1337 4 X 8a 0. 07338 0. 801 0.07283 0.07331 0.07400 XLBe Ca ' -0. 00044 55 .58 194. 00143 0. 381 -0.00021 193.22283 -0.00040 194.69535 -0.00070 _____________ 194.08610 CL ____ Cd - 0. 0001 1 1 1 8.6 0.00001 . 0.00026 0.00005 _ X Co 0. 00065 34 .54 0.00049 0.00055 0.00091 X Cr 0. 0 0101 59 . 65 0.00066 0.00170 0.00066 _______ - X Cu -0. 00005 17 5.0 -0.00002 -0.00017 0.00002 _________________ X Fe -0. 02766 21 . 65 -0.03294 -0.02115 -0.02889 2Tk 6. 33551 0. 749 6.29110 6.32983 6.38561 Xjvjg 80. 1047 9 0. 531 79.64100 80.19626 80..477 1 1 X Mn 0 . 26583 0. 489 0.26433 0.26663 0.26653 ___Mo 0. 00229 16 .49 0.00185 0.00256 0.00244 Na 55. 68 647 0. 994 55.10489 . 55.74742 56.2071 2 'ifcr _______ __ A XNi Pb 0. 00313 1 1 .66 -0. 00035 104.9 0.00272 0.00000 0.00324 -0.00073 0.00343 -0.00032 X_Sb 0 . 00087 133.3 -0.00022 0.00075 0..0021 0 ___Se 0. 02384 6. 690 0.0256'6 0.02269 0.02316 __ Sn 0. 0.01 1 9 93 . 49' 0.00119 0.00007 0.00231 A Sr 0 . 5 84.45 0 . 739 0.67940 0.68443 0.68952 Ti 0. 00106 25 . 80 0.00075 0.00122 0.00123 T1 0 . 00243 48 .68 0-. 00372 0.00139 0.00219 _ 2Iv 0 . 00069 14 . 18 0.00073 0.00076 0.00058 __ Y 50438. 00000 0 . 709 50722.00000 50556.00000 50036.00000 X-2n 0 . 01005 10 . 13 0.00938 0.00955 0.01122 _____. 104 DUPO 503 07347 f'age: 2 LANCASTER LABORATORIES Run Name: 9626807T62 Tube: 28 2583832 t C}!C>X.S> *.***. 10 0-100. DF 1.96268 57 2 00 02.8, , 09/25/96 00: 10 INSTRUMENT ID 0 5 936 ELEM X Aa *A1 As B A Ba X Be Ca Cd X Co X Cr X Cu A Fe A.K ' X Mn Mo Na A_Ni __ Pb . -X-Sb Se Sn Sr Ti T1 Xv __ Y . XZn . AVG (ppm) %RSD #1 0.00003 496.7 0.00025' 0.01009 17.02 0.0.0 97 0 -0.00044 436.0 -0.00009 0.30898 0.230 0.30819 0.12397 0.291 0.12366 r0.00069 3.749 -0.00066 104.59131 0.867 103.86262 -0.00017 80.10 -0.00025- 0.00121 27.58 0.00085 0.00035 145.8 0.00075 -0.00058 29.45 -0.00071 0.32859 2.351 0.31986 3.12587 0.559 3.11998 31.75245 0.484 31.57907 0.76244 0-. 59 8 0.75821 0.00795 8.827 0100721 50.36048 0.485 50.46219' 0.00134 16.32 o:ooi15 -0.00015 345.8 0100007 0.Q0020 793.0 0.00191- -0.00250 63.26 -0.00096 -0.00064 188.2 -0.00020 0.55556 0.349 0.55354 -0.00017 20.16 . -0.00017 0.00009 2042. -0.00204 0.00003 764.5 0.00025 50441.00000 0.287 50397.00000 0.00951 6.077 0.01018 INTEGRATIONS #2 #3 REREAD REDIG . -0.00006 0.00860 -0.00253 0.30917 0.12437 ' -0.00071 104.30334 -0.00001 0.00152 -0.00022 -0.00066 0.33137 3.14554 31.80631 0.76185 0.00861 50.53747 0:00130 0.00072 -0.00130 -0.00240 0.00205 0.55742 -0.00021 0.00172 0.00003 S 0 3 2 3.00000 0.00921 -0.00007 0.01197 0.00129 0.30957 0.12389 -0.00070 105.60798 T" -0.00024 0.00127 0.00053 -0.00038 0.33454 3. 11208 31.87196 - 0.76728 0.00804 50.08179 TZ 0.00158 -0.00033 0.00000 -0.00413 0.00010 0.55572 -0.00014 0.00060 -0.00020 50603.00000 0.00915 105 DUP050307348 LANCASTER-LABORATORIES Run Name: 9626807T62 Tube: 29 2583833 /S-D3L5 **** _ 1 00-100.DF1 ,. 962685720002 , 8 , / ,09/25/96 00 :15 INSTRUMENT ID: 0 5-93 6 ELEM JLa9 _XA1 As __B ' jL8a XB Ca Cd X Co X Cr iS_Cu X Fe JLK 'K Ma j_Mn Mo !Tl\la Xn i ' Pb Xsb ___Se Sn Sr Ti T1 Xv __ V 4rZn AVG (ppm) %r $? -0.00018. 320.3 0.04471 8.067 -0.00113 253.0 0.05408 2.876 0.07486 0.753 -0.00084 28.28 169.83081 0.600 -0.00005 128.5 -0.00039 30.19 0.00113 18.25 +0.00075 29.89 -0.00325 924.7 1.67737 0.929 SO.10843 0.592 0.00692 2.051 0.00113 66.85 41.97229 0.682 0.00166 7.889 -0.00096 77.30 0.00057 377.4 0.15963 2.420 0.00182 74.06 0.43755 0.593 0.00097 27.45 0.00336 134.3 0.00077 33.31 49649.00000 0.888 0.01 199 2.693 #1 0.00035 0.04805 0.00179 0,05584 0.07551 -0.00107 170.85575 -0.00013 -0.00026 0.00136 -0.00067 0.02370 1.69473 60.51211 0.00708 0.0019.2 42.20974 0.00175 -0.00179 6.00249 0.16386 0.00328 0.44050 0.00116 0.00609 0.0010? 49199.00000 0.01187 INTEGRATIONS #2 -0.00081 0.04088 -0.00392 0.05289 0.07453 -0.00084 168.81724 -0.00002 -0.00049 0.00097 -0.00100 -0.03578 1.67284 59.83720 0.00683 0.00040 42.05309 0.00151 -0.00079 -0-.00179 0.15873 0.0 00 62 0.43655 0.00067 -0.00185 0.00062 49667-. 00000 0.01174- #3 ' REREAD RED IS -0.00009 0.04519 -0.00126 0.05351 0.07454 -0.00060 169.81942 0,. 00000 -0.00042 0.00106 -0.00057 0.00230 1.66455 59.97599 0.00684 0.00109 41.65402 ' 0.00173 -0.00032 0.00103 0.15629 0.00156 0.43559 0.00110 0.00585 0.00063 50081.00000 0.01235 ZH B. .. ....MHttv "... .ILlPHlhln ' I! AWV 106 DUP050307349 LANCASTER LABORATORIES Run Name: 9 6.2 6807T62 Tube: 30 2583834 S xxxx 100-100.DF1,962685720002.8,, 09/25.496 00:19 INSTRUMENT ID 0 5 93 6 ELEM' X Aa OfLAI As X Ba JL.Be Ca __ Cd X-Co X.Cr JLCu X^e XK AM 9 XMn Mo XNa XNi Pb XSb __ Se ' __ Sn _TSir ___TI _A VY Y' 2n AVS (ppm) 35RSD #1 0.00040 77.76 0.00924 12.11 -0.00160 1 18.4' 0.03213 2.611 0.00173 2.648 -0.00061 12.14 0.01010 167.9 -0.00006 591.9 0.00027 207.8 0.00035 463.4 0.00019 30.23 0.02633 17.14 0.11370 14.17 0.01619 28.60 0.00143 14.10 -0.00057 140.7 0.20996 78.79 0.00043 236.9 0.00098 106.7 0.00135 98.55 -0.00015 356.0 0.00023 789.9 6.00028 32.59 0.00024 28.58 0.00000 41512 0.00011 936.9 50660.00000 .612 0.01169 2.922 0.00011 0.00865 . -0.00158 0.03254 0.00168 -0.00053 0.02923 -0.00004 -0.00017 0.00118 0.00012 0.02158 0.12048 0.02110 0.00161 0.00034 0.28519 0.00038 0.00127 -0.00001 0.00043 0.00100 0.00037 0.00023 -0.00112 0.00074 50305.00000 0.01201 INTEGRATIONS #2 #3 ' REREAD RED I 6 0.00035 0.01053 -0.00352 0.03117 0.00173 ->0.00068 0*. 00424 -0.00045 0.00007 -0.00152 0.00024 0.02684 0.09530 0.01189 0.00121 -0.00091 0.02028 -O '. 00056 -0.00018 0.00142 -0.00025 -0.00187 '0.00018 0.00018 0.00128 -0.00111 50795.00000 0.01133 0.00073 0.00853 0.00023 0.03269 0.00177 -0.00061 -0.00316 0.00031 0.00091 0.00139 0.00022 0.03056 0.12532 0.01560 0.00148 -0.00114 0.32442 0.00148 0.00186 0.00264 -0.. 00064 0.00157 0.00028 0.00031 -0.00015 0.00070 50880.00000 0.01173 ^ . 107 DUP050307350 32 LANCASTER LABORATORIES pun Name: 1 ube: 31 9626807T62 CRI 09/25/96 00:23 INSTRUMENT 10: 05936 f LEM A " AT As B Ba Be Ca Cd Co "'~"Cr Cu fe K Ha Mn Mo Na Ni Pb ,, -Sb' ' Sn Sr Ti __ T'l V ___Y AVG (ppm) %RS0 #1 '0.02119 1.631 -0.00464 3 5.47 0.01827 8.472 0.01050 3.749 O.OOQ18 31.01 0.01062 1.622 -0.04465 2.650 0.01044 0.743 0.10618 0.730 0.02170 1.603 0."051 14 0.646 0.02754 1 5 ..79 0.10678 6.794 0.00138 231.5 0.03197 0.823 -0.00005 1584. 0.11842 63 .'96 0.08592 0.250 0.00649 11.70 0.11887 1.713 0.00754 17.93 -0.00080 82.82 0.00005 5.796 0.00006 116.2 0.02323 10.39 0. 10855 0.434 51743.66796 0.015 0.04375 2.307 0.02119 -0.00427 .. 0.01988 0.01084 0.00013 0.01080 -0.04366 0.01051 ' 0.107 07 0.02146 0.05148, 0.02705 0.10546 -0.00063 0.03226 -0.00100 0.03408 0.08576 0.00717 0. 1 192.1 0.00721 -0.00100 0.00004 -0.00001 0.02086 0.10909 51739.00000 0.04412 INTEGRATIONS #2 43 REREAD' RE.OIG 0.02154 -0.00645 - 0.01815 0.01007 0.00024 0.01045 -0.04.432 0.01036 0.10566 0.02155 0.05111 0.02345 0.10027 0.00507 0.03176. 0.00032 0.14051 0.08584 0.00664 0.12071 0.00639 -0.00006 0.00005 0.00008 0.02569 0.10823 51739.00000 0.04261 0.02085 -0.00321 0.01680 0.01058 0.00016 0.01061 -0.04596 0.01045 0.10580 0.02210 0.05082 0.0321 1 0.11460 -0.00029 0.03188 0.00051 0.18066 0.08617 0.00567 0.11668 0.00903 -0.00134 0.00005 0.00014 0.02313 0 : 10833 51753.00000 0.04452 108 DUP050307351 r' .-i n e : LANCASTER LABORATORIES loin Name: 11 ibe : 32 9626807T'62 ICSA 09/25/96 00:28 INSTRUMENT ID: '05936 HEM Aa As __ Ba Be __Ca Cd Co Cr __ Cu fe __K __ Mg __ Mn __ Mo __ Na Ni __ Pb Sb __ Se __Sn Sr Ti T1 V Y Zn AVG (ppm) %RSD -0.00011 1T3.3 53S.67504 0.199 -0.00006 3464. 0.04781 1.130 0.00842 0.837 -0.00001 1023. 552.59082 0.316 -0.01004 4.314 0.00127 7.682 0.00125 54.05 -0.00153 3.660 218.02842 0.281 0.10276 1 .075 556.43829 0.289 O'. 00S29 0.525 -0.00026 786.2 0.18459 40.73 0.00014 395.7 -0.00281 27,30 0.0V178 25.28 -0.00894 15.93 0.00815 24.24 0.02106 0.171 -0.00109 7.595 -0.00168 2 87 ..5 0.00041 99.77 47497.33203 0.257 0.00380 9.510 #1 -0.00026 536.15130 -0.00221 0.04777 0.00843 0.00006 553.48040 -0.01047 0.00116 0.00098 -0.00153 218.36997 0.10149 557.11791 0.00625 0.00215 0.12206 0.00037 -0.00315 0.00852 -0.00854 0.01032 0.02105 -0.00118 0.00387 0.00088 47450.00000 0.00349 INTEGRATIONS #2 -0.00004 535.96539 0.00234 0.04730 0.00835 0.00003 550.57751 -0.00961 0.00129 0.00202 -0.00147 217.31874 0. 10351 554.59906 0 .'00631 -0.00141 0.26801 -0.00050 -0.00193 0.01435 -0.01052 0.00769 0.02103 -0.00101 -0.00505 0.00025 47636.00000 0.00370 #3 REREAD REDIG -0.00003 537.90838 -0.00033 0.04837 0.00849 ____________ ___ -0.00012 553.71459 -0.01004 0.00135 ____________ ___ 0.00075 -0.00158 218.39656 0.10329 557.59796. 0.00630 ________________ -0.00154 ________________ 0.16370 0.00056 -0.00336 ________________ 0.01247 -0.00776 0.00644 0.02110 -0.001 08 _______ -0.00388 0.0.0010 47406.00000 0.00420 _____ _____ 109 DUP050307352 p fi 9 e ?>4 LANCASTER LABORATORIES Hun Name: 9626807T62 f u b e : 33 ICSAB 09/25/96 00:32 INSTRUMENT ID; 0 5 936 EL EM A? __ Al As B Ba __ Be __ Ga Cd __ Co __ Cr __.Cu Fe __ K __ .Mg Mn ___Mo __ Na NT __ Pb __ Sb __ Se Sn Sr __ Ti T'l V __ Y __ .Zn AVG . (ppm) %RSD #1 INTEGRATIONS #2 0.22310 0.062 0.22294 533.18226 0.135 533.89636 0.11005 3.489- . 0.10756 0.02955 4.556 0.03089 0.53523 0.246 0.53664 0.52056 0.356 0.51843 550.36755 0.431 547.63275 0.99980 0.463 0.99447 0.51668 0.363 0.51456 0.52901 0.501 0.52595 ' 0.55439 0.276 0.55606 216.33816 0.358 215.44909 0.10788 8.699 . 0.09757 551.69232 0.120 551.02014 0.52765 0.226 . 0.52628 - 0.00030 212.8 0.00016 0.19433 60.46 0.10011 1.00837 0.462 1.00345 0.04999 2.994 0.04878 0.64336 0.622 0.63874 0.0437*6 2.316 0.04436 0.0056.0 25.60 0.00720 0.02089 0.182 0.02090 -0.00098 9.470 -0.00109 0.10045 4.929 0.10028 0.53997 0.197 0.53897 47708.G0000 0-340 .47522.00000 1.01145 0.664 1 . 00374 0.22313 532.45196 0.11448 0.02957 0.53403 0.52146 551.57727 1.00217 0.51815 0.53041 0.55305 216.68827 0.11593 551.70568 0.52823 . 0.00100 0.32599 1.01273 0.04953 0.64585 0.04434 0.00443 0.0209 1 -0.00092 0.09560 0.54109 47822.00000 1.01457 #3 REREAD RED IG 0.22322 533.22845 0.10813 0.02820 0.53503 0.52180 551.89270 1.00277 0.51733 0.53067 0.55406 216.87713 0.11012 552.35119 0.52844 -0.00025 0.15690 1.00893 0.05167 0.64549 0.04259 0,00517 0.02084 -0.00094 0.10550 0-. 539 86 47780.00000 1 .01605 110 DUP050307353 LANCASTER LABORATORIES Run Name: 962S807T62 Tube: 34 CCV 09/25/96 00:37 in s t r u m; n t 3D: 05936 EL EM Aa AT AS B Ba Be Ca Cd __ Co. Cr Cu Fe __ K Ma __ Mr? . __ Mo Na __ Ni ___Pb j__ Sb __ Se Sn Sr Ti __ T) __ V . V1 __ 2n AVG (ppm) %RSD #1 INTEGRATIONS 42 0.51608 26.14243 0.52287 0.52563 0.50325 0.53524 27.51834 0.52399 0.52070 0.53137 0.51346 26.81942 26.40522 26.44093 0.52510 0.53191 26.32738 . 0.52600 0.51775 0.49765 0.. 5 1587 0.53069 0.50918 0.5 2'808 0.52017 0.53035 .50134.66796 0.53594 2.349 2.335 2. 173 2.455 2.236 2.747 ` 2. 939 2.887 2.523 2.730 2.018 2.687 1 .702 2.510 2.704 2.434 1 . 839 2.686 2.177 1-. 164 1 .059 3.270 2.431 2.500 2.603 2.479 1.916 3 .16 2 0.52997 0.50763 26.84052 25.70780 0.53587 0.51481 0.54044 0.51678 0.51612 0.49527 0.55220 0.52606 28.45128 27.01041 0.54146 0.51517 0.53569 0.51118 0.54799 . 0.52124 0.52529 0.50598 27.64829 26.34124 26.89765 26.01649 27.20409 25.99675 0.54146 0.51594' 0.54649 0.52176 26.86821 25.93251 0.54226 0.51673 0.53053 0-. 50921 0.50378 0.49226 0.52214 0.51215 0.55067 0.51936 0.52339 0.50072 0.54323 0.51904 0.53525 0.50904 0.54551 0.52203 49035.00000 50813.00000. 0.5555 1 0.52622 \ 43 R EREAO REDIG 0- 51063. 25.87898 0.51793 0.51968 0.49836 0.52746 27.09332 0.51534 0.51522 0.52487 0.5091 1 26.46873 26.30151 26 .12197 0.51791 0.52747 26 . 18322 0.51901 0.51350 0.49691 0.5133 1 0.52203 0.50343 0.52196 0.51623 0.52352 50556.00000 0.52608 111 MDUPO 50307354 LANCASTER LABORATORIES Run Name: 9626807762 Tube : 35 CCB 09/25/96 00:41 INSTRUMENT ID: 05936 ELEM Aa AT As B Ba Be Ca Cd Co ~Cr Cu Fe K Ma Mrs Mo Na Ni __ Pb __ Sb $e .... Sn Sr Ti __ TI __ V Y __ Zn AVG (ppm) %RSD 0.00008 363.9 0.04148 57.72 -0.00186 94.64 0.00386 16.71 0.000)4 5T.88 0.00023 22.67 0.00071 3801. 0.00010 166.7 -0.00015 244.9 0.00026 167.6 0.00004 118.2 0.04039 21.66 0.11368 0.858 0.04929 50.17 0.00026 53.09 0.00120 50.07 0.17171 14.36 -0.0001 1 382.8 0.00132 24.80 0:00537 15.52 -0.00058 555.4 0.00132 136.3 0.00011 65.56 0.00014 7 6.56 0.00504 14.12 0.00027 65.60 52028.00000 0.099 0.00074 10.67 #1 0.00034 0.06908 -0.00104 0.00446 0.00022 0.00029 .0.03185 0.00000 -0.00036 0.00073 0.00006 0.05066 0.11423 0.07781 0.00042 0.00188 0.15.662 0.00036 0.00095 0.00633 0.00208 -0.00071 0.00020 0.00026 0.00513 0.00030 52015.00000 0.00065 INTEGRATIONS #2 #3 REREAD 0.00012 0.02906 -0.00065 0.00317 O'. 00012 0.00019 -0.01370 0.G0031 -0.00036 0.00017 0.00009 0.03864 0.11426 0.03641 0.00022 0.00074 0.15832 -0.00026 0.00144 0.00496' 0.00036 0.00269 0.00007 0.00010 0.00428 0.00003 51984.00000 0.00078 -0.00023 0.02629 -0.00388 0.00394 0.00007 0.00021 -0.01601 0.00001 0.00027 -0.00012 -0.00001 0.03337 0.11255 0.03365 0.00015 0.00097 . 0.20017 -0.00043 0.001 570.00482 -0.00421 0.00197 0.00006 0.00005 0.00569 0.00044 52085.00000 0.00078 Data .Reviewed by: M'U<j2M3 4-25-3*' Data Verified by: 112 DUP050307355 ' * > a e : Lancaster Laboratories h ta Reviewed By: tocu^5 ^f-ZM<3 0a ta Ver ified 8 v: Analyst:' 243 Data file Name: 27QQ4T62.DAT Run Nam: 9627004T62 nstrument Parameters: Rinse Time: Individual Integration Time: Total Integration Time: 60 sec 10 sec 30 sec Clement fig fi I As P Symbol r. A1 L 'Lr o "- u 7 <y /. KO *4n MCr'J o *'i ' i:* Lb > "* \fx, Lr 1i ri V r 2n Element Name Si Tver A! unii num Arsenic Boron Barium Beryl 1 i um Calcium Cadmium Coba 11 Cnromium Copper I r on Potass i urn Klagnes i um Manganese mol ybaenurrSodium N ~i c k e i Lead L eac An timony Selenium Selenium .Tin S tron tiuin Titanium Thallium Vanadiurn Yttrium 2i nc Wave!enqthfnm 328.06 308.21 189.04 249.67 d93 . A0 3 13.04 317.93 226.50 228.61 2 57.. 7 I 3 24.75 27 1 .44 766.49 ??9.07 2 57.6 i 2 0 2.0 8 33 0.23 2' -i ! . t* 0 220.35/1 220.35/2 2'0 S . 83 / 1 196.0?/? 196.02/1 189.9 8 421.55 334.94 190.86 292.4tf 371.03 2 0 6.2 0 113 DUP050307356 \ $ The 6 l L TR$ CE :Cr uses a Crawf oro-Kunse 1 nan Noise Recs-jct i on Tfcnmqi-'f f or ieed arid sr "ieriiuiTi. Tnis r-quvs tne uti1i~stion of tne first ana second order .wave!engths in the calculation of eecn of these mere is ) determlnstions . The 6 1 E TRAC" I CP' a'iso ut i "I ~ z cs Yttrium .as- an intern*'i standard to compensate Tor f ! uc tua t one? i.n neou 11 uti cr. sna plasma roncitions. A'll Yttnum readinas are expressed in -counts. > .` ) Page: 2 > LANCASTER LABORATORIES %9 Run Ns me : 96 2 7004T6? INSTRUMENT ID: 0593 Tube: > ) EL EM `1 SO CONC (ppm) AVG INTENSITY RATIO 09/26/96' %RSD 09:11 INTEGRATIONS #2 3 Aa ) __ AT ' As .__ B ) ___3 a Be Ca ) ___Cd __ Co Cr > ___Cu F __K > -__ Mg __ Mn __ lio ) __ Na Ni ___Pb __ St> ___Se __ Sn ' Sr Ti __ T'l > ___V __ Y ' __ 2 n ) 0.000 0.000 0.000 0.000 0.000 o. 000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.00 0 0.000 0.00 0 0.000 0.000 0.000 0.000 0.000 0 . 000 N/A 0.000 -0.00297 4.248 .. 0.01864 0.674 0.00002 3192 . .0.00008 43. .5 3 0.00073 6.876 -0.04131 0.971 -0.00005 551.8 0.00257 14.26 -0.00053 3 2.74 -0.00031 7 1.46 -0.00661. 4.657 -0.00262 15.91 0.00460 2.577 0.00068 17.84 0.00291 11.33 -0.00207 2 8.76 0.001 1 5 1 10.4 0.00047 156.0 0.QQ22S 1 04.4 0.00226 1 ?'. 4 ' -0.02493 17.15 -0.00464 36.5 Cl 0.00299 11.68 -0.00464 7 1 . 44 -0.00081 49.5.1 0.0 0 0 54 3 8.63 33299.33203 0.679 0 . Cl 0 0 1 4 S 0 A *'. -0.00295 0.01853 0.00098 0.00005 0.00068 -0.04091 0.00026 0.00253 -0.00038 -0.00005 -0.00643 -0.Q022Q 0.00455 0.00077 0.00324 -0.00160 0.00208 0.00074 0.00229 0.0025 0 -0.01999 -0.00295 0.00318 -0.00667 -0.00050 . 0.00066 33555.00000 0.00 0 23 -0.00310 0.01862 -0.0-0057 0.00006 0.00078 -0.04172 -0.00027. 0.00295 .,-0.00072 -0.0Q039 -0.0069-7 -0.00262 O'. 00473 . 0.00054 0.00289 -0.00274 0.001S9 0.00102 0.0Q4S8 0.0 0 i 9 6 -0.027.50 .* '-0 . 00633 0.00.319 -0.00081 -0.00126 0.00063 33125.00000 0 . 00006 -0.00285 0.01878 -0.00033 0.00012 0.00072 -0.04130 -0.00015 0.00222 -0.00048. -0.00048 -0.00644 -0.00304 0.00451 ' 0.0007? 0.00258 -0.00186 -0.00030 -0.00036 -0.00012 0.00237 -0.02730 -0.0 04 63 0.00258. -0.00644 -0.00066 - 0.00030 33218.00000 0.00015 > 114 DUP050307357 I .ire: o LANCASTER LABORATORIES 1 ' ij n N 3 me : S 6 27 0 041 b 2 INSTRUM ENT ID; 059; lube: [ L.E h 2 S'l^ CONC (ppm.) AV6 INTENSITY RATIO 09/26/96 5SRS0 41 0 9:15 INTEGRATIONS #2 43 __A1 [__Ca __ f e __ K __ Mg __ Na ___ Y 50.000 50.000 50.000 50.000 50.000 50.000. N./A 3.88746 3.88772 4.19430 5.65133 4.236 64 0.66701 .32642.00000 0.173 0.245 0. T27 0.343 0.102 0.124 0.270 3.88676 3.88513 4. 19783 5.65118 4.24162 0.66506 32542.00000 3.89452 3.8 7 97 2 4.18814 5.67079 4.23479 0.65761 32709.00000 3.8 8 1 1 0 3.89830 4. 19 693 5.63201 4.23351 0.66736 32575.00000 115 DUP050307358 I 5Cit-- : LANCASTER LABORATORIES !uh Name : g 5 27 0G4T62 lubt*: l . L. M 3 S2 s AvG CONC (ppm.) INTENSITY RATIO __ An __A(i 8 __ Bo __8*> __C d ___C o __ C u __ Mn __ N-l Pb __ st-. ___Sr--T'l __Y __ /11 1 .000 1 . 000 1 . 000 1 ; 000 1 .00 0 1 .000 i . 000 1 . 000 1 . 000 1 .000 1 .000 i .000 1 .000 l .000. N /A i .000 0.8 51-13 0.31545 0 . -1 02 S 8 1 . 537 14 1.98670 3.88318 0.42390 0.92S7-1 9'. 52430 . 0.84931 0.76136 1.23978 42.42720 0.08775 33036.33203 G . 1 63 93 09/2-6/9 6 09:21' INSTRUMENT ID:- 0593 SR SO 0.554' 1.516 0.808 0.486 0.725 0.6 09 0.632 0.785 0.570 0.236 0.865 0.300 0.282 1.403 0.285 0 . &62 INTEGRATIONS # 1 #2 0.85565 0.30993 0 . 1 D174 1.52866 1 . 97012 3.85604 0.42082 0.92179 9.46315 0.85145 0.75390 1.23577 42.28963 0.08635 33142.00000 0. 1 6259 0.86439 0.31808 0.10300 1.53991 1 . 99627 3.89950 0.42572 0.93119. 9.56697 0.84900 0.76638 . T. 24 043 42-.48471 0.08867 33007.00000 0.16472 #8 0.86334 0.31835 0. 10330 1 . 54283 1 . 9937 1 3.89399 0.42515' 0.936 1 6 9.54277 0.84748 0.76380 1.24314 42.50728 0.08822 32 960.00000 0. 164 3 0 116 DU P050 307359 LANCASTER LABORATORIES l-I.M "*me: (Iff1*1 4 96270Q4T62 S3 ! 1 1 t'' il ' il 1i " ,/ f CONC (ppm) 1 .000 1 . 000 1 . 000 T .000 1 . 000 '1 .000 N/A A VC INTENSITY RATIO 0.84416 1.26394 0.62885 1.05653 5.40113 1.47624 32874.00000 09/26/96 . INSTRUMENT 10: 09:25 059: %RSD 0.276 0.607 0.040 0.203 0.077 0.198 0.246 INTEGRATIONS n i #2 0.84647 1 . 255.29 0.62856 1.05709 5.40589 ,1.47942 32789.00000 0.84421 1.26655 0.62901 1.05836 5.39799 1.47566 32950.00000 #3 0.84180 1.26998 0.62898 1.05416 5.39950 1.47364 32883.00000 117 DUP0503 07360 Page : LANCASTER LABORATORIES Run Name: Tube: '5 9527 004T62 ICV 09/26/96 09:29 INSTRUMENT ID: 0 5936 EL EM A' t __ .41 __1As B __ 6 a Be __Ca ___Cd __ Co __ Cr ' __ Cu ___Fe __ K ___Mg __ hr, ___mo .__ Na Ni __ Pb ___'ib S& ___Sn __ Sr __ Ti __ T'l ___V V __ In AV6 (ppm) SRSD #1 0.65002 29.33331 0.64561 0.64174 0.63/35 .0.63921 29.49375 0.63231 0.64116 0.61680 0.65029 '29.5 5323 29.92016 29.40117 0.64210 0.62450 29.56549 0.64537 0.63536 0.6077 3 0.62098 0.6 1758 0.62170 0.62831 0.O3496 0.51574 32014.00000 0.63245 4.310 ' 4.071 4.037 4.477 4.452 4.451 4.489 4.674 4.365 4.245 4.1 90 4.548` 3...888 4.431 4.427 4.584 3.3 b b 4.887 3.. 654 4. 130 3.286 4.560 4.543 4.343 3.441 4.3 97 3 .5 3 6 4.502 0.68236 30.71224 0.67564 ' 0.67480 0.67010 0.67198 31 .-02044 0.66640 0.67340 0.64698 . 0.68167 31.10255 31.26146 30.90255 0.67488 0.65590 30.70839 0.68178 0.66203 0.63617 0.64438 0.65002 0.65429 0.65978 0.65757 0.64691 30713.00000 '0.66530 INTEGRATIONS #2 43 REREAD REDIG Q.63191 28.62157. 0.62879 0.62279 0.61986 0.62076 28.66018 0.61381 0.62307' 0.60016 0.63265 28.69769 29.31501 ' 28.56485' 0.62422 0.60261 28.92463 0.62645 0.61966 Q . 58867 0.60683 0.59936 0.60430 0.61108 0.61408 0.59804 3?77 $ finnnn 0.6 1460 0.63579 28.66611 0.63241 0.62762 0.62210 0.62488 28.80062 0.61672 0.62700 0.60325 0.63654 28.85946 29.18400 28.73609 . 0.627 20 0.61397 29.0 6344 0.62788 0.62439 0.59834 0.61175 0.6 0334 0.6 0 6 5 0 0.61407 0 /63313 0.60227 32554.00000 U.61747 sssssiii* 118 DUP050307361 LANCASTER 'LABORATORIES ..,(ri Name: 9 6 2 7 0 0 4 T 6 2 i utn*> 6 ICB c. KM _ _"~A 1 73 77.0 * '77.6 => __ c, Jj:d Co \__C r Lu __ F __ K __ lvlct 7>n '__Mo -J i 77. 6 b '__Sc- 'I n jr f1 ri ~,y r 7..ri AV6 (ppm) "RSD -0.OOO04 0.02291 0.00040 0.00406 -0.00019 -0.00016 -0.00419 -0.00027 -0.00007 0.Q0032 0.00056 . 0.02889 0.11032 0.02311 0.00030 0.001 63 0.79195 0.00041 -0.00052 0.00 173 0.00018 0.00150 0.00016 . -0.00004 -0.0 Cl 0 2 2 -0.00 0 03 3 28 28.33 7 03 0.00007 123.6 9.422 511.5 4.202 30.00 68.25 103.0' 54.76 1110. 50.78 0.11 2 3 2.95 6,551 8.237 14.05 56.24 4.1 .25 98.14 239.9 7 9.52 3 13.3 46.45 ?4.20 1 87.9 1 1 28 . 2 10.6 r>. o 0 547.6 09/26/96 09:3 INSTRUMENT ID: 05936 INTEGRATIONS #1 42 -o.o.o on 0.02484 -0.00190 0.0 0426 -0.00013 -0.00006' 0.00046 -0.00044 -0.00004 0.00033 0.00056 0.03656 0.10218 0.02525 0.00034 0.00243 0.10795 ' 0.00070 -0.00190 0.0031 0 0.00082 0.00184 0.00021 0.00004 - 0.00 1 47 0.00001. :3 ?.00000 0.00057 -o:ooooi 0.02058 0.00098 0.00396 -0.00019 -0.00028 -0.00807 -0.00025 0.00017 0:00015 0.00056 0.03187 0.11280 0.02239 0.00026 0.00062 0.20265 -0.00005 ' 0..00056 0.00034 -0.00027 0.00069 0.00015 -0.0001 0 -0.00183 0.00000 32826.00000 -0.00016 #3 REREAD REDIG ' -O.OOOOi________________ 0.-02331 0.00214 0.00396 -0.00025 -0.00Q13 ,, -0.00497 -0.00014 -0.00048 ' 0.00047 : ________ 0.00056 _____ _ _ 0.01823 ____________ ___ 0.1 1599 _ 0.02167 ________________ 0.00032 0.00185 J 0.26525 0.00059. -0.00023 0.00174 O.0DOOO __ 0.00196 0.00013 -0.00007 _____________ 0.0 0 2 6 4 _______ _______ -0.00011 3 2 3 7 7 .00 0 0 [i -0.00017 119 DUP050 307362 rage: 8 LANCASTER LABORATORIES Run Name: 9627004T62'Tube: 7 . CRI . 09/26/96 09:1 INSTRUMENT ID: 05936 EL EM Ag __ A1 As - S. __ Ba __ 8e __ Ca Cd __ Co __ Cr Cu __ Fe __ K __ Mg __ Mn ..__Mo N -3 _j'H __ P& __ 3 b S s* Sn Sr Ti __ T'l __ V y Zn Ave (ppm) %RSD 0.02169 1.611 -0.00171 46.14 0.01897 21 . 24 0.00502 10.17 -0.00018 43.56 0.01024 0.483 -0.04270 5.025 0.01002 0.075 0 . 10535- 0.612 - 0.02051. 1.694 0.05364 0.647 0.02487 11.40 0.10587 3.282 0.01008 41.75 0.03 162- 0.348 0.00076 169.9 0.02878 51.5 1 0.08433 0.704 D.00705 3.116 0 . i 1 S 1 8 l`. 781 0.01077 12.22 -0.00091 76.49 0.00005 3 3.0 0 -0.00022 52.42 0.01718 '! G . 0 2 0. 10261 0.629 33032.66795 0.095 0.04201 ( .. d 0 4 INTEGRATIONS *n #2 0.02188 -0.00220 0.022Q5 0.00472 -o'. 00010 0.01023 -0.04039 0.01002 0.10491 0.02013 0.05330 0.02814 o:T0970 0.01472 . 0.03151 0.00068 0.03888 0.08474 0.00708 0.11507 0.01203 -0.00149 0.00007 ' -0.00027 0.01 5.3 5 0.10188 3065.00000 0.04 1 54 " 0.02190 -0.0.0080 0.02045 0.00561 -0.000180.01020 -0.04308 0.01003 - 0.10609 ' 0.02058 0.05399 - 0.02338 0.10499' 0.00901 0.03173 0.00209 0.01176 0.08461 0.00681 0.11491 0.01086 -0.00112 0.00004 -0.00009 0.01877 0.10309 33031.00000 0.04177 #3 REREAD REDIG 0.02 '129 -0.00215 _ 0.01441 0.00473 -0.00025 0.01030 -0.04463 ' _______ 0.01002 ________________ 0.10504 0.02031 0.05364 `0.02309 0.10292 _ 0.00651 0.03162 -0.00049 ________________ 0.03572 0.08365 0.00724 0.11857 0.00940 _______ -0.00013 0.00004 -0.00 031 _____ _ _______ 0.01741 _______ 0.10237 33 00 2.000 0.0 ___ ____________ 0.04273 ________ ________ 120 DU PO50307363 {v>n : u LANCASTER LABORATORIES, R-ui'i Nif1 * : 9527 004162 lull'-.' : 8 IC S A , 09/26/96 09:44 INST RU ftE WT 10: 05? 3 6 i: L E14 AV6 fppm) %RSD #1 INTEGRATIONS #2 #3 REREAD RED 16 Ao 0.00014 345.7 0.00052 -0.00040 0.00031 _____________ __ __ A "1 515.74053 0.220 514.42974 516.30535 516.48645 _ ' __ A:.' ___e 0.00026 697.5 0.01343 1 .555 0.00243 0.01326 -0.00071 0.01.366 -0.00091 0.01336 ________________ __B a 0.00846 0.199 0.00845 0.00844 0.00847 ______ __________ '8 e ' -0.00050 3 5.82 -0.00029 -0.00056 -0.00064 ___ C* 506.85455 0.114 506.38446 '506.67840 507 .50076 _ Od -0.00194 9.636 -0.00181 -0.00186 -0.00216 _______ . A Ce> __ Or 4 Cu 0.00122 34.83 0.00131 13.59 -0.00067 14.24 0,. 00 125 0.. 00134 -0.00073 ' 0.00078 0.00112 -0.00073 0.00164 0.00147 -0.00056. __Jr & 202.27117 0.202 201.81011 202.41375 202.58967 A K ___Mg O'. 09922 5.003 520.59570 0.279 0 . 10486 S18.93682 0.09553 521.13774 0.09726 _ ' 521.66253 __ __Mn 0.00619 1 .339 0.006 2 3 0.00609 . 0.00624 __ Mo 0.00080 363.0 0.00399 -0.00179' 0.00023 : J__N.*t 0. 1 6787 32. I 9 0.12064 0 . T5615 0.22681 _ Ni 0.00166 1 8.09 0.00156 0.00200 0.00142 __ P'b -0.00040 77 2.0 -0 . GO 234' -0.00208 0.003 21 _______' __ 'ib 0.00598 52.03 0.00537 . 0.00443 0.01114 __ St- -0.01016- 14.56 -0.01133 - 0.. 0 1 0 6 6 -0.00850 ________________ ___On 0.00556 63.25 0.00261 0.00946 0.00462 Sr 0 ..02068 0 . 11 2 0.02065 0.02069 0.02070 fi __ T 1 -0.00121 6. 132 -0.01116 5. 156 -0.00125 -0.011 1 5 -0.00125 -0.01059 -0.00112 -0.01174 _______ __ V 7 -0-00458 14.50 30395.33399 0.36? -0.00400 5 2 ? . 0 0 0 0 0 -0.00531 30352.00000 -0.00445 3 031 1 .00000 ?n 0.00339 70.96 '0.0023 1 0.00171 0.006 1.5 ____ ) 121 ' I r.V vi -.'A- ' DUP050307364 -age: 10 .LANCASTER LABORATORIES un Name:- 9627004T62 Tube: 9 ICSAB 09/26/96 09:49 INSTRUMENT ID: 0503f. EL EH Aa __ AT As __ B __ Ba Be Ca Cd __ Co ___Cr __ Cu __ Fe __ K __ Pig __ hn __ Mo ,,__Na NT __ Pb' __ Sb __ Se __ Sn Sr TT __ T1 V __ V __ 2n AVG (ppm) 3SRSD 0.23187 2.888 528.36621 3.069 0.10473 3.678 0.03109 4.094 0.55826 2.925 0.50830 2.712 . 519.08428 3.390 0.99998 3.047 0.52410 2.919 0.50162 3.071 0.59556 2.857 206.53732 37073 0.10089 7.687 530.35626 2.892 0.53057' 3.055 0.00097 85.96 0.23082 55.90 1.01601 2.807 0.05135 3.405 0.63 15 i 1 . 843 0.04143 9.150 0.00680 15.41 0.0 2 1 1 6 ? Q ^ -0.00124 11.55 0.10430 4.277 0.51717 2.334 2 9829.331-59 8 3.0 57 0.37329 ?,. 19 8 #'l 0.22860 520.14129 0.10918 0.03032 0.55100. 0.49951 507.32165 0.98057 0.51498' 0.49136 0.-58S10 202-. 59849 0.09523 322.80017 0.52062 0.. 00009 0.08227 0799848 0.05098 0.SZ289 0.04-4 2 5 0.00551 0.02084 -0.00123 0.1026 0 0.50863 0235.00000 0.95580 INTEGRATIONS #2 0.23953 547.04608 0.10237 0.03256 0.57697. 0.52420 539.31854 1 ..03510 0.54176 0.51934 0.61486 '213.86055 0.10973 548.56341 ` .0.54928 0.00106 0.31519 1.04892 0.05388 0.64475 0.04291 . 0.00586 0.02188 -0.00139 '0 . 10 936 0.S34 1 0 28785.00000 1.01403 #3 REREAD REDIG 0.22745 517. .91 1 19 _____ 0.10266 _____ __________ 0.03040 j 0.54682 0.50120 510.61273 0.98426 ___________ ____ 0.51554 _ 0.49417 0.58272 _____ ; 203.15292 0.09771 521.20513 0.52182 0.00176 0.29499. 1.00062 0.62687 0.05069 0.03712 _______ _______ 0.00804 0.0 207 ? ____: -0.00110 0 . 1 0 0 9 3 _____________ 0.50878 304 6 8.0 00 00 _______ 0.96 5 0 4 _____ _____ 122 DUP050307365 /-I a ` LANCASTER LABORATORIES uii Name: 9S27004T5 [ ube : 10 CCV 09/26/96 . . 09:54 INSTRUMENT ID: 0598 6 .. L E M Aa HAs__A 1 __ 6 a __.Be "__Ca _ Cd __ Co __ Cr .Cu __ f e __ K ` __ Mg ___.Mn __Mo ' Ha ___r1i '__Pb ___5 b __ Se .5 n ___Sr Ti T'l __ Y __ 2 n AVG (ppm .1 %RS0 0.53110 24.61554 0.51469 0.52027 0.5046 2 0.51024 25.06071 0.51041 0.51124 0.49236 0.51954 24.57594 25.46312 24.50018 6.51503 0.49413 24.91196 0.51473 '0.51156 0.48157 0.50962 0.51122 0.49605 0.50076 0.51297 0.49650 32465.66601 0.51064 0. 1370.107 0.169 0.569 0.301 0.025 0.054 0.132 0.354 0.079 0.245 0.103 0.184 0 . 134 0.17 1 1.021 0.4 6 S 0.280 0.415 0.97 7 0.55 0 0.372 0.256 0 . 173 2 . 15 5 0.315 0.262 0.127 #1 0.53127 24.58694 0.51569 0.51803 0.50287 0.51029 25.07256 0.50965 0.50927 0.49196 0.51881 24.54914 25.41747 24.57165 . 0.51411 G.48902 2 5.046 1 1 0.51531 0.50917 0.47630 0.5069 (i 0.51128 n.49458 0.49976 0.51366 0.49492 562.00000 0.51013 INTEGRATIONS nz . - 0.53173 '24.63906 0.. 51429 0.51916 0.50534 0.51034 25.06381 0.51062 0.51162 0;49238 0.52101 24.59955 25.51119 24.63648 0.51587 0.49426 24.85547 0.51580 0.51323 0.48507 0-50945 0.50929 0.49690 0.50133 0.52366 0.49805 32435.00000 0.51137 #3 REREAD REDTG ' 0.53030'24.62062 0.5'140 3 _______ 0.52363 0.50565 0.51009 25.04575 ______; 0.51096 0.5 1 2 S3 _ 0.49273 0.51880 24.57912 25.46070 _______ ' 24.59240 0.51511 _ 0.4991 1 _ 24.83429 O'. 51 309 0.51 228 _______ ______ 0.483 64 0.51250 0.51309 0.49665 ________ 0.50113 0.50158 0.49653 32400.00000 0.. 5 104 1 ______ 123 DUP050307366 3<;>e=': 1*2 LANCASTER LABORATORIES ftUn Name: Tube: 1 1 9527004T62 . CCB 09/26/96 09:59 INSTRUMENT 10: 05936 EL CM Aa ___$ 'i AS __ B __ Ua __ fie Ca Cd __ Co __ Cr__ Cu Fe __ K __ Mg __ hn __ Mo ___Na __ N i __ Pb __ 'jb __ 3e Sn Sr TT T'l __ V __V __ 2n AV6 (ppm) 5SRSD 0.00024 9 8.40 . 0.06076 40.01 -0.00153 71.45 0.00628 7.262 -0.00012 61.40 -0.00035 27.32 0.02150 VI 8.6 -0.00029 87.51 -0.00026 46.51 -0.00027 16 9.5 0.00092 11.74 0.05253 7.819 . 0.10692. 4.555 0.0633 6 38.84 0.00026 18.04 0.00149 5 8.50 0.06776 41 .48 0.0000 1 8121.. 0.00012 114 9. 0.00 197 7 2.3G 0.00253 1 0 3.9 0.00056 270.8 0.00012 26.86 -0.00003 8.9 02 0.00145 34 5.9 -0.00023 126.2 32628.66601 0.114 0.00058 3 1.74 ' #1 INTEGRATIONS: ... #2 #3 REREAD REDIG 0.00024 ' '0.08883 -0.00026' 0.00579 -0.00003 -0.00026' 0.05087 -0.00002 -0.00019 -0.00057 0.00091 0.05711 ' 0.10450 0.09178 0.00 0.30 0.00248 0.03556 -0.00001 0.00102 0.00353 0.00307. -0.00027 0.00015 -0.00008 0.0064 1 -0.00024 32613.00000 . 0.00053 0.00000 0.04700 -0.00221 0.00637 -0.00017 -0.00045 0.00891 -0.0003?. -0.00040 -0.00050 0.00082 . 0.04917 0.10374 0.04891 0.00021 O'. 00084 0.08036 -0.00098 -0.001470.00070 -0.00032 -0.00035 0.00009 -0.00009 0.00157 -0.00051 32669.00000 0.00077 ' 0.00 049 0.04644 -0.00211 0.00669 -0.00015 -0.00033 0.00472 -O'. 00054 -0.00019 0.00025 0.00103 0.05132 0.11253 0.04938 0.00028 0.001 1 5 0.08737 0.00103 0.00081 0.00168 0.00485 0.00232 0.00010 - 0 . 0 0 O' 0 7 -0.00363 0.00006 325 98.0000 0 0.0 0 0 3 9 124 A DUP050307367 LANCASTER LABORATORIES Run Name: 9627004T62 ' Tube: 12 PBW 'P&lO *.** * , 100-i;00,DF1,962685720002,8, , ' 09/25/96 10:04 INSTRUMENT ID: 0 5936 , EL EM Aa A'l As b Ba BefOb jZC6 Co Cr Cu Fe K lla .Mn Mo Na N1 Pb __ Sb _S& __ Sn Sr Ti _rr __y ___r __ tZn AVG (ppm) 2RSD 0.00036 0.02202 -0.00216 0.00782 -0.00025 -0.00030 -0.03204 -0.00029 - 0.00031 0.00036 0.00035 0.04121 0.10560 0.02719 0.00087 0.00115 0.10166 .0.00021 -0.00004 0.00198 0.00095 0.00180 0.00004 -0.00013 -0.00274 -n . o00 1 3 32825.56796 0.0085? 13.99 18.82 23.04 13.56 4.45 18.15 4.641 20.43 134.6 3 5.29 19.52 14.13 4.650 7.279 1 .479 3 5.99 20.52 2 0 6.8 7 62.9 118.0 1 33.2 14 .31 3 1.22 50 . 57 77'. 0.0 4 8.55 0 . 12 2 1 4.30 INTEGRATIONS #1 #'2 . #3 REREAD RED IG 0.00037 0.02201 -0.002.59 0.00664 -0.00025 -0.00033 -0.03137 -0.00024 0.00031 0.00026 0.00035 0.04192 0.10010 0.02529 0.00038 0.00101 0.09054 0.00030 -0.00042 0 . [104 5 1 0.00052 0.00170 0.00003 -0.00020 -0.00321 -0.00018 32794.00000 0.0 0 8 3 9 0.00040 0.02617 -0.00230 0.00812 -0,00025 -0-. 00033 -0.03100 -0.00028 0,00074 0.00033 0.00029 0.03506 0.10714 0.02924 0.00088 0.00081 0.12573 . 0.00059 0.00024 -0.00013 0.00288 0.00210 0.00005 -0.00014 -0.00459 -0.00016 32812.00000 * 0.00987 0.00030 0.01788 -0.00161 0.00870 -0.00023 -0.00023 -0.03374 -0.00036 -0.00010 0.00051 0.00043' 0.04664. 0.10956 0.02703 0.00086 0.00163 0.08871 -0.00026 0.00004 0.0 0 I 5 9 -0.00054 0.0 0 1 6 2 0.00006 -0.00006 -0.00043 -0.00006 32871.00000 fl . ml? JJ 125 DUP050307368 f aae: '14 LANCASTER LABORATORIES Run Name: 9627004T62 Tube:' 13 LCSW ****, 1-1 ;DF1 .'9626-857 20002.8. , 09/26/96 10 : 09 INSTRUMENT IP; 05936 ELEM A ci __ AT As B __ 8a Be j/Ca ___Co __ Cr Cu Fe ___K < ha __ Mn __ Mo __ Na N1 Pb __ Sb __ s __ Sn __ Sr n ___n V__ Y __ Zn AV'G (.ppm) %RSD SI 0.05467 5.866 0.05334 2.23069 6.460 2.15454 2.205 13 5.993 2. 139"I9 2.23258 5.992 2.15885 2.19279 6.175 2.12401 0.05364 4.328 - 0.05249 4.26833 6.185 4.13871 0.05464 5.787 0.05311 0.54320 5.949 0.52729 0.21107 6.155 0.20512 0.27530 5.939 0.26651 1.107 1 5 5.887 1.06820 3.94539''4.859 3.84601 2.10263 6.248 2.03858 0.5 5055 6.119 0.53376 2.13196 6.455 2.04891 4.05254 4.736 3.94253 Cl. 5 56 27 6.231 0.54199 0.55179 5.158 0.5342 0 0.54226 6.636 0.51979 2. 13774 5.499 2.06905 4.26104 6.063 4.13509 1.06665 6.284 1 . 03305 1.04951 6.193 1 . 01633 2. 19240 6.561 2.10806 0.53394 6.035 0.51720 31912.66601 4.817 32629.00000 0.55524 6 . 1 1 7 0.537-7 3 INTEGRATIONS 42 - 43- REREAD REDIG 0.05833 2.39690 2.35731 2.38700 -2.-34878 0.05631 4.57210' 0.05827 0.58039 0.22598 0.29416'1.18240 ' 4.16641 2.2537 5 0.58934 2.29083 4.274I9 0.59579 0.58463 0.58377 2.27349 4.5 58-23 1 . 14384 1.12440 2.35849 0.57109 30148.00000 0.59439 0.05234 2.14061 2.11891 2.15188 2.10558 0.05212 4.09419 0.05252 0.52192 0.20213 ' 0.26522 1.07085 . 3.8237? 2.01555 0.52856 2.0 5 6 14 3.94090 0.53102 0.53653 0.52323 2.07068 4.08980 1 .0 23 07 ' 1 .007 80 2. 1106 5 0.5135 8 3 2 95 1 . 00000 0.53360 3 126 DUP0503 07369 i'sae' LANCASTER LABORATORIES Run N a rn e : 9 6 2 7 0 Q 4 T o 2 Tube: 14 2583226 1 00-1 00.. DF TO, 96 26857.2000 2 &., , 09/26/96 10:14 INSTRUMENT K' 0 S f- EL EM ___Aa __ A 1 As __ B 8a __ Be Ca __ Cd Co __ Cr __ Cu __ E e __ K __ Mo __'rtn MID 5>a __ N T P'b __ Sb __ Se __ bn Sr Ti __y __ r __ 2n $ VS (.'ppm) %F(SD INTEGRATIONS #2 0.00Q50 32.74 0.02348 5.808. -0.00057 271.8 0.05275 1.17 8 0.01566 .1.193 -0.00041 9.499 6.69885 0.409 -0.00033 50.74 0.00038 37.78 0.00026 17 5.8 0.00095 17.79 -0.03053 3 0.3 1 0.36738 0.881 2.77224 0.492 0.08100 0.267 0.00534 29.84 4.91494 1.618 0.00167 4 8.91 -0.0.0003 33 09 . 0.00148 1 27.8 0.00061 45 2. 1 0.00423 37.04 0.05415 0.347 0.0 001 8 96.50 0.00845 67.59 0.00016 19 9.2 32647.66601 0.1-53 0.007 1 8 4.095- 0.00069 0.02479 -0.00082 0.05346 0.01536 -0.00038 6.66720 -0.00047 0.00053 0.0006.5 0.00095 0.03357 0.37013 2.. 7 5 6 8 'i 0.08078 0.00717 4.91455 0.00258 -0.00127 0.00 0 2 6 0.00373 0.00604 0,05394 0.00038 0.0 1 1 2 2 0.00047 32696.00000 0.0 [i 7 1 0.00047 0.02358 0.00VI0 0.05234 0.01563 -0.00040 6.71524 -0.00014 0.00038 0.0003-9 0.00111 0.03789 0.36820 2.78269 0.08121 0.00466 4.99466 0.00143 -0.00002 Q.0036? -0.00153 0.00345 0.05429 0.00009 0.00188 0.00018 3 2 651.00000 0.00694 #3 fREREAD RED 3 0 0.00035 0.02206 - -0-. 0`020 1 0.05 243 0.01549 -0.00045 6.7141.0 -0.00036 >0.00023 -0.00025 . 0.00077 0.02014 0.36381 2.77723 0.08103 0.00420 4.83559 0.00100 0.00118 0.00051 -0.00036 0.00321 0.05424 0.00006 0. . 0 1 2 2 5 -0 . 00 017 32595.00000 0 . 0 07 5'! 127 D UP050307370 Pane: LANCASTER LABORATORIES Run Name: 9627004T6? Tube: 15 2583226 ' UP**,100-I 00.OFIO.962685720002.8. ,' 09/26/96 . 10:19 INSTRUMENT Ip: 050:4.5 ELEN AVG (ppm) %RSD #1 INTEGRATIONS #2 __ Aa 0.02345- 0.545 0.02344 0.02333 __ A1 0.46741 0.121 0.467 7 8 0.46770 As 0.02051 4.543 0.01990 0.02005 __B 0.27766 0.574 0.27623 0.27738 8 a 0.47191 0.111 0.47185 0.47247 __ Be 0.01109 0.390 0.01106 0.01106 Ca- 7.72734 0.494 7.68880 7.72806 __ Cd ` 0.01104 0.972 '0.01099 0.01096 Co 0.115.33 0. 135 0.11518 0.11549 ___Cr 0.02226 1 .496 0.02208 0.02207 __ Cu 0.05792 0.3 93 0.05778 0.05780 Pe 0.24860 5.847 0.23183 0.25766 __ K ' 2.38345 0.136 2.39201 2.38561 __ Mg 3.84313 0.219 3.83868 3.837.84 __ Mn 0. 1 1453 0.356 0.11*15 0.11447 . Mo 0.21487 0.80 0 0.21423 0:21357 _j'Ja 7.33989 1.147 7.25368 7.34410 __ Ni 0.09435 1.03 6 0.09342 0.09418 Pb . 0.01234 14.86 0.01085 0.01439 __ Sb 0.1183 8 2.403 0.11510 0.12010 '__ Ss A __ Sn 0.01178 3.322 0.60232: 0 . P$ 1 0.011.33 0.59648 0.01193 0.60493 Sr 0.07575 0.094 0.07568 0.07582 Ti 0.1111 3 0.2 7 'J 0.11079 0.11124 __ Tl 0.02467 2 0.7 5 0.01683 0.02673 _____ v __ Y __ 2. n 0.11038 0.339 32771.66796 0.18 3 0.0507 9 1 . i 8 8 0 . 10 998 32707.00000 0.05 0 15 0.11044 32782.00000 0.0513* #3 -REREAD REDIG 0.02358 _______________ 0.46676 _______ 0.02158 0.27938 0., 47 142 0.01114 __ 7.7.6517^ 0.01116 _____ ;^ 0.11534 0.02265 ______ ; 0.05819 0.25630 2.38773 . 3.85286 0.11496 0.21682 _______ ________ 7.42190 0.09545 0.01177;. 0.11994 0.01207 : 0.60556 0.07574 0.11136 0.02844 0.1 1 07 2 32326.00000 0.05 0 5 o _______ ^____ 128 DUP050307371 LANCASTER LABORATORIES F;un Name: 9627004T62 . Tube: IS 2583226 36 0***, 100-100tDF10; 962685720002.. 8, f 09/26/96 10:24 INSTRUMENT I'D: 05935 EL EM AVG (ppm ) %RSD Aa 0.00045 70.72 AI 0.00661 38.57 As -0.00105 179.0 B 0.04986 1.461 Sa - 0.01518 0.503 be -O'. 00032 28.44 Ca 6.67235 0.652 __ Cd -0.00037 34.61 Co 0.00034 197.5 __ C r ' 0.00000 7406 . Cu . 0.00094 24.03 Fa 0.02968 17.19 ___K . 0.34696 0.467 Ma 2.75506 0.435 __ Mn 0.08009 0 .488 Mo 0.00214 25.82 4.92550 3.512 ___N i 0.00033 99.93 __ rb 0.00095 9 6.57 __ Sb 0.00302 41.24 __ Se 0.00106 16 5.3 ____$ n 0.00320 6 2.8 ! __ Sr 0.05379 0.300 __ Ti -0.00014 95.30 __ Tl 0.00183 19 6.2 -0.0003? 106.0 Z> 32967.65796 0. 13 1 __ 2n 0.00748 . & O #1 . INTEGRATIONS #2 ft3 REREAD REDIG 0.00019 0.00391 t 0.00324 0.04969 0.01509 -0.00028 6.62762 -0.00023 -0.00038 -0.00028 0.00069 0.02380 0.34662 2.75318 0.07970 .' 0.00156 4.84748 0.0006 9 0.00083 . 0.00 1 6 1 0.00310 0.00403 0.05362 -0.0002' 0.00195 -0 . 0001 3 33014.00000 0.0 0 7 5 9 0.00036 0.00900 0.00030 0.05066 0.01522 -0.00025 6.67484 -0.00049 0.00095 -0.00035 0.00113 0.03298 . 0.34553 2.76478 0.08008' 0.00218 4.80523 0.00030 0.00007 0.00345 -0.00001 0.00091 0.05380 -0.00015 -0.00182 -0.00080 32961.00000 0.00728 0.00081 0.00691 -0.00025 0.04923 ' 0.01523 -0.00042 6.71459 -0 : 00039 0.00046 0.00061 0.00100 0.03227 0.34372 2.77724 0.08048 0.00266 5.12381 0.00001 0.00191 0.0039 9 0.00011 0.00460 0.05395 0.00000 0.00536 -n . ono 1 2 32928.00000 0 . 007 6 ' % 129 DUP050307372 k p5oe: 1 & LANCASTER LABORATORIES Run Name: 9627004762 Tube: 17 2583226 Eb&FS R-** *-. 100-100.DF10.962685720002.8. , ' 09/26/96 10:28 INSTRUMENT ID: 05936 EL EM Aa AT As B 8a . Ca ___Cd . Co __ Cr Cu Fe K ..Mg .Mn ___Mo i __ N i __ Pb ___3b ..S e __ Sn ___'Sr Ti ___n y ___Y __ 2r. AVG (ppm). %RSD 0.00549 5 ! 226 *0.21844 1.205 0.00248 54..99 0.25632 0. 1 24 0.22394 0.287 0.00466- 2.724. 7.17122 0.43 6 0.0051 5 4.133 . 0..05247 0.353 . 0.02091 1 . 877 0.02694 0.720 0.13237 5.844 0.68182 0.613 3.00521 0.411 0. 1.3443 0.461 0.20480 0.121 5.42170 1.283 0.05555 1 .737 0.00127 109.3 0.05264 5.279 0.0021 1 76.40 0.42564 0.861' 0. 15764 0.3 22 0.10412 0.412 0.00762 65.38 0.05121 0.469 32466.66601 0.401 0.05561 0 . 5 8 8 ' INTEGRATIONS #1 #2' 6.00571 0.22133 0.00105 0.25669' 0.22469 0.00452 7.20606 0.00538 0.05256 0.02117 0.02705 0. 14126 0.68564 3.0193 0 0.13509 0.20492 5.45183 0.05649 0.001 1 8 D . 05260 0.00 234 0.42949 0. 1 5823 0.10461 0.002! 5 0.05099 32320.0 00 0 0 0 . 03566 0.00516 0,21781 0.00378 0.25608 0.22363 0.00473 7.14551 0.00496 0.. 05226 0.02046 0.02671 0.12874 0.68247 2.9.9620' 0 . 13386 0 . ?045 1 5.34213 0.05456 0.0027 1 0.04988 0.00039 0.42220 0. 1S735 0.10383 0.00879 0.05116 3 2 5 1 0.00000 0.0557 2 #3 REREAD REDI6 0.00559 0.21617 0.00261 ' 0.25620 0-22352 0.00474 . 7.16209 0.00512 0.05260 0.02111 0.02704 0.12712 0.67735 3.00012 0.13434 0.20496 5.47113 0.05561 -0.00007 0.05543 0.0036 1 0.42522 0.15734 0. 103Q 1 0.01191 D . 05 ! 46 32570.00000 0.05524 130 DUP050307373 . `nt>' : IS LANCASTER LABORATORIES K,Name: 9627Q04T62 iuh*; 18 2583226 4^S=>FL. til' * . 10 0-1 00, DT50 . 962685720002,8 . : 09/26/96 10:33 INSTRUMENT ID: 0 59 3 r- 1 1. F. M A<? ~Z~Al As _3 __8 a "J5 fr Ca 3d _Jlo 3;r Cu Fs. __ K __Ma > Na J'b Z'.-,b _ ~Sn r* .. "li r1 v TZy- /n AV6 (ppm) SSRSD #1 0.00006 672.5 0.00204 6 0.9 0 -0.00243 33.2 6 0.01482 4.26 r 0.00271 0.666 -0.00039 52.78 1.25155 0.214 -0.00023 1 S'. 68 -0.00026 146.9 0.00023' 87 . 64 0.00049 20.89 0.02629 39.97 0.14798 0.088 0.54353 0.490 0.01558 0.404 0.00114 24.43 0.90067 4.913 0.00022 16 0.7 -0.00067 21.91 0.00141 7 8.10 -0.00058 224.4 0.00343 23.97 0.01044 0.165 -0.00027 56.89 -0.00027 327.0 -0.00020 103.5 32691.00000 0.206 0.00761 5.063 ~o. 00044 0. 0 017 2 -0 . 00153 0. 01410 0. 00270 -0. 00015 1. 24932 -0. 0001 9 0. 00002 0 . 00040 0. 00041 0. 01416 0. 14800 0 . 54113 0 . 01562 0 - 000 9 6 o. 93750 -0 . 0 0 0 1 9 -0 . 00078 (1. 0001 6 -0. 00 119 0 . 0 04 1 4 0 . 01045 -0 . 00044 0 . 0 0 0 54 -0 . n 0 0 2 9 32734. 00000 0 . 007 29 INTEGRATIONS #2 If 3 . REREAD RED 1 * 0.00021 ' 0.00342 -0.00309 . 0.01505 .0.00273 -0.00046 1.25453 -0.00028 -0,00069 . 0.00029 0.00045' 0.03253 0.14810 0.54640 0.01561 0.00100 0.91292 0.00045 -0.00072 0.00183 -0.00147 0.00362 0.01046 -0.00023 -0 . 00121 -0.00035 32613.00000 0.007 5i 0.00043 0.00099 -0.00269 .0.01 53 0 ' 0.00270' -0.00055 1.25081 -0.00023 -0.0001 1 0.00000 0.00060 0.03219 0.14784 0.54307 0.01551 0.00146 0.35158 0.00041 -0.00050 0.00224 0.00091 0.00253 0.01042 -0.000 i 4 -0.00014' 0.00003 3 27 26 ,-OOGOO 0 . [10 8 0 d 131 DUP050307374 P'aae : 2 0 LANCASTER LABORATORIES -lun I'iame : 9627004T62 Tube: 19 2583222 R-^5^ 100-100.DEI.962685720002.8 0 9/2 6/96 10:38 INSTRUMENT ID: 05938 EL EM ___A a ___A1 __ As __ ;& __ 8 a B& X^a XCd __ Co __ Cr ___Cu __ F 6> __ K __ Ma __ Mn __Mo __ N a __ Ni __ Rb __ Sb __ So __ Sr, Sr__ Ti __ TI 'y Y }. i*i AV6 (ppm) %R1SD 0.00004 8 2.14 0:00922 15.43 -0.00131 2 27.1 0.05169 2.176 0.02865 01178 -0.00098 2.010 .283.82244 0 . 1.26 -0.00025 7 7.49 0.00095 40.70 0.00045 3 7.39 0.00069 16.54 -0.09721 7.900 3.58104 0.633 97.98741 0.208 0.35612 .0: 168 0.0013 1 97 .36 45.73367 0.417 0.01019 5.911 0.00083 127.6 0.00264 74.55 0.02413 2.251 0.00056 1-7 9.9 0.59197 0.228 -0.00082 5.610 0.00074 208.7 0.00007 4 3 1 . 0 31574.33393 0.06 2 0.00 85 5 6.0 3 9 ' INTEGRATIONS #1 #2 #3 REREAD REDID 0.000070.01077 -0.00449 0.05078 0.02-872 -0.00098 288.52819 -0.00019 0.00139 0.00042 0.00080 -0.10551 3.60719 98 . 1 9248 0.35597 0.00061 45.. 93 142 0.01079 -0.00014 0.00140 0.02367 -0.00043 0.59349 - 0.0 0 0 8 l 0.00002 0.00033 31 565.00000 0.00894 0.00000 0;00889 0.00142 0.05134 0.02865 -0.00096 288.70834 -0.00010 0.00072 0.00064 0.00057 -0.09036 3.56691 97.78468 0.35561 0.00053 45.54958 0.00958 0.00196 0.00491 0.02473 0.00052 0.59091 -0.00086 0.00 2 53 0.00018 31597.00000 0.00796 ' 0.00004 0.00798 -0.00087 0.05294. 0.02862 -0.00100 289.23080 -0.00045 0.00072 0.00030 0.00070 -0.09575 3.56902 97.98508 0.35679 0.00278 45.73502 0.01019 0.00067 0.0 0 1 6 0 0.0239? . ' O.OO15 9 0.59151 -0.0007" -0.00032 -0.00028 315 6 1 .00000 0 Cl 0 r. 7 4 VlA. !;...... 132 DUP050307375 LANCASTER' LABORATORIE S un Name: - 9627.004T6 2 rube: 20 2S83223 R.SH Ci F >* **' 1 0 0 -1 0 0 . D F 1 0.9 6 2 6 8 5 7 2 0 0 Q 2.8 , f 09/26/96 10:43- INSTRUMENT ID': 0593c- r L E11 AUG (ppm) %RSD ___Ag ' - 0.00039 43.59 '__A 1 G-. 00S12 29 . 1 2 As -0.00219 52.94 0.04074 0.637 ___3 a 0.00495 0.86 9 Be ^. -0.00069 21.06 -qfcCaTV 20.7 2910 0.353 -iCd --0.00028 24.65 __ Co 0.00069 33.77 __Cr . 0.00036 26.64 Cu 0.00076 19.36 __ Fe 0.03298 1 T.7 8 __ .K 0.42713 0.130 __Mg 8.12536 0. 183 __ Mn 0.07674 0.109 Mo 0.00150 27.01 V-Na 5.95420 0.957 __N i 0.00108 29.52 i-b 0.00025 74. 15 __ ,Sb ' 0 . .0 0 0 9 9 261.9 0.00223 80.50 __ Sn 0.00163 96.28 'ir 0.14814 0.143 Ti -0.00013 44.79 __T1 0.00249 119.5 y -0.00001 1 698 . __ Y 32310.00000- 0.229 __kn 0.00790 4.7 59 INTEGRATIONS #1 #2 0.00059 0.00629 -0.00350 ' 0.04104 0.00492 -0.00056 20.81195 -0.00033 0.00052 0.00047. 0.00093 0.03668 0.42660 8.14179 0.07684' 0.00154 5.97717 0.00133 0.00041. 0.00373 0.00043 0.00344 0.14837 -0.00007 0.00215 0.00014 2391.00000 0.008 8 2 0.00029 0.00426 -0.00184 0.04056 0.00500 -0.00068 20.67307 -D.00020 0:00095 0.00032 0.00071 0.02893 0.42771 8.11282 0.07668 0.00107 5.49614 0.00119 0.00004 -0.00145 O'.00402 0.00072 0 . 14795 -0.00 0 1 9 -0.00 030 -0.00025 32294.00000 b.00 7 5 9 #3 REREAD REDIG 0.00029 ________________ 0.00782 -0.00125 0.04062 0.00493 -0.00085 20.70228 -0.00031 0 .00059 0.00029 0.00064 _______ 0.03331 _ 0.42707 8.12148_____________ __ 0.07672 0.00188 5/88928 , 0.00072 0.00030 _______ ________ 0.0007 1 _______ _ 0.00223 0.0007 2 ; 0.14810 -0.00015 0.00563 0 . ooo 0132245.00000 0.00 7 7 0 ____ 133 DUPO 503 07376 LANCASTER LABORATORIES Tun Name: 9627004T62 Tube: 21 2583224 ****, lOO-100fDF10t 962685720002r8: . 09/26/96 10:48 INSTRUMENT ID: 0 59?-6 EL EM ___Aa ___A'l As ___B ___3 a __ Tie Ca __ Cd Co __ Cr ___Cu ___Fe ;__ k __ Mg __ Mn ,,__Mo _2(LNa . Ni ___rb ___Sb ___$& ___$ n ___Sr~ Ti ___11 \, ___Y __ Zr> AVG (ppm) %RSD 0,00021 62.48 0.00073 481.1 -0.00205 29.50 0.03423 2.418 0.00432 1.621 -0.00041 91.90 ' 18.95 27 6 1.480 -0.00017 77.50 0.00026 146.5 0.00020 284.3 0.00059.42.72 0.01209-80.64 0.39336 1.121 7.39882 1.478 0.06766 1.484 0.00088 41 .39 5.43372 2.198 0.00121 37.18 0 . 6 0 1 3 9 "105.0 0.0025Ci 96.6 8 0.00067 157.8 0.00191 145.9 0.1-3506 1 . 455 -0.00028 15.12 0.00218 143.3 -0.00020 187.6 32571.33398 1.321 0.00158 6.158 #1 0.00015 -0.00008 -0.00145 0.03422 0.00438 -0.00070 . 19.13923 -0.00010 0.00015 -0.00029 0.00035 0.00084 0.39831 7.46145 0.0 6 8 4 0 0.0 0 1 2 7 5.49486 0 . 00090 0.00284 -0.00003 0.00.16 9 0.0 0 1 5 7 0 .13 6 5 8 -0.00033 0.00319 -0.00015 3229 1.. 00000 0 . 00173 INTEGRATIONS *2 #3 REREAD REDIG 0.00012 0.00459 -0.00204 0.03506 0.00435 -0/00055 19.08905 -0.00033 -0.00005 0.00007 . 0.00089 . 0.01811 0.38987 7.46254 0.06807 0.00053 5.29609 Ci.0017 3 -0.00009 0.00 27 5 0.00077 -0.00069 ' 0 . 13576 -0.00027 -0.00132 -0.00061 2556.00000 0.00153 0.00036 -0,00230 -0.00 26 6 0.03340 0.00424 0.00001 18.63001 -0.00008 0.00068 O'. 0.008 2 0.00083 0.017.34 0.39189 7.2724? Q.06652 0.00085 5.51020 0.00101 0.00144 0.00478 -0.00043 0.00488 0. 13 2 8 4 -0.00024' 0.00469 0 .0001 5 33067.00000 0. fi 01 4 8 134 DUP050307377  aae : !L$ ' $ ; r *$X "#$$"#%; s - %un N3m: Tube: 22 9627004T62 ' CCV - 09/26/96 10:53' INSTRUMENT 10: 0 593 6 LLEM Aa AT AS B 8a Be C Cd Co Or Cu Fe __ K Ma Mri Tlo Na Ni P? sb_$&* _Sn Sr Ti __ T) V 1Y 2n Ave (ppm) RSD 0.53294 0.077 24-61204 0.120 0.52193 0.109 0.52130 '0.390 0.50503 0 . 1 25 0.51407 0.250 25.17161 0.179 0.51369 0.156 0.51301 0.134' 0.49515 0.198 0.52098 0.182' 24.82878 0.217 25.51037 0.298 24:73406 0.114 0.51703 0.06? 0.49726 0.644 25.09176 0.367 0.51500 0.505 0.51120 0.700 0.48145 1.144 0.51018 0.904 0.50026 0.788 0.49569 0.069 0.50262 0.016 0.51391 1 .598 0.49888 0.236 32370.33398 0.212 0.51404 0.678 #1 0.5332.1 24.57927 0.52256 0.51899 0.50434 0.51555 25.22150 '0.51406 0.5-132 8 0.49615 0.51996 24.88122 25 .'43145 24.72581 0.51735 0.49358 25.00158 0 . 5 1736 0.5070" 0.47594 0.5066 6 0.50349 0.49534 0.50257 0.50668 0.50012 3 2408.0 00 0 0 0.51785 INTEGRATIONS *2 0.53247 24.63688 0.52143 0.52284 0.50516 0.51326 25. 13336 0.51277 0.5135-1 0.49419 0.52184 24.77344 25.58325. 24.71075 .0.5166.6 0.49934 25.18581 0.51221 0.51324 0.48146 0.50845 0.49587 0.4957 1 0.50259 0.51221 0.49777 3?4 1 ? . 00000 0:51099 S3 ' REREAD REDIG 0.53316 - 24.61997 0.52180 0.52208 0.50558 . 0.51339 25.1599? 0.51424 . 0.51 222 0.49509 0.52115 24.83168 25.51641 24.76561 0.51709 0.49888 25.08788 0.51544 0.5133 0 0.48696 0.51541 0.50144 0.49602 0.50272 0.522 8 4. 0.49876 32291.00000 0.51329 135 DUP050307378 rage: 24 LANCASTER LABORATORIES l,'un Name: 9627G04T62 f ube : 23 CCB 09/25/96 10:58 INSTRUMENT ID: 0593f, AVG INTEGRATIONS 1 LEM (ppm) %RSD #1 #2 #3 REREAD REDIG Act 0.00052 46.84 0.00080 0.00044 0.00033________________ __A1 0.01247 40.43 0.-01 739. 0.01272 0.00731 AS 0.00011 2023 . 0.00166 0.00127 -0.00259 _______ _______ "__8- 0.00831 7.089 0.00896 0.00813 0.00783 _ Ba -0.00017 69.63 -0.00004 -0.00019 -0.0002? Be -0.00032 57.56 -0.0001 2 . -0.00049 -0.00034 ______ _ Ca -O'. 00282 215.7 0.00411 -0.00529 -0.00729 ________________ Cd- ' -0.00010 56.27 -0.00003 -0.00015 -0.00013 _ A __ Co Cr 0.00005 822.2 - -0.00004 1 288 . 0.00039 Q.00044 0.00024 -0 ,-0 0 060 , -0.00047 0.00004 Cu 0.00070 33.85 0.00098 ' 0.00061 0.00052 Fe 0.04219 IS. 56 0.04913 0.04229 0.03515 __ X 0.11157 1.016 0.11261 0.11036 '0.11174 __ Mg 0.02739 1 9.43 0.03268 0.02747 0.02203 __ Mn .0.0003-4 1 2.2.9 0.00039 0.00031 0.00031 _______ _______ __ Mo 0.00212 84.88 0.00355 0.00272 0.00009 _ ___N a Ni A __ Pb 0.09328 64.7 3 -0.00002 960.5 0.00028 608.6 0.02635 0.00016 0.00161 0.10931 0.00009 0.00091 0.44369 _______ -0.00033 -0.00 1 67 __ Sb 0.00227 S G . 6 2 0.00095 0.00305 0.00281 _________ __ Se 0.00190 10 0.2 0.00187 0.00001 0.00383 _______ ________ Sn Sr tt T1 __ V __ Y __ Zn 1 - 0.00198 71.07 0.00038 23.5 0 -0.00006 225.5 0.00254 10 2.4 -0.00.013' 13 5.3 32862.33203 0.3 23 0.00088 53.33 0.00191 0.00048 0.00010 u.0 0 0 2 8 -0.00008 32983.00000 u.U0038 0.00060 0.00033 -0.000 1 1 0.00195 -0.00033 32782.00000 0.00095 0.00342 '0.00032 -0.00018 0.00539 _______ 0.00001 3 2 8 2 2.00 00 0 _______ 0.00132 _______ t 136 DUP050307379 />< : 25 LANCASTER LABORATORIES :un Name: 9627004i&2 Tube : 24 2583226 100-100.BF1.9626857 20002,8, 09/26/96. 11:03 INSTRUMENT ID: 05936 -.LEM Aa .... At As B Ba Be >Cca yCCd Co Cr Cu Ee K Mci Mn Mo Na __ N i Mb Sb Se 5n Sr Ti __ T1 V __ r __ in AVG (ppm) SJRSD 6.00019 190.2 . 0.02369 16.87 0.00098 159.4 0.46014 0.. 167 0.15861 0.227 -0.00071 9.891 69.418.49 0.259 -0.00015 123.8 0.0 0247 8.715 0. COOS 2 49.27 0.00096 '23 vS 8 0.03679 31.94 2.87729 0.348 28.75773 0 . 261 0.82685 0.140 0.01121 5.003 52.18195 0.434 0.00646 8.088 0.00110 147.1 0.00092 102.2 0.00123 202.7 0.00000 19 649 0.55459 0. T69 -0.00033 25.17 -0.00014 2 932 . 0.00115 10.38 32117.66601 0.311 0.01359 2.474 #1 0.00051 0:03414 -0.00082 0.45926 0.15844 -0.00079 69.55384 -0.00015 0.00272 0.00105 0.00106 0.04260 2.87428 28.79821 0.82739 0.01064 52.07189 0.006730.00091 0.00020 0.00400 0.00060 0.55465 -0.00026 -0.00041 0.0012' 32010.00000 0.01396 INTEGRATIONS #2 #3 RREREAD REDID -0.00022 0.00030 0.02486 ' 0.02707 0.00193 0.00184 0.46067 0.46050 0.15836 - 0.15902 -0.00068 -0.00066 69.21578 69.48085 0.00003 -0.P0033 0:00234 0.00235 0.00035 0.00105 ' 0.00070 0.00111 0.02326 0.04450 2.85911 ' 2.88847 28.67081 28.80416 0.82552 0.82766 0.01176 0.01122 52.03 108 52.44289 0.00679 0.00586 -0.00041 0.00281 0.00199 0.00 0 5 8 -0.000.89 0.00059 -0.00121 0.00059 0.55362 0.55549 ' -0.00042 -0.00031 -0.00420 0.0041 9 0.001 13 0.00104 32208.00000 0.01330 3213S.00000. 0.01851 13? nja?. DUP050307380 . Page: 2 6 .LANCASTER LABORATORIES Run Name: 9S27004T62 Tube: 25 2533226 Up**_ ioo-100,DF;1 .962585720002.8. . . 09/25/96 INSTRUMENT ID: 1 1:08 0 5 93 6 ELEN - Aa __ AT As 8 8a . Be Ca Cd ___Co ___Cr ___Cu __ Fe __ K Mo __ Mn .__ Mo -__ Na :__ Mi fib _5b Se __ Sn Sr __ Ti ___T1 __ V___Y __ 2 n AVG (ppm) %RSD m 0.02403 0.826 0.02421. 0.48649 0.802 0.48800 0.02197 15.19 ' 0.02467 0.69015 0.324 - 0.69267 0.61697 0.166 0.61749 0.01084 0.278 0.01085 69. 17506 0.200 69.33288 - 0.01140 0.566 0.01144 0.11855 0 ,-547 0.11929 0.02252 1 . 250 0.02278 0.05914 0.300 0.05923 0.26944 2.153 0.27588 5.10144 0.304 5.11917 29.31002 0.159 29.36369 0 . 3 4 S 2 3 0.110 0.84728 0.. 2 2 573 0.671 0.22452 53.27803 0.283 53.44601 0.09829 1.393 0.09982 .0.01 17 3 10.49- 0.01315 0.12402 2.362 0.12739 0.01179 15.07 0.01115 0.61524 0.212 ' 0.61667 0.56731 0.118 0.56777 0.11255 0.193 0.11280 0.02284 13.42 0.02492 0.11263 0.206 0.11255 32174.00000 0.172 312207.00000 0 . 1 ' 444 ; 0 . 169 0.11428 INTEGRATIONS #2 #3 REREAD R E 0 10 0.02381 0.48206 G.0'2300 0.68939 0.61579 0.01087 69.12454 0.01143 0.11805 0.02256 0.05894 0.26461 5.09010 29.27832 0.84549 0.22524 53.23464 0.09785 0.01093 0 . 1 2 2 57 . 0.01380 0.61493' 0.5S654 0.11244 0.01932 0.11289 32205.00000 0.11464 0.02405 0.48942 . .0.01823 0.68839 0.61763 - 0.01081 69.07075 0.01133 0.11832 0.02222 -0.05926 0.26783 5.09504 ' 29.28806 0,84591 0.22743 53.15343 0.097 1 9 0 .. 0 1 1 1 2 0.12210 0.01043 0.6141? 0.56762 0. 112 4 0 0 . 02428 0.11244 3 21 10.00 00 0 0.1144 1 138 Vl* t', S' if '*rV DUP050307381 > n '' <' LANCASTER LABORATORIES ;^ur, n t iio : 9627004T62 Till'''' 0 '* * ' | ' 26 i 0 0- ' 2583226 } 1 0 0.D F 1 .962685720002.8. 09/26/96. 11:13 INSTRUMENT ID: 0 5 93 6 EL F.M _____Aa H$ 1 _A bw __ Cr Cu f K Ho (v; r * Mo ri a N -i sP s? :-n Sr 1i 11 \ 7n AVG ' fppm) %kSD O.00022 52.37 0.01947 58.17 -0.00138 265.0 0.-45826 .5.286 0.16059 5.495 -0.00147 7 0.40 70.17050 5.570 -0.00022 80.38 0.00264 12.71 0.00043 34.8/ 0.00045 108.0 0.04223 6.416 2.93895 4.26 1 . 29.07451 5.552 0.83056 5.497 0.01128 4.886 52.50991 4.311 0.00755 17.46 -0.00006 344.0 0.00212 7 0.41 0.00241 21 .40 0100048 518.1 0.55 243 5.509 -0.00030 46.78 0.00009 .3092. 0.00079 32.49 31312.66601 4.255 0.01074 10.29 INTEGRATIONS #1 #2 43 REREAD RED] G- 0.00023 0.01327 0.00124 0.44403 0.15503 -0.00081 67.53324 -0.00029 0.00256 0.00057 0.00082 0.03936 2.86170 28.04346 0.80038 0.01062 51 . 19250 0.00622 -0.00032 0.00304 0.00301 -0.00025 0.54258 -- 0 , 00 0 2^ 0.003 1 5 0.0 0 0 5 5 32164.00000 0.00990 0.0-0032 0.01259 -0.00558 0.44452 0.15617 -0.00094 68.31658 -0.00037' 0,00301 0.00046 0.00065 0T 04258 2.87171 28.24438 0.80822 0.01138 . S1.2 13 11 0.00758 -0.00003 0.00039 0.00207 0.00328 0.'54658 -0.00019 -0.00287 0.001.06 31997.00000 0.01034 0.00009 0.03254 0.00017 . 0.48623 0 . 17086 -0.00268 74.66168 -0.00002 0.00235 ' 0.00027 -0.0G010 0.04475 '3.08344 30.93500 0.88309 0.01169 55.12412 0.00886 0 . 0001 5 0.00293 0.00216 -0.00157 0.59814 -0.00046 0.00001 0.000? r, 29777.00000 0.0 1 ? 0 0 13 DU PO50307382  'age: 28 LANCASTER .LABORATORIES V Run Name: 9627004T62 Tube : 17 2583226 R.-D^F-S , 100- 100.DFl.962685720002,8. 09/26/96 INSTRUMENT ID: 1 1 : 18 05936 EL Efi Aa ___A1 As B 8a Be Co ___Cr ___Cu ~T e __ K Ho ___Mn __ Mo __ Na Ni ___Pb __ Sb __ 3e Sn Sr Ti ___T1 y __ Y __Zn AVS fjapm) ' %RSD #1 INTEGRATIONS t2 0.05442 0.153 2. 1351 1 0.205 0.04250 '5.952 2.57028 0.039 2.25334 0.122 0.05241 0.020 72.81276- 0.066 0.05247 0.087 0.53436 0.108 0.20519 0.055 0.27218 0.230 1.0690-8 0.477 7.06222 0.545 30.54917 0.141 ' 1.35123 0.144 - 2.07108 0.439 55.72035 0.207 0.54164 0.3 9*5 0.02122 3.323 0.52450 0.317 0.01167 10.33. 4.27932 0.2 7 4 1.61659 0.213 1.05225 0.092 0.05169 10.79 0.51510 0 1 0 8 31893.33398 0.128 0.53365 0.36 0.05439 0.05436 2.13249 2. 13266 0.04018 0.04520 2.57027 2.56925 2.25573 2.25033 0.05242 0.05240 72.84292 72.75659 0.05249 0.05241 0.53495 . - 0.53433 0.20529 0:20507 .0.27 27 2 0.27149 1 . 0.6424 1.06859 7.10190 . 7.02490 30.55803 30.50226 1.35159 . 1 .34919 2.06340 2.06872 55.83846 S5.60683 0.53926 0.54340 0.02203 0.02077 0.52639 0.52323 0.01032 0.0126-5 4.27 66 6 4.26915 1 .62020 1 . 0 524 7 1.61331 1.05119 0.04525 0.5151? 0.0 548 6 0.51453 31 930.00000 31901.00000 0.53137 0 . 53473 #3 REREAD RED 16 0.05452 2.14020 0.04212 2.57130 . 2.25397 0.05242 72.83878 0.05249 Q.53379 0.20522 0.27232 1.07442 7.05986 30.587 1 9 1.35305 2.08112 55.71576 0.54225 0.02085 0.52389- 0.01205 4.29214 1 . 61628 1 . 05809 0.05497 0.51565 81649.00000 0 . =18 4 8 140 DUP050307383 VsCJ* ' - 29 LANCASTER LABORATORIES un Nmet 9627004T62 rub6)1 28 2583226 100-1 00,0F5..962685720002,8, . 09/26/96 11:23 INSTRUMENT- ID: 05936 1 LE11 A A'l As 8 Ba 1.S& Ca Cel J"Co Cr Cu K Ma Mn MO Na Ni Pb __ Sb S 6) 5n. Sr 1i ri v Y 2r. AVG (ppm) %RSD '0.00042 45.76 0.00625 3 8.19 -0.00200 149.0 0.09701 1 . 538 0.03136 0.434 -0.00041 10.73 '13.65068 0.236 -0.00015 61.49 " 0.00108 10.30 0.00038 99.93 0.00066 13.03 0.03579 21.20 0.59071 0.462 5.60650 0.266 0 . 16380 0.181 0.00550 3 7.91 10.07317 0.812 0.00204 43.32 0.00002 8275. 0.00072 17 8.7 0.0021 9 74.28 0.00566 19.86 0.10916 0.182 0.000 14 135.3 -0.00116 150.6 0.00025 13 3. 1 32621.66601 0.298 0.00925 5.905 INTEGRATIONS #1 #2 0.00024 0.00359 -0.0042-1 0.09757 0.03131 -0.00043 13.62085 -0.. 00021 ' 0.00117 0.00039 0.00060 0.02739 0.59012 '5.59001 0.16357 0.00787 9.98863 0.00146 -0.00045 0.00123 0.00291 0.0044? 0.10907 0.00003 -0.00159 -0.00 0 1 2 32698.00000 0.0 0 9 -? 5 0.00040 0.00695 -0.00318 0.09814 0.03151 -0.00043 13.63615. -0.00021 0,00096. 0.00000 0.00076 0.04215 0.53833 5.61908 0.16369 0.00469 10.15210 ' 0.00307 -0.00139 0.00170 0.00333 0.00663 0 . 1 0938 0.00038 0.00076 0.00037 32S 1 2.00000 0.0 [i 8 6 6 #3 RRIEREAD RED !tS 0.00062 0.0 0 820 0.00139 '0.09531 0.03125 -0.00036 13.69503 -0.00004 0.00110 0.00075 ' 0.00062 0.03784 0.59369 5.61040 0.16413 0.00393 10.07877 0.00161 0.00191 -0.00075 0.00032 0.00593 0 . 10902 0.0000? -0.00266 0.00051 32655.00000 0 .00974 141 DUP050307384 -ape : 30 LANCASTER LABORATORIES un Name: 9627004T62 lube: 29 2583227 At,xx _ 1 00- TOO,DF10,962685720002 .. 8 , . 09/26/96 11:28 INSTRUMENT ID: 05936 !'.LEM' Aa AT As B Ba Be GX Cd __ Co Cr __ Cu Fe __ K Ma __ Mn __Mo ^.Na _Ni rb ___Sb __ Se ,___Sn __ Sr Ti ___II __ V __ Y __ Zn AVG (ppm) SSR'SD 0.00031 0.01690 0.00160 0.01225 0.00760 -0.00074 22.06639 -0.00015 -0.00023 0.00063 0.00049 0.03151 0.34532 8.78118 0.02071 0.00120 5.49323 0.00163 -0.00085 0.00260 0.00262 0:00559 0.07112 0.00020 0.00307 0.00029 32154.66601 0.00406 42.97 7.125. 80.34 6.311 0.367 25; 54 0.399. 118.6 261.2 49.24 19.62 213.37 1.117 0.310 0.173 39.09 2.160 27.02 i 74.7 59.87 2 5 .39' 33.92 0.435 51 .83 75.95 A Ci 3 ? . 0.272 13.32 SI 0.00016 0.01630 0.00081 0.01256 0.00758 -0.000.66 22.01223 -0.00004 -0.00094 ' 0.00033 . 0.00038 0.03813 0.34197 8.78346 0.02068 0.00171 5.37773 0.00127 0.00038 0.-00 0 87 0.00313 0.00578 0.07133 0.00008 '0.00038 0.00038 3 2130.00000 0.00345 INTEGRATIONS' . #2 S3 REREAD 0.00034 0.00042 0.01829 0.016T2 0.00308 0.00090 0201137 0.01281 0.00763 0.00759 -0.00096 -0.00060 22216800 22.01895 -0.00035 ' -0200005 0.00022 0.00000 0.00095 0.00062 0.00057 0.00051 0.04060 0.01579 0234954 0234446 8.80728 8.75281 0.02075 0.02069 0.00112 0.00078 5.61485 5.48711 0.00212' 0.00149 '-0.00251 -0.00044 0.00390 0.00302 0.00187' 0.00286 0.00739 0.00361 0.07126 0.00027 0.07076 0.00025 0.00423 0.00461 0.00034 32082.00000 0 . 0 fi 4 A 1 0.00016 32252.UOOOO 0.004 3 8 142 DU PO50307385 , '(!<' : 31 LANCASTER LABORATORIES Name: 9627004T52 30 2583330 3dC>XS . , 100-100,DF10,962685720002,8, , 09/26/96 INSTRUMENT ID 11:33 - 0 5 936 ( I. r M Ag A1 ~' At It IS a Itf? C4 '"cu 1.', o or i;u 1"** K Mp Mn HO 'V Nri ^ N1 I'D _:.r* ' ,Cs * j r 'r 11 - --11 V r ' r* AVS . . (ppm) %RSD #1 INTEGRATIONS #2 0.00028 133.1 0.00234 49.36 -0.00219 .184.8 0.03801 0.696 0.01076 0.456 -0.00058 10.75 6.67135 0.576 -0.00038 42.26 0.00023 108.4 0.00014 232.4 0.00051 42.94 0.04558 10.91 0.54630 0.303 2.3'6404 0.405 0.02354 0.633 0.00129 40.34 4.61200 2.181 0.00007 1 0 2 2. 0.00006 17 17. 0.00166 128.0 -0.00029 705.7 0.00384 42.74 0.05147 0.160 -0.00018 6 5.61 0.00243 178.9 -0.00017 266.2 32494.33398 0.375 0.00741 10.7;; 0.00021 0.00287 . -C.00095 0.03774 0.01071 -0.00052 6.63216 -0.00051 -0.00004 -0 .-00021 ' 0.00026 - 0.04950 0.54443 2.85079' 0.02337 0.00076 4.55293 -0.00037 0.00035 0.00313 0.00022 0.00194 0.05139 -0.00020 0.00674 -0.00074 32634.00000 0.00713 0.00069 0.00313 0.00109 0.03827 0.01075 . -0.00064 ' 6.70901 -0.00020 6i0 0045 0.00047 0.00064 ' 0.04726 0.54759 2. 85884 0.02365 0.00129 4.72815 -0.00037 . 0.000 96 -0.00078 -0.00261 0.00475 0.05147 -0.00005 0.00255. 0.00021 32441 .00000 0.00680 #3 REREAD RED 10 -0.00005 0.00101 -0.006720.03801 0.01081 -0.00057 6.67288 -0.00044 0.00030. 0.00018 . 0.00064 0.03999 0.54688 2.87249 0.02361 0.00180 4.55491 0.0 0 0 97 -0.00 1 13 0.00264 0.00149 0.00483' 0 . 05155 -0.00030 -0,00198 0.00000 32408.00000 0.008 8 1 143 * > * IT TStnv < ; DUP050307386 '-'aae: 3 2 LANCASTER LABORATORIES '<un Nam: 9627004T62 f ube: 31. CRI 09/26/96 11:38 INSTRUMENT ID: 05936 L E M' AVG (ppm) &R3D #1 INTEGRATIONS #2 #3 REREAD REDIG Aa 0.02244 4.214, 0.02195 0.02353 0.02184 __ AT. 0.00588- 138.4 0.00431 0.01470 -0.00136 As ' 0.0Z14S 8.284 0.02324 0.019S8 0.02154 __ B 0.00417 6.669 0.00413 0.00446 0.00391 __ Ba 0.00005 133.3 0.00013 -0.00005 . -0.00001 __ Be 0.00992 3.073 0.00997 0.00959 " 0.01019 __ Ca -0.04507 5.299 -0.04308 -0.04442 -0.04772 __ Cd Q . 0 10 13' 3.626 0.00986 0.01.055 - 0.00997 A __ Co ___Cr 0.-10-994 4.386 0.02112 3.401 0.10656 0.02066 0.11546 0.02195 0.10780 .0.02.075 ___Cu 0.05532 3.67 1- 0l. 05375 0.05761 - . 0.05459 __ F 0.03485 29.63 0.04050 0.04113 0.02293 __ K 0.10316 8.415 0.09313 0.10801 0. 10833 ___Mg 0.01407 14.90 0.01259- 0.01647 0.01314 __ Mn. 0.03281 4.216 0.03173 0.03437 0.03232 __ Mo -0.00019 226.4 0.00029 -0.00055 -0.-00032 __ Na 0.14526 45.87 0.15038 0.21119 0.07720 __ Hi 0.08754 4.124 0.08547 0.09171 0.0 8544 _Pb O'. 00603 12.75 0.00522 0.005 1 1- 0.00676 ___Sb 0.12344 4.714 0.12034 ' 0.13016 0.11984 ___Se A __ Sn 0.01049 5.481 0.00001 5971 . 0.01115 -0.00081 0.01022 - 0.00044 O'. 0 100 9 0.00040 Sr 0.00007 51.75 0.00012 0.00007 0.00004 Ti -0.00020 29.33 -0.00018 . -0.00015 -0.0 00 2-6 __ TI 0.02258 1 1 . 7 2 0.02150 0.02560 0.02065 v __ Y ___Zn 0. 10738 4.3 57 32159.00000 3.377 0.04385 4 . i 00 0.10414 33018.00000 0.04234 - 0.11274 30938.00000 0.04584 0. 105 25 3-25 2 1 .00000 0.0433 7 144 DUP050307387 *'3 CJ ' LANCASTER LABORATORIES Run Nae: Tube : 32 9627004T62 ICSA 09/26/96 11:43 INSTRUMENT 10: 059 3 c- ELEM Aa Al As a ' Ba Be c Cd Co Cr Cu ' f K Ma lln no Ns Ni Pb "ito .j t-'Sn Sr Ti T1 V T Zn AVG (ppm) %R$Q #1 ' -0.00004 821.2 526.69573 0.020 ' -0.00268 143. r 0.01583 6.443 0.00856 0 .-666 -0.00081' 25.25 520.72332 0.290 . -0.00291 20.34 0.00059 27.64 0.00116 14.04 0.00006 592.2 . 207.48063 0 . 142 0.09966 ' 2.309 530.87548 0.069 O'. 0 063 9 1 .659 -0.00140 75.84 0.1 1669 35.52 0.00045 50.14 -0.00125 235.0 0.00822 45.10 -0 . 0 09'84 3 6.29 0.00598 25.24 0.02115 0.209 -0.00134 7.073 -0.01600 35.13 -0.00398 16.97 29716.66601 0 . 252 0.00349 29.10 0.00016 526.57269 -0.00253 0.01693 0.00857 -0.00075 520.14349 -0.00345 0.00046 0.0.0133 0.00014 207.46932 0.10103 530.67218 0.00650 -0.00094 0.13665 0.00020 -0.00226 0.00754 -0.01378 0.00754 0.02119 -0.00129 -0.01020 -0.00362 29707.000C0 0.00452 INTEGRATIONS #2 #3 REREAD REDIG 0.00020 -0.0005-1 526.74932 526.76525 -0.00660 0.00108 0.01565 0.014-91 0.00861 0.00850 -0.00105 . -0.00065 519.58526 522.44128 -0.00301 -0.00227. 0.00077 0.00054 0.00114 0.00101 -0.00033 0.00037 207.19056 207.78201 ' 0.09700 O'. 1 0094 531.29852 530.65582 0.00629 0.00639 -0.00065 -0.0026-2 0.06903 0.14439 0.0006.3 0.0005 t 0.00207 -0.003 58 0.01223 0.00490 -0.'00893 -0.00681 0.00586 0.00453 .0.02114 0.0211 1 -0.0012S -0.00145 -0.01639 -0.0214 2 -0.0 047 6 ?o f ,44 00000 -0 . 00355 29799 . GOOD I' 0.00347 0.00249 145 DUP050307388 LANCASTER LABORATORIES' -;un Name: 9627004T62 Tube: 33 ICSAB 09/26/96 11:48 INSTRUMENT ID: 0SQ36 EL EM Aa A1 . As 8 Ba Be C<3 Cd ___Co Cr Cu Fe _J<. ....Mg __ Mn _ Mo . Na __N 1 __ Pb ___Sb __ Se ___Sn __ Sr Ti T1 __ V Y __ Zn . AVS (ppm) XRSD . ` 0.22971 0.880 522.99114 0.500 0.10970 3.336 0.03186 2.337 0.55326 0.542 0.50675- 0.717 518.00872 O'. 939 0.99863 0.822 ' 01.52261 0.610 0.500S7 0.782 0.58867' 0.340 205.95799 0.693 0.10210 6.540 525.88616 0.581 0.527715 0.656 0.00185 57.63 0.22579 5 5.25 1.01541 0.863 0.05060 2.237 0.52549 0.852 .0.04213 1.6"! 6 0.00649 58.23 0.02100 0 . S 69 -0.00116 7.208 0.09617 5.228 0.51439 0.763 29999.66601 0.831 0.97960 0.635 #1 " . O'. 23202 525-. 98333 0.11271 0.03217 0.55662 0.51094. 523\60552 1 . 007 93 0.52594 0.5.0487 0.59070 207'i 60704 0 . 10979 529.38653 0.53175 0.00078. 0.3534 7 1.02544 0.05076 ' 0.61380 0.04215 0.01073 0.02116 -0.00106 0.09067 0.51891 29716.00000 0.98670 1NTE8RATI0NS #2 0.22829 521.12577 0.10562 0.03101 0.55085 0.50481 515.67205 0.99561 0.52233 0.50003 0-.58669 205.16569 0.09869 523,74981 0.52586 .0,00184 0.22446 1 . 00922 0.04939 0.62629 0.04145 0.00345 0.02091 '-0.00120 0.09731 0.51240 30184.00000 0.97701 ' #3 ' , REREAD REDID-' 0.22881 ;__ 521.86328 0;.1 1 07 5 _ 0.03240 ________________ 0.55230 _______ ______ 0.50449 5V4.74853 '0.99234 0.51957 ____________ 0.49712 0.58861 ______ L _ 205.10124 _______________1 0.09781 _______ ________ 524.52209 0.52565 0.00292 _____; 0 . 0994-1 1.01156 0.0516$ _______ 0.63037 0.04281 0.00530 0.02093 _______ -0.001 22 ______ ; 0.10053 0.51185 30099.00000 0.9 7 5 0 S ____ _______ 146 DUP050307389 1n 'i * : I l'\ LANCASTER LABORATORIES Klin 9627004T62 f rih* ' ,J4 ccv 09/26/96 11:52 INSTRUMENT ID: 05938 tl. EM Vuf//AiKrfrjt ft ''""pm -J--* , **Gel Co rj l i K "TM Hf* Kir*1 Mu `"m 1 f'> Lb '; *- *:i r p *1. r| 1l 7 1 /n AVG (ppm) %RSD 0-. 53460 24-71133 0: 52502 0.52317 . 0.50763 . 0.51530 ' 25.31466 0.51620 0.51603 0.49649 0.52169 24:80064 25.63673 24.71869 0.51910 0.50088 , . 25.04985 . 0.51902 0.51629 0.48416 0.51364 0-. 5 0408 0.49912 0.50404 0.51388 0.50049 32267.33398 0.51562 0 ..593 0.673 0.482 0.388 0.687 0.642 0:777 0:691 0.655 0.739 0.586 0.629 0.772 0.552 0.702 1 . 588 0.601 1.189 0.37 7 1.445 1.193 1.114 0.636 0.667 1.509 0.670 0 ..301 0.755 ' tfl INTEGRATIONS #2 - .#3 REREAD REDIG 0.53402 24.68840 0.52360 0.52132 0.50736 0.51497 25.26742 0.5.1623 0.-51390 0.49451 0.52179 24.76224 25.61780 24.73978 0.51793 0.49388 24.97757 0.51724 0.51685 ' 0.47790 0.50781 0.50627 0.49912 0.S0311 0.50883 0 .49936 3 2 245.0000(1 0.515 5'3 0.53176 24.55760 0.52351 0.52285 0.50429 (0.51217 25.14592 0.51262 0.51426 0:49422 . 0.518.58 24.66723 25.44878 24.57276 0.51617 0.49922 24.94834 0.51394 0.51412 0.48286 0.51306 0.49769 0.49595 0.50124 0.50999 0.49785 32374.00000 .0.51177 0.53803 . 24.88800 0.5279a 0.52535 0.51125 0.51877 25.53092 0.519760.51994 0.50072 0.52470 24.97245 25.84363 ' 24.84351 0.52319 .0.50953 25.22313 0.52589 0.51789 0.49173 0.52004 0.50326 0.50230 0.5 077 8 . 0.52281 0.50427 32183.0onno 0,5 195.6 . 14V DU PO50307390 Page: 36 LANCASTER LABORATORIES Run Name: Tube: 35 9627 004T62 CCB 09/26/96' 11:57 INSTRUMENT 10: 0 5 936 tLEM Aa __ AT As __ B __ Ba Be Ca ___Cd __ Co Cr Cu ___F K --Ms__ Mn __ Ho __ Na Ni __ Pb __ 5b ___$ .__ Sn ___Sr ri __ T1 ___V __ Y __ In AVG (ppm) %RSD 0-.00007 529.8 0.03315 7. 132 -0.00069 341.7 0.00494 12.45 -0.0001 1 1 6. 9 6 -0.00066 30.62 -0.00115 155.7 -0.00028 75.94 -0.00061 35.02 0.00041 22.12 0.00037 83.61 0.03236 10'. 59 0.10466 2.726 0.04028 6.983 0.00018 36.81 0.00167 35.63 0.09540 64.25 -0.00042 177.5 -C. 0.0005 1033. 0.00255 77.43 0.00180 81.78 -0.-000 1 2 958.0 0.00010 24.22 -0.00024 42.91 0.00428 53.86 -0.00015 123.0 3 2324.333 98. 0.39 2 0.00015 367.2 #1.. . -0.0.0015 0.03580 -0.00036 0.0043.2 -0.00009 -0.00046 0.00062 -0.00018 ' .-0.00085 0.000330.00042 0.02845. 0.10143 0.04121 0.00025 0.00180 0.16145 0.00006 0.00009 0.00136 0.00347 0.00062 0.00012 -0.00032 0.00674 0.00006 32462.00000 -0.00034 INTEGRATIONS #2 0.00053 0.03125 . -0.00321 0.00555 -0.00013 -0.00065 -0:00110 -0.00052 -0.00042 0,00040 0.00065 0.03379 0.10569 0.04251 0.00018 0.00220 0.04034 -0.00004 -0.0007 1 0.00483 0.00130 0.00052 0.00010 -0.00012 0.00394 -0.00022 32299.00000 0.0007 8 43' REREAO RED 13 -0.00015 0.03239 0.00149 0.00496- -0.00011 -0.00087 -0.0-0296 '-0.00013 -0.00057 1 0.00051 0.00003' 0.03485 0.10686' 0.03712 0.0 0 0 1 1 0.00100 0.08442 -0.00128 0.00045 0..00145 0.00064 -0.00153 0.00007 -0.00027 0.00217 -0.00029 32212.00000 0.00003 ' - 148 DUP050307391 37 LANCASTER LABORATORIES ijn f- 96 27 004T62 tub*' ' 36 2583831.0?Sd5 * X * * , 100--1G0.OF10.962685720002.8,, 09/26/96 12:02 INSTRUMENT ID: 0 5 936 aEH .Ay A 'I A* u C,a Cd Co Cr _Cu F y K MO Mri Mo K) i Pb Sn !>r 11 Ti AVG (ppm) %RSD 0.00029 37-. 3 5 0.02268 33.14 -0 .-00279 19.18 0.01794 1.921 -0.00744 3.882 -0.00098 18.55295 -0.00025 0.00020 0.00005 0.00048 0.02803 0.62892 7.69833 0.02749 0.00122 - 5.28217 0.00116 0.00042 0.00177 0.00307 0.00246 0.06944 -0.00015 -0.00081 0.00032 31762.66601. 0.0051 1 49.33 3.622 50.63 .251.2 671.5 25.50 17.56 3.216 3.369 3.728. 67.51 4.6-13 19.51 417.7 96.63 62.09 63.67 3.438 25.91 245.5 7 6.95 2.989 6.938 INTEGRATIONS #1 #2 #3 1 0.00031 0.03119 -0.00225 0.01828 0.00778 -0.00154 19.32776 - -0.00037 -0.00005 0.00028 0.00048 . ' 0.03088 0:65213 7.99785 0.02867 ' 0.00058 5.55.867 0.00090 0.00227 0.00372 0.00504 0.00065 0.07219 -0.00019 -0.00188 0.0 0 0 4 1 30667.00000 0.0 0 5 4 b ' 0.00018 0.01993-0.00332 0.01794 ' 0.00728 -0.00068 18.12853 -0.00026 0.00081 -0.00040 0.00061 0.02234 0.61508 ' 7.55.093 0.02678 0.00092 5.09856 0.00123 0.00022 0.00050 0:00294 . 0.00346 0.06815 -0.00014 -0.00203 0.00003 32273.00000 0.00 51 4 0.00040 0.01593 -0.00281 0.01759 0.00727 -0.00072 18.20255 -0.00011 -0.00013 a.00029 0.00036 0.03087 0.61954 7.54621 0.02703 0.00215 5.13926 0.00133 -0.00123 0.00109 0.00123 0.00326 0.06797 -0.000 1 i 0.00(48 0.00050 32348.00000 0.00474 RED] 6 149 DUP050307392 Paae: 38 fitrf fiidA LANCASTER LABORATORIES Run Name: 9627004T62 Tube.: 37. 2583832 / -&>X/S ****t100-1G0.DE10 .962685720002.8 , 09/26/96 12:07 INSTRUMENT 10: 05936 ELEM Aq __ A 7 __ As B __ Ba __ Be Ca __Cd Co __ Cr Cu ,. Fe ___K __ Mg __ Mn Mo __ Na __ NT __ Pb __ Sb __ Se __ Sn Sr ___ Ti __ T7 __ V __ Y __ 2n AVG (poml %RSD 0.00029 0.01099 0.00080 0.04286 0.01240 -0.00066 10.01337 . ' -0.00023 -0.00010 0.00007 0.00070 0.06239 0.34906 3.0633-7 0.077S3 0.00083 4.72215 0.00042 .0.00146 -0.00027 -0.00035 0.00326 0.05557 -0.00021' 0.00323 0.00015 32384.00000 0.00720 94.92 45.38 1 77'. 5 2.937 U269 ' 33.31' 1.430 55.80 199.0 472.9 46.13 18.64 6.121 1.465 1.386 138.3 2.328 4 23.7 37.94 294.8 471.3 38.16 1 . 236 9 2.18 107.4 17 2.4 0.960 10.3 9 INTEGRATIONS #1 #2 0.00009 0.00558 .0.00088 0.04148 .0.01222' -0.00041 9.85204 -0 ..00036 -0.00033 0.00000 0.00057 0.05602 0.32452 3.01262 0.07639 0.00108 4.60236 -0.00058 0.00090 (1.000 1 1 -0.00072 0.00460 0.0547 8 -0.00028 =-0.0005 1 -0.00014 32741.00000 0.00636 0.00061 0.01542 -O'. 00066 0.04395 0.01244 -0.00075 10. 12569 -0.00010 0.00008 0.00043 0.00107 0.07582 0.36358 ' ' 3.09792. 0.07836 0.00183 4.81846 0.00247 0.001-48 0.00026 -0.00181 0.00302 0.05588 0.00000 0.00633 0.00039 32240.00000 0.00780 #3 REREAD REDIG 0.00017 0.01197 0.00218 0.04314 0.01253 -0.00082 10.06238 -0.00024 -0.00006 -0.00022 0.00046 0.05534 0.35906 3.07958 0.07814 -0.00042 4.74562 -0.00062 0 . 00201 -0.00120 0.00147 0.00214 0,05604 -0.00035 0.00386 ' 0.00022 32 171. 00.000 0.00744 150 DUP0503 07393  <0 LANCASTER LABORATORIES Run 9627004T82 r,,b' 38 . 2583223 09/26/96 ^ V. *- ' 0 0 ~ 1 o o , D F 1 f 962685720002,8.. , ' ' 12:12 INSTRUMENT ID: 05936 EL EM A 5* A1 A H B B ^Cd llll Co Cr Ou F& K Mo Mn Mo N U *1 Rh so !;*& Sn Sr T-'i n V Y __ /n AV6 ; . (ppm) %RS0 0.00011 48.0.5 ' 0.05519 1 .'571 -0.00099 283.3 0.37412.0.666 0.05291 0.637 -0.00108 16.78 210. 15130 0.803 -0.00026 32.21 0.00497 12.23 .0.00024 106.2 0.Q01 10 37.48 0.11771 20.33 4.25788 0.750 83.55701 0.550 0.76076 0.641 0:00588 4.459 63.08239 0.552 0.00622 7.372 0.00098 108.5 0.00186 161.5 0.00053 696.9 -0.00001 1 5668 1.51930 0.451 0.00030 76.36 0.00152 133.4 .0.00035 83.51 3164,5.00000 0.030 0.00983 11.49 INTEGRATIONS' #1 M2 *?3 REREAD RED 16 -0.00048 ' 0.05526 -0.00126 0.37135 . 0.05252 -0.00093 208.2041 1. -0.00036 0.00445 0.00013 0.00065 0.09052 4.2253383.02648 ' 0.75517 0.00590 62.68104 0.00656 -0.00019 -0.00146 0.00055 . -0.00021 1 .51193 0.00004 0.00378 0.00064 31636.00000 0.00854 0.00061 0.05601 ' 0.00194 0.37619 0.05310 -0.00128 211.20480 -0.00019. 0.00482 0.0-0005 0.00119 0.13564 4.25910 83.85146 0.76413 0.00560 63.31122 0 .-00641 0.00125 '0.00440 -6.00319 0.00208 1.52452 0.00036 -0.00014 0.00006 3 1 644.00Q00' 0.01067 O'. 00021 0.05428 ' -0.00366 0.37482 0.053 TO -0.00103 211;04499 -0.00023 0.00564 0.00054 0.00146 0.12697 `4.28922. . 83.79309 0 .76299 0.00612 63.25492 0.00570 0.00191 0.00264 0.00424 -0.00190 1.52294 0.00049 0.00092 0.0003? 31655.00000 0.01027 151 ) DUP0S0307394 i-'age: 40 LANCASTER LABORATORIES Run Name: 9627004T62 Tube: 39 2583224 44^0'PF' ****; 100-1 00, OF 1,962685720002 ,'8, , 09/26/96 12: 17 INSTRUMENT ID: 05936 * EL EM Aa ___A1 As __B___Ba Be ^Ca i^Cci __ Co._ __ Cr ' __ Cu _.JF a . __ K __ Mg Mn . Mo __ Na __ Ni Pb __ Sb __ Se . __ Sn Sr __ Ti __ n - V ___Y __ 2n AVG (ppm) %RSD #1 0.00016 226.9 0.01430 16.25 -0.00309 -81.12 0.32104 0.216 O'. 05117 0.567 -0.00100 20.04 ; 211.43548 0.400 -0.00012 70.89 . 0.00493 7.670 0.00062 42.39 0.00072 21.31 0.04360 48.43 4.03562 1.021 83.50205 0.307 0.73839 0.238 0.00644 17:50 62.29665 0.727 0.00760 7.603 -0.00035 225.2 0.00173 49.74 0.00046 213.9 0,. 00200 63.82 1.51899' 0.417 -0.00053 14.90 0.00187 133.9 0.00029 48.17 31585.33398 0.447 0.01203 2.017 0.00029 0.01686 -0.00096 0.32177 0.QS149 -0.00123 211.25750 -0.00005 0.00500 0.00092 0.00067 r 0.04867 4.08058 83.743840.73868 0.00633 62.80651 0.00694 0.00000 0.00092' 0.00162 0.00263 1 . 52612 -0.00063 0.00159 0.00016 31423.00000 0.01229 INTEGRATIONS #2 #3 REREAD RED IS -0.00026 0.01230 -0.00246 ' 0.32033 0:05092. -0.00085' 210.69284 -0.00008 0.00452 0.00043. 0.00059 0.02040 3.99963 83.23310 0.73650 0.00537 61 .94007 0.00803 -0.00127 0-. 00164 0.00008 0.00285 1.51396 -0.00064 -0.00048 0.00045 31630.00000 0.01199 0.00046 0.01375 -0.00585 0.32097 0.05109 -0.00092 ; 212.35609 -0.00021 0.00527 ' 0.00050 0.00089 0.0617-3 4.02666 83.52923 0.73998 0.00762 62.14337 0.00782 0.00020 0.00264 -0.00030 0.00053 1.51690 -0.00048 0.00450 0.00027 31653.00000 0.0 1 1 8 1 152 DUP050307395 41 LANCASTER LABORATORIES i-gn IMm 9627004T62 -fubw; 40 2583225 'f*.t , (QG-IOO.DFI. 9626857 20002.8 , , 09/26/96 12:22 INSTRUMENT ID 0 5 93 c EL EM Act A'l Aj * W--B __0(S STcrf ___ cr __Cu F& ___,K __ KlU __ Mri -_ho ___Nfl NT ___ Rl*t __ Sl> __ J>ea __ 5n Sr T'i ___l 1 V' __y 1n . AVG (ppm) %RSD 0.00031 98.24 0101054 19.92 -0.00049 511.5 0.07002 1 . 527 Q.1143G 0.195 -0.00081 2,771 125.92391 0.454 -0.00023 48.83 0.00441 13.51 0.00088 36.51 0.00112 11.06 -0.01438 71.95 2,10837 0.716 . 49.67541 '0.104 0.69289 0.198 0,.00288 2 4' .'3 0 36.24118 0.602 0.01436 4.645 -0.00053 -263.6 0.00207 79.67 0.00355 24.0 5 0.00104 43.05 0.34561 0.227 -0.00040 20.38 -0.00044 1160. 0.00130 4.194 31795.33398 0.052 0.0104.1, 3.643 #1 -0.00003 . 0.0098,9 0.00213 0.06883 0.11412-0.00079 125.47232 -0.00034 0.00503 0.001250.00098 -0.017432.1001049 ..61663 0.69142 0.00342 36.04892 0.01383 -0.00212 0.00287 0.00374 0.00072 0.34489 -0.00037 0.00523 0.00124 31776.00000 0.01003 INTEGRATIONS #2 #3 RREREAD RED 16 0.00043 0.01289 -0.00296 . 0.07030 . 0.11455 ` -0.00083 125-73133 '0.00011 0,00384 0.000,69 0.00115' -0.02285 2.12581 49.69599 0.69311 0.00211 36.47850 0.01415 0.00063 0.00017 0.00261 0.00084 0.34645 -0.00049 -0.00470 0.00131 31804.00000 0.01079 0.00054 ' 0.00884 -0.00066 0.07091 0.11424 -0.00080 126,56809 -0.00024 0.00436 ' 0.00069; 0.00122 -0.00284 2.09920 49.71362 0169415 0.00305 36.19610 0.01511 -0 ..00013 0.00316 - 0.00429 0.00155 0.34550 -0.00033 -0.00185 0.00136 31806.00000 0,0 1 0 41.1 153 DUP050307396 Page: 42 LANCASTER LABORATORIES. Run Name:. 9627004T62 ' " Tube: 41 2583227 A***, 100-100,DF1 ,'962685720002.8, . : .09/26/96 12:27 INSTRUMENT ID:. 05936 EL EM Aa A1 As B 8a , Be XCa XCd Co Cr Cu Fe K' Mq Mn . Mo Na Ni ___Pb __ Sb __Se Sn. Sr Ti __ Tl (__ V y 4n AVG' (ppm) %RSD #1 INTEGRATIONS . #2 , #3 . REREAD RED 16 0.00016 126.9 0.1 1805 1.05 0.00243 103.0 . 0.06108 1.181 0.07579 o.. 221 -0.00104 -7.841 . 224.44313 0.520 0.00010 104.5 ' 0.00057 '68.63 . 0.00107 27.48 0:00137 23.82 0.09637 `1 1 .07 2.92713 0.417 89.15540 0.385 0.20339 0.322 0.00659 '11.12 56.46310 0.144' ' 0.01147 10.29 0.00191 59.28 0.01025 8.'631 0.03265 4; 264 0.00118 133.7 0.70907 0.261 0.00278 2.165 0.00202 117.5 0.00286 11.49- 31453.33398 0.341 0.01591 1.653 0.00002 0.11697 0.00396 0.06036 0.07562 -0..0-0095 223.10585 0.00008 0.00079 0.0G121 0.00172 0.09983 2.94120 ' 88.78842 0.20265 0.00699 56.45472 0.01206 0.00140 0.00926 0.03183 -0.00064 0.70745 0.002-76 0.00264 0.00290 31560.00000 0.01591 0.00007: 0.11779 .-0.00045 0.06109 0.07595 -0.00112 224.96513 O'.OOOGO : 0,0001.1 '0.00126 0.00107 0.08439 2.91931 89.46887 0.20390 0 : 00574 56.54856 0.01012 0.00322 0.01097 0.03426 0.00214 0.71108 0.00273 0.00403 0.00316 31345.00000 0.01564 0.00041 ' 0.11940 0.00377 0.06180 0.07581 -0.00106 225.2584^ 0.0D022 0.00079 0.00073 0.00132 0.10488 2.92088 ' 89.20892 ` 0.20362 - 0.007 03 . 56.38602 ` 0 .'01 225 0.00113 0.01051 0.03186 Cl . 00203 0.70867 0.00284 -0.00060 0.0025 1 31455.00000 0.01616 154 i DUP050307397 / P K} 43 LANCASTER LABORATORIES (inn Name: - 9627004T62 Tub J 42 2583830. DOVE'S 100-100,DF1/9626857 20002,8 r 09/26/96 12:32 INSTRUMENT ID: 05936 EL EM . $v o (ppm) *RS0 , #1 INTEGRATIONS ' #2 #3. 'REREAD An 0.`00023 146.0 -0..00008 0.00060 0.00019 .. "$i 0.01094 19.35 0.01241 ' 0.00851 0.01189 As -0.00024 648.1 0.00035 0.00095 -0.00203 .U 0.32595 0.749 0.32488 0.32422 0.3287$ 8a -0.11791 0.174 0.11805 0.11767 0.11801 0# -0.00098 16.70 -0.00079 -0.00109 --0.00105' SfCa 73.30468 0.276. 73.21475 ' 73:16247 73`. 53683- VCd -0.00039 19.33 -0.00048 -0.00038 -0.00032' . t'o . 0.. 00127 12.08 - 0.00110 0 .' 0 013 2 0.00139 Cr 0.00020 149.3 -0.00013 0.00027 0.00046- A ""'Cu 0.00063 V5.-69 0.00063 0.00054 0.00074 ' F & 0.22723 3.233 0.223ro 0.22289 0.23572 K 5.76762 0.538 5.80336 ' 5.74712 5.75236 Mp ' 31.09099 0.240 31.12611 3-1 .00512 31.14175 Mn 0.25258 0.105 0.25254 0.25233 0 . 25286 Mo 0.00966 5.216 0.00909 . 0.01005 0.00985 Nrt ' 50.76529 0.625 5V.12262 50.51609 .- 50.65717 Mi 0.00249 10.09 0.00221 0.00254 0.0027V Mb 0.00094 i 0.1.3 0.00206 0.00040 0.00038 $D 0.00189 53.23 0.00280 0.00080 0.00208 'i 0.00051 378.0 0.00163 -0.00173 0.00165 Sn 0.00535 6.345 0.00508 0.00573 0.00523 A !>r n 0.55519 0.280 0.0002V 16.87 0.55645 0.00017 ' 0.55345 0.000 23 0.55568 0.00024 _____1 l v . -0.00249 151.2 0.00026 60.77 -0.00685 0.000 1 1 -0.00046 ' 0.00025 -0.00016 0.00043 Y 31837.00000 0.285 - 31871.00000 3 ISOS.00000 31734.00000 __ /'n 0.00958 9.140 0.01059 0.00905 0.00910 155 DUP050307398 LANCASTER LABORATORIES Run Name: 9S27004T62 Tube: 43 ' 2583831 ' ****. lQQ-1'00,DEI ,962685720002 :8, , ' 09/26/96 ' 12:37 ' INSTRUMENT ID: 05936 ELEM Aa __LAI . As B" __ Ba . 8e Wc a XCd Co ___Cr J__Cu. Fe _K __ Mg'' __ Mn __ Mo ; Na Ni __ Pb _^_Sb ___Se ___Sn ___Sr T1 T1 V __ Y __ 2n AVG (ppm) %RSD ' #1 -0.00006 69.07 0.04715 4.042 -0.00206 90:91 0.T3777 0.352 0.07723 ,0.462' -0.00122 13.68 . 1 192.61022 0.409 -O.'OOOI 6 136.4 0.00047 64.22 0.00030 119.2 0.00082 2.300 -0.02953 19.95 6.42020 0.731 79.73394 0.386 0.27714 0.355 0.00244 37.67 56.33201 0.538 0.00483 40.98 0.G0090 68.92 0.00095 156.4 0.02763 5.220 0.00280 97.47 0.70492 0.464 0.00053 14.36 -0.00094 173.8 0.00087 32.25 31325.00000 0.342 0.009 7 8 &.079 -0.00012 0.04831 -0.00189 0.13759 0.07764 -6.00124 193,49.043 . --0.00038. 0.00041 -0.00010 0.00083 -O'. 03387 6.47388 80.07570 0.27820 0.00351 56.67977 '0.00344 0.00091 -0.00072 0.0270? 0.00129 0.70859 0.00044 -0.00255 0.00077 31201.00000 0 , 00906 INTEGRATIONS #2 ' -0; 00005: 0.04495 -0.00401 0.13740 0.07704 -0.00137 19>T. 96656 -0.00017 0.00019 0.00042 0.00080 .. -0.02282 6.38660 79.47628 0.27625 0.00189 56. 19275 0.00395 0.00152 G.00214 0.02655 0.001 16 0.70276 0.00058 -0.00104 0,00066 31386.000Q0 0.00997 #3- ' REREAD REOIG -0.00002 _____ . .0.04819 -0.00027 0.13832 0.07701 ______ _ -o;ooro4 192.37370 _______________ O'.00006 _______. _____ _ 0.00079 ______ 0.00057 _ 0.00034 -0.03189 6.40013 .. 79.64985 _______ : 0.27699 0.00194 56. 12351 0.007 10 0.00027 0.00143 ________" 0.02927 _ 0.00596 0.70332 ^ 0.00057 0.00074 ______ _ O.OCnio _________ _________ 131338.00000 n .01016 _______ 156 DUP050307399 PA (It* 45 LANCASTER LABORATORIES !;uti : 962700-4T62 ll?* : 44 2583332 1 >>X "S 10 0-100,OF I.9626857 20002. 8, , 09/26/96 12:42 INSTRUMENT ID: 05936 I'.H M "$ f |! *l># 'd n V,; f1 <> Co cr Ou ] t V MU Mr i Mi") 'Hfl in Vh sh 'jtS LP or `l i tl V r 7n ' Ave . (ppm) %RSD #1 0,00015 143.1 O'. 01241 3.632 -0.00295 62.28 0.31147 .0.611 . 0.12763' 0.666 -0.00073 22.64 ` 103.37725 O'. 531 -0.00033 34:90. 0,00088 21.94 0.00024 51 . 90 0.00082 23.38 0.33435 4.063 ' 3.05530 0.641 31.11323 0.578 0.78662 0.480 0.00806 7.47 0 49.47684 0.628 0.00321 26.40 0.00075 174.4 0.00129 85.09 0.00012 1776. 0.00102 2 1 0 . -1 0.55837 0.516 -0.00045 13.36 -0.00214 87-. 90 -0.00018 81 .00 31971.56601 0.540 - 0.00955 1 . 737 0.00019 0.01241 -0.003.79 0.30943 0. 12667 -0.00054 102.74988 -0.00027 0.00073 0.00009 0.00095 0.33346 3.04876 30.90660 0.78226 0.00750 49.20494 0.00409 0.00174 0.00254 . 0.00009 -0.00007 0.55517 -0.00042 0.00003 -0.00004 32171.00000 0.00935 INTEGRATIONS #2 #3 RiEREAD .REDID 0.00034 ' 0.01286 -0.00422^. 0.31178 ' 0.12789 -0.00087 103.77292 -0.00026 0.00 no 0.00031 0.00090 0.34836 3.03982 . 31.19874 0.78898 0.00870 49..40976 0.0024-0 0.00124 0.00051 -0.00200 0.00351 0.55915 -0.00041 -0.00324 -0.00016 31856.00000 0.00965 -0.00008 0.01195 -0.00084 0.31320 0.12831 -0.00077 103.60897 -0.00047 . 0:00080 0.00031 0.00060 0.32123 3.07733 31.2343? 0.7 8861. 0.00798 49.81583 0.00314 -0.00073 0.00081 ' 0.00227 -0.00035 0.56078 -0.00052 -0.00323 -0.00034 31878.00000 0.00964 157 DUP050307400 Page: 46 LANCASTER LABORATORIES Run Name; 96270G4T62 Tube:. 45 2583833 . :*:**:*: Q 0 " 100,DF1,962585720002,8 r r 09/26/96 12:47 INSTRUMENT- ID: 05936 ELEM. AVG (ppm) %RSD #1 ' INTEGRATIONS #2 #.3 REREAD REDIG Aa ' 0.00036 107.4 0.00031 AT 0.05559 '2.799 0.05571 As -0.00152 131.8' -0.00016 B 0.05487 2.519 0:05645 , .BS Be 0.07701 0.380 -0.00079 16.51 0.07716 -0.00084 X Ca ' 166.10227: 0.356 166,65406 . -0.00039 26.02 -0100035 Co - . -0.00025 35'. 55 ' -0.00031 Cr 0.00101 17:83 0.00089 Cu 0.00124 8.486 0.00126 Fe- 0.01850 78.53 0.03080 ___k 1.65582 0.490 1.66349 Mq _______ 58.59210 0.374 58.73626 __ Mn 0.00712 0.589 0.00714 ___Mo 0.00207 1-2.02 0.00233 __ Na 41.49222 0.382 41.40862 Ni 0.0.021 8 57.86 0.00242 Pb ' -0.00071 3 1 . 27 -0 . 00052 __ Sb . 0.00419 49.84 '0.00 640 __ Se . __ Sn- Sr Ti '__ Tl v __ r __ Zn 0.16210 0.00115 0.43912 0.00071 0.001 22 0.00075 31756.66601 0.01254 0.935 153.4 0.346 22.89 415.8 3o . 3 0.424 4.505 0. 16111 0.00181 0.44001 0.00090 -0.00116 0.00099 31673.00000 0.0129 6 0.00004 0.05398 -0.00057 0.05427 0.07721' - -0.00088 166 . 17 576' -0.00051 -0.00031 ' 0.00092 0-.0OT13 0.02225 1;65667 58.70069 .0.00714 0.00183 41-. 67547 0.00082 -0.00096 0.00224 0. 16385 0.00250 0.43998 0.00066 -0.00222 0.00045 3 1685.00000 0.01276 0.00025 0.05709 -0.00384 0.05388 0.07668 -0.00064 165.47702 -0.00031 -0.00015 0.00122 0.00134' 0.00246 1.64731. 58.33937 0.00707 0.00205 41.39257 ' 0.0033 2 -0.00067 0.00394 0.-16136 -0.00085 ' 0.4373 6 0.00058 0.00705 0.00082 31912.00000 0.0119 (i 158 DUP050307401 47 LANCASTER LABORATORIES ur, : 96^7004 i 62 Tube: 46' CCV 09/26/96 12:52 INSTRUMENT ID-: 05936 EL EM __,,A __ AT __ Ar __J3n __ .B* ,Ca __ Cd __Co ___Or - Cu __ F __ K .Mg __ Mn __ No J_Nn __ N 1 __Rh __\ b ___ _sri ___>r __ I'l __ T"l ___1/ __ v Zn AVG (ppm) 5SRSD .0.54813 1 . 962 25.21118 1 .773 0.53379 1 . 578 0.53807 2.048 0.51909 1.954 0.53414 '2.096 26.24389 2.043 0.53486 2.188 0.53486 1.915 0.51396 2.010 0.53334 1.957 25x81180 2. 136 25.98122 1.411 25.40609 2.005 0.53575 1 .957 0.51513 1.252 25.37681 0.701 0.53727 2.355 . 0.53383 2.135 0.49916 0.885 0.52713 1.621 - 0.52275 2.184 0.51000 1.976 0.51828 1.931 0.53047 2.508 0.51706 2.050 31905.33398 1-. 492 0.53846 1.921 :41 0.55051 25.72407 0.54273 0.55071 0.53078 0.54706 26.86306 0.54837 0.54668 0.52589 D.54527 26.44842 26.39659 25,98926 0.54786 0.52220 25.56671 0 . S 51 5 8 0 .'54695 0.50414 0. .53638 0.53589 0.52161 0.52981 0.54570 0.52928 31358.00000 0.55009 INTEGRATIONS #2 43 ' - REREAD 0.54102 24.90270 0.52599 0.53048 0.51266 ' 0.52724 ' 25.92007 0.52784 0`. 52855. ` 0.50822 0.5258625.48324 25.70274 25.04802 0.52952 0.50940 25.21363 0.53268 0.52636 0.49571 0.52561 0.51522 0.50344 0.51190 0.52109 0.51027 32202.00000 0.53029 ' ' 0.54287 25.00677 0.53264 0.533.0 2 0.51381 0.52812 V 25.948575 0.52837 . 0.52935 0.50778 0.5 2 8' 8 9 25.50374 25.84433' 25.18099 0.52937 ' 0.51378 25.3501 0 0:52755 0.52817 0.49763 0.51944 0.51712 0.50496 0.51312 0.52461 0.51164 32158.00000 0.535 0 0 159 DUP050307402 Page: 48 LANCASTER LABORATORIES Run Name: Tube: 47 9627 004T62 . CCB - 09/26/96. , .12:57 INSTRUMENT .ID: 05936 ELEM ' Aa __ AI As B. 6a Be __ CaCd ___Co Or Cu Fe -K Ma ' __ Mn ___Mo ___Na NT __ Pb Sb ___Se __ Sn Sr TT __;T1 V __ Y __ Zn $v g (ppm) %RSD . #1 . INTEGRATIONS #2 43 ' REREAD REDIG 0`. 00022 60.07 0.01843 8.048 -o.ooior 164.8 0.00567 3.266 -0.00020 5.637 -0.00036 27.77 . --O'. 02159 6.218 -0.00027 37.64 0.00043 80.92 0.00056 64.49 r 0.00076 22.97 0.03215 3.951 " 0.11186 2.200 0.02005 7.004 0.00017 13.48 0.00143 19.95 0.15013 3 5.24 . 0.00032 144.2 0.00074 240.6 0.00378 35.05 0.00116 210.4 0.00068 463.9 0.00015 6.464 -0..0001 1 2 8.38 0.00262 2 50.6 0.00016 1' 1 5 . 2 32719.66601 0.243 0.00138 39.07 0.00008 ' 0.01727 0.00031 '0.00545 -0.00019 -0.00029 -0.02010 -0.00.036 . 0.00003 0.00018 0.00062 0.03115 0.11158'.' 0.01844 0.00015 0.00159 0. 12219 -0-.0001 9 -0.00128 0.00504 0.00372 -0.00206 0.00014 -0.00007 0.00195 -0.00002 32800.00000 0.00076 0.00022 0.00035 0.01792 ' 0.02010 -0.00046 .-0.00289. . 0.00577 ' 0.00578 -0.00021 -0.00019 -0.00030 -0.00047 -0 ..02198 ' -0.02270 -0.00016 -0.00028 0.00060 0.00067 0.00091 . 0.00058 ' 0.00D96 ' 0.00072 0.03358 0.03172 Q.10954 0.11444 0.02101 0.02070 0.00019 0.00019 0.00161 0.00110 0.11705 0.21116 0.00045 0.00070 0.00215 0.00137 ' 0.00239 0.00391 -0.0.01 14 0.00090 0,00420 -.0.00007 0.00016 .0 .000 1 6 -0.00012 -0.00013 -0.00359 0.00952 0.00016 0.00035 32718.00000 32641.00000 0.00169 0.00170 160 DUP050307403 LANCASTER LABORATORIES 9627004T62 lion I ul>r * * * , .Irt I Od 2583834 F&l'&S I 0 0 , D F 1,982 6857 20002.8, 09/26/96 13:02' INSTRUMENT ID: 05936 A SB .Ba Be l./; Cd j',o "c r "Cu f (9 'k " MCi j'lri _Mc> Na '|J1 >b * Sb b__ Uri 1--:-'r T'l "^H V 2n A/6 (ppm) %RSD - 0.00023 61.71 0.01577 17.11 -0.00150 108.9 0.03763 1.165 0.00152 0.837 -0.00.040 2.290 0.00035 132.0 -0.00043 9.021 0.00007 870.5 . -0.00023 14 2.3 0.00149 15.58 0.02605 15.41 0.11345 2.667 0.01908 15.88 0.00149 3.095 0.00080 42.22 0.16660 45.33 0.00208 32.83 0.00040 '86.60 0.00108 130.0 -0.00156 1.57.2' -0.00009 1131. 0.00022 -7.823 -0.00015 50.12 -0.00036 798.4 -0.00026 6 2.88 2726.00000 0.225 0.01084 5.969 #1 0.00037 0.01575 0.00030 0.03785 0.00152 -0.Q0039 0.00051 '-0.00043 G_ 00067 -0.00042 0.0017,20.02853 0.11194 0.02097 0.00147 0.00062 0.16936 0.00131 0.00078 -0.00033 0.00089 0.00020 0.00020 -0.00006 .-0.00322 - 0.0004 6 3 2795.00000 0.01137 INTEGRATIONS #2 #3 . REREAD REDIG 0.00025 0.01848 -0.00192 . 0.03713 0.00153 -0.00041 . 0.00073 -0.00039 0.00016 0.00015 0.00150 0.028-15 0 . 11694 0.02070 0.00155 0.00059 0.24155 0.00262 0.00033 0.001 09 -0.00156 0.000'820.00023 -0.00018 0.00260 -0 . 00014 32648.00000 0.01012 0.00008 - 0.01308 -0.00288 0.03792 0.00151 - -0.00040 -0.00017 -0.00047 40.00062 - -0.00042 0.00126 0.02142 0.11148 0.01559 0.00147 0.00120 0.08889 0.00232 0.00009 0.00248 -0.00401 .-0.001.32 0.00021 -0.00020 -0.00047 -0.00019 32735.00000 0.01102 16i DU P0503 07404 LANCASTER LABORATORIES Run Name: Tube.: 49 9627004T62 'cRl' 09/26/96 ' INSTRUMENT ID: 13:07 05936 ELEM. ' Aa AT As B ' * Ba ' __ Be C'<3 Gd ' _Go Or Cu . Fe __ k __ Mg __ Mn __ Mo . Na NT __ PbSb __ Se ___Sn __ Sr __ Ti j__T1 __ V __ Y __ Zn ' AVG (ppm) mso #1 INTEGRATIONS #2 #3 REREAD REDIG 0.02186 -0.00910 0.01985 0.00291 -0.00016 0.01067 ' -0.04032 0.01052 0.10896 0.02075 0.05433 0.03099 0.. 10373 0.0104.6 0.03251 0.00089 0.08662 0.08828 0.00794 0.11962 0.01120 -0.00095 0.00004 -0.00019 0.02160 0.10579 33 33 0.66796 0.04382 1 .'(72 12.17 13.38 9.726 17.20 0.716 4,'240 3.170 0.527 3.235 0.158 26.72 4. 123 16.47 0.348 118.2 65.77 1 .728 15.45 2.780 27.56 108.6 60.56 40.31 7.537 0.294 0.236 1 . 906 . 0.02190 -0.00860 0.02247 0.00292 -0.00016 ' 0.01075 -0.04044 0.01013 0.10837 0.02024 0.05423 0.02441 0.10353 0.00929 0.03250 -0.00021 0.08989 0.08734 0.00869 0.12115 0.00890 0.00013 0.00005 -0.00022 0.02104 0.10605 33295.00000 0.04363 0.02159 -0.01037 0.01716 ' 0.00263 -0.00020, 0.01060 -0.04197 0.01075. 0.10900 0,02050 0.05438 0.02827 0.09956 0.00965 0.03241 0.00189 0.02808 0.08746 0.00860 0.11580 0.01471 -0.00106. 0.00001 . -0.00026 0.02343 0.10544 33276.00000 0.043 1 0 0:02210 -0,00833 0.01993 ' 0.00319 -0.00014 0.01067 -0.03855 0.01066 - ' 0.10952 0.02151 : 0.05437 0.04030 0. 10811 ' 0.01244 0.03263 0.00100 0.14190 0.09004 0.00652 0.12189 0.00999 ' -0.00193 0.00006 -0.00010 0.02032 0 . 1 0586 33421.00000 0.04474 162 DUP050307405 .'..ni- S'l LANCASTER LABORATORIES <1111 l"i'rr'e: niliw; 50 9627004TS2 . ICSA 09/26/96 13:12 INSTRUMENT ID: 05936 1 ! 1 f'1 AU - "A 1 ' fUJ l;** (:> ...ij -- , M ....i H | rt 'Viu Hu ii <. 11 n ' Ilf ' f 'I' ,h * 1 iw 'tfl M' 11 ' 11 "7 , /n AVG (ppm) %RSD . 0.00046 36.73 526.43231 1.104 -0.00319 10.50 0.01833 6.462 0.00861 -1.053 -0.00045 56.90 ` 531.19934 0.946 -0.00347 5.011 0.00,102 27. 16 , . . 0.00165 21,65 '-0.00006 610.1 2.10.53103 0.900 0. 101 27 5.409 532.14910 0.838 0.00556 0.718 0.00064- 162.1 '0.25709 23.45 0.-00197 50.73 0.00045 431.2 0.01431 22.44 -0.00758 15.62 0.00740 38.32 0.02115 0.986 -0.00115 2.432 -0.01041 23.55 -0.00249 33.84 30415.66601 0.877 0.00373-47.96 . 0.00065 519.88018 -0.00358 0.01826 0.00853 -0.00026 526.04449 -0.00327 0.00079 0.00193 0.00038 .208.58444' 0:09547 527.06695 0.00651 -0.00031 0.32579 0.00148 -0.00096 . 0.01085 -0.00893 0.OO41 2 0.02091 -0.00118 -0.01145 -0.00152 30706.00000 0.00293 INTEGRATIONS' #2 #3 REREAD RED 16 0.00039 ' 0.00033 528.43475 530.98199 -0.00299 -0.00301 0.01719 0.01 956' 0.00859 0.00871. -0.00034 .-0.00074 531.46911 536.0843.5 -0.00356. -0.00359 0.00094. o:00133 0.00179 0.00125 -0.0.0041 ' -0.00017 210.80279 212.35586 0.10197 0.T0636 ' 532.82141 536.55895 0.00656 0.00661 0.00049 0.00174 0.21297 0.23250 0.00313' 0.00132 -0.00036 0.00269 0.01439 0.01720 -0.00669 0.00909 -0.00713 0.00899 0.02122 0.02131 -0.00112 -0.00115 -0.00760 -0.01216 -0.00288 -0.00307 30360.00000 30181.00000 0.00248 0.00578 * 163 DUP050307406 LANCASTER LABORATORIES Run Name; 9S27004T62 Tube: 51 ICSAB 09/26/96 13:17 INSTRUMENT ID: 05936 LM Aa ___A1 ___As ___B ___Ba Be Ca Cd- Co. : Cr . ' ___Cu ___Fe_ ___K Ma ^Mn __ Mo __ Ns Ni __ Pb. __ 5b ___Se __ Sn Sr Ti __ T1 __ V __ Y __ 2n AVG - (ppm) %RSD 0.23157 529.25970 0.11271 . 0.03067 0.56007 0.51783 529.33050 1:02287 0.53227 0.51048 0.59508 210.09428 0;.09908 531.75482 0.53877 0.00062 0.24690 1.03650 0.05183 0.63434 0.04505 0.0085C 0.02127 -0.00129 0.09190 0.52382 30405.00000 1 .00752 0.625 0.866 3.387 3.386 0.851 0.609 0.613 0.538 0.653 0.664 1.034 0.656 2.872 0.696 0.544 3 2 2.0 30.67 0.207 7.825 1 . 14 6 4.286 39.06 0,600 9 . 234 5.5 69 0.451 0.7 60 0.713 INTEGRATIONS ' #1 #2 #3 REREAD REDIG 0.22991 523.96484 0. 10836 0.02954 0.55467 0.51444 526.80578' 1.01815 0.52839 O'. 50791' O'. 58824 208.64758 0.10057 527.48211 . 0.,53573 0 . OO094 0.30012 1 . 03524 0.04741 0.62603 0.04687 . -0.01213 0.02112 -0.00121 0.09750 0.52165 0668.00000 1.0 04 23 . . 0.23224 531.96398 0.11429 0.03159 '0.56372 . 0.51836 528.19042 . - 1.02154 ' 0.53331 0,50921 0.60019 210.23983 - - .0.09580 533.74023 0.53900 -0.00152 0.16020 1.03527 0.05272 ' 0.63951 0.04302 0.00560 0.02132 -0.00143 0.08746 0.52348 30234.00000 1 . 00257 0.23256 S3 1 . 85021 _______; . 0.1 1550 _______ ' _____ 0.03086 J______ _______ 0.56182 0.52069 532.99523. , 1 . 02892 0.5351 1 _____________ O'. 5 1 432 : '0.59680 211.39541 0.10087 534.0421 1- 0.54159 _______ ' 0.00244 0.28038 ______ .. _____ 1.03898 ______; 0.05537 0.63749 0.04527 . 0.00778 0.02136 -0.001 23 _______. 0.09075 0.52634 _______ _______ 30313.00000 _______ ________ I .01 577 _______ 164 DUP050307407 Jaae: 53 LANCASTER LABORATORIES Run.Name: Tube: 52 9627004T62 CCV 09/26/96 13:21 INSTRUMENT ID: 05936 ELEM Aq A1 As B ___Ba Be Ca Cd Co __Cr Cu Fe _K Ha __ Mn __ Ho . Na N1 :__ Pb __ Sb __ Se __-JS n ' Sr __Ti __ T1 V __ V __ Zn ' AVG (ppm) %RSD 0.53710 0.813 24.74460 0.667 0.53144 0.906 0.52691 0.691 0.50806 0.669 . 0.52793 1.006 < .25.98742 1.035 ; 0.53042 0.747 - 0.52815 1,029 0.50680 1.213 , 0:51993 0.622 25.35507 0.753 25.54660 0.459 24.83837 0.733 0.52865 0.858 0.5091 1 0.724 25.03948 0.948 0.53252 1 .558 0.52210 0.842 0.49949 0.579 0,51938 0.573 0.51226 1.917 0.50092 0.700 0.50892 Q .797 0.52220 1.613 0.50923 0.708 33102.66796 0.51 2 0.54446 1 . 023 INTEGRATIONS 4*1 #2 #3 REREAD REDIG 0..53969 . 24.80769 0.53296 0.52799 0.50914 0.53193 26: 1965.5 0.53406 0.53294 0.51117 0.52089 25.47430 25.61472 24.92962 0.53229 0.50804 25.28554 0 .'5391 0 0.51815 0.49974 0.51612 0.52110 0.50274 0.51105 0.51537 0.5 1 233 33145.00000 0.54799 0.53956 24.86883 0.53531 . 0.52990 0.51079 0.52996 26:08186 0.53100 0.52927 0..50947 0.52258 25.45607 . . 25.5,1403 24.95697 0.53010 0.51322 .25.02136 0.53526 0.52684 0.50226 0.52196 0.51399 0.50315 0.51147 0.53-162 0.51009 3 7. 9 1 6.0 0 0 0 0 0.54735 0.53206 . 24.55729 0.52604- 0.52286 ' 0.50425 0.52190 25.68384 0.52619 0.52224 0.49977 0/51633 25 .T3483 25.41 104 -24.62851 0.52357 0.50608 24.81154 0.52319 0.52130 0.49648 0.52005 0.50169 0.49688 0.50424 0.51962 0.50527 3: 3247.00000 0 . 53804 165. DU PO50307408  a a e : 54 LANCASTER LABORATORIES un Name: 9627004T62 ube: 53 CCB 09/26/96 INSTRUMENT 10: 13:26 0 593 6 :LEM AVG (ppm) %RSD Aa __ AT As 8 Ba Be Ca Cd__0 __ Cr. __ Cu Fe __ K __ Mg __ Mn __ Mo __j\ie Ni __.Pb __ Sb __ Se Sn Sr __ Ti __ Tl __ V __ Y ___,2rt . . 0.00007 105.2 0.05567 42.91 . -0.Q0 040 514.7 0.01 166 2.401 -0.00023 27.40 -0.00020 58.01 0.00802 33 8.1 -0.00024 61.55 . -0.00013 155.4 -0.0001 1 297.5 0.00066 2 5.27 0.04557 21 .98 0.10843 2 . 847 0.06298 42.02 0.00009 36.86 0.00118 68.12 ' 0.08235 89.7/ < 0.00006 1593. 0.00061 12 9.2 0.00262 19.00 0.00110 23 2.4 0.00330 24.04 0.00007 34.95 -0.00016 70.74 0.00299 13 9.5 -0.00015 210.3 32379.33203 0.135 0.00088 84.85 INTEGRATIONS #1 #2 #3 REREAD REDIG 0.00013' 0.08325 0.001.34 0.01166 . -0.00015 -0.00008 . 0.03916 -0.00014 -0.00025 0.00008 0.00083 0.05671 0.10688 0.09351 0.00009 0.00178 0.16346 . 0.00087 0.00126 0.00221 -0.00183 0.00365 0.00009 -0.00004 0.00094 -0.00038 32895.00000 0.00131 0.00010 0.04249 -0.00190 ' , 0.01195.' - -0.00025' -0.00019 -0.00469 -0.00016 0.00010 0,00008 0.00087 0.04269' 0'.-11199 `0.04891 0.0 0 01 3 0.00149 0.06488 0.00044 -0.00026 0.00317 0.00289 0.00385 0.00007 -0.00017 0.00780 ' 0.00022 32914.00000 0.00131 -0.00001 0.04128 --0.00124 0.01139 -Q.00027 -0.00032 -0.01041 -0.00041 -0.00025 -0.00049 0.00049 0.03730 0.10642 0.04652 0.00006 0.00026 0.01872 -0.00112 0.00084 0.00246 0.00223 0.00239 0.00004 -0.00028 0.00023 -0.00031 32829.00000 0.00001 ` D 3 "t a Revi ewe cl by : 166 DUP050307409 Furnace Data 167 DUP05030741 0 LANCASTER LABORATDRIES GRAPHITE FURNACE ATOMIC ABSORPTION DATA REVIEWED X y t zv\ DATA VERIFIED BY DATA I-in: NANFJ. Aifcftj I-RAT RUN MAMEs .'362&SB1F04 ANALYST::. 3. 3.4 INSTRUMENT NOs BA7BA BKO CORR.i BZ ELEMENTS AS Concentration is used to ,wva!uLi if saMt>l=.> ro-.m l. i; * are within calibration ran tie. 168 DUP050307411 RUN NAMEs 96269011"04 PAGES 1 .ANALYSTS- 114 TUHEs SAMPLE 90 1 09/24/96 21s09 Cl. ASS 1 VCll. /UT 0 AUG (ppb) KRPP AUG ab& 1.1600 11.6 -0.001 LANCASTER LABORATORIES INSTRUMENT IDs 04724 GEAA ELEMENT: AS FUOL. PI- BATCH NUMBER 81 BURN 1 BURN 2 -0.002 -0.001 TUBEs. SAMPLE S10- " 2 09/24/96 21:: 13 Cl. ft6fi IVOL/WT '@ AUG Imsb) i&RPD AUG ab& 9.7900 5.4 0.027 FUOL PF BATCH NUMBER 0. 1 BURN 1 BURN 2 0.026 0. 029 TUBEs SAMPLE S20 3 09/ 24/96 21:: 1.7 Cl. $s s :;. 1VOL/WT 0 AUG < ocb) XRPP AUG abs 21.0200 7.3* 0. 057 FUOL PF BATCH NUMBER 01 BURN 1. BURN 2 8. 8154 8.060 TUBE: SAMPLE S40 4. 09/24/96 21s 21 Cl. ASS IVOL/WT 0 AUG < oi:)Li> #RPD AUG abs> 43.2600 5.6 0. 124 FUOL PF BATCH NUMBER 61 BURN 1 BURN 2 0. 129 8. 119 TUBEs SAMPLE S60 S' 09/24/96 21 sGS Cl. ARC IVOL/WT 0 AUG < oob) jSRPD AUG abs 59.7100 2.3 0. 164 FUOL PF BATCH NUMBER BURN 1 BURN 2 8.160 8.167 TUBES SAMPLE 860 6 09/24/96 21:: 29 Cl. ASS IVOL/WT 0 AUG < oob) JCRPD AUG...aba 60.6700 0.9 0.246 FUPL PI- BATCH NUMBER 0i BURN 1 BURN 2 0.250' 0-247 TUBEs SAMPLE ICV 7 09/24/96 21s 3 4 Cl. ASS 1VOL/WT 0 AUG < Dob) JtRPD AUG abs ' 53.4700 1.0 0. 164 ^RECOVERY = 106.9 FUOL PF BATCH NUMBER 01 BURN 1 0.163 BURN 2 0.166 169 DUP05 0307412 RUN MAIIEs 9626901F04 PA BE : P. ANALYS T s 114 TUBE: SAMPLE ICB & 09/24/96 21 a 36 Cl. ASS JUOL/WV 8 AUG <ppb) JCRPD AUG abs .1.6000 76.6 0.002 LAMCAOTEii LAOORATOR X EG IN ST RUN ENT Il>: 84724 OFHA GLFi'lEN fAS FUOL DF BATCH NUMBER 8 1 . BURN 1 BURN 2 0.005 -0.000 TUBEs SAMPLE CRA 3 09/24/96 21s 42 CL ASS IWL/UT & FUOL DF BATCH NUMBER 3 1' AUG <ppb) KRPD AUG abs BURN 1 BURN 2 12". 4100 1.0 0.336 -0.036 0.036 TUBEt 10 SAMPLE ecu 1 09/24/96 21s 46 C:L AST; lUOL/UT . i" AUG <ppb) %RPD AUG abs 42.3980 1.7 0.130 ^RECOVERY = 106.3' FUOL DF BATCH NUMBER 0' i BURN 1 0.131 BURN 2 0.12 TUBE: 11 SAMPLE C.CB. I . 39/24/96 21s53 ' GLASS .FUGL/UIT 0' FUOL . 0 DF BATCH NUMBER AUG(ppb? XRPD AUG abs 1.0600 17.6 0.001 BURN 1 BURN 2 0.001 i". 000 12 09/24/96 21s54 ' .... Z.L.ZZ2.Z Cl. ft&O 3 VGL/WT hhkk 100 AUG <cab) ytRPD AUG ab-i 13088 129.6 0.001 FUOL DF BATCH HUMBER 108 1 962681856001 BURN L BURN 2 RR RP 0.005 -0.t302 13 09/24/96 21:59 'Cl. A Si.: I UCIL/MT j; A )t 100 ZZZZZZ AUG (ppb) *RPD AUG abs 21.4400 8.3 0.364 ^RECOVERY - 180.7 FUOL I)F BATCH NUMBER 188 1 962681856801 BURN I. 0.864 BURN r> 0.064 170 DUP050307413 RUN NAME':" 9626901F04 PAGEs 3 ANALYSTS IN TUBE 14 . 09/24/96 22s03 - CL ASS TVOL/WT ZZZZZZ **** 3. AVG < ppb) *RPD AUG *bs 42.1200 2.4 0.129 LANCASTER LABORATORIES INSTRUMENT IDs 0-472-4 GFAA ELEMENT: AC F-VOL PE BATCH NUMBER 1 1 962631856001 BURN 1 BURN 2 RR la) 0.127 8.131 TUBE a IS SAMPLE LCSW 09/24/96 22a07 C:[. A SC 3 VOL/NT ZZZZZZ AVG <ppt)) XRPD AVG abs "60.7700 1.3 0.18? FVOL Pi- BATCH HUMBER 1 1 962661056,881 BURN I. 0.169 BURN 2 0.166 /RECOVERY * 93.2 TUBE; 16 SAMPLE 09/24/96 22 s 12 CL. ASf; IVOL/WT $* 108 FVOL DF BATCH NUMBER 100 1 962661056801 ZZZZZZ AVG<DDb> JCRPD AVG abs BURN 1. BAJ.RH._C. RR RP 1.2700 100.7 0.001 8.084 -0.001 ____ 09/24/96 22 a 16 Cl. ACC IVOL/WT .** ):-)h :Ak 188 ........ . . ..... . .. * ' ......... ..... *" "***" FVOL PF X $t ' h Nu mX ; r 100 1 96,2661056001 AVG <DDb> jtRPD AVG abs 19.1300 0.6 8.857 BURN 1 0. 057 BURN 2 0.057 ' /RECOVERY ~ 69. 3 TUBEs ZZZZZZ 16, 09/24/96 22 a 28 Cl. ASS if VOL. /WT . 4;->: 188 AVG < DDb) /RPP ftV t!l * 'o :> 0. 6700' 99.7 -8.001 19) SAMPLE 563206 09/24/96 22s2S CL ACC if VOL/WT -i;-i A :i 88 AVG <ppb) /RPP AVG abs ' 16.9600 2.0 0.057 /RECOVERY 94.6 FVOL 1)1- BATCH NUMBER 100 1 96,2661;0 56001 BURN.. 1 BURN 2 RR RP 8.801 -0.002 .. .. - -------------------------------- FVOL DF BATCH NUMBER 108 1 96266105686)1 BURN L 8. 05? BURN 2 0. 056 m DUP050307414 RUN NAIIEs 9G26901F04 PAGE s 4 ANALYSTS 1.1.4 TUBES 20 SAMPLE zz_z_z2z5z63207 89/24/96 2E! s 29 ' Cl ACC ;tVOI,/WT 108 8.3300 . zywi* 252.2` 6- Ave *b* -0.002 /TUBE s 21 / SQ.MPL E 2563207 89/24/96 -22 s 33 cu>fi: ifyOL/WT 100 zzzzzz AUGJi3j?>. /RI-'B AVG *bs_ 19.1608 0.1 0.057 54RECOVERY 95. 9 I..ANCA3 ICR I ..AllORATORIES INSTRUMENT II>; 84724 OF Art. ELCMFH f.: AS FUQL _i>E._ BATCH, NUMBER 188 1 962661056081 suatL-L s,u.asL..ii m. ; 0.000 -0.003 FVOk ...M_ B8XCjH,,_WU!aBER 108 1 962661056081 X u r i.._l 0.057 aysttJi 0.057 t u X ; s 22 SAMPLE CCU 2 09/24/96 2236 QJ. ACC IUOL/UIT 8 AUDlaabL .!iPB ' AUG. Ab*. 41.9000 2.3 8.126 1 #F<ECOUERY 104 .6 EmL _J_ BATCH_NUMBER 81 SySJELJL 0.126 SMSJ1_2 0.130 IUBE; 23 SftMPLE CCB 2 @9/24/96 2242 $' ' IVOL/WI 8 AUG<js.Eb>. Ay.G_.abs 1.020.0 31.4 0.001 EiiSk -ML. 3&QXH.Jjuj|IE.A, 81 fi.yBiL.1 BUEfcL h . -0.000 8.001 LUMi 24 777777 "yL ..LJLL7L 2563286 09/24/96 22 s 46 SILML 1ZQL/WT . 106 fiVGJimbl. SBES. ftMfi..aha. 0.4200 ,163.9 -0.081 ESifiL _j w l ,, X $t ' h .n u mX ; r 108 1 962661056001 BURN t BURN 2 RR Ri> 0.000 -0.883 ___ 2563280 Z2Z222 09/24/96 22.: 50 QLBMi imzwi :i. 80 A9G(DDb) &SEB. 20.4680 1.2 0.061 ^RECOVERY 102.4 EMSk 100 BA.ICH ...HUMBER 1 962661056801 g.(,JR.EL_L 0.061 BIJIW.Q 8.062 RUN NAMES 962S901F04 PAGEs V. ANALYSTS 114 ZZZZZ2 09/24/96 22:54 CLMill J..VJtkZ3il U 188 AUG < pctbL ZSBEJ5L AftQ-^kl 1.5300 24.2 0.002 LANCASTER LAOQRATORIES INSTRUMENT IDs 04724 G!rA A ELEMENT : AG FOOL . DF,._ MICtL..NUi!!iliB. 100 1 962631056081 OUKM.. !,. mtL-3.' BE Bft 0.081 0.003 BlSEi 27 SfiMELE 2533209 89/24/98 22 si 50 . Cl. ASS :t VOL/UT U *>* '188 ZZZZZZ AUG <ppb? 20.0908 AUG...aba 0.7 8.868 ^RECOVERY = .92.6 FVQL. _J>._ BATCH., NUMBER 188 1 962831058001 gyfiJbL-k 0.068 IiiMJi.,.2 0..060 ZZZZZZ 89/24/96 23 s83 Cl. ASS IVOL^WI D-i; 5 88 AUG <ppb> *SEft AU_ailSi. 8.9600 25.6 8.000 FUOL 1>F... &ATCH_.,NUHBER 180 1 962631056001 BURN...:i BJjMJl BE Eft , 0.001 --0.800 .............. ... TUBE; 29 SAMPLE ' 533289 89/24/96 23*07 - .SL6ML IV.QkZ.wj: " !> A 108 ZZZZZZ AUG <ppb>_ XRPft AUG,,a.b_% 19.5000 2.2 B.05S a'.RECOVERY = 97.5 FVQL _ftF__ BATCH...NUMBER, 100 1 962631.056001 BjJEii-i 0.057 ayM_E 0.059 BABEs 30 SAMPLE ZZZZZZ3"Ui30 09/24/96 :23s 1 1. Cl. ASS TVOL/WT r -j : * 180 U AVBtjafib) gfiPft AUG aij-> 40 .9100 0.5 8. 125 . FUOL. F_ BATCH NUMBER 180 1 962631056801 BURN .1 SyAfcLS. BE Eft 0.126 0.125 -- -- TUBE:. 31 SAMPLE ZZZZZZ 89/24/96' 23*13 ' CLASS :i VOL/WT 8 F VOL DF BATCH NUMBER 0 1 auftijifitaL jejssft $u g ^m. . SJUBUJ. 59.0900 8.4 0.132 0.131 ftUEhLJ. 0.133 ^RECOVERY = NOT APPLICABLE 173 DUP05 0307416 RUN NflMEs 9626901F04 p $' ; : s 6 ANALYSTi 114 LANCASTER LAGORATOR 2 ES INSTRUMENT I3>: 04724 OFAA ELEMENT.! AS TUBE : 32 ' 09/24/96 23 s19 Cl ASS TV 01 /NT 180 FVOL DF BATCH NUMBER 100 1 962661056801 AVG < ppb? SEES.* AVG BURN t BURN H RR r j > 4-6900 42.1 13.813. 0.017 0.006 33 ssasaiti 89/24/96 23s4 Cl- ACC 3 VOL/WT 1.8 zzzzzz AUG(ppb) *RPP AUG abs 22-2900 2.6 0.067 FVOL I>F BATCH NUMBER 180 1 96S6S1856881 BURN 1 0.066 BURN 2 0. 066 ^RECOVERY * 67.0 TUBEs 34 SAMPLE CCU 3 09/24/96 2 3 s 26 Cl. ACC TVOL/WT 0 AVG<ppb) tfRPP AUG'. ab$ 41.7780 . 0.3 .. 0.126 ^RECOVERY * 104 .4 FVOL DF BATCH NUMBER 81 BURN 1. 8. 126 BURN 2 8. 126, TUBEs 35 SAMPLE CCB 3 @9/24/96 23 s 32 Cl. ACC TVOL/WT. 0 FVOL DF BATCH NUMBER 01 AUG<ob> J6RPP AUG &bi . 1.6600 33.4 0.883 BURN 1 0 . 084 BURN 2 0.001 TUBEs 36 SAMPLE ZZZZZZ2583*23 09/24/96 23 s 36 CL ACC :i UOL/WT * $; *>: s* *>:*sc 180 4! / \ AUG < Rob> jAiPP ftVO Cib'r> 0.5580 90. 1 "0.001 * '* * * ......... ' ~ --;* -------- ----- FVOL DF BATCH NUMBER 188 1 962661056081 BURN 1. 0.800 BURN 2 ~0.082 RR RD ---- t /j &E s 37 SAMPLE 2563623 09/ 24/96 23 48 Cl ACC TVOL/WT >t- >:A * 108 ZZZZZZ *RPP AUG abs 20.3800 0. 6 8.061 ^RECOVERY 181 .5 FVOL DF BATCH NUMBER 100 1 962661056001 BURN 1 0.. 861. BURN 20.861 174 ' DUP050307417 RUM MAMEs 9626*3011-04 PAGES 7 ANALYSTS 114 TUB a a 36. SAMPLE zzzzzz *k 384 09/24/96 23s44 (:l. ASS TWL./WT 100 flVG'tppb? XRPP 70A cU>':> 1- 9000 37 . e.iia LAMCASTER LABORATORIES INSTRUMENT ID: 04724 0!TA A ELEMENT-.; AS FUQL _D BATCH NUMBER 100 1 962661056001 BURN i. BURN 2 ft Ft RD * 0.005 0.002 TfJBli: s 39 SAMPLE 2563624 09/24/96 23340 Cl ASS ' .TUCiL/WT >;-s:-::A' 100 ZZZZZZ AU6<PPb> flRPP AUG ab& '19.7600 1.1 0.059 ^RECOVERY 09.-3 FUQL PF _ BATCH NUMBER 180 1 962601056001 BURN 1 0.059 BURN ft 0.060 TUBES 40 iAMPlir ZZZZZZ S5a3F5 09/24/96 23s52 ci. $&& :i v p l /w t -x-itiH;-;; 1 A AUG C p t*b> T.R.PJ). AUG a B " " r."57i' .55 7? 0T002 FUQL PF BATCH NUMBER 100 1 962601056001 BURN I. BURN 3 ftft RJ> 0.004 0.000 TUBES 41 SAMP Lis 2563825 09/24/96 23sS6. Cl ACC JUPL/UT ' **A* 100 ZZZZZZ AUG <ppb) flftpp AUG abs 20.6300 2.4. 0.862 J5REC0VERY - 96.3 FUQL 1>F BATCH NUMBER 180 1 962601056801 ' 0.861 BURN ft 0.064 TUBE s 42 SAMPLE jtZZZZZ 2583826 09/24/96 00 s00 CLASS IVCO.../NT'. *** 100 FUQL 180 PF BATCH NUMBER 1 962601856881 U (\ AUG (pab) gtRPD AUG wil>- 0.7300 110.9- - 0.800 BURN I. BURN 2 ft ft RP 8.002 -0.802 TUBlfo 43 SAMPLE 2503026 89/25/96 00304 Cl. A SC: AHIL/UT 188 ' FUQL 100 PF BATCH HUMBER 1 962681056081 777? r: AUG < ppb) i*RPP AUG abs 21.4508 2.5 8.864 BURN i 0.063 BURN r> 0^066 JiRECOVERY 187.2. 175 DUP05 0307418 RUN HA ME s 9626901F84 PAGE s ft ANALYST a 114 TUBES 44 SAMPLE ZZIZZ2563627 09/55/96. 00:0ft Cl ASS IVOL/WT 188 AUG (ppb) /RPD A VO a *> > 2.0680" 12.6 0.004 LANCASTER LABORATORIES INSTRUMENT IDs 84724 0!" AA ELEMCM f ; AS FVOL I>F BATCH NUMBER 108 1 962661056081 BURN 1. BURN 2 RR RD 0.004 0.803 ZZZZZZ 09/25/96 00:: 13 C(. ASA I VOL/UIT ft )( 188 FVOL DF BATCH'NUMBER 100 1 962601056001 AVGIPOb? ' iltRPP AVG afas BURN 1 2270680 "4.9 8.869 , 0.066 BURN 2 0.871 /RECOVERY ~ 184.0 TUBES 46 SAMPLE CCV 4 09/25/96 00:: 1.7 ' Cl. ASS 3 VCIL/UT . FVOL 00 DF BATCH NUMBER 1 AVG < ppb? /RPD AVG abs BURN I. BURN 2 42.6300 2.4 0.131 0.133 . 0.12ft /RECOVERY ~ 186.'6 TUBEs 47 SAMPLE CCB" 4 ' 09/25/96 00 s 21. CL ACS \l'VOL/WT 8 AVG <Db) /FiPD AVG aba 1.9900 18.6 8.004 FVOL DF BATCH NUMBER B1 BURN 1 , BURN 2 0. 003 0.004 0.9/25/96 00:: 25 Cl. ft SC IVOL/WT {:** .180 AVG <ppb> /RPD AVC alivi 1.9300 3.0 . 0.~003 FVOL DF BATCH HUMBER 100 1 9626ftI056002 BURN I. BURN 2 RR RD 0.004 0.003 09/25/96 80s29 Cl. ABC 1 VOL/NT ::i: fi-i: 188 e.vfi.laafei.. &Sfi. $ v g abt, 22.6400 1.6 0.069 /RECOVERY * 104.6 FVOL DF BATCH NUMBER 108 1 96266105600 BURN I. 0.066 BURN 2 0.870 176 DUP050307419 RUN '$(; : s PAGE: ANALYST: 9626901F04 ?. 114 TUBEs 3 89/25/96 08s 33 Cl. ASS iruOl./UT v.-iHcr. 3 AUG (nob) iSRPP AVO aiH " 42.8200 _0.& ~0.:L3.t LAHCfiOTP.li LABORATORIES INSTRUMENT IDs 04724 QFAA ELEMENT:: A3 FUOL DF BATCH NUMBER 1 1. 9&B&S 1 056002 BURN 1 BURN 2 RR Rip "0.131 8.132 SAMPLE i..csw LJL%ij^>P, 09/23/96 00s3? ' ci- $s ;.- t u o l /u t i:KKBa:ft .1. FUOL DF BATCH HUMBER i 1 962681036002 AUG (oab) iURPD AUG abs 64.3800 0.5 0.199 BURN I. 0.196 BURN 2 0.200 ^RECOVERY = 103. 6 TUBES SAMPLE 09/25/96 00:: 41. CLASS TUOL/UIT . * .100 FUOL .1.00 PF BATCH NUMBER 1 962661056082 AUG(nob? KRPD AUG abs 1.2200 148.3 0.081 BURN I. BURN 2 RR RR 0.003 -8.803 __ ' _2 09/85/96 00s46 Cl. ASS IfUPL/WT* FUOL : A* 180 ' " l00 PF BATCH NUMBER 1 962681056802 AUG (anb) XRPD AUG abs 18.6600 3.1 5.056 BURN I. 8.85? BURN 2 8.054 TUBE: ^RECOVERY = -a'/a-e- (gjcOb^SI ^3.3 Hu 54 09/25/96 80s58 CtASS IUDL/UT FUOl- PF BATCH NUMBER 100 100 1 962661056002 AUG < ppb) XRPP AUG ab-A 0.2200 125..4 -0.082 BURN 1 BURN 2 RR RR -0.803 -0.00l" SAMPLE 2363223 09/25/96 00.54 C-l. ASS II UOL/WT u A- 108 or ft AUG <ppb> *RPD AUG abs -18.5400 10.3 " ~0.055 ^RECOVERY' 92.7 FUOL DF BATCH NUMBER 10"i 1 962681036002 BURN I. 0.031 BURN 2 0.060 177 DUP050307420 RUN NAMES 962690IF04 PWGEs :1 8 ANALYSTS 114 LANCASTER' LABORATORIES INSTRUMENT ID: 84724 OFAA ELEMENT: AG TUBE s 56 SAMPLE , _, 2563224 09/25/96 B0159 Cl. ASS .T UOL/WT i;-)h : *>;): 100 FUOL 3)F BATCH NUMBER 1B0 1 962661056002 y/ \ Vj AVG <p-pb> /RI-'P AVG aiw ' 0.4200 391. i -0.(301 BURN ). OUk N r; RR r j > -0.005 0.002 ___ ___ TUBE# 57 1 SAMPLE 2563224 09/25/96 01:0.1 Cl. ASS I VOL/WT A 108 HGOfFA AUG (DDb) XRP'D AUG abs 16.3880 3.5 . 0.055 JSRECOUERY 91. ''} FUOL 1)F BATCH HUMBER 100? 1 962661056002 BURN 1. 0.053 BURN 2 0.056 TUBE s 56 s $mp l ; : CCU" 5 09/25/96 01s07' : 01. AGS IVOL /LIT 0 AVG<Pob) XRPP AUG abs 42.4900 1.2 0. 130 ^RECOVERY -- 106.2 ' FVOL 1)1- BATCH NUMBER 01 BURN 1 . BURH 2 0.131 '0^ 1,29 TUBEs 59 SAMPLE CCB 5 09/25/96 01:: li Cl. AGS !l UOL/WT 0 FVOL DF BATCH NUMBER 01 ' AVG<ppb> ^RPO AUG abs BURH 1 BURH 2 1.2800 81. l' 0.001 0.804 -0.001 RftW'Sr TUBE; 60 SAMPLE 2563225 09/25/96 01s15 Cl. ASS IVGL./WT ')--h 108 k /) AUG (DDb)' *RPD 1.150(3. 4.7 A y l f A * > *:s 0.001 ------ TUBE:: 61 SAMPLE 2563225 ` 09/25/96 01.:28 CLASS 1UOL/WT A 100 AUG ( DDb) 3SRPD AVG abs 21.6908 5.6 0.065 ECQUERY * 106. A FVOL DF BATCH NUMBER 188 1 962661856082 BURH i. 0.001 BURN 2 0.001 RR RD ___ ___ FVOL DF . BATCH NUMBER 180 1 962661056002 BURN L 8. 062 BURN 2 8.066 - 178 DUP050307421 RUN NAttEs 9&26901F04 PAGE: .13 ANALYST; 114 R<D^5F 09/25/96 @1:24 CLASS: :i VOL../UT Us:#** 160 .AUG (pob) ZRPD AUG &i>vi 1.930(3 16.3 8.003 LANCASTER LABORATORIES INSTRUMENT ID: @4724 OF A A ELEMENT;! AS FVPL 1>F BATCH HUMBER 166 i 962&ai8se>B0e BURN -L BURN 2 !~<R RD 0.603 0.004 TUBE! 6\3 SAMPLE' 2533226 09/25/96 01s 23 C:), ASS IWL/WT U s; >: s; A 108 AVG <ppb> /RPP AUG aba 20.9780 4.2 0.063 PVOL 1)F BATCH NUMBER 108 1 962631856882 BURN I. 0.065 BURN 2 0.061 FVPL. I>F BATCH NUMBER 180 1 962631856802 BURN I. BURN 2 RR RD 6.000 8.003 TUBE s -65 BAMPL.E 2563226- 09/25/96 01.! 37 ' l mu :i v o l /u t D-x A-y. 106 AVS < D p b) /RPP AVG abs 21.8208 2.7 0.BG& /RECOVERY 162.2 FUOL DF BATCH NUMBER 100 1 962631856002 BURN i. -0.067 IJRN_ 0.064 09/25/96 81.: 41. CL ASP ~.l VOL/UT 180 t p p b) /RPp_ AL:'iL_.aiL:i .4900 0. 1 iTi30 FVPL DF BATCH HUMBER 100 1 962681856002 BURN' L BURN 2 RR RD 0.130 0.130 ZZZZZZ 09/25/96 01s46 Cl. ACL: 1 VOL/UT VT * *)*A 8 FVPL DF BATCH NUMBER 81 AVG(ppb) /RPD ' AVG abs BURN I. 62.6600 0.1 0.193 8.193 BURN 2 8~ 193 /.RECOVERY -- NOT APPLICABLE 179 DUP050307422 RUN NAME! 9686901FB4 PAGE* :i V ANALYSTS 114 TUBE: SAMPLE 63 09/25/96 81:58 Ol. ASC IVOL/WT ^j A' ^SF" 100 AVG<ppb) KRPD AVG &> 3.4600 13.1 0.003 I..ANCAO rER LABORATORIES INSTRUMENT IB: 04724 GFAA ELEMENT: AS FVOL DF BATCH NUMBER 100 1 968631056002 BURN 1 ; BURN A RR RD ".007 0.010 / TUBEs. 39 ' SAMPLE 3533287 @9/25/96 01:54 Cl ASS I VO I-/LIT 100 FVOL BE BATCH NUMBER "l00 1 962631056002 ' __ ' AVGSppb) *RPB AVG abs, BURN 1 BURN .7 2379700 3.7 " 0.072 0.071 8.074 siRECOVERY = 102. 4 TUBES 70 SAMPLE CCV 6 09/25/96 01:59 Cl. AS':C :< VOL./WT 0 AVG < ppb) *.RPO. AUG abs 43*4300 a. 1 0.133 ^RECOVERY = 103.. 6 FVOL BE' BATCH NUMBER 81 BURN 1 0.. 131 BURN... .8. 0. 135 TUBE:: 71 SAMPLE CCB & 89/25/96 02:03 Cl ACS.: TVCU./WT 0 , FVOL BF BATCH HUMBER 01 AVG<ppb) JfiRPD AVG abs.. 15400 1.3 0. 008 BURN 1 BURN 2 0.002 0. 802 nJBEjL 72: 09/25/96 02:07. SAMPLE Cl as s s :; > JVOL/WT i)XS ******' 1 00 AVG'Copb) JiRPB ftVC 3l}':> 0.7400 124.6- 0. 000 FVOL BF BATCH NUMBER 100 1 968631056002 BURN 1. BURN 8 RR RB -0. 082 0. 002 ` -TUBE:: 731 SAMPLE 3533330 09/25/96 82:11 ci, a s s ; I VOL./WT AVG<opb> JiRPD AVG abs 22.5600 2.4 8.063 ^RECOVERY = 11 ci m $ FVOL BF BATCH NUMBER 180 1 962631056002 BURN 1. 0.069 BURN 8 0.067 18 DUP050307423 RUM NAMES 962690IF04 PACE s 1 ;s ANALYST s 114 TUBES 74 SAMPLE. 09/25/96 (:|. ACC S5ft3i*3> 5SbXS-: 02 s 15 :rvoi. /w t 100 ojy AVG < p p b > /RPI> AVG ab-i 0.5400 36. 4~ -0.001 LANCASTER LABORATORX ES XNSTRUMENT IDs 04 724 GFAA CLEMEN T: AS FVOL DF BATCH NUMBER 100 1 362631056002 BURN L BURN 8 RR ED -0.002 0. 000 _____ ___ /rUBEs 75 / SAMPLE 1 253333.1 09/25/96 02 s 19 CLAUS' TVOL/WT 186 .FVGL 100 DF BATCH HUMBER 1 962631056008 cSSbisA WG<ppb> ' *RPP AVG abs .BURN l 20.7400 Aw? 0.062 ' 0.064 BURN 8 0. 060 `/RECOVERY = 103. TUBE a 76 SAMPLE 533332 09/25/96 02#23 c:i. $ ;;;:: :i =? ) /u t .... . FVQL DF BATCH HUMBER. 100 1 962631056002 AVG <ppb) %RPD A VC ab-> 1.3300 12.7 0.002 BURN I. BUuH 2 Aft RD .0.801 8.802 A 77 09/25/96-02;:27 SAMPLE Cl. AST; J VOL/WT FVQL DF BATCH NUMBER 8533332 ft* 100 100 1'962631056002 ibOxsA AVG < ppb> ZRPD AVG' aba 21.4500, 1.3 0.064 BURN 1. 0. 064 BURN 8 0.065 /RECOVERY 180 - & .. ...... . ........ ' " " ------ -------------- - TUBES 73 09/25/96 02131 . SAMPLE Cl. ACC XVOL/WT FVOL......DF BATCH NUMBER A 8533333 1.00 100 ' 1 968631056082 V/ vV /5C>X5 AVG < ppb) / i*RPD ft MG ci b*r> BURN 1. BURN 8 HR RD ,8.7580 33.3 0.000 8. 001 -0.002 TUBES 79 SAMPLE 2533333 89/85/96 02 :35 Cl,ACC :r v o l /w t s j m->:k A# 108 1 ^iTSf> AVG <nob) ZRPD AVG abs 21.7900 1.3 0.065 /RECOVERY 109.8 FVOL DF BATCH NUMBER 180 1 962631056002 BURN 1. 0.865 BURN 8 0 &)?:>& -f DUP050307424 RUN NAME: 9626901F04 PAGE s 14 ANALYST: 114 . TLJBEs B 6 09/25/96 SAMPLE Ct ASS 2503034 1" & I tlS U AUG < p p b > %RPD 0.9000 157.5 02s40 TUOL/UIT 100 AUG ab-i 0.000 I..ANCAGTsi I..AIfORAT0R1ES INSTRUMENT IDs 04724 FRA EU-MF.N f : AS FUQL DF BATCH NUMBER 100 1 962601056082 BURN l BURN r> r r 0.083 -0.003 r jd TUBE s SI SAMPLE 25034134 09/25/96 02s44 CLASS IUilL/UT 100 FUQL DF BATCH NUMBER 180 1 962601056802 F&i AUG (nab) jttRPD AUG abs .BURN ). 22.3500 7.2 8.067 0.064 BURN 2 0.071 ^RECOVERY e 111.0 TUBE:: 62 SAMPLE; CCU 7 09/25/96 02;; 40 Ct ASS TVPL/UIT 0. FUQL 0 DF BATCH HUMBERT 1 AUG < ppb) 14RPD AUG abs 43.5600 2.0 8. 133 BURN. 1. 0. 13 I, BURN 2 8.136 sIRECOUERY = 100.9 TUBE;; 03 SAMPLE COB 7 09/25/96 02:52 CLASS IUOL/MT- FUQL. DF . BATCH NUMBER 081 A OidS-ifijaki. SBE.fi. AUG abs BURN 1 BURN 2 1.0000 sT. 0 .003 0.805 *5.ii BATA REUIEWED BY DATA-VERIFIED BY A 182 DUP05 0307425 LANCASTER LABORATORIES GRAPHITE FURNACE ATONIC ABSORPTION DATA REVIEWED BY DATA VERIFIED BYs DATA HIF NANEs. PBE&ftie RUN NAMES 9626901F03 ANALYST<66 ' IWSTRUWEWT HO: 63613 DKG COiiR : BZ ELEMENT: PB Concentration is used to evaluate if calibration range?. =. ; r*.>u (. Us arc- within 183 DUP050307426 RUM NAME : 9626901F03 PAGE: :i ANALYST: 6 TUBE* 1 SAMPLE ' SB '09/24/96 SB s 46 CLASS JVOL/WT 0 AUGCo&b) *RPD AVG abs a.uses 0.0 0.010 1..ANCA3TE1 i LAB0RAT0R1E! INSTRUMENT IDs 03612 Gi'-'AA ELEMENT;: PB F-VOL DF -BA-TCH HUMBER 01 BURN 1 BURN 2 0.012 0.009 TUBES SAMPLE S3 S 09/24/96 20 s 53 r.t AE:t:: :iv o l /w t 0 -AUGCDDb) jCRPD AVG aba 3.0000 4.4 0.025' FVGL I>F BATCH NUMBER 01 BURN 1 BURM 2 0.025 0.026 TUBES SAMPLE S9 3 ' 09/24/96 201! 56 CLASS IVGL/WT 0 A VS (oob) S*RPD AVG abft 9.0000 .a- & 0.065 FVQL 1>F BATCH NUMBER 01 BURN 1 BURM 2 '0.066 0.061 TUBES SAMPLE S1.5 . 4 09/24/96 21s 03 ci. a s s :: XVOL/WT FVGL DF BATCH NUMBER 0 81 AVGUrmb) *RPD AVG abs BURN 1 BURN 2 15.0000 1.6 0.149' .- 0.147 0.151 TUBE : SAMPLE ssit 5 -09/24/96 21b 06 Cl. ASS XVOL/WT 0 . FVGL 0 DF BATCH NUMBER 1 AVG(DDb) SiRPD AVG ab,,& 30.0000 0.7 0.270 BURN 1 BURN 2 ' 0.269 0.871 TUBE s SAMPLE S3 60 6 09/24/96 21:: 13 Cl. ASS .XVGL/UT 0 AVGCrmb) %RPD AVG abs 60.0000 0.5 0.468 FVGL DF BATCH NUMBER 0 1 BURN 1. BURN 2 0.46L 0.464 TUBE s SAMPLE XCV 7 @9/24/96 21s17 . Cl ASST XVOL/WT 0 AVG(Dob) JSRPD AVG aba 19.9300 a.a 8. 191 ^RECOVERY * 99.6 FVGL DF BATCH HUMBER 0 1' BURM l 0.192 BURN 2 0.191. 184 DUP050307427 RUN NAME : 96269011-03 PAGE s P ANALYST: 66' TUBE a ' SAMPLE ICB 6 09/24/91 2is22 CL ASS:. iv g l '/w t 0 AUG < DDb) JSRPD AUG abs . 0.4200 99.9 0.004 La n c a s t e r l a d o r a t d r ie INSTRUMENT II>: 03612 OFAA ELEMENTS PB FUOL DF BATCH NUMBER. 01 BURN 1 BURN 2 0. 007 0.000 TUBE s SAMPLE" CRA 9 i 09/24/96 21:26. CL A SB IJOL/WT -0 AUG <pb> ' JiRPD AU3 abs 4. 2900 5.2 $.037 FVOL DF BATCH NUMBER 01 BURN 1 BURN 2 0.036 0.036 TUBE: 10 SAMPLE ZZ2ZZ2 09/24/96 21:31 CL ASS:: TUGL/WT 0 ' FUQ'L DF BATCH NUMBER 01 AUG(nob) JCRPD AUG abs 23. 2800 3.7 0.219 TUBE s 11 SAMPLE CCV 1 09/24/96 21:36 ci. a s s :; IUCIL/WT 0 BURN 1 BURN 2 0.213 0.224 ...... ......... ... .. .... .............. FUOL DF BATCH NUMBER 01 AUG(ppb) 7SRPD AUG abs 23. 9200 1.7 0.224 BURN 1 0.221 BURN 2 0.226 ^RECOVERY - 95. 7 TUBE : 12 SAMPLE CCB 1 , 09/24/96 Els 41 CL ASS aVOL/WT 0 FUOL DF BATCH NUMBER 0 1 '. AUG (DDb) JRPD AUG abs 0. 5900 50.0 0.005 BURN 1 BURN 2 0.007 0.003 ----- -- '...... - -....* ------- ^ ,,....... ..................*----- . ....... . . . . . ,............ ... .. .... .... .. M ... TUBES 13 09/24/96 (2 1 m SAMPLE 2563166 2ZZZZf CLASS IVOL/WT 56' FUOL DF ' BATCH NUMBER 50 1 9626-35715001 V AUG(ppb) XRPD AVG abs - 6. 0900. 0.5 0.075 .... ..... .... ~ .............................. .... ........... ...... . . .. BURN 1 0.075 V BURN f> 0.075 RR RD -y $ - 185 DUP050307428 RUM NAME 5 9626901F03 PAGE: ANALYST s 66 AHiL H' 1 PER LABORA TOR1ES INSTRUMENT IDs 03612 GF Aft ELEMENT : PB TUBE 14SAMPLE 2563166 09/24/96 HI 5 50 CL ft SC 3 VOL/NT SB EVOL DF BATCH NUMBER 50 1 962635715801 zzzzzz AVG < Bia&) /RPD AVG abs 19.3900 4.4 0.167 BURN 1 0. 193 BURN 2 0. 16:1? /RECOVERY 56. 5 TUBE s 1 5 09/24/96 HI:: 5 4 SAMPLE Cl ASS IVOL/UT 2503166 B->t SB zzzzzz V AVG(ppb) /RPD AVG abs 2.4780 5. 1 0.821 ... . . . . 4.. " ...... FVOL 50 DF b a t c h Hu mb e r 1 962635715801 BURN 1. BURN_2 RR RD 0.022 0.020 _|^ ___ TUBE s IS SAMPLE 2503100 19/24/96 211; 59 Cl ACC 3 VOL./WT I'HHt x xA-x- . 50 ZZZZZZ ftVG<jjpb) /RPD AV6 abs 14-. 4308 3.1 0.143 FVOL I>F BOTCH HUMBER 50 1 9626357150B1 BURN I. -BURN g 0. 146 0.140 "/RECOVERY " 59.0 TUBE s 17 SAMPLE ' zzzzzz 8563166 09/24/96 22;: 94 CL ASS IVDL/UT R SB y. AVG < ppb) /RPP ft VC ab 14., 3800 0.3 0.142 FVOL DF BATCH NUMBER 50 1 9626357 i 5081" SUCH 1 BURN r> 0. 141 8."l42 TUBE; IS 09/24/96 22509 SAMPLE 250316S Cl. ft SC JVPL/WT K*u*-:cfi 50 zzzzzz ftVG< ppb) ZRPP ftVG abs 26,6600 0.7 0.247 /RECOVERY 62.9 EVQL DF BATCH HUMBER 50 1 962635715081 BURM 1 0.245 BURR 2 0.240 TUBE 5 19` SAMPLE 563623 09/24/96 22;: 13 CL ASS 3V0L/UT ** 50_ AVG (nob) /RPP AVG ab- 26..1100" 6.1 0.241 FVOL DF- BATCH HUMBER 50 2 912635715001 BURH I. BURN 2 RR Ri> 0.~230 0.251 186 * DUP050 307429 RUN NAME: ' 9626901F03 PAGES 4 ANALYST s 66 TUBE s 20i SAMPLE 2563623 09/24/96 22 s 16 ci. a s ;> JUOI../UT s; 50 2Z2Z2Z AUG <'iDDb) 5SRPD AUG abs 44.8200 2.3 _0.371 JtRECOUERY 93. 6 I.. A H C A*- i T f . R 1. A 0 0 R A T 01 : iE G INSTRUMENT 10; 03612 GFAA ELEMENT PB FV01. OF BATCH HUMBER 50 ` ' a 962635715001 BURN 1 0.365 BURN 2 0.377 TUBE s 21 09/24/96 SAMPLE . 2563000 Cl. ASS *: ZZZZlc AUG ( d d Is ) JiRPD 2.5000 . 1.0 22 s 23 :r u o l /w t 50 AUG abs 0.021 FUOL. DF BATCH NUMBER 50 1 962635715001 BURN t BURN 2 0.021 0.021 TUBE: 22! SAMPLE 2583000 09/24/96 22s27 CL ASf: TUOL/WT A 50 zzzzzz AUBCd d U) JCRPD AUG Abe `15. 1100 0. 1 0. 150 *RECGUERY = 0 FUOL DF BATCH HUMBER 50 1 96263571500l" 'BURN- 1 ~8- 150 BURN 2 ' 0~ 150 TUBE s 231 SAMPLE ecu a 09/24/96 22 s 32 CL AS;: TUOL/WT 0 AUG(DDb) 5CRPD AUG abs 24.9900 0.6 0.232. j<RECOUERY = 100.0 FUOL DF BATCH NUMBER 0^ BURN 1 0.231 BURN 2 .0.233 TUBES SAMPLE CCB 2 i 09/24/96 22 s 37 Cl. ASS JUOL/WT FUOL DF BATCH NUMBER 0. 0 1 AUG < DDb) KRPD AUG abs 37.7 0.008. BURN 1 . BURN 2 ' 0.010 0,,"086 TUBES SAMPLE >BW 3 09/'24/96 22 s 41. C.l. ASS TUOL/WT i 100 AUG <pt>b> JCRPD 0.6700. 5.7 .................... . . .AUG 3. 006 FUOL Dr BATCH NUMBER 100 1 962681056001" BURN I. I1JRN ft RR~ Rj> 0.005 3. 006 U .... ........... `.... """""'157""" DU PO50307430 ! 1 ROW NAME: 9626901F83 PA BE : l.i ANALYST: 66` TUBE: ES SAMPLE PBW 09/24/96 22 s 46 C l. A S S IVOL/UT >; Kft* .180 ZZZZZZ AUG < Disb> tfRPD AUG abs 21.4100 1.4 0.284 /RECOVERY = 107'.0 I..ANCAU TEA LABORATORIES INSTRUMENT IDs 03612 Gi"AA ELEMENT:: PE< FVOL I) F BATCH NUMBER 180 1 968661056801 BURN 1 BURN 2 0.201 ' 0.286 TUBE: SAMPLE zzzzzz LCSW X 87' 09/84/96 22:: 58 ' SI. ASS TVOL/WT *h ; 1 AUG < Dob) EG.6300 JiRPD 1.1 AVG tib'i 0. 199 FVOL DF BATCH NUMBER 1 1 962661056001 BURN i. BURN 8 RR RD 0. 197 0.280 _________ t u X ; :; as SAMPLE L..CSU 09/24/96 2Es 55 Si. ASS IVOL/WT 1 zzzzzz AVG<Dobit /RPD AUG abs 42.6580 3.5 0.357 /RECOVERY = 109 . 1 FVOL. DF BATCH NUMBER 1 I 962661856001 BURN 1. 0. 366 BURN 8 0.349 TUBE asi SAMPLE asssaes ZZZZZZ 09/24/96 23 s 00 SI. AST: JVOL/WT 180 X AVG < DDb) 1.0408 JiRPD 44.4 flVG $ !)' 0.009 FVOL DF BATCH NUMBER 108 1 968661056081- .BURN 1. BURN 8 RR RD 0.012 0.006 ___ TUBE: 30i s $mp l ; ; assaae'i 09/S4/96 23u0'i . SI. ASS JVGL/WT A 100 ZZZZZ2 AVG (ocb) JiRPD W(3 $ bs 13.3600 0.6 0.132 ^RECOVERY = 61. 7 FVOL. DF BATCH NUMBER 100 1 962661056001 BURN 1. 0131 BURN r> 0. 132 TUBE 31 s $mp l ; zzzzzzasssees 09/24/96 23s 89 SI. AST: JVGL/WT >:* 100 X AVGCopb) JiRPD AUG $ 0.9200 12.3 0.006 FVOL D'F BATCH NUMBER 108 1 968661056081 BURN 1 BURN 8 RR RD 8.007 0.006 _________ 188 J DUP050307431 RUN NAMES 9626901F03 PAGES C ANALYSTS' 68 ' ` i.. $ n c $ . rrn r i..$ i:< a r $ t ? r l it X INSTRUMENT 'IB: 03812 GFAA ' ELEMENT.! PB TUBE s 32 SAMPLE 2583206 09/2-4/96 23:14 ' * ' + $, ;:.- luriL. WT f uol ' A00 100 X ; 5X $ ' - ./0X ; 1 1 962681056001 ZZZZZZ AUG(ppb) *RPP AVG abs 14.5600 1.3 0.144 BURN :l. 0.1.43 BURN H 0.146. ^RECOVERY = 68,2 TUBE s 33 SAMPLE zzzzzz2583207 . 09/24/96 23s'.6 CLASS TUilL/klT 100 .'AUG < pob? *RPP AUi?i ab-a 1.4900 6.5 0.0l"3 FUOL. DF BATCH NUMBER 100 1 962681056801 BURN I. BURN 2 RR RJ> 0.013 0.012 TUBE s -34 SAMPLE 2583207 09/24/96 23s23 CL ASS 1U0L/UIT >:*: A* 100 / FUOL 100 1>F BATCH NUMBER 1 962681056001 ZZZZZZ AUG < gob) -*RPP AUG aba BURN I. . 13. 7508 5. 8. 0. 136 0. 141 BURN 2 0. 130 ^RECOVERY = 61.3 TUBE: 35 SAMPLE CCU 3 , 09/24/96 23s27 ' CLASS TV0L/V3T .0 'FUOL 1>F BATCH NUMBER ill AUG < ppta> XRPP AUG abs . BURN 1 26.8200 1.0" 0.240 0.238 BURN 2 0.242* ^RECOVERY = 104.1 TUBE; 36 SAMPLE CCB 3 09/24/96 23s32 CL ASC TVOL/UT 0 AUG <? ? I:s > KRl-'ft . AUG abs 1.0500 . 1.4 0.009 FUOL -BF BATCH NUMBER 01 BURN 1 BURN 2 .0.009 8.009* TUBE*. 37 09/24/96 23:36 SAMPLE 2583208 Cl. A SC miL/UT leg zzzzz^: 1C AUG <ppb) ARP I) AVG a ""l.ll00 .6.6 " 0.089 FUOL 180 BATCH .NUMBER i 962681056001 BURN \ BURN r> RR RD 0.010 0.009 -----18 8 DU PO 50307432 RUN NAME: 96269taIF03 PAGE: V ANALYST: 68 LANCftO PER LABORATORIES INSTRUMENT Il>: 03812 G!~Art ELEMENT PD TUBE: 33 SAMPLE 2533203 09/24/96 23:41 a $l u iyj:u./y.l *;?* KA# %m f v o l ? f X $t ' h n u mX ; r 100 1 962661056001 ZZ2Z22 AVGCppb) XRPP ftVG abs 15.2400 0.1 0.151 BURN I. 0.131 BURN 2 0.151 /.RECOVERY ~ 70.6 TUBE: 39 09/24/96 23s46 SAMPLE 2563209 2Z2ZZ2 Cl. ASS IWL/UT U>< ):>: 100 AUG <p 13 b) XRPP AUG ab-= 0.6600 13.5 0.007 FVOL DF BATCH HUMBER 100 1 962661056001 BURN I. BURN 2 RR RjD 0.008 0.007 TUBE: -40 SAMPLE 2563209 09/24/96 23:50 Cl ASS IVOL/WT . U*k A* 180 FVOL 100 PF BATCH NUMBER 1 962681056001 ZZZZZ. AVG < 13pb) /RPP AVG abs ""15.2600 ,0.6- 0.151 BURN 1. 8.152 BURN 2 0.1SI /.RECOVERY = 72.0 TUBE: 41 09/24/96 23 s S3 SAMPLE zzzzzzavia:ia&s P- Cl ASS if VOL/WT FVOL PF BATCH NUMBER k 100 . 100 1 962661056001 A AVI?X AVG(DDb) 5CRPD 0.7400- 5.2 0.006 BURN I. BURN 2 RR' RD 0.006 0.006 ___ 1__ A TUBE: 42 09/25/96 80s 80 P- :RSAMPLE . Cl ASS IVOL/WT FVOL PF BATCH NUMBER A 2563209 hk i k 180 108 1 962681056001 2Z2ZZZ (AVG DDb) XRPD AVG abs BURN 1. 16.9100 1.7 0.183 0. 183 i. 16(3 =/RECOVERY 94. 6 1 TUBE: 43 09/25/96 000'> A SAMPLE 2583209 ZZZZZZ R ;-Cl. ASS 3 VOL/WT im : 188 FVOL IF BATCH NUMBER 100 1 962681036001 (AVG 1313b) /RP& AVG et'o-.l 2BURN t BURN RR RD "l5.6580 "1.9 0.155 . 0.157 0.153___ 190 DUP050307433 RUN HANEs 9&26901F83 PAGES 6 ANALYST s . 66 LA MCA: > TER LABORATORIES INSTRUMENT IP: 03612 f GFAA ELEMENT ; PB TUBE s AA SAMPLE 7.117.17. 09/25/96 60s 09 CLASS TVOL/WT ` ftWWMWft# 0 AUG < nob) JiRPD Allis abs 30.9100 . 0. 277 FUOL DF BATCH NUMBER ' 01 BURN 1. 0.272 BURN 2 .0.261 SSRECOVERY WOT APPLICABLE TUBE s 45 SAMPLE 09/25/96 00: ;3 Cl ASS :i uriL/wr 563210 4:4: 1.00 zzzzzz XV, AUG<Dtib> 5CRPD AVG 1.9500 5.0 0.016, FUOL 100 PF BATCH NUMBER 1 962661056001 BURN 1. BURN RR RD 0.019 0.014___ . ..... . .... . TUBE s 46 SAMPLE 563210 ............ ....... . -- -- ------- ---- ..................... ------.......------------------------ 09/25/96 00s ia Cl. ASS J UOL/WT !: 100 FUOL DF BATCH NUMBER 100 1 962661056001 zzzzzz AUG 'I Dob) *RPD AUG- abs 15.0900 3.3 .0.150 BURN 1 0. 153 BURN 0. 146 ^RECOVERY 65. 7 TUBEs 47 SAMPLE CCV A 09/25/96 00 a 3 Cl ASS TuOL/WT 0 AUG(DDb) ?RPD AUG abs 26.1600 0.0 0.241 ^RECOVERY = 14.& FUOL PF BATCH NUMBER 01 BURN 1. 0.241 BURN 2 0.241 TUBE; 46 SAMPLE; CCB A 09/25/96 08 a 27 Cl. ft Of; TUDL/tJT 0 FUOL PF BATCH HUII BEE? 01 ftVG'(nob) . *RPP AUG abs BURN 1 BURN a 076080 24.~2' 0.007 . 0.006 0,006 TUBEs AS SAMPLE 09/25/96 00s32 ci. Acs :r uoL'/wf 2563623 2ZZZZZ j : k ->:k k TM I SO AUG < ppb) *RPD AUG alw 1.0000 16.8 " 0.006 FVOL PF BATCH NUMBER 100 1 962661056001 r BURN I, BURN r; . RR Rp 0.007 , '0.009 191 DUP050307434 RUN I-I fa ME s 9636901 Ft) 3 fa fa ut::: s ANALYST; 68 TUBE; 'SB. SAMPLE 583823 09/5/9ii 80 s 37 Cl ASS TVOL/WT . K >:-*Ac- 100 ZZZZZZ AV.t31e.abi: ?CRPD AV6 abs 13.7400 1.9 0.136 ^RECOVERY 63. 7 ' ' 234 6247Lfai'icfaG ri.$ $ ;? INSTRUMENT li): 8381 CFAA ELEMENT' PB FVQL DF PATCH NUMBER 100 . 1 96681056001 BURN I. 0.134 BURN 0.137' TUBE;' 51 09/25/96 00.: 41 ` - SAMPLE ukftML TVOt./WT 583624 ZZZZZZ ***: 108 Vs AVG<tmb> JtftPD y\ 0.9600 1.1 0.808 FVQL PF BATCH NUMBER 100 1 962681056801 BURN 1 BURN RR RD 0.008 0.008 TUBE! 52 SAMPLE 583804 09/25/96 80 a 46, Cl $s h TVOL/WT -i: A* .100 ZZZZZZ AVG<ODfo> JSRPD AVG abe 13.4380 7.4 0. 132 SCRECQVERY = 62. A FVQL PF BATCH NUMBER 100 * 1 968681056001 BURN ']. BURN 2. 0.123 ' 0.139 / TUBE! \J ul 09>25/96 80s 51 SAMPLE Cl ASS TVOL/WT 583825 ZZZZZZ % AUG (ppb) y.RP 0.8500 18.2 100 hA VC A ':'t 0. 007 FVQL 1>F BATCH NUMBER 100 1 966 &i05 6B@T i'jiJ;Vl't t. BURN r; RR RD 8.088" 0.807 . ' TUBE; 54 SAMPLE 583825 09/25/96 08; 58 ' Cl ACC IVGL/WT A-k .1.00 ZZZZZZ AUG ( cob) sCRPD AVG ab& 13.5800 0.2 0. 134 ^RECOVERY * 63* 6 FVQL PF BATCH NUMBER 16 1 962681056001 BURN 1 0.134 BURN :> 0,134 TUBE;. 55 SAMPLE zzzzz/5a36E6 . 09/25/96 8 la 80 Cl. ACC TVOL/WT -K 188 V A .............................. .. AVG <ppb) 0.8680 . . . ... .... -/RPD A VO a 14.7 8. 887 ....... ................... FVQL PF jiflTCH NUMBER 180 1 966 S1056001 BURN I. BURN P. RR RD 8.006 "13.004 192 DUP050307435 RUN NAME! PAGE s ANALYSTS 9626901F03 !0 68 TUBE; 56 SAMPLE 2583826 09/25/96 81*05 Cl. ASS IUOL/WT it ):j;-A 180 AUG <ppb> JCRPD ftVG AbB :Z2 12.*600 1.7 8. 124 ^RECOVERY 59. 0 LANCASTER LA.BORATURIEG INSTRUMENT I'D: 03812 GFAA ELEMENT PB EUOL DF BATCH NUMBER 180 1 9626810568Wl BURN 1. 0. 123 Bu r n 2 8.125 TUBE s 57- * SAMPLE zzzzzz 25*3827 09/85/96 01;; 1 CLASS IUCL/WT 3t*KKKXX .1.88 AUG /RPP AUG *!> A 0.7800 1.9 0.007 FUOL DF BATCH NUMBER 180 1 962681056081 BURN 1 BURN 2 RR RjD 0.006 0.887 v TUBE s 56 SAMPLE H & 3 is c?y - 09/25/96 01 a 1.4 CL AWT 1UOL/WT Aii 188 zzzzzz AUGippb) /RPP AUG abs 22.6900 2.9 0.215 A/RECOVERY' ~ 114 h EUOL DF BATCH NUMBER 180 1 962681056001 BURN 1. 8.220 BURN 2 8.211 TUBE s 59 09/25/96 01 a 19 SAMPLE CL ASS 1UOL/WT FUOL DF BATCH NUMBER A DCU 5 8 01 ' AUG <ppb) /RPD AUG aba 26.0100 0.1 0.240 BURN l 0.24B BURN 2 8. 240 /RECOVERY = 104.0 TUBES 60 SAMPLE CCB 5 9/25/96 91s2'i CL ASS 1UOL/WT 0 FUOL IF BATCH NUMBER 01 A AUG<ppb> TURPS AUG A I? s BURN 1 BURN 2 1.0500 25. 6 0. 009 0.010 0.007 Pai/i TUBE s SAMPLE PBW " 09/25/96 01 a 2 3 Cl. ASS IUOL/WT i; i 100 AUG < emb) JCRPD A.V..Q_ 0.8508 23.5 8. 007 FUOL D:- BATCH NUMBER 100 1 962681056002 BURN 1. BURN f? RR RD 0. 088 8.006 193 DUP050307436 R UH HAME: 96S6901F 03 PAGE s :l :i ANALYST: 68 TUBE s 62 SAMPLE PBW 09/25/96 01s33 <:! ASS TUOL/Ut , 100 P&l DA AUGCoab) /RPD AUG aba 23.0400 2.3 0.217 /RECOVERY * 111.0 LANCASTER I..AB0ft ATUR S. ES INSTRUMENT ID;' 03612 OF AA ELEMENT:: PB FUOL DF BOTCH NUMBER 100 1 962681056002 BURN 1 0.220 BURN ? 0.213 TUBE s SAMPLE LCSW LCSU3 . 63 09/25/96 CM. ASS AUG (nob) J4RPD 21.8100 1.2 01s 38 TUOL/WT 1 AUG abs 0.207 FVOL DF BATCH NUMBER 1 1 962681056002 BURN 1. Bl (AM 2 RE ftD 0.205 0.288 ___ ___ TUBE: 64 SAMPLE . LCSU 89/25/96 01:: 43 . C:l ASS . TVOL/WT '.i w k A at 1 FUOL 1 DP BATCH NUMBER i 962681056002 AUG (nob) #RPD AUG abs . BURN I. 44.8700 1.7 0.372 0.367 BURN 20.376 /RECOVERY- '115 . 3 * ......... ` TUBE: 65 @9/25/96 81:: 4 7 SAMPLE Cl. ASS: TVOL/WT FUOL DF BATCH NUMBER 2583222 , , . :188 100 1 962681056002 RTSS'S-F <L/ X AUG (nob) /RPD AUG abs 8..5300 99.9 0.004 BURN 1. BURN RR R'D 0.009 0.000 _________ TUBE: 66 SAMPLE 2583222 09/25/96 01:52 CM. ASS TUGL/WT Ok 108 *' " **'' ** - " -- FUOL DF BATCH HUMBER 188 1 962681056002 AUGCoob) JiKPD AUG abs 13.6900 .1.2 0.135 BURN i. 0.136 BURN r 0.134 /RECOVERY = 68. 4 --------------------------- ..... ....... ... . . ..... ; . ... TUBE: 67 SAMPLE 2583223 09/25/96 01 s 57 CM. ASS II UOL./WT 3 80 esH-br XvV AUG(nob) XRPD. AVG 0.2100 23.5. 0. 002 .. > .< ...M * -- -- -- -I,,,,. FUOL 100 DF BATCH NUMBER 1 962681056002 * BURN 1 BURN 2 -RR i-.-I) 0.002 . 0.001 , ___ 194 DUPO 50307437 RUN NAME s 9626901F03 PA0Es IE ANALYST I 6 LAMCAG f Eft l..ABORATORIES INSTRUMENT .IDs 83812 GFAA ELEMENT:) PB TUBE: 68 SAMPLE 2533223 89/25/96 02 : 08 Cl .TUOL/WT K-A 1 00 . FUOL ~188 DF BATCH NUMBER 1 962631056002 A AVGtDob) .'TIPP'D AUG abs BURN I BURN 2 12.5280 2,7 0.122 8.128 0.125 ^RECOVERY = t2. & TUBE : 69 SAMPLE 2533224 ' 09/25/96 02:08 Cl AOS - TUOL/WT 100 X AVGOaobl WPB AUG aba 0.0500 99.3 0.000 FUQL' DF BATCH HUMBER 1B0 1 962631056002 BURN * 1 BURN RR RD '.081 0.800" TUBE: 70 SAMPLE 8533224 09/25/96 82:11 Cl ASS t u o l /w t uttK-i;-)! A* 100 4&&PFA AUG(DDb) VCRPD AUG abs .13.2100 14.8 .0.130 JCRECGUERY = 66. 8 FUOL DF BATCH NUMBER 180. 1 06,2831058002 BURN 1. "0.118 BURN 2 .0.143 TUBE: 71 SAMPLE CCU 6 09/25/96 02: 16 Ct ASS TUOL/WT 0 AUG <ppb> *RPD AUG abs 85.1088 1.7 0.233 ^RECOVERY - 100i. 4 FUOL DF BATCH NUMBER 81 BURN 1 0.238 BURN 2' 0.230 TUBE: 72 SAMPLE CCS 6 09/25/96 02128 Cl. ACC TUOL/WT 8 FVOL DF BATCH HUMBER 81 AUG Snob) 0.6300 i JSRPD 61.1 AUG abs .0.005- BURN 1 0.088 BURN 2 0.003' TUBES 73 SAMPLE 2533225 .' 09/25/96 08:: 25 Cl. ASST TUOL/WT . " 10B X M. AUG {or,b> -siRPD 0.6800 13.5' 0.006 , ......... ................................. . . . . .................. FUOL DF BATCH NUMBER 188 1 '962631856082 BURN. I. BURN 8 RR RjO 8.085 87086 195 DUP050307438 RUM NAME9626901FW3 PAGE;; :i C ANALYSTS 68 LAMCAS f ILK .AUORAVuR i EG INSTRUMENT IPs 03312 OFAA ELEMENT : PB TUBE a 74 SAMPLE 2583225 89/25/96 82:38 c:i.$s s j v o l /u t s' -k k >:-Ah 100 e.AH'S-FA AVG <ppb) XRPP AVG aba 2070700" 8-8 8.193 f v p l . PF BATCH NUMBER 100 1 962631056802 BURN 1, 0-193 BURN 2 0.193 /RECOVERY = 108-4 TUBE a 75 SAMPLE 2533226 89/25/96 02:34 Ci. ASS :t VOL/NT 1.80 AVG <ppb) /RPD AUG atw 8.2108 68.0" 8.002 FVOL PF BATCH NUMBER 100 1 962631856802 BURN I. BURN 3 RR RJD 0.803 ~8 801 TUBEs 76 SAMPLE . 2533226 89/25/96 02 a39 CLASS 1VOL/UT 100 AUG(cab) /RPD AUG aba 13.3188 7.0 0.136 /RECOVERY 69.8 FVOL PF BATCH NUMBER 100' 1 962631856002 BURN t 0.138 BURN 2 0.143 TUBES 77 SAMPLE 2533226 09/25/96 02 a 4 4 Ci. ACC 1 VPL/UIT 100 AUG (ppb) /RPD AVG ai)':i 0.3700 32.5 0.003 FVOL PF BATCH NUMBER 100 I 962631056,082 BURN I. BURN 2 Rfi R 0.002 0.004 TUBE s 78 SAMPLE 2533226 09/25/96 0Sa 40 Ci. ASS JVQL/WT !>*** A* 100 -CiA AVGtppb) /RPD AUG alas 14.3400 0.5 0.142 /.RECOVERY = 71.7 ' FVOL PF BATCH NUMBER 100 1 962681056002 BURN 1 0.14C BURN 2 8. .141 lUBEs. 79 SAMPLE 2533226 09/25/96 02 a 55 Cl. ACC T VOL /MT R ** ):>; 186 AVG <ppb>. /RPD AVC ab-i 18.5588 0.1 0.138 FVOL PF BATCH NUMBER 108 ' 1 962631056802 BURN I. BURN 2 r r 8.130 8.138 RD 196 DUP050307439 RUM NAME PAGE s ANALYST s 9626901F03 :i A 66 LAMCAOTER LABORATORIES INSTRUMENT TBs 03612 V GPAA 1TLEi'IGM fPB TUWEs 68 ' SAMPLE Z2Z2ZZ 09/25/96 02 s 56 CL ASS iu o l /w t RttKKttAtt 0 flUGCppb) iXSRPP AUG a I? s 31.21(30 12.7 S.279 FUOL DFr BATCH NUMBER 0 1 BURN 1 0.254 BURN 2 0.304 ^RECOVERY =. MOT APPLICABLE TUBES SI SAMPLE 2563227 09/25/96 Cl. ASS RPf 2>SF. XV/ AUG (? o Li ) *RPP 0.3100 14.3 03 s 02 JVGL/WT 100 V Li ci O j 0.003 FUOL DF BATCH NUMBER 100 - 1 962661056002 BURN 1. BURN 2 RR RD 0.002 ' 8.003 ___ TUBE s S2 SAMPLE 2563227 09/25/96 03 s 07 CLASS JUOL./WT ::-x 3h :Ah 180 AUG < ob> %RPD AUG abs 12.3200 2.7 0.120 SSRECOVERY 61. 6 TUBE s S3 SAMPLE CCU 7 09/25/96 03:: 12 Cl. ACC JVOL/WT 0 . AUG(oob) XRPP AU(3 abs 25.5300 1.9 0.236 JiRECGUERY = 102:. 1 TUBEr 64 SAMPLE CCB 7 09/25/96 83:: 16 CLASS I UOL/U)T 0 'AUG < oab> SRP AVG abs 0.6000 11.4 0. 005 FUGL. DF BATCH NUMBER 100 1 962661056082 BURN L 8. 123 BURN 2 0. 116 * ' ................ .. ~~ FUOL ...DF BATCH NUMBER 01 BURN 1 . 8.233 BURN 2 0.239 * * * '* ` ' " . , .. ------------ FUOL DF BATCH NUMBER 01 BURN 1 BURN 2 0.006 0.085 TUBES 65 SAMPLE 2563638 09/25/96 03 s 21 ' l $s s :: :i VOL /WT *:*: ' 100 ' 'Is ftVGdiob) StRPD A VC ell?*:! 0.2600 63.3 0.002 FUGL DF BATCH NUMBER 100 1 962661056002 BURN 1 BURN 2 RR RD 0.003 0.. 881 -- 197 DUP050307440 qv-widKifr...... i^^;^.v--.'. - RUN NAME:; 9626901F03 PAGE:: .15 ANALYST: 66 t u X ; : s ae SAMPLE 2583838 09/25/96 03:26 Cl ASS . :i VOL/WT *;-};w A-h 100 3) CiCi-L_<Saf\ AVG < Dials) XRPD AVG afas 14.4100 4.2 0.143 ^RECOVERY 72.0 I .ANGAG (': ! : EmBORh i'UK $ !.... INSTRUMENT ID: tl-stuT ora $ ; l ; m; n t .; p X FVOL DF BATCH HUMBER 100 ' f 962681056002 BURN l 0. 14? BURN rt 0. 130 TUBE: 67 SAMPLE asasas 09/25/96 03:30 Cl. ASS 1VOL/WT :;>:>:>: ;100 v AVG < ppb> flRPP . A VO a 'q -a 4.6200 2.2 0.040 FVOL 1)F BATCH NUMBER 180 1 962661056002 BURN I. BURN C; RR RD " 0.039 0. 04l" TUBE:' 66 SAMPLE 2563833 09/25/96-03:33 ' (:l. ASH 3 VOL/WT 180 FVOL PF BATCH NUMBER 180 1 962661856082 AVG<ppb> *R1-`P AVG abs .- BURN 1 17.9680 14.4 - 0.175 0.193 BURN 2 0.157 Sf.RECOVERY ~ 66.6 TUBE: 69 SAMPLE 2J&3V3 09/25/96 03,! 39 01 ASS :i VOL/UIT 100 AVG <pnb? *RPP AVG aii-i 0.4680 29.3 8.804 FVOL DF BATCH HUMBER 188 1 962661856802 BURN 1 BURN C; RR Ri) 0.005 0.003 ___ TUBE: 98 SAMPLE 2583832. 89/25/96 03:44 Cl ASS JVOL/WT W 18 AVG(DDb> *RPP AVG abffi 14.2488 3. 6 8. 141 ^RECOVERY = 71.2 FVOL DF BATCH NUMBER 100 i 962681856002 BURN 1. 0. 144 BURN 0 0. 137 TUBE : '91 SAMPLE 2583833 09/25/96 '03 ; 49 Cl A Si; IVOL/WT 180 AVG < ppb) XRPD AVG abs 8., 2400 28.1 8.082 FVOL BF BATCH NUMBER 108 1 962681056082 BURN i. BURN 2 RR R]D 0.082 8.002 198 DUP050307441 RUN NAME.! 9626901F03 PAGE s if. ANALYST! 66 TUBE s 92 SAMPLE 2563633 09/25/96 83:53 ci. $88 iv o l /w t 188 i^bX'SA AVG<ppb> . KRPP AUG abs "14.2700 1-6 0.141 ^RECOVERY = 71.4 LANCAG f ER LABORATORIES INSTRUMENT ID: -, 83612 orAA ELEMENT 4 PB f vol 188 p f X $t ' h n u mX ; r 1 9626610S6082 BURN 1 8.143 BURN 2 0-140 TUBE: 93 SAMPLE 2563634 89/25/96 03s56 Cl/ $s ;-:: IIVOL/WT *** 180 FBi CiS V, X AVG v ppb) ?SRPD " 8-1100 44.7 AVG abs 0.001 FVOL DF BATCH NUMBER 108 1 962661856002 BURN I. BURN 2 Rft RP ~0.001 0.001 ;____ ___ TUBE: 94 SAMPLE 2563634 09/25/96 04s83 CLASS :r v o l /w t . *: $:** Am 188 FVOL 180 PF BATCH NUMBER . 1 962661856002 - AVG < PDb) 34RPP AVG abs 22.0980 3.6 0. 209 BURN 1 8.204 BURN 2 0. 214 ^RECOVERY '110 .4 TUBE s 95 SAMPLE CCV 6 09/25/96 04 s7 . CLASS :r v o l /w t 8 AVG (nub) SiRPD ftVG._a.tas. 25.6980 2.2 0.236 ^RECOVERY = 102 .6 FVOL DF BATCH NUMBER 01 BURN 1 0. 234 BURN 2 0. 241 TUBE: 96 SAMPLE CCB 6 -09/25/96 04 s 12 Cl. ASS I VOL/WT 0 AVG < DEr b ) JCRPD AVG abs 0.3400 76.6 8. 083 FVOL' DF BATCH n u mX ; r ; . 1 BURN 1 BURN 2 0.884 0. 801 DATA REVIEWED 'BY DATA VERIFIED BY; 199 DUP050307442 LANCASTER LABORATORIES GRAPHITE FURNACE ATOMIC ABSORPTION DATA REVIEWED BY: *7 DATA VERIFIED BY: / |(V{ DATA FILE NAME: PB26903 RUN NAME: 9676902F03 ANALYST: 859 ' INSTRUMENT NO: 03812 RK6 CORR: BZ ELEMENT: PB 200 DUP050307443 RUN 9$:; : : 9626902F03 PAGE : 1 ANALYST: 859 TUBE : SAMPLE SO 1 09/25/96 05:47 CLASS JVSUWI 0 AVG/oobl %RPD AVG abs 0.0000 0.0 -0.007 LANCASTER LABORATORIES INSTRUMENT ID: 03812 GFAA ELEMENT: PB F VOL ...1OF BATCH NUMBER 01 BURN 1 BURN 2 -0.007 0.000 TUBE: SAMPLE S3 2 09/25/96 05:50 CLASS is u j u w t . 0 AVGCDDb^i %RPD AVG abs 3.0000 0.0. 0.035 F.y0.L JCL. BAICilJiUM&EB. 01 BURN 1 BURN 2 0.035 0.000 TUBE : SAMPLE so 3 . 09/25/96 05:52 CLASS iy.QL/WT .0 AVGFoob') %RPD AVG abs 9.0000 0.0 0.091 FVOL DF.... BAICH.J.MMBEE 0 1' BURN . 1. BURN 2 (i .091 0.000 TUBE : SAMPLE S15 4 09/25/96 05:55 CLASS IV01,ZWT 0 FVOL OF... BATCH NUMBER 01 A AVGifpobl ' %RPD AVG abs BURN 1 BURN 2 15.0000 0.0 0.156 0.156 0.000 TUBE : SAMPLE S30 5 09/25/96 05:58 CLASS IVOL/NT 0 FVOL DF BATCH NUMBER 01 A AVG/oobl 9!RPD AVG abs BURN__1_ BURN 2 30.0000 0.0 0.290 0.290 0.000 A A TIJRf: 6 09/25/96 06:00 SAMPLE CLASS T VOL/WT FVOL DF BATCH NUMBER S50 0 0 1 AVGI Dob') SRPD AVG abs 60.0000 O.O 0.483 BURN V BURN 2 0.483 .0.000 TUBE r SAMPLE 1CV 7 09/25/96 06:03 .Q.LAJSS IVQ.L./WJ 0 AVG (Dob'S 2SRPD AVG abs 18.8900 0.0 0.193 ^RECOVERY = 94 . 4 FVOL .DF BATCH NUMBER ' "6 1 BURN 1 0.193 BURN 2 0.000 201 DUP050307444 RUN NAME: 9626902FQ3 PAGE : 2 , ANALYST; 859 TUBE; SAMPLE. i' X ; 8 09/25/96 06:05 CLASS. IliQL/MT 0 AVGfoobl %RPD AVG abs 0.4500 0,0 0.005 LANCASTER LABORATORIES INSTRUMENT ID: 03812 GFAA ELEMENT: PB FVOl -P.F_ BATLH..NUMBER 01 BURN JL BURN 2 0.005 0.000 TUBE ; SAMPLE CRA 9 09/25/96 06:08 CLASS IVOL/NT 0 AVSfoobO %RPD AVG abs- 3.0500 0.0 0.036 Em ...D.E,,. BATOH_JiUJlBER 01 BURN.. 1 BURN 2 0.036 0.000 TUBE:' 10 SAMPLE CCV 1 09/25/96 06:10 GLASS. LV.0.UW.I 0 AVGfDDbl %RPD AVG abs 24.1400 . 0.0 0.240 ^RECOVERY * 96 .6 FVOL QF_ BATCH.NUMBER 01 BURN J_ 0.240 BURN 7 0:000 TUBE: 11 SAMPLE CCB 1 ` 09/25/96 06:13. . CLASS I VOL /WT 0 AVGfoDbl 5SRPD AVG abs 0.3900 0.0 0.005 F VOL OF BATCH NUMBER 'o 1 . BURN 1 BURN 2 0.005-' 0.000 TUBE: 12 SAMPLE 2583168 09/25/96 06:15 CLASS I VOL/NT u****0* 50 zzzzzzq> CONC foobl' V.5400 BURN 1 0.018 TUBE: 13 SAMPLE 2583168 09/25/96 06:18 CUSS. IVQUWT y****1* 5Q ZZZZZZl CONCfoobl 4.4600 BURN 1 0.050 . Em .OF ._. BATCH.NUMBER 50 1 962635715001 , FVOL DF BATCH NUMBER 50 1 962635715001 TUBE: 14 SAMPJLE 2583168 09/25/96 06:20 . &LAS.S m&JML (j****2* 50 ZZZZZE ^ CO_NC fpp.b> BURN 1 .... 7 cSBO'O...." .... 0". 082 Em. JJL- BAJSJH NUMBER 50 1 962635715001 '. DUP050307445 RUN NAME: 9626902F03 PAGE: 3 ANALYST: 859 IlifiLi. 1-5 SAMPLE 2583168 09/25/96 06:23 CLASS IVOL/WT U**:**3* 50 V CONCfppbl BURN 1 9.9300 0.100 2ZZZZZ 5 LANCASTER LABORATORIES INSTRUMENT ID: 03812 6FAA ELEMENT: PB LV.QL J2JL. &ATC.H_N_UME.E.R. 50 1 962635715001 X INT CORR COEF SLOPE Y. INT 3.74101 0.99248 0.00556 0.02080 R | I TUBE: 16 SAMPLE 2583168 no/95/9K 06 26 ' CLASS IVOL/WT 0****0* 50 CONCfppbl ZZZZZZq> 1.4600 BURN 1 0.017 FVPL ,,PL. BA.Tm..MMKB 50 1 962635715001 TUBE: 17 SAMPil 2583168 09/25/96 06:28 CLASS IYQLZWI 0^**1* 50 ZZZ22Z| CONCCpobV 4.6500 BURN 1 0.052: LVQL 50' 1 962635715001 TUBE:. 18 SAMPLE 2583168 09/25/96 06:30 CLASS I VOL /WT. D****2* 50 ___ CONC/ppbl 9.3800 BURN 1 -0.095 F.VOL. J2... BATCH..NiiMBIR 50 1 962635715001 TUBE: 19 SAMPLE 2583168 09/25/96 06:32. CLASS IVOL/WT 0****3*. 50 V Z2ZZZZ ^ CONCfppbV 10.6100 BURN 1 0.108 FV.OL. OF... BATCH NUMBER 50 -i 962635715001 X INT CORR COEF SLOPE Y INT 3.25949 0..98120 0.00632 0.02060 TUSF: 20 SAMPLE 2583168 . 09/25/96 06:35 CLASS IVOL/WT R****0* 50 ZZZZZZCt) 13.5400 BURN 0.140 FVOl OF BATCH NUMBER 50 1 962635715001 203 DUP050307446 RUN NAME: 9626902F03 PAGE: 4. ANALYST: 859 TUBE: 21 SAMELt- 2583168 09/25/96'06:37 CLASS' I VOL /WT R****1* 50 ZZZZZZ I CONCfoobl 17.3500 BURN...1 0.178 LANCASTER LABORATORIES INSTRUMENT ID: 03812 GFAA ELEMENT: PB FVOL DF 8AT.CH,,mMB,ER . 50 1 962635715001 TUBE: 72 SAMPLE 2583168 09/25/96.06:40 . CLASS mUMT R***2* 50 zzzzzz a CONCfppbl . 19.9400 BUSfeLl 0.202 FVOL DF_ BAICH HUMBER 50 1 962635715001 TUBE: 23 SAMPLE 2583168 09/25/96 06:42 . . CLASS IVOL/WT R****3* 50 V CONC(pabi BURN i . 25.3200 0.250 ZZZZZZ'3 FVOL DF BATCH NUMBER 50 1 962635715001 Y TNT CORR COFF SLOPE Y TNT 19.68927 0.99233 0.00708 0.13940 RR TUBE : 24 SAMPLE 2583000 09/25/96 06:45. CLASS T.VOL /NT *****0*. 50 F.VQL J)F_ BATCH NUMBER . 50 -1 962635715001 ZZZZZZCD CDNCfppbl 1.5200 BURN 1 0.018 TUBE: 25 SAMEL E 2583000 09/25/96 06:47 CLASS IVOL/WT ' gg 'ZZZZZZ| CONC fppbl 6.1900 BURN 1 0.067 FVOL JBJL. BATCH NUMBER 50 1- .9626357 15001 TUBE: 26 SAMPLE 2583000 09/25/96 06:49 ' l $s s imywx ^ 50 ZZZZZZ a CONC(? o hi 10.6900 , BURN 1 .0.108 FVOL DF BATCH NUMBER 50 1 962635715001 204 DUPO 50307447 RUN NAMF: 9626902F03 PAGE': 5 ANAI YST: 859 TUBJE: 27 SAMEkE 2583000 09/25./96 06:52 CLASS IVOL7WT *****3* 50 CONC (ppbl 13.7800 BURN ,1 0.142 Z2ZZ2Z3 TUBE: 28 SAMPLE 2583831 09/25/96 06:54 SkASS miUMl *****o* 50 o /5iC>X3' S> CONC/'ppbl 0.2900 'BURN 1 . 0.003 I ANCASTFR LABORATORIES INSTRUMENT ID: 03812 GFAA ELEMENT: PB E.V0L ,,P_F._ BATCH...NUMBER .50 1 962635715001 X INT CORR COEF SLOPE Y INT = 2.63923 RP 0.99672 _ 0.00826 0.02180 RD _ fVQL ,.DF_ BATCH NUMBER . bo .. i 962634Js.ooi/*' TUBE: 29 SAMPLE 2583831 09/25/96 06:57 CLAS.S imi/WX *****; )* 50 <^>>TSI C.QHQ.CBBfel 4.0000 BURN.J. 0.046 FVOl 50 DF BATCH NUMBER 1 96263571500^ 8-HSl, CD TUBE: 30 SAMPLE 2583831 09/25/96 06:59 ' l $s s imuwx ***:**: 2* 50 BURN 1 0.084 FVOL JBA BATCH NUMBER 50 i 9626574-500/i' TUBE: 31 SAMPLE 2583831 09/25/96 07:02 CLASS I VOL/NT *****3* , 50 CONC(pnbl 11.9000 BURN 1 0.122 FVOL OF BATCH NUMBER 50 1 96263^1500/^ / X INT * CORR COEF = SLOPE = Y TNT = 0.56962 RJR 0.99952 0.00790 "' 0.00450 RD "" TUBE : 3 2 SAMPLE CCV 2 09/25/96 07:04 CLASS I VOL/NT O' FVOL _HE_ BATCH NUMBER 01 AVGfppbl %RP0 AVG ahs BURN 1 24.9600 0.0 0.247 ~0.?47 BURN ? O.OOO" %RECOVERY =99.8 205 DUP050307448 RUN NAME: 9676907F03 PARE : 6 ANALYST: 859 TUBE: 33 SAMPLE CCB 2 09/25/96 07:07 CLASS I VOL/WT 0 AVCK? ? M 1 %RPD AVG abs 0.6700 . 0.0 0.008 LANCASTER LABORATORIES INSTRUMENT ID: 03812 RFAA ELEMENT: PR FVOf. DF BATCH NUMBER 01 BURN 1 BURN 2 0.008 0.000 DATA REVIEWED BY: DATA VERIFIED BY: 206 DUP050307449 LANCASTER LABORATORIES GRAPHITE FURNACE ATOMIC ABSORPTION DAT A RFVIEWED BY DATA. VERIFIED BY: DATA FILE NAME: SE26811.RAT PUN NAME: R626901F05 ANALYST: 68 INSTRUMENT NO: 04725 BKO CORR: R7 ELEMENT: SE "ar*Cnnoentrati on Is used to isvalua+'ef Tf 4 4aiBT<s'`rftsults wTEFiin calibration range. 207 DUP05 0307450 RUN NAME : 962690TF05 PARE : 1 ANALYST: 68 TUBE : SAMPLE SO 1 09/25/96 01:23 SLASS LYQL/wi 0 AVGfDDbl %RPD AVG abs -1.1600 24.9 -0.001 LANCASTER LABORATORIES INSTRUMENT ID: 04775 GFAA ELEMENT: SE - FVOL OF BATCH NUMBER 01 BURN 1 RMRN 7 -0.000 -0.001 TUBE: SAMPLE S5 2 09/25/96 01:27 CLASS IVOL/WT 0 AVG/onbl 35RPD AVG abs5.0700 5.4 0.015 FVQL BE BABLH NUMBER 01 BURN 1 BURN 2 0.016 0.015 TUBE : s $mp l ; SI 5 3 09/25/96 01 :3 1 CLASS. LYQL/.WT 0 AV6fDDb> *RPD AVG abs 14.0800 0.1 0.043 FVOL DF BATCH NUMBER .0 1 gURN_1 BURN 2 0.043 0.043 TIJRE : SAMPLE S2 5 4 09/25/96 01:35 CLASS mum 0 AVGfppbl %RPD AVG abs 22.7400 5.4 0.065 E.VOL J2JF... B_AiatLMjyMM,R 01 BURN 1 BURN 2 0.062 0.067 TUBE : SAMPLE. S40 5 09/25/96 01:39 CLASS IVOL/WT 0 AVG(pobl %RPD AVG abs 38.8100 0.7 0.102 LY.QL .J?. E_ 01 ' BURN 1 BURN ? 0.107 0.101 TUBE : SAMPLE S50 6 09/25/9.6 01:43 CLASS T VOL/WT 0 AVGfnnbl %RPD AVG abs 49.2000 5.4 0.126 FVOL DF BATCH NUMBER 01 BUPN 1 BURN ? 0.121. 0.131 \ TURF.:.. SAMPLE ICV 7 09/25/96 01:47 CLASS IYQUWI 0 AVG/Db1 %RPD AVG abs 19.2200 7.0 0.050 ^RECOVERY -.96.1 FVOL _Qf_ B.AT_Q.tL.N.U.MB.ER 01 BURN 1 ' BURN. 2 0.053 0.048 208 DUP050307451 RIJN NAME: 9626901F05. PAGE : 2 ANALYST : 68 TUBE : SAMPLE ICR 8 09/25/96 01:51 ' CLASS im/Mi 0 AVG (DPb',i %RPD AVG abs -0.8200 45.2 0.000 LANCASTER LABORATORIES INSTRUMENT TO: 04725 GFAA FLEMENT: SF FVOL OF BAICH_.iiUMB.LR 0 1 BURN 1 BURN 2 0.001 -0.000 TUBE : SAMPLE CRA t 9 09/25/96 01:55 CLASS. IY-QL/.WT 0 . AVG(DDbl %RPD AVG abs 4.1200 8.8 0.013 FVOL DF BATCH NUMBER 01 BURN 1 BURN 2 .0-013 0.012 TURf,JL 10 SAMPL1. CCV 1 09/25/96 01:59 CLASS IVOL/WT . o AVG(oob1 %RPD AVG abs 24.2400 0.7 0.063 %RECOVERY -97..0 FVOL QF BATCH NUMBER 61 BURN 1 0.063 BURN 2 0.06? TUBE: 11 SAMPLE CCB 1 09/25/96 02:03- CLASS Miffl 0 AVGianki. IBEEL AVG abs -1.4100 16.4 -0.001 FVOL DF BATCH NUMBER 01 BURN 1 BURN 2 -0.001 -0.002 JMLx. 12 SAMPLE- PBW `P&LO 09/25/96 02:0.7 CLASS JV.0UWI *:*:*:*:**;*: 1QQ AVGfnpbl %RPD AVG abs -1,4100 12.5 -0.001 tVOL ,,0F._ BATCH NUMBER 100 1 962681056002 RURN 1 BURN 2 R& R0 -0.001 -0.001 ' TUBE : s $mp l ; PBW 13 09/25/96 i07:11 CLASS a:*** 1VQLZWI 100 AVG Loobl %RP0 AVG abs 10.4000'- 1.6 0.028 %RECOVERY = 104 .0 ,J)F BATCH NUMBER 100 1 962681056002 BURN 1, BURN 2 0.029 0.028 209 DUP050307452 RUN NAME: 9626901F05 PAGE: * 3 ANALYST: 68 LANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA ELEMFNT: SE TUB Li 14 SAMPLE LCSW 09/25/96 02:16 CLASS T VOL /WT' ***::*:** i L-CSl ^' * AVG^oDbl %RP0 AVG abs 8.6300 2.3 .0.024 FVQl. ...P.F_. 8ATpH_N.ymF-R -) i 96268105.6002 BURN 1 BURN ? RR RD "0.023 0.024 __ __ TUBE : 15 SAMPLE LCSW 09/25/96 02:20 CLASS mu/Hi i AVG fDobl %RPD AVG abs 20.1700 .1.0 0.053 %RECOVERY =115 .4 FVQL ...QF BATCH NUMBER 1 1 962681056002 BURN 1 0.05? BURN 2 0.053 TUBE : 16 SAMPLE 2583222 09/25/96 02:24 CLASS imM 100 X AVGfoebl ERPD AVG abs -2.8900 12.2 -0.005 FVOl. QF BATCH NUMBER 100 1 962681056002 BURN 1 BURN 2 RR RD -0.004 -0:005 __ TU &fE_j_ 17 SAMPLE 2583222 09/25/96 02:28 CLASS IV.0L/WT 100 R.SSSFA AVGimbl IRPP_ AVG abs 7.6700 3.4 ' 0.021. ^RECOVERY =76. 7 FVOl DF BATCH NUMBER 100 1 962681056002 BURN 1 6.022 BURN 2 0.021 TUBE: 18 SAMPLE 2583223 09/25/96 02:32 CLASP. IVOL/WT 100 X AVG/DDbl 5KRPD AVG abs 15.8200 5.5 0.0.42 FVOL QE.... LATCH.mMBFP 100 1 962681056002 BURN 1 BURN 2 RR RD 0.043 0.040 __ _____ TUBE : 19 SAMPLE 2583223 09/25/96 02:37 CLASP IvPL/iLT 100 4 DipPj AVGfpabl %RP0 AVG abs 25.2100 . 0.7 0.065 ^RECOVERY =93.9 FVQL 100 _P_E 1 iAimjiymER 962681056002 BURN 1 'nTofiS' BURN ? 0.065 210 DUP050307453 RUN NAME: 9626901F05- PAGE : ANALYST: 4 68 TUBE: 20 SAMPLE 2583224 09/25/96 CLASS 4C*CYPi- XV j AVGCobbl -2.5900 %RPD 1.1 02:41 IVOL/WT 100 AVG abs -0.004 LANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA ELEMENT: SE FVOL PE BATCH NUMBER 100 1 962681056002 BURN 1 BURN 2 RR RD -0.004 -0.004 __ ___ TUBE: 21 s $mp l ; 2583224 09/25/96 02:45 CL.ASS 1VOL/NT ****>Cfn^T. 100 MbtyPF'A AVGIoDbl %RPD AVG abs 7.3700 5.5 0.0?'1 %RECOVERY - 73. 7 FVOL .._D.E ... BAlCtf...fc!JUMBR 100 1 962681056002 BURN J. 0.020 BURN 2 0.021 TUE: s $mp l ; CCV 2 22 09/25/96 02:49 CLASS lvo.iy.wi 0 AVGfDDbT *RPD AVG abs 22.8200 0.4 0.059 %RECOVERY *91. 3 FVOL PF .... BALCJiyLUMBEE b- 1 BURN 1 0.059 BURN 2 0.059 TUBE: 23 SAMPLE. CCB 2 09/25/96 02:53 CLASS. IVOL/WT 0 AVGfoobT *RPD AVG abs -1.2000 3.5 -0.001 Fm. .HE BATCH NUMBER 01 BURN- 1 BURN..2 -0.004 -b.obi TUBE: 24 SAMPLE. 2583225 09/25/9 6 02:57 CLASS ^w-T%w4* "T* 14. *&r .4x lyoiywi 100 V AVG Coobl XRPD AVG abs 1.6700 10.4 0.007 FVOL DF ... RAXClOiUaiBSE nob 1 962681056002 RtJRN 1 BURN 2 RR RD 0.006 0.007 r- TUBE: 25L SAMPLE 2583225 09/25/96 03:01 CLASS IVOL/WT st:***:*:^:* -j q q AVG/Dta1 35RPD AVG abs 11.8200 2.9 0.032 ^RECOVERY * 1011.5 FVOL. ,,.Q.. B.A10.H .n u mX ; r 100 1 962681056002 BURN 1 0.031 BURN 2 0.032 211 DUP050307454 RUN NAME: 9676901F05 PARE: 5 ANALYST: 68 TUBF^j... 2 6 s $mp l ; 2583226 09/25/96 03:05 CLASS jm,/WI 100 V AVG(p ? M %RPD AVG-abs 1.3300 12.2 -0.001 l. ANCASTFR LAB ORATOR T E 6 INSTRUMENT ID: 04725 GFAA FIFMF.NT: SE FVOL Q.F BATCH NUMBER 100 1 962681056002 BURN _1 BURN 2 -0.001 -0.001 TUBE : 27 s $mp l ; 2583226 09/25/96 03:09 CLASS IVOL/WT y**:#:*^* 100 RSViDFA AVG/pob 1 %RPD AVG abs 9.7600 1.5 0.027 %RECOVERY 97 .6 FVQL 100 BATCH Nl MBER 1 96268105 6002 BURN 1 "67027 BURN 2 0,026 TUBE: 28 ' 09/25/96 03:13 SAMPLE 2583226 CLASS LV.QUMI Q****** 1QQ & v AVG ( p p M %r p ? AVG abs -0.9500 7.0 0.000 FVOL OF BATCH ill MGER 100 1 9*626810!, 6002 BURN 1 BURN ? a -6,000 6.000 RD I!(BE : ?q SAMPLE 2583226 09/25/96 03:17 CLASS IVOL/NT 0****A* 100 R-b^DT-Cifi '%B& AVG abs 9.8800 3.3 0.027 ^RECOVERY = 98.'8 FVOL pF B.ATCH_ JAMSEB 100 1 662681 56002 BURN 1 .6.026 BURN 2 0.028 TUBE: 30 SAMPLE 2583226 09/25/96 03:21 GLASS JV0L/W1 R****** 100 V AVG fp p M %RPD AVG *bs 8.0700 0.3 0.022 FVQL JQMF_ BATCH HUMBER. 100 1 962681U56002 BJ.IRN, 1 BURN 2 ?|r . RQ, 67 022 0.022 TJJBLi. SI ;$<>?; 2727.12 09/25/96 03:25 CLASS imjMI R***^* o FVQL. 0 BATCH NUMBER 1 *RPD AVG abs BURN 1 19.2800 2.0 0.050' ~6.050* BURN 2 0.051 %RECOVERY = NOT APPLICABLE 212 DUP050307455 RUN NAME: 9626901F05 PARE: 6 ANALYST: 68' TUBE r 32 SAMPLE 2583227 09/25/96 03:29 CLASS. IVOL/WI V AVGfppbl %RP0 AVG ahs ~19.9000 1 .9 0.05? I. ANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA ELEMENT: SE FVOL DF BATCH NUMBER 100 1 962681056002 R1.IRN__1 BURN 2 Rfi. IT 0 53'. 0.051 TIJBE_L S3 SAMPLE 2583227 09/25/96 03:33 CLASS I VOL /WT *****A* 100 R.A'SSF'A AVG.CBJBb.1 XSEB. AVG abs 28.7000 1.8 0.074 %RECOVE'RY = 88. 0 F.VOL J).F._ BALCH ...NUMMR. loo i 962681056002 BURN 1 0.073 BURN 7* . 0.075 TUBE: 34 SAMPLE CCV 3 09/25/96 03:37 . CLASS iv q $ /mi 0 AVG/pobl %RPD AVG abs 22.3200 1.4 0.058 ^RECOVERY = .89 .,3 FVQL _.D..F.... RAIM.JHUJffi.ER 01 BURN 1 6.058 BURN 2 0.057 XUBEj. 35 SAMPLE CCB 3 09/25/96 03:41 ' CLASS IVOL/WT 0 AVG/pobl' %RP0 AVG wbg -1.0900 83.9 0.000 E.V.PL JDL. BAICH__NU.MB.LR 01 R1.JRN 1 BURN ? 0.001 -0.002 TUBE: 36 09/25/96 03:45 SAtP_LE '2583830 CLASS IVOL/WT ***:**: i 00 c>6s>xs V AVGfnabl %RPD -0,8200 28.2 0.000 F.V0.L 100 BURN 1 - 6.001 BATCH NUMBER 1 962681056002 BURN 2 R/f"\W' -o.ooo TUBLl 37 SAMPLE 2583830 09/25/96 >03:49 CLASS lmjQSL *****A* i 00 FVQL. Jiz_ BAKHJHiUSBIE 100 i 962681056002 5DC5XSA AVG(pabl %RPD AVG abs RIIRN_1 9.4200 3.1 0.026 ' 0.026 BURN 2 0.025 %RECOVERY = 94.2 213 DUP050307456 RUN NAME: 9626901F05 PAGE: 7 ANALYST: 68 TUB E: 3 8 s $mp Li 7583831 09/25/96 03:53 CLASS im/WT ******* IQQ V AVGfppbl *RRP AVG abs 1*7 .46001 5.4 0.046 I. ANCASTER LABORATOR I E 5 INSTRUMENT ID: 04725 GFAA ELEMENT: SE FVCH, QF BATCH NUMBER ' 'lOO 1 962681056,002 BURN 1 BURN 2 '6.047 0.044 TUBE: 39 5fei>.lX 2583831 09/25/96 03:57 QJLA5S IV.QL/.MX ******* 100 LV.QL -P,,. SMfiW H JMBER 100 1 9626810 56002 ^ 25<Rr\~r=2s AVG/oobl %RPD AVG abs RURN 1 BURN 2 ^ ?8.5 200 0.4 0.073 0.073 0.073 56RECOVERY = 110.6 TUBE: 40 SAMPLE 2583832 09/25/96 04:01 CLASS IVOL/WT ******* 100 / IN.0X5 V AVGfDDbl %RPD AVG abs -1.0600 14.3 0.000 F.VQL D.F ... BATCH j UMBER 100 . 1 962681 56002 BURN 1 BURN ? -0.Q01 -0.000 JR RD TUBE: 41 SAMPLE 2583832 09/25/96 04:05 CLASS. IVOL/WT ******* 100 FVpL. .DF,,. BAIPJL- UMBSR 100 1 962681C 56002 A (rvJVT<;A AVGfpohl %RPD AVG abs BURN 1 BURN 2 11.8700 4.0 0.03? 0.031 0.033 %RECOVERY - 118.2 TUBE: 42 09/25/96 04:09 SAMPLE CLASS IVOL/WT F.V.QL D.F BATCH.J UMBER 2583833 ******* 100 .100 1 962681C 56002 1 ^cyx S \r5 V AVGfppbl 35RPD AVG abs RURN 1 BURN 2 F A 109.6400 1.9 0.275 0.279 0.271 > OVER CALIBRATION RANGE TUB: 43 ' SAMPLE 2583833 . 09/25/96 04:13 CLASS IVOL/NT ******* 1QQ LV..QL JXF_ BfeICM.JJmB.FE 100 1 962681056002 iSbXSA AVGfppbl %RPD AVG abs 126.3100 1.0 0.317 BURN 1 . 67319 BURN 2 6.314 214 %RECOVERY = NOT APPLICABLE OVER- CALIBRATION RANGE DUP050307457 RUN NAME: 9626901F05 PAGE : 8 ANALYST: 68 TUBE: 44 s $mp l ; 2583834 09/25/96 04:17 atC*:L*A*:S*S*:* IVOL/WT 100 , V AVGfppbl %RPD AVG abs -1.0000 4.1 o.ooo b t ANCASTER l $r o r $t o r t f s INSTRUMENT ID: 04725 GFAA ELEMENT: SE FVOL JUL BATCH NUMBER 100 1 962681056002 BURN 1 BURN 2 -0.000 -0.000 i/MT TUBE: 45 SAMPLE 2583834 09/25/96 04-.21 CLASS iv o l /w t *:* ****: 100 AVG/pobl 95RPD .AVG abs 12.4000 2.5 .0.033 %RECOVERY 124 .0 FVOL 'DF BATCH NUMBER 100 1 962681056002 BURN 1 0.034 BURN 2 0.033 TURF: 46 SAMP],! CCV 4 09/25/96 04:26 ' l $s s TVOL/WT 0 AVGfppbl %RPD AVG abs 22.7700 2.9 0.059 ^RECOVERY *. 91. 1 F.VQL J2L.. BATCH NUMBER 0 .1 BURN 1 0.058 BURN 2 0-060 TUBE: 47 SAMELJE. CCB 4 09/25/96 04:29 CLASS TVOL/WT 0 FVOL. 0 PF &AIJl.N-Lif4B.lEB 1 AVG/ppbl RPD AVG ahs -0.5900 208.1 0.001 RURN 1 BURN ? o.no3 -o'Tooi TURLl -48 SAMPLE pfJW 09/75/96 04:33 CLASS IVOL/WT ***:*::*:** iq q v AVG/DPbl %RPD AVG abs -1.1700 33.3 -0.001 F.y.P.l. DF BATCH NUMBER 100 1 96268105600%} BURN 1 BURN 2 RR , RD "o. ooo' -0.001 / / TURF: s $ Br i; PBW 49 09/25/96 04:37 ' l $s s , imiwi ***.*** 100 Lvm. _? f ,, X $t ' h n u mX ; r 100 1 962681056002 AVGfpobl %RPD AVG abs: 1 1.4700 5.5 0.031 BURN J. BURN 2 6.0~3.0 0.032 ^RECOVERY =0.0 & 215 DUP050307458 LANCASTER LABORATORXES GRAPHITE FURNACE ATONIC ABSORPTION DATA EEV.CEWED BY 5 DATA VERIFIED BY t DATA FHF NAMFi- CFP&90J ..RAT RUN NAMEx S&a&S0aF0S ANALYST : SOS INSTRUMENT WO; 04725 OKO CORR : B2 ELEMENT ; BE Coneervbrat ion is'used to evalu&to i. f > am <ve-.m I. <;> avo within c it 1 :i. b'ration ran i| e . 216 DU P050307459 RUN NAI'lEs 96269021-05 RAGE s . :i ANALYST: 609 ' LANCASTER LABORATORIES ; INSTRUMENT ID: 04725 ' Ol'AA CLEMEN V.-. SC TUBE: SAMPLE 30 1 09/25/96 09:05 Cl. ACS IUOL/WT 0 FUOL DF BATCH NUMBER 01 AUG tomb) *RPD AUG abs 0.0000'190.3 0.006 BURN 1 BURN 2 0. 819 -0.083 TUBE r. SAMPLE h) 1j 2 09/25/96 09:09 Cl. ACS IUOL/WT 0 ....... ....... . --. -- -- --* --* ** ' FUOL DF BATCH NUMBER 01 A VGi.ll&h>... fv'RP.O AV6...abs. 0.. 0000 0.2 0.006 BURN 1 BURN 2 0.006 0.006 TUBE s SAMPLE SIS 3 09/25/96 09-11.3 Cl. ACt: m:n. /u r 0 " ........* \ * " ................. @ AFUOL DF X $ ' ... NUMBER 81 AUG (DDb) tfftPD AUG abs 19.-3300 4.0 0.030 BURN l BURN B 0.030 0. 029 TUBE s SAMPLE ui c!, i.* 4 09/25/96 09:17 Cl. ASS i uoL/wr *0 FUOL D1- BATCH NUMBER 01 AVG(DPb) %RPD AUG abs 26.7900 1.1 0.053 BURN 1 BURN a ' 0.052 0.053 TUBE: SAMPLE S48. 5 ' 09/25/96 09:21 CLASS TVOL/WT 8 * * ` ......... ' FUOL DF:" BATCH NUMBER 01 AUG < ppfo) 34RPD AVG abs 40.9700 1.4 0.066 BURN 1 BURN a 0. 067 0. 065 TUBE: s $mp l ; SUB 6 09/25/96 09s25 ' i . $s ;:: j v p l /mt ` f uol . 8 ? f X $t ' h 1 n u mX ; r AUG <Ri3b) SRl-'P AUG aba BURN 1 BURN a A 5i.4aete 0. i 0.1 Is i. ii &, 0. i 10 TUBES SAMPLE feu " 7 09/25/96 09329 Cl ASS IUOL/WT FUOL - e 0 Df- BATCH MUMPER 1 AUG (nab) *RPD AUG abs 16.5400 1.0' 0.039 BURN :l. BURN 2 0.039, 0.039 217 "/KECOUERY = 92.7 A DUP050307460 RUN NAME: %a69ttaF0S PAUL 5 AMALYSTs 809 TUBE::. SAMPLE 1CB ft 09/23/96 09:33 a. $' ' XVOL/WT 0 ayj&ip-abi ? QMG^m -2.9200 6.3 "0.009 L$n ' $s t ; r l $X o r $t o r i; s INSTRUMENT ID: B4725 01" A A ELEMENT.: SE FUOL.. 1)F BATCH .NUMBER 01 fiURN.. 1. X u r n ...a -0,009 0- 009 TUBE.a. SAMPLE CRA 9 09/25/96 09 s 37 Cl, ASS I UOL/WT 0 AVG<Ja.EiLL &RPJB. AUG aba S.3500 3.6 0.003' Em JBE BATCH NUMBER ft 1 BUBW. .1 tUEt-LE 0.003 0. 003 .mfi!;- s 10 SAMPLE CCU 1 09/23/96 109341 Cl. ACC IUOL/WT 0 AUG (cpb) ttKPD AUG abs. 24 .370 1.6 0.052 JtRECOUERY = 97- S FUOL DF BATCH NUMBER ft 1 BURN 1 0.051 X ur n a 0. 052 [UfilLs. 11 SAMPLE CCB 1 09/25/96 09 s 45 Cl. ACC JUOL/WT 0 ,FUOL DF 0 1 M UHI.<ER aufiiJiPM. s ; ps l AUG ab -a .9700 7.2 -0.009 gysfeUL GUBtL ~0. 009 0. 009 lUBEs 12 SA11PLE 2503225 09/25/96 09:: 49 ct.fiqc J UOL/WT >: :i 00 Ri^Sf u * . AUGt&afi>. ir p ? AU(1 alH. .2500 8.2 -0.003 f w l ...DF BATCH_.iiynfimi 100 1 962681056002 StUftH-Ju -0.003 -0.003 RE Eft --........... - TUBES 13 SAMPLE 2563225 09/25/96 09 s S3 Cl, ACC JUOL/WT w -j h :A 100 RftH'SFA .$v g : p r t> 9 .6500 EEE 4.0 mk. s &k 0.019 ECQUERY = 96.5 FUOL ' DF . BfilGH NUMBER 100 1 962681036002 syRtLi 0.020 SUEE J1 0.018 218 DUP050307461 RUN NAME: 962696SF05 PAGE : ANALYSTS 609 UJlfiJL :L 4 SAMPLE asasaat. 89/25/96 09 : 57 mL/u]; l.l a: 100 AYiBBb>_ *RP AVG *0* -a.6300 1.9 -0.009 LANCASTER LABORATORIES INSTRUMENT IDs 84785 OTA A ELEMENT.: GG EV.P.L ,,..DF BATCH...NUMBER. 100 1 962661056002 oymu. BURN 8 RR RD -0.009 -0.009 iuji 15 SAMPLE abaaaaa . 09/25/96 10 a 01 Cl ASS IVOL/W1 Ui; !: :: A-k 100 EVGL ._ BATCH...HUMBER. 108 1 968661056002 R.>3>OFA 7.66W0 AVG abr=. BURN 1. 2.7 0.015 . .0.015 BUIRN 8 0. 014 '/.RECOVERY * 76. a IWSEj l 16 SAMPLE 2563826 09/25/96 10:06 CL QSC IVJ3k/WT 3 00 AL y X 0VGifiEJ>>- *k p AVG iw -3.2500. 0.1 -0.010 EVQk ..BE_ SAJCH._n u i,!&.; r 180 1 962661856008 BURN ,8 RR UJ2. -0.818 -0.010 sms,i. 1? SAMPLE 2563226 09/25/96 10 a 10 Cl. ASS IVCL/WT T> A >< 100 ^DSCFTiA AVGUiEbjL *Rpj> AVG abs 7.2900 6.5 0.014 /RECOVERY = 72. 9 EVQL DF BATCH NUMBER 100 1 962661056082 BURN l . BURN a 0.813 0. 815 IU1&L 16 SAMPLE 2533226, 09/85/96 10X 14 Cl ASS iv o l /w t R ;>: : 100 VS X ayiiiruab> *k p ? am abs. 6.6600 6.0 0.012 PVOL J)F BATCH HUMBER 180 . 1 962661856002 aiasH j . BURN 8 RR RD 0.018 '0.013 ___ IUJBEj l 19 S$mp l ; s . zzzzzz 09/25/96 104 16 Cl A!|S IUOJ./WT Rk k **A* 0 Em, ...BE- BBICH...n u mX ; r . 31 AV`Gj.aab>.. 2LRP& AVQ ^b%. 17.3600 1.5 8.036 BURN.. 1 0.036 BURfcL 2 0.037 /RECOVERY. *> MOT APPLICABLE 219 DUP050307462 RUM Mum;:: 9626902F05 PAGE s 4 ANALYST k 609 LANCASTER LftB0RftT0RIES INSTRUMENT IDs 04725 OFAft CLEMEN f: GE TUBE, s 28 SAMPLE 2683227 09/25/96 10:22 Cl. ACC I VCU./WT >; >: >; x x x ->: 10 FVOl . BE BATCH NUMBER 108 1 962681056002 AH/ AUG i p isL ) SCRPD ft V G K\ b ":i 20. .1.900 3.5 0.042 TUBES 21 SAMPLE 2583227 09/25/96 18 s 26 CL ABC JVOL/WT u- .180 BURN 1, 0.041 BURN 2 0.044 RR -- ... . ... . * ............... ... " '* RD ....- FVOL I>F BATCH NUMBER 108 1 962681856802 KJ\ Fft AUG <oob) %RPI) AUG abs 29.3200 0.8 0.063 BURN L 0.062 BURN 2 0.068 Si RECOVERY = 91. 3 .......... ................. TUBE: 22 SAMPLE CCV 2 .............. ..... .... . . ........ . . . -.................... .....-- --------- ------ 09/25/96 10.:80 ' CL ACC TVOL/WT FVOL. DF BATCH HUMBER 81 AVG<ppb> ZRPft AUG- abs 23.4800 0.7 0.050 BURN JL 0.050 EUSfcLfi. 0.850 /RECOVERY 93. 9 TUBE: 23 SAMPLE CCB 2 09/25/96 lOs.i'i Cl. ACC JVOL/WT 8 ............... * * * - *' ~ - ... .. -- -- -- -- FVOL DF BATCH NUMBER 8 1 AUG : pnlj) Si R P.D AUG abs -0.5300 457.6' -0.004 BURN 1 BURN 2 -0.007 , 0.000 TUBE; 24 SAMPLE 09/25/96 18.: 38 ' l $' ' :r v ' il /w t FVOL DF BATCH HUMBER 2563630 k k - 100 108 1 962661056002 A 30C.XS BAUG <X Ii ) /RPD AUG a'os BURN I. BURN 2 RE RB --3. 4500 9- 2 ,--0.010 -0.011 -0.010. TUBE s 25 SAMPLE 2583638 09/25/96 1042 CL ACC JUOL/UT 100 t-UOL. I>F BATCH NUMBER 100 } 962681056002 SOOX-Sft AUG <ppfa> /RPO AUG abs 6.6900 1.4 0.017' BURN 1 ~0.017 BURN f> 0.017 A sfRECOVERY 86.9 220 DUP050307463 RUN NAME:: 962&902F85 PAGE s ANALYST; 5 809 BWE.iL SO SAMPLE asa3B3i 09/2S/96 10*46 CLaSiSi IVOL/WT :: i:>: i:;>; 100 AVG < p fib) 18.3900 XJIEP_ 6.a 0.yG_BLi. (3.(338 LANCASTER LA 00ftA TOR IES INSTRUMENT IDs 04725 OS ft A ELEMENT : GC FOOL ....P.F_.._ 100 1 962661056082 O.U.KH...1 S!MU1 8B. lie. 0.(337 0.040 ............ . UABE.*. S 7 SeflE-kS. 2583631 (39/25/96 3.0:: 50 Cl A00 iyCL/WT A* 100 ------ ^s&xsA $ yo <pps> xgM em.Ab& ' iysiLi. w j u k a 28.6300 4.2 (3.(361 0.059 0.86:3 /.RECOVERY = 102.4 TUBES 26 09/25/96 10 s 55 ' SAMREE 2563632 cusii msum s X ayiiiaBiB. sysEfi. aafi-aia. -2.7 400 0.0 ~0.008 FVOL ...BE... 100 1 962681056002 s,y.n...a m m -0.008 -0.(306 TUBES. 29 SAMPLE 2583832 89/25/96 10s59 ci Ace TypE/wx 100 Em. -.5~ 100 1 962681056002 tDDXSA AVG.ifi.EbL BE 0V(L_abg. SUBSLJl 10.0800 8.1 0.020 8.021 SUSiUl 0.019 /RECOVERY - 100.6 TUBES 38 89/25/96 11x83 SAMPLE CLACC lyOL^jfO: 2583833 *** 100 ISCfX/S V amifiEbl 2-BEfi. 26.0900 1-9 0.056 FVOL _.D__ 100 5 962661056002 fitLMH.il B& E& 0.056 0.055 jfyp'}___ IMBEi. 31 SAMPLE 2583633 9/25/96 11x07 , CJjiOC LVOkLMI 10 aye,.iEfita>. /Rft A.VG...alw 39.8100 0.5 0.066 /RECOVERY 137.2 Em j q j l _ mmuamsm' 180 5 962681056002 BUISiL-L 8.086 aJMHJI 8.086 % 221 DUP050307464 us ~ RUN NAME s 9&a690aF5 PAGE 3 6 wHALYS'l : 609 IUMj . 3 a Si I MALE 2563634 09/25/96 11:11 GLMLL IMBLZH1 I'.v.y.-v.r.r.r. :l.00 F6\CsS ayfi.ifi.Rkl. 25EEB. ay.Q,,ak;i. -3.060(3 4.7 -0.(309 I ..AN Cft: rrEi 5 I..A IB }!' : A TOR .1. INSTRUMENT ID: 0472 OF AA CLEMEN r ?. OC f vol 100 SLQifiiijiyjaeEE 1 962601056002 omw, !., B& !:iU> -0.009 -0.009 ............... ; rUBE:. 33 SAMPLE 2063634 09/25/96 llslS GL&lili IM >: A 100 FVOL ...J>F- BATCH..NUMBER 100 1 962661056002 FSi &SA. aw<.fi.fikl SBEft ayJL..*M. BURN.J. 10.55(30 .a.a 0.021 0.021. BURHJI 0.(321 /RECOVERY = 105.5 TUBE: 34 SAMPLE CCV 3 09/25/96 11 8 19 ELfiMl imZMI 0 ev&iaakX 2BE8. AytLzM, 24.4100 1.2 0.052 FV.O.L _ ,, BfiJEH.JllUMBER 01 -gUBEJL 0.051 smLS. 0.052 /RECOVERY = 97.6 ;r.UBEs. 35 SAMPLE COB 3 09/25/96 11*23 ELBMi imZMl 0 aysi.RRk>.. z X ; j ? em..afe& -2.6400 21.6 -0. 0(39 f v o l ,j >_ MIEM.AMHM 0` 1 BJJJSN.JL SUBMJg. -8.006 -0.010 TUBE: s $mp l ; PBU 36 09/253/96 11:27 EL01& iyfiL../MI * 180 V tmisstel. SEES. 0Vfi....&k;=i -4.0(3(30 1.7 0.011 FVOL .OF._ S.aiQH,,NimBER 100 1 962661056881 aMfcLJ, -0.(311 -0.011 TUBE: 37 SAMREF PBU 09/25/96 11s38 CLASS LVP.LZMI A 108 -'Em, _JJL_ BfiimJiUHIIB. 100 1 962661056001 ` amiaakL z; ; s . saiiM siuaui s ms m-s . 9.5408 18.9 0.019- 0.(317 0.020 /RECOVERY =95.4 222 DUP050307465 1. H NC A 3 T C ft L I'-I G!j ft ftT uft .(L S SKAMHITE FURNACE ATONIC ABSORPTION o $t A vu-:ir:i l ? ? y ; p^*^ qlllh ^ Of) l A f"H.r HAITI" :: :1 .. RAT RUN NAMEs S6S?lfeSF05 ANALYST ASS INSTRUMENT NOs 04780 TJKG CORA : DZ ELEMENT t SE l.. t C? I i l. { cl tlOfl 3. Is 3A is- ts* il a l i b r- a t- i oN iv a n cj e ,, C) P;' V i_\ ,t <,< r\'l', li- l. t .> a hi j') 1. >U L i; -: e\ V :.v W 1 T:li 3. T. 223 DUP050307466 .-ui-i h o O; s 96P7J.0Er05 .t-'OCE :: :i ANALYST i 859 TUBES. SAMPLE lo 1. 09/H7/96 0i s :L 8 :i VOL/WT 0 AVGJj ^M BEP. ft 70 aG'-. 0 Ml'lMM 0.0 -0.003 i..0Ni...)-r> L h j-.i i j; h i u k .i. l E IN S I E U HE M T :r. 3) s 0 4 ' 8 5 ij I'h A CLCMCNT,; SC f v o l _ ,j > f BATCH.-NUMBEft. 0 3. BUITH.....A. GURW...CI -0.003 0.000 iHJt'EjL a :>0Hl-'l . 09/27/96 03. s 3. ; Ci,.OS.U TVOL/ifiT. 0. ' ftVG <P.P.b>. *BER AVG..*M.' 0.0000 w 0. 013 FVOl,.....?>.!" BATCH .NUMBER 0 .ymi..i fiii'itL-g. 0. 03.3 0,, 00 0 I.URE.l. SAMPLE. .1. 3 09/87/96 03. s 16 (Law; IVQL/.WJ. 0 ft VG <p.pb>. J&RPJD AVG *.b* IS.0900 -0.0 0.038 FVOU.... l>i: .. BOTCH..HUMBER. 81 BURN. 3, -BURN... 2 8.033 0. 000 TUBES 4 pmELt. 09/87/96 01 8 3.8 <:), X C-u lyfik^wj. 0 AV6.ie.pM. x r E'-S. Q.VG_aM 83;, 6300 0.0 0.060 FV_Pk _fiF BAJCH,,NUMB.K 01 mm.. I BURN.. S. 0,, 060 0. 000 .UJJ?is. SAMPLE 40 S 09/87/96 03..S80 GLBi'5.;. IV-Q.GZWJ. 0 ftyGtppbJL *&?.> 0V6.. Ahfe. 37., 3700 ,0.0 0.09 t. F VOL PF. BAlCEI.Jt!.UHBEk. '0 1 PUBSLA. X DEFGi 8.091 0.000 i..yL=. TBITEkT, ST'W 6 09/87/90 03. s pa liAfc&L lyoL/wj.- EVfiL. ..at... BQ..).Gi::L!.yJiy,!<. 0 0 3. flVG(ppb) %.RPj>. flv.6_s.fe~.. 49.89U0 0.(3 0 . 3. 3. 4 BliRH..1 X HIn.. a. 8. 3.3. 4 0.00 0 TUBFs SAMPLE u;v 7 09/27/96 01s PS GLflsiU iVfiL^WJ. 0 AV6.<Jj .p M. *SJA flV0...Abj1,. 3.9. 0100 0.0 0.045 ^RECOVERY - 95. 0 FVOL 'DF . BATCtL.NUMBER. 01 &yN_i. 0.04S BURN...S. 0.000 DUP050307467 RUN II ft ME i Ph OEs I-.) N ft L Y 3 f: 9687102EU5 i'' 659 VLIBtLs, 7`iUPEE TCB 6 09/87/96 01 s 87 EL h u X . 1. V'( H,/W L 0 Q.y0.iE.Rh?2. -0.7500 ALE... afeft. 0.0 0. 000 1.. AW CAB ICE LABORATORIES INSTRUMENT IDs 04785 or A A GEENEWT SE f:.y.Qk .. P.F ... MM MUMBLE 01 BURN 1. BURW...8 0.000 0. 000 TUBES. OKA 9 09/87/96 01s89 GLftlUi 1V0L/W! F.yo.L Mlkl!...NUIMK 0 0i avGjiipM. sse& ays...sM. mm..1. BURN..a 4.5400 0.0 0.01a 0.0.1. 0.000 mmx is sfiaekiL i;t;V 1 09/87/96 01::.'J1 SLMli im/JL 0 ftv.GiRpb>. '*R- as...&&*.' 84.6800 0.0 .0.057 ^RECOVERY - 9a. 5 Em, _!>__ iieiS:!...!.yiiB.Ha 0 :l. 0.057 BUR.a,.E 0.000 TUBES 11 09/87/96 01 s.1.1 SRI'IPUE CI,fti,S IVOL/WI FVOL ...O.L... BATCH... tiU.19.jWt:;l;< ^ CCB 1 0 0. 1 rtwtiiaa3a>. ERLS. 'ayfi_*tes. !iufilj, mJRbLJT -0.6900 0.0 0.000 0.000 0.000 TUBE: 1 2 SAMPLE 8533633 09/87/96 0.1. s3S . ci. $X u t v o l /w t j 00 fiQNlfeRb>. 14.360ld feiJMbL t 0.034 FOOL OF BA'TC.H .NUMBER ' 100 10 968661056W08 TUBES. 13 SAMPLE, a ">63633 09737/96 01s37 CJ, ^1. IVOL/WI :: :i 100 FVOL. . J>E .... geiH,,NUM@ER. 100 10 968661056003 CONClRb>. 19.5000 BURN 1 0.046 TUBE :. 14 BAWPLE 2563663 09/87/96 01s 39 { [ A1?U TVDL/WT . 100 ^ COHC <PDb> 83. 9(100 iiMEbLA. VI. 006 l".yOU..... DF,, IftTCi}.NUMBER .1.00 IB 968661056008 225 DU PO50307468 N Pr u n $; QJ$KLM ANALYST . 9G87108F0S 3 859 TUBEs. IS Z$[\]; p58 836 09/87/96 0J.! 41 Cl. ft SC ] VOI../WT ':: >: >: >: -i: C->; 180 l^c>xs3 cuNc_<.m?-b.L e.^000 ByBiLi 0.. 066 R S$ ' $' rrift T$X UV$WUVX; Y INSTRUMENT IBs 04785 SPAA ! l..!-.i,|!lM'f> . sp F;y0 L I>F BATCH NUMBER 100 10 ScRca1066008 X TNT CORK GOLF" SLOPE Y I NT 1.8 . ..SO0?5 0,.99693 s.esaie 0.03460 EE RO TUBE:,. IS SAMPLE 8633879 09/87/96 01s43 CLLfiML im/JsLI U.)i>:K0- 100 B*fiL _L_ MI.A...!.agM..fcL 100 5 968691056001 '-'ZZZZctF CfiMCiRfthZ. 19.9000 BUBM..J, 0.047 TUBES 17 . CAMPLE 8536879 09/87/96 01s45 GLtE-Si IMfiL/WX s: 100 ZZZZZZ l cuHC.(.fiab>. 84.4800 gu&SiJL 0.057 FUGL. . J_ -BATCH ...NUMB; :R 100 5 968691056001 TUBCs. 16 SAMPLE 8565879 09/87/96 01j47 <11, ASS lyOL/WI U-> >: 100 ZZZZZZ 5 g.Q,N,iB.eM. . 86.6300 ByfiMLi 0.066 FOOL......?>F.. AI..El;:! ...NUMBER 108 S 968691056001 TUBEs 19 ^$_`a; 8065879 09/87/96 01s49 nLAAi: lyaL/wx U > >: );C>; 100 38.9600 eugN-l. 0.076 ZZZZZZ 3 FVQL 100 tAJ.cttjfcLUjasE.& . 5 968691056001 X INC COER CUEF SLOPE Y 1NT 8 4.. 33185 0.. 99976 0.00198 0.04710 m B TUBES 80 SAMPLE. 8536879 ' 09/87/96 01s 51 <"!. ACC TOOL/.LIT 100 ZZZZZZ'$> fiPHGJtftPfe? 80.5300 BU!iN,,.l. 0. 04 6 FMOL .DP... BATCH..NUMBER 100 5 968691056001 226 DUP050307469 RUN NAMEt 9627102F05 PAGE s \ ANALYST* 659 l $n ' $' . (;' : l $X o r $t o r i; s 3 N8TRUPIEWT 31): 04725 GPAA !"l..!"i`!GNTCP TUBE: H:l. SP!Lg. 8585279 09/27/96 03:53 IVOL/WI FVOL :t-k 100 , 100 BlCHJNUf1BER 5 96269105fcti01 222277 | c.!)!;:ic..ifcRbL 24.. a 1 MW SUISliJL 0-056 TUBE: 22 s $mp l ; . 09/57/96 01*55 CLASS lyOL/Wt T>)v 100 ZZZZZZ 5 QOfcic ,iai3jbL 28.4100 0,. 066 FVOL I)F . BATCH ..NUMBER. 100 5 962691056001 I.UBE..!;.. 23 SA.JLE 2505279 09/27/96 01557 GLfi&U 3V0L/WI I>* **;( 100 32.4700 eyrn-i. 0.075 ZZZZZZ 3> FVOL E>_ BAT.DW...|;tyM.E!i 100 5 962691056001 X T.NT . = 27.. 191.01 R. RD. CORK COEF * 0. 99912 .... ......... ... SLOPE - 0.00178 Y 3NT 0.04640 TU6E* 24 Sf5kg. c!5tt282 09/27/96 01359 fJL&lii-i 1WL/M1 M-x 10.0 ZZZZZZ yoNc.iafi.fel.24.5500 0.. 05 / Em. ..ml ... msmm. IBM 5 962691056001 TUHE:,. 25 s $mp l ; 2565282 09/87/96 02:00 TVpL/WT *:! . :100 ZZZZZZ ONC.iiJabi. 29.2500 gimjL ^.068 FypL .. 1)F... BAJCH NUMBER 100 5 962691056001 TUBE: 26 SAMPLE. 2565262 09/27/96 02:02 ciAns IffiM :: x >: 100 ZZZZZZ <5 fiflHfiiMJriL. 32.4400 B-U-BM.. l. 0.075 EVOL . F_ BATCH....NUMBER 100 5 962691056001 237 DUP050307470 RUN Nh HL : JoS /10l- 03 b c$ ; ; ANALYST: .S9 IN.!..?. SAMPLE asaseaa CQMC(ppb) 36,54(8S ZZZZZZ3 s 04 IVyL/WT 180 BURN 1 . (364 LAMCh g fGR .t-HtfOi'CH i uk.u. INSTRUMENT T 0 r, 047c3 OF A A ELEMENT : SC F.yOL ... PF.. BATCH... NUMBER 1 00 5 962691056081 X lMr 33. a4891 RR. CORF: COEI" 0. 99S'S-0 SLOPE * 0.88176 Y I NT 0.05760 ft i) 11 ILL : 2i RUMPLE 89/S'7/96 0Ss86 Cl ACS IVOL/WT pi: 3 88 ZZZZZZ^ CQMC(nob) 9.a08 BURN .1. 0. 024 FOOL..... ])F._... BATCH NUMBER 180 10 962691056808 TUBE: 9 SAMPLE asasave (39/a?/96 easea GLBilii JVPI-/UT 5> ;i sr 108 zzzzzz J CQMC < ppb? i4.6988 BURN .1 u.ias FVClL.. PF BATCH HUMBER 100 lo 96269iX s&X X s TUBE:. 30 SAMPLE 3505290 09/27/96 Basil Cl, ACS. IVOL/WT Fh h ; 100 ZZZZZZQ CQMC < PPb) 1a.5900 BURN 1 0. 044 FyOL PF .._ BAT 0H... NUM B E R 100 10 962691856002 TUBES. SI SAMPLE 2565290 09/S7/96 02 a 13 Cl ACli IVOL/WT r>K*:K3 100 83.1200 BURN 1 0.854 ZZZZZZ 3 FVQL PI- BATCH NUMBER "l08 ' 10 96269i056002 X tWT * . 12.32333 RR CORK COEF 0.99929 1__, SLOPE = 0.08190 Y IHT 8.02448 RD T U B E s 32 SAMPLE CCV 2 09/ S 7 /9 6 82 s IS 01 MRS IVQL/WT. 8 A VC (ppb) jtRPl) AVG abfe 24.5508 0.0 0. 057 .^RECOVERY ~ 90.2 F VOL. DF BATCH NUMBER 01 BURN 1 0. 857 BURN a 0.800 228 DUP050307471 RUM Nh MEs 9687108F0S PAGE; .5 ANALYST : 359 I.UBEs. 33 3A.NP_l...E. CCB 8 89/&?/96 08s 17 IVOL/WI 0 A.VQ..lppJt.>. *RJ> ftVfi... 0.5.1.00 0.0 0.001 i.. A w c A s t r:: R t... $ ao r ft'r o r n: s INSTRUMENT IDs 04725 o f $$ ; l ; m; n t sc EVfik '_ML_ micHjsiyriSER 0i BURN 1 BURN...2 0.001 0.000 TUBE 8 34 GBiiiiip 2535292 89/27/96 63;: 3.0 GLftiili JVOL/WT >:u -k .100 C.pWCi.RK.k>.. 1.3.1500 BUB.W..1 ' 0.032 F.VOL ....ME.. BAI.C>;!..HU!IBER. 100 . 10 93259:1855002 TUBE: 35 SAMEL!. 255589? 09/27/95 02s21. GLM& im/Jg. >: KK* 1 m 100 17.4300 fiUSJUL 0.041 Mk _36J::'_BftIH_Nyf!!ME 180 ' 10 958591055802 JUBEs 35 SAMPLE 2555292 09/27/95 02s23 cirnfi. xm^oa K ?* 100 21.9400 BUBJU, 0.051 Em. ..J>.,, BATCH ' NUMBER 100 10 9585910550I 02. TUBES. 37 SAMPLE, 2535292 09/27/95 02a25 ; CkiCk XWL;/UTL. 100 CCiNC (ppb> 25.2500 BURN J, 0.. 051 E.y.QL......J>_ BATCH HUMBER 108 10 952591055002 X T N i' CURE CUEF SLOPE Y I NT 15..3402 I. 0.99953 0.'00194 0.03170 RJi Rj> .... ............_ I.UBEs. 33 SfiMPkE. CCU 3 09/27/95 02 s 87 k!,M& XkQL/MI 0 AVGCopb) ?1RPD aye... ah* 84.0180 0.0 0. 855 SRECOUERY * 95. 0 FVQL DF BATCH NUMBER 01 BURH....1 0.055 BM8Ji_S 0.080 229 DUP050307472 LANCASTER LABORATORIES GRAPHITE FURNACES ATONIC ABSORPTION DATA REVIEWED BY: DATA VERIFIED BYs ^T>6' q(zSh^ DATA FILE NAMETl. r?&302 RUN NAI'IE 5 96E6'30SF01 ANALYST!: 659 INSTRUMENT NQs 02603 DKG CORR.! BD ELEMENT: TL 230 Concent-ratiov* is used to evaluate if sample resuLts are within cal iteration -range. DUP050307473 RUM MAN Es 9626982F0.L i-'l IL.L s :l ANALYST : 859 TUBE a SAMPLE St) 1 89/25/96 05:23 CL ASS :r v o l /w t 0 AVG(DDb) XRPD AUG abs 0.0000 0.0 0.014 i .h Hi.h ') i. ASu R H 1 U K 1 L b INSTRUMENT ID: 02 683 GFAA lit J:!MEN f T L FVOL DF BATCH NUMBER 01 BURN 1 BURN 2 0.019 0.009 TUBE i SAMPLE Si0 a 89/25/96. 05 s 27 CL ASS JVOL/WT .0- AVGloob) SSRPD AVG abs 10.0000 7.3 0.049 FVOL DF BATCH NUMBER: 01 BURN 1 BURN 2 0.047 0.052 TUBE: SAMPLE sae . 3 09/25/96 05:38 CLASS IVOL/WT 0 AVGCoob) -JiRPB AUG abs 0.0000 9.6 0.116 FVOL. !>F BATCH NUMBER 01 BURN 1 BURN 2 0.118 0.126 TUBE: SAMPLE S40 4 09/25/96 05:34 CLASS IVOL/WT 0 FVOL DF BATCH NUMBER 81 AVG < Dob) *RPD AVG abs 40.8000 3. 1 0.222 BURN 1 BURN 2 . 8.217 3.227 TUBE: SAMPLE S68 5 09/25/96 0536 CL AST; j v o l /w t 0 AVG<OBb> SiRPD . AVG abs 60.0000 0.1 8.338 f v o l ' 1>F BATCH NUMBER 01 BURN 1 BURN 2 0.336 0.336 TUBE : ' SAMPLE S68 6 09/25/96 05:41 CL ASS 1VOL/WT 8 AUG < oob> 5RPD AUG abs 60.0000 7.1 8.399 FVOL DF BATCH NUMBER 01 BURN 1 BURN 2 0.420 0.379 TUBE: SAMPLE ICV 7 09/25/96 05:45 Cl. ASS JVOL/WT 0 AVG C ? ? b) IKRPD AVG abs 49.3400 1.2 0.276 ^RECOVERY = 96., 7 FVOL DF BATCH NUMBER 0, 1 BURN 1 0.278 BURN 2 0.274 2Si ri^iSGS :.: . \".. ~,;.;t\si*&L DUP050307474 RUN NAIIEs 96ii6 982l: Ml PAGLs 2 ANALYST! 659 LANCASTER LABORATORIES 2 NS TftUM2 MT IBs 826W3 OFAft ELEMENT : TL TUBES SAMPLE ICB S 09/25/96 05s46 Cl. ASS JVOL/WT 0 FVOL DF BATCH NUMBER 01 * AVGCDDb) JCRPD AVG aba BURN 1 BURN a -0.9000 95.8 -0.. 804 . -0.001 8. 007 TUBE! .SAMPLE CRft 9 09/25/96 05 s 51 Cl ASS JVOL/WT 0 . AUG(DPb) sfiftPD AUG abs 12.3880 8.0 0.863 FVOL DF BATCH NUMBER 81 BURN 1 BURN 2 0.06? 0.860 TUBE: 18' SAMPLE ZZZZZZ 09/25/96 05 s 55 CLASS JVOL/WT . ttKK*K '0 AVG (DDb) *RPD AUG abs 31.5900 4.H 8. 180 FUGL DF- BATCH NUMBER 0' 1 BURN 1 BURN 2 0. 185 0.174 TUBE ? 11 SAMPLE CCV 1 , 09/25/96 85 s 58 Cl. ASS TVOL/MT .8 FVOL 0 DF BATCH MUMBER 1' . AVG<ppb> *RPD AUG abs ' BURN 1 41.0000 3.9- <3.228 0.23'T BURN E 0.222 SSRECOVERY 102. S TUBES 12 SAMPLE CCB 1 09/25/96 06 s 08 Cl. ASS ' 3 VGL/UT 0 AUG<DDb) XRPD AUG abs 0.2088 99.9 0.801 FUOL DF BATCH NUMBER 01 BURN 1 BURN'2 0.602 0.080 TUBE: s $mp l ; : . PBW ZZZZZZ V XV 13 ' 09/25/96 06 s 05 CL' ASS JVOL/WT ,\; j : >; ?: os >:o: 108 AVG < DDb) XRPD AVG iitVii -0.8900 49.6 -0.004 FVOL DF BATCH NUMBER 100 1 962681056801 BURN t BURN 2 RR RI) -0.003 -0.806 _________ 232 DU P0503 07475 RUN HAi'lLs y&asy&aFWl PAGE- 3 ANALYST! 059 .TUBE s SAMPLE PBW i 09/25/96 06 : 09 CL ACC I VOL/LIT 4;-ft 100 ZZZZZZ ftVC(GDb) 5SRPD AVG Abs 22.0600 12.3 8. 129 ^RECOVERY 110 .3 i..$ Nn$ Ci s'.-:R u-utoRn't ui. il .i INSTRUMENT ID: 0260 3 GFAA ELEMENT.: TL FVOL DF BATCH NUMBER "Tee 1 968661856001 BURN I 0. 140 BURN 2 0. 113 TUBES SAMPLE zzzzzzLCSW .V I 09/25/96 06 s 12 CL ACC IVOL/WT s;-x xxxxx 1 AVG<ppfo) pfiftP'D AVG ab-:i 47.2300 0.4 0.264 FVOL DF BATCH.NUMBER . 1 i 962631056001 BURN 1. BURN 2 RR Ri) 0.265 0.263 ___ TUBES SAMPLE LCSU ZZZZZZ , 89/25/96 ,06 s 15 . ' CL ASC iv g l /u t A 1 AVG <Db> *RPD AVG abs 63.5180 8.9 0.366 ^RECOVERY -- 186 - C? . FVOL DF BATCH NUMBER i 1 96263i056001 BURN 1 0. 366 BURN 0. 371 t uX ; s SAMPLE 2533205 ZZZZZZ V. ' - 89/25/96 86s 19 Cl ACC IVOL/WT -i: :l 88 AVG<DDb> ?LRF'D AVG abs ,-2.0300 33.0 -0.818 FUOL DF BATCH NUMBER 108 ' 1 962631056801 BURN t. BURN 2 RR RD -0.807 -0.013 TUBE s : t SAMPLE 2533205 09/25/96 06 s 23 CI.ACC TVOL/WT -k ft* 108 ZZZZZZ AVG<DDb) ' XRPD AVG abs 19.2500- -1.3 0. 112 ^RECOVERY' = 96. 2 FVOL ~ DF BATCH NUMBER~ 188 1 962661056801 BURN 1 0.110' BURN 2 8.113 ZZZZZZ TUBE s : SAMPLE 2533206 1 09/25/96 06 s 26 CL ACS TVOL/WT X-XSHfrXX-X 108 AVG <? ? b> #RPD AVG ab^ -0.9708 10.9 -0.085 FVOL DF BATCH HUMBER 180 1 962631056001 .BURN 1 -0.005 -0.084 233 DUP050307476 RUM NAME s 9626982F01 PAGE 2 ANALYST: 659 J UDE: 28 SAMPLE 2563286 09/25/96 06:29 Cl. AS!; JUOL/WT ' 180 zzzzzz AUG(nob) %RPD AUG abs 19.3780 2. 4 0.1.13 ^RECOVERY = 96. 8 LANCASTER LAID Rh Vu RIES INSTRUMENT ID 02603 GFAA GLGMEM r TL FUPL. JDF PATCH NUMBER 100 1 968661056001 BURN I. 0ull3 BURN 2 0.111 TUBE: 21 09/25/96 06 :s 33 SAMPLE 2583287 ZZZZZZ. Cl. ASS JUOL/WT JCK*K)C 100 AUG <Disb> /RPD AUO ab>i X -1.2700 10.4 -0.086 TUBE: 22 SAMPLE 2563287 09/25/96 06:36 Cl. ASS IUOL/WT il Sli'.iiiiPt* 3 00 ZZZZZZ AUG < DDb> XRPD AUG abs 19.5900 6. 9 0.114 &RECQUERY a 98. 8 . ' ' FUOL DF PATCH MUMPER 108 ' 1 962661856001 BURN BURN RR RD -0.006 -0.08? FUOL DF BATCH NUMBER 180 1 962681856881 BURN t. 0. 109 BURN 2 8. 120 TUBE s 23. SAMPLE CCU 2 89/25/96 06 s 40 Cl ASS JUOL/WT 0 AUG < ooh> *RPP AUG- bs * 44.0000 7.6 0.245 ^RECOVERY = 110.0 FUOL DP PATCH MUMPER 8 BURN -1 0.232 BURM 2 0.256 TUBE: 24 SAMPLE CCB 2 89/25/96 06:: 4 3 CL ASS IUOL/WT 8 AUG(DDb) ytRPD AUG abs 0., 1700 99.9 8. 801 FUOL DF BATCH HUMBER 8 BURN 1 BURM 2 0.804 -0.882 TUBE: 25 09/25/96 06 a 46 SAMPLE zzzzzz Cl $ ;:;!:; JUOL/WT 180 AUG<DDb> i*RPD AVG A -1.2600 58.5 -0l886 .. ........... . . , 4 ... ..... .... . . . . - ... ,, , . ...... . FOOL DF BATCH MUMPER 180 i 962681856001 BURM I. BURM 2 Rf< RD -0.884 -0.889 2-34 DUP050307477 RUM NAME s 9626902F01 PACE: ANALYST: 659 TUBE: 26 SAMPLE 2563200 09/25/96 .06:50 CL ABS TVOL/WT s;-); xx-xAx 3.00 ZZ2ZZZ AVG i ppb) /RPD AVG abs TaTeeBa ?.'s 0.106 ^RECOVERY = 93.0 i-i-> i Eh Eh p u r h i u k L;..- INSTRUMENT ii): 82 6U.* OFftft ; l ; m; n t s t l FVOL DF BATCH HUMBER 100 1 962661056001 BURN 1 8.11 2 BURN .1 0.181 TUBE! 27 SAMPLE 2563209 zzzzzz 09/25/96 06:53 Cl. ASS TVUL/WT U->:xx->: , 3.00 V AVG < ppb) *RPP AVG_aksL --1.5400 99.9 --0.BBS FVOL DF BATCH NUMBER 188 1 962661056001 BURN 1. BURN 2 Sf?) RD 0.804 -0.019 jR ___ TUBE; 26 ' SAMPLE 563209 09/25/96 06s57 Cl. ASS . .TVOL/UT ll****A 100 zzzzzz AVG <ppfa) /RPP AVG abs 20.8100 23.2 0.116, ^RECOVERY 100.0 FVOL DF BATCH NUMBER 108 1 962661056801 BURN t 0. 896 / BURN r 0.137 TUBE: 29 89/25/96 07a00 SAMPLE Cl. ASS IVQL/UT 2563209 !)- 180 zzzzzz X AVG (DDb)' XRPO AVG abs 0.7500 23.8 0.084 TUBE; 30 SAMPLE 2563209 09/25/96 07s03 Cl. ASS JVPL/MT IHix >:>: A* 100_ ZZZZZZ AVG (DDb) -*RPP AVG abs 16.7000 10.1 ,0.107 ^RECOVERY 93.5 FVOL DF BATCH NUMBER 108 1 962661056081 BURN l BURN 2 RR RP 0. 804 8.803 \ FVOL DF BATCH NUMBER 100 1 962661056001 BURN' I. 0.115 BURN 2 8.100 ' TUBE; 31 SAMPLE ZZZZZZ1' 09/25/96 07s06 CL ASS TVOL/UT R-x :-k m 3.00 AVG (ppb) SRPP AVO abs. 44.0380 0.7 0.245 FVOL DF BATCH NUMBER 180 1 962661856001" BURN 1 B1JRM r> RR R 0.246 0.244 235 DUP050307478 RUM NAME s 9626902F01 PACEs i ANALYST: 659 I ..A M CAS f ft I .A B ijft A T 0 ft IE IHST ft UFIEMT IDs 02603 GCAA ELEMENT TL TUBES. 32 d$efg; ZZZZZZ 09/25/96 07s 10 ci ftu;:: iu o i /u r RK*A* 0 01 AUG(ppb? ERPD AUG abs, 57.5900 1.6 8.324 BURN 1 0.326 BURN 0.320 /.RECOVERY = MOT APPLICABLE TUBE;' 33 09/25/96 07:13 SAMPLE Cl ASS JUQL/MT 563210 ZZZZZZ : ' .100 % AUG ( ppb) /RPD AUG ab-* ""3.9000 7. 3 -0.819 FUOL !>F BATCH NUMBER 188 1 962661056801 OUftN 1 . BURN 2 f<R Rj? -0.016 -0.020 ---- ---- TUBE i 34 SAMPLE 563210 09/23/96 07:i 17 C). ASS lUOL/UT hh$ ' 100 zzzzzz AUG(ppb? . ZRPD AUG abs 17.3900 11-1 0-09.7 /RECOVERY => 67.8- FUOL i?F BATCH NUMBER 100 1 962661856801 BURN 1 0. 090 BURN 2 0. 105 TUBE; 35 SAMPLE CCU 3 09/25/96 07:20 Cl. ASS JU0L/WT 0 AUG < ppb? r-RPD AUG abs 42.3000 4.3 0.235 /RECOUERY 105.6 FUOL DF BATCH NUMBER 01 BURN 1 8.242 BURN 2 0.226 TUBE: 36 SAMPLE ` ' CCB 3 09/ 23/96 07:23 Cl. ASC . JV0L/4JT 0 AUG(PPb? JS.RPD. AUG a bs 1.0600 .99.9' 0.005 FUOL DF BATCH NUMBER 01 BURN 1 BURN 2 0.002 8.889 TUBE: 37 SAMPLE 2563623 09/23/96 07:27 CL AST: IVOL/UT K*K1HSX 10 ZZZZZZ X.V AUG(ppb? /RPD AUG abs -2.6900 52. 0 -0.014 FUOL DF BATCH NUMBER 100 1 962661056001 BURN 1 BURN RR RI> -0.019 -0.009 2Sf DUP050307479 RUN h h s m: : 9626902F01 PAGEs 7 ANALYST: ess TUBE s 38 SAMPLE 2563623 09/25/96 07 s 30 Cl. ASS IUOL/UT KCBKKfl# 180 zzzzzz AUG(ppb) '/RPD AUG alas 20.2200" 0.0. 8.119 ^RECOVERY - 101.1 LA ML A:'VC 1S< I..HVU jRATUH J. Lu 1NS'l KUMLN T ID: 028U-> GFAA CLEMEN I : TL FUOL PE BATCH NUMBER 100- 1 962681056001 BURN I. BURN 2 0.120""' 0.116 TUBES- 39 09/25/96 07:;33 . SAMPLE Ct ASS 1U0L/UT 2563624 ZZZZZZ )!* 180 RUG <ppb) /RPP AUG <ab-.s -2.3700" 13.9 -0.812 FUOL PF BATCH NUMBER I80' 1 962661056001 BURN L BURN 2 RR RP -0.010 -0.013 ..... ...- TUBE; 40 SAMPLE 2583824 09/25/96 07 ; 37 I Cl. ASS JUOL/MT ' x-A 100' zzzzzz ' AUG<ppb) 54RPP AUC3 abs 20.9600 13.9 ` 0.123 ^RECOVERY = 104.6 FUOL PF BATCH HUMBER 100 1 962661056001 Y BURN I BURN 2 8.111 0.135 TUBES 41 SAMPLE 2563625. ZZZZZZ 09/25/96 07.; 40 CLASS X VOL/UT 100 AUG<ppb) *RPD. AUG abs -2.5400 99.9 -0.012 TUBES 42 SAMPLE 2563625 09/25/96 07 s A'l Cl. ASS SVOL/UIT *' A* 100 ZZZZZZ AUG < ppb> *RPD AUG abs 21.8500 1.0 0.124 JSREC0UERY = 105.2 TUBEs 43 09/25/96 07s4? SAMPLE 2563626 ZZZZZZ Ck ASS XUOL/UT 100 AUG < ppb> XRPP AUG abs -0.3000 99.9 -0.001 FUOL PF BATCH NUMBER 100 i 962681056001 BURN 1. BURN 2 RR RP -0.003 -0.022 ___ ,,.,,,,, mi- II 1 lulu L_.J 1 ! -Iir 1U. I FUOL PF BATCH NUMBER 100 1 962681056001 BUF<N 1 0. 123 BURN r> 8. 124 \ FV01. PF BATCH `ijkX ; l 100 1 962681056001 BURN L BURN 2 RR Ri) -0.007 0.004 237 A DUP050307480 RUN NAME: 9626902F01 PAGE: 6 ANALYST; 859 LAMCAO IT.R LABOArtTuKlLb INSTRUMENT ID; 82683 OFAA . ELEMENT J TL TUBEj 44 SAMPLE 2583626 09/25/96 07s51 CL ASS 1VOL/U1T 100 FVOL 100 DP BATCH NUMBER 1 968601056001 ZZZZZZ AVG(ppb) %RFD AVO abs BURN I. 19.6700 9.4 0.115 . 0.123 BURN 8 0. 107 JS RECOVERY = 98.4 TUBE: 45 .09/85/96 SAMPLE Cl. ACC 2583627 zzzzzz :i AVG(ppb) XRPD 0.9980 80.3 07 s 5 'i 1VPL/UT 18 AUG ab-=> 0.005 FOOL ,, j)F BATCH NUMBER " 100 1 968681856001 BURN l BURN 7 RR RD 0.002 0.008 _ ___ TUBE: 46 SAMPLE 25S38B7 09/85/96 7s57 ' Cl. ASS I VOL /WT A* ` 100 FVOL PF BATCH NUMBER 108 1 968681056081 ZZZZZZ AVG<ppb? %RPD AVG abs 20.7900 1.2 8.122 BURN 1 0.183' BURN 3 0.181 ^RECOVERY = 104.8 TUBE: 47 .SAMPLE CCV 4 09/85/96 08:01 ` Cl ASS IVOL/WT 0 AVG < ppb? SRPb AVG abs 43.550 8.0 0.842 ^.RECOVERY = 108.9 FVOL PF BATCH NUMBER 0 1. BURN 1 0.239 BURN 8 0.846 TUBE; 48 SAMPLE CCB 4 - 09/85/96 08s84 . Cl. ACC IVOL/UT " AVG < ppb) XRPP AVG abs -8.8900 67.1 -0.001' FVOL PF BATCH NUMBER .0 1 BURN 1 -0.002 BURN 2 -0.001 TUBE : 49 SAMPLE 09/85/96 08:07 Cl. ASS !f VOL/LIT KKK 108 AVG < ppb) XRPP AVG alls -1.7808 30.7 -0.80S FVOL PF BATCH NUMBER 188 1 968681856802. BURN I. BURN f> RR Rjt) -0.010 -0.007 238 DUP050307481 RUM NAME s 9626902F01 PAGE; 9 ANALYST; 659 TUBE s 50 SAMPLE PBW 09/25/96 Bflsll Cl. ACi. TVOL/WT A 100 'P&uoA AVG <ppb> ?tRPP AVG &bs 22. 1200 4.6 0.129. ^RECOVERY = 110.6 LANCA:5 i'CR LABORATuKi EC INSTRUMENT II>s 02603 GFAA. ELEi'ICN r TL FVOL DF BATCH HUMBER 10 1 962661056002 BURN 1 0. 134 BURN 2 0.125 TUBES 51 SAMPLE LCSW 09/25/96 06s14 CL ASS IVOL/WT >i K##* 1 AVG < apfa) #RPP AVO aba 47.650 0.6 0.267 FVOL DF BATCH NUMBER 1 1 962681056802 BURN I. BURN 2 RR RP 0.269 0.266 ___ ___ TUBEs 52 SAMPLE LCSW 09/25/96 06s16 ' Cl ASS IVOL/WT k *mk A* .1 FVOL DF BATCH NUMBER ,1 1 962661056002 L.C^>l OA AVGdsob) ygRPP . 67.5700 3.2 AVG abs ` . BURN 1 0.365 0-357 BURN 2 0.374 ^RECOVERY 96.6 '' TUBES 53 SAMPLE 2563222 09/25/96 00:21 Cl. ACC IVOL/MT **** 100 X AVG <ppb) SRPD AVG ab* -1.6200" 36.3 -0.0-06 FVOL DF BATCH NUMBER 100 1 962661056002 BURN 1 BURN 2 ' RR RD -0.006 -0.010 ___ ___ TUBEs 54 09/25/96 06:25 A SAMPLE Cl ASS IVOL/UT FVOL I)F BATCH NUMBER 2563222 * A* 180 180 " 1 962661056002" R 55SF/2| SiRPP AVG abs 20.8800 . 2.2 0.116 BURN l 0. 120 BURN 2 e. ii6 ^RECOVERY = 100.4 . TUBE; SAMPLE 2563223 09/25/96 08 s 28 ' Cl ACC :i VOL /WT 3:4;->:)! 185 RSHOF' JK AVG(ppb) -1. 1680" XRPD 23.6 AVG ab-.-i -8.086 FVOL DF BATCH NUMBER 100 1 968681056082 BURN 1 BURN 8 RR RD -0.005 -0.007 239 DUP050307482 RUN NAME a PAGE: ANALYSTS 96269021-03. i8 859 LANl h l I HR I.. ABORA i (JK i EL INSTRUMENT IDs 02803 I3FAA CLEMEN fTL TUBES 56 SAMPLE 2583223 09/85/96 06s32 C:L ASS IUDL/WT i; ); k >; A 188 ^H5FA AUG(opb) sCRPD AUG abs .17 ,, 9400 3 4 0.181 FUOL DF BATCH NUMBER 100 ' 1 962661056802 BURN 1 0, 184 BURN r> 0.099 ^RECOVERY = 69.7' i TUBE; 57 SAMPLE , , 2563224 . . HCs ^Pf 89/25/96. 06 s 35 Cl. ASS IVOL/WT' ft . 100 AUG <opb> #RPD AUG ab-i -1.3008 99.9 . "0.006 FVOL DF BATCH NUMBER 108. 1 962681056002 . BURN l BURN 2 ft ft R0 8.000 -8.013 \ TUBE; 58 SAMPLE 2533224 09/25/96 08s39 - Cl. ASS TVGL/WT $>' j :-A-h 188 FVOL 100 1 I)F BATCH NUMBER 1 962661056002 HDCyfF'A AUG < opb) *RPD AUG abs BURN l 19.2000 - 2.3 0.111 8.109 BURN 2 8. 113 tfRECOUERY 96. 0 TUBE; 59 SAMPLE CCU 5 89/25/96 06s 48 CL ASS J.UGL/WT 0 FUGL 8 DF BATCH NUMBER 1 . AVG<? ? Ii > 42.3000 5CRPD AUG abs 7.1 ; 0.235 BURN 1. 8.223 BURN -2 0. 247 sSRECQUERY = 105l.d -------- ...--- ......... . ..... . .. ... ...... TUBEs 60 "SAMPLE CCB 5 09/ 25/96 CL $s s :; . . . ..... . .... .. .... . . . ...... ....... 08 s 45 TVGL/WT 8 FVOL DF BATCH 0 1. ____ __, NUMBER AUG(cob) /.RPD AUG aba 0.6900 . ,89.6 0.033 BURN 1 BURN 2 0. 806 8.801 TUBE; 61 SAMPLE ,, j, 2563225 09/25/96 03 s 49 CL ASS TVGL/WT it- 108 * FUOL DF BATCH NUMBER 100 . 1 962681056002 X/ AUG <oob> *KPD AUG ab*i -1.3600 18.0 -0.087 BURN l -0.006 ..... ... ..................... . .... .. .. .... ...... . ....... BURN '-0.088 RR RD ---- --------- 240 DUP050307483 RUN i tlll'IE ; 96269M2F01 PAGE: :l .i ANALYSTS 659 l ..AMCAGTFR LABu Rh FUH ills INSTRUMENT 12;: 02603 O!7 A A -SiJ.iinGNT t Tl. TUBE; 62 SAMPLE 2583225 09/25/96 06; 52 CL ACC TVOL/UT , FVOL 188 100 DF' BATCH NUMBER 1 962681056002 S, Ffif AUG(ppb) XRPD AUG abs ' BURN 1. '21.0500 11.6 0.123 0~113 BURN H 0.134 ^RECOVERY = 105.2 TUBE: 63 SAMPLE 2583226 RXbSCir 09/25/96 06:56 CL ASS TUOL/UT LlMXKKttSi 180 -1.7600 18.7 -0.009 FOOL BF BATCH NUMBER 108 1 962661056002 BURN L BURN RR RD -0.008 -0.010 ___ ___ TUBE: ( f SAMPLE 2583226 09/25/96 08 " 59 Cl'ASf. TVOL/UT U:!xx->:ft 100- FA AUGtoob) JSRPD flVG ct b s 19.7600' 10.4 0.116 ^RECOVERY '=> 98. 8 FUOL DF BATCH NUMBER 100 1 962681056002 BURN L BURN 0.107* 0.124 TUBES 5 SAMPLE 2583226 09/25/96 B9:03 CL ASS XUOL/WT- ' Dxx }: 100 FUOL DF BATCH NUMBER 108 1 962661056082- x AUG(Dob > XRPD ftVG c<o*^ -1.S100 -96.0 -0.007 BURN ). BURN RR RD -0.002 -0.012 TUBEs i 6 SAMPLE 2583226 09/25/96 09 s 06 Cl. ASF: IVOL/WT n***fl 100 AUG ( DDb) 19.7500 3CRPD AUG abs 7.4 V 0.116 ^RECOVERY = 98. a FUOL DF BATCH NUMBER 188 ' 1 962661056002 BURN L ' BURN 2 0.122 0.110 TUBE; (, 7 SAMPLE 383226 09/25/96 09 s 10 CL Also 3T VOL/WT f,*,K*** 1.00' FUOL DF BATCH NUMBER 100 1 962661056002 AUG < ? ? Ij ) *r p ? AUO Abs BURN I. BURN 2 RR RD 45.7100 o6 0.255 > 0.248 0.261 241 DUP050307484 RUN NAMES 96269021-01 PAGE: 3P ANALYSTS 659 TUBES 66 SAMPLE 2ZZZZZ 89/25/96 09 s 13 ci. $mm :; IVOL/UT R *** A* 8 LANCASTER I..ABO RAT UR X E! INSTRUMENT IDs 02603 Ol'AA ELEMEN f ; TL ' - FVOL 0 1>F BATCH NUMBER 1 AVG <ppb> /RPD AVG Abs ,59.2300 0.3 0. 334 BURN 1 8.334 BURN 2 0.333 '/RECOVERY = NOT APPLICABLE TUBES 69 SAMPLE 25$3227 09/85/96 '09:17 CL ASS IVOL/UT !;>: *>: 180 AVG < ppb> . # ' A VO ab-j "-1.2700 '99.9 . -0.086' FVOL DF__ BATCH HUMBER 100 ' 1 962661856802 BURN 1 -0.011 .{ BURN r> -8.0.01 RR KD. _ __ TUBES 70 SAMPLE 2563227 89/25/96 09s20 CLASS IVOL/WT 100 AVG < ppb) /RPD AVG abs' ,17.9600 0.6 8.182 FVOL DF BATCH NUMBER 180 1 962661056802 BURN 1 0. 10 2 BURN C 0.101 /RECOVERY = 69.9 TUBEs 71 SAMPLE CCV 6 09/25/06 89s2*1 ' CLASS TVOL/UTT .8 -FVOL DF BATCH NUMBER B1 AVG <ppb> . RD AVG abs . BURN I. .42.0000 ' 0.5 0.236, . 0.'239 . BURN 2 0.237 /RECOVERY * 107.8 TUBE s 72 SAMPLE CCB 6 09/25/96 09s27 Cl ASS IVOL/WT ~0 AVG i pisb) /RPD AVG abs 0.2000. 99.9 0.001 FVOL DF BATCH NUMBER ~0 1 BURN 1 BURN 2 0.082 0.000 TUBEs 73 09/25/96 09 :i 30 SAMPLE Cl. ASS TVOL/UT 2563630 * 100 cS>BC>XS V AVG < ppb? . /-Ri'-'D- AVG abv, -8.4580 99.9. ~-8.002 FVOL DF BATCH NUMBER 100 1 962661056002 BURN 1 BURN 2 -0.086 .'0.804 & RD 243 DUP050307485 RUN NAME: 9626902F01 PAGE s .1 3 ANALYST; 359 TUBE: 74 SAMPLE 2533830 09/25/96 09:34 IVOL/WT A * 108 i2) iMiXL 5)f-\ AVG Cppb> SiRPD AVG abs 19.6400 2.8 0. iis ^RECOVERY = 93. 2 LANCASTER i u k il j INSTRUMENT ID; 02303 GFAA ELEMENTTL FVQL DF PATCH MUMPER ICC) 1 962631 056082 BU!SN_A 0-113 ft URN 'T 0.117 TUBE; 75 SAMPLE 2533331 09/25/96 09:37 Cl. ASS IVOL/WT it -/C-5C- 4! -K&K 100 ' V AVG < ODb) yppp AVG abv. - -8.3700 99.9 -0.002 FVQU DP BATCH NUMBER 100 1 962631056002 BURN .1. .BURN 2 BB<7 BJB. '0.001 -0.00-4 JL ff TUBE; 76 SAMPLE 2583331 . 09/25/96 89:41 Cl ASS IVOL/WT 4:- A>: 100 <3SbXSft < AVG(cob) XRPP 13.9300 . 9.3* VG 113> 8.109 ^RECOVERY FVDL DF BATCH NUMBER 100 1 962631056802 BURN l 0.103 BURN a 0.117 . 4* 0> If TUBE; 77 SAMPLE 533332 09/25/96 09:44 CL ASS IVOL/WT * 5.00 y. AVG <DPb> XRPD AVG - --1.2380 37.6 -0.806 . FVQL DF BATCH HUMBER lea . i 5&a&ai05fc002 i BURN t BURN 3 RR -RD -0.002 -0.810 [/__ TUBE: 73 SAMPLE 2583332 09/25/96 09:43 CL ASS IVOL/WT y xA: 108 FVOL DF BATCH NUMBER 100 1 96263 1056802' 1 AVG(oob> XRPD AVG abs 'BURN t BURN 3 22.6000 a. 4 ' 8.132 0.140 0.124 ^RECOVERY' 113.0 - TUBE: 79 SAMPLE c? tu Q. 3 & 3 3 89/25/96 09:51 CL ASS IVOL/WT ; *4Ht -U 4i: 100 v AVG C oob> 3CRPD AVG. a i.):> __ ,0.2480 99.9 8. 001 FVPL DF BATCH HUMBER 100 1 962631056002 BURN l BURN 3 0.000. 0.602 243 DUP050307486 RUN NAME : 9626902F01 PAGE: .14 ANALYST: ' 859 ' TUBE: 30 SAMPLE 2533833 09/25/96 09:55 ' l $s s :; TVOL/WT 4* A 108 Sb'X^A AUG < nob) *RPD AVG abs 19.9000 12.E 8.117 ^RECOVERY " ,99.5 LANCAH TER LHBUKA'I URILS INSTRUMENT ID: 82303 .GFAA 'ELEMENT.! TL FVOL DF BATCH NUMBER .100 1 962631056002 BURN 1. 0. 107 BURN 2 0. 127 TUBE: SI 09/25/96 09:53 SAMPLE ' 2533334 . Cl ASS lUOL/UT * 100 P6>i tys . y AUG < ? p h) y.RPD AUG a ow 2.2100 11.fc . 0.011 FUOl. IiF BATCH NUMBER 100 1 962631056082 ,BURN ( BURN 2 Rg CD 0.010 0.012 TUBE a 32 SAMPLE 2533834 , 09/25/96 10:02 Cl. ASS UJQL/UT k A-x 100- fSt&SP, AUG < DDb) J5RPD AUG abs 20.1200 14.3 8.113 sSR.ECOUERY = 39. & FUOL DF BATCH NUMBER 100 BURN 1. .0.106 BURN 2 8.131 TUBE: 83 SAMPLE CCV 7 09/25/96 10:05 Cl. ASS TVOL/WT . 8. AUG (DDb) tfRPD AUG abs 44.2900 3.7 0.247 FUOL DF BATCH NUMBER 0.1 BURN I. 0.253 BURN 2 0.-240 ^RECOVERY = 1101.7 TUBE: 84 SAMPLE CCB 7 09/25/96 18:83. ci $s s :; :i VGL/WT 0 AUG <i3pb) *RPD AUG abs 0.4600 72.6 ' 0.-008 FUOL DF BATCH NUMBER @ 1. BURN 1 BURN 2 0.001 0.083 BATA REVIEWED BY DATA VERIFIED BY 244 DUP050307487 LAMCftSTER Lftb 0 RftTDRIES GRAPHITE FURNACE ATOMIC ABSORPTION DATA REVIEWED BYs DATA VERIFIED BY Dft'l ft Flit' NAMES ! LL`09B9 HUN NANEs `:?ti:690 BED 1 ANALYST i; &m I NBl'KUrit:. Mi NO: WEtiOS mr u CORR D? EL E ME N't ; TL Conceri1:t a-tio xt u!-od 'bo evaluctb*^ >. ! 'iAiiip lo eaili brafcion ram)e. l L:> 245 wi.*bb*ivi DUP050307488 RUN Ni-lHE s 9626903FU1 PACE s :l ANALYST: 609 TUBE: SAMPLE 30 1 09/25/96 12s 25 CLASS IVOL/WT 0 AVG < Diata) #RPI> AUG ^b-> 00000 0.0 -0,017 LANCA3 I'RH L$ .w u i'Al 1'UK.lt INSTRUMENT IBs 026v; GE A A ELEMENT.: TL 1-v o l 0 X; i X $t ' h MIJMBI.-.K BURN 1 BURN e -0.019 -0.014 TUBE: SAMPLE SIB 2 09/25/96 AGs 24 CL ASS I VOL/LIT 0. FVOL 0 DF BATCH NUMBER. 1 AVG(Bob) JiRPD AVG aba 10,. 0000 2.5 0. 067 BURN 1 BURN e 0. 066 0. 065 TUBKs. SAMPLE 820 3 ' 09/25/96 IGs 32 Cl. ASS I VOL/LIT 0 AVG < ppb) '/RP.D .AVG aba 20.0000 5.2 0. 121 FVGL I)F BATCH NUMBER 01 BURN 1 BURN 0. 125 0,,ll6 TUBES SAMPLE SAB A 09/25/96 12s*36 ' CL ASS IVOL/WT & FVOL ..F_ BATCH MUM BEK 0i A rtVtj < i;>ob)' #RPD AUG abg_ BURN 1 BjJRM_a. ~40.0000. 5.4 ~ "0.22?" . 0.236 0.219 TUBE: SAMPLE 868 5 09/25/96 12 s .59 CL ASS I VOL. /WT 0 AVG(ppb> XRPB AVG abs 60.0000 1.6 0. 313 FVOL. BF__ BATCH NUMBER 01 BURN -1 BURN 2 0. 317 0.310 TUBE: SAMPLE S60 6 09/25/96 12s 43 CL ASS :r v o l /w t 0 AVG <msb> i*RP AVG aba 60.0000 3.0 0.395 FVOL m- BATCH NUMBER 0. 1 ' BURN 1 BURN 2 0.367 0. 404 TUBES SAMPLE ICV 7 09/25/96 12n45 CL ASS T VOL/WT 0 AVG < p rxb) ZRPD .AVG aba 46.7100 0.5 0.259 ^RECOVERY* 93.4 FVOL DF BATCH NUMBER 01 BURN l 0.256 BURN 2 0.260 246 DUP050307489 RUN NAME s 9686983K G.I. PAGE s ANALYST: 609 TUBE s SAMPLE ICB 6 09/ 3/96 Ct ASS ' T ?3 0 :i WL/WT 0 AVG < ppb) /RPD AUG abs -0.3500 83.6 -0.008 i.. A M i, A: i f;.; i.. $ ;.i u !'; 1111 j i i. INSTRUMENT IDs 0860 GFAA ELEMENT; TL FUOL DF BATCH NUMBER 01 Bu r n i -X u r n b -0.008 '0.003 TUBE * SAMPLE CRA 9 09/83/96 18 5 5.1 Cl. ASS 1 UOl. /WT 8, AVG<DPb> /RPD AUG abs 9.6408 19.6 0.064 FUOL DF BATCH HUMBER 01 BURN 1 BURH 8 0,055 0.073 TUBE:. .1.0 SAMPLE 2ZZZ22 09/83/96 18 s 36 CLASS TVOL/UIT *:***** 0 FUOL I>F BATCH NUMBER 01 AUG <ppb) /-RPD AUG abs BURH 1 BURH 8 301.6800 3.0 0.180 0.184' 0. 177. TUBEs. 11 SAMPL.E bcv i 09/85/96 13 s 00 Cl. A SC :i UOL/UT i FUOL DF BATCH HUMBER 0i AUG <ppb> /RI-'D AUG abs 48.1500 8.9 0.838 BURN 1 0.833 BURH g 0.848 '/.RECOVERY *105.4 TUBE; 18 SAMPLE CCB 1 09/85/96 13s03 Cl. ASS lyOL/WT FUOL DF BATCH HUMBER SOI AVG <oi3b> XRPD RUG abs '.0.6100. cola i.*i04 BURH 1. BURH S 0.006 0.008 TUBE; 13 09/85/96 1306 SAMPLE C! ASS TVOL/WT 8563869 U->;*; y- 100 ZZ2Z2Z AVG < ppb> /RPD ' AVG !.) , 1.. 0900 31.1 0.007 PVOL DF BATCH HUMBER 100 1 968661056001 BURhl l BURN 8 {& RD 0.009 0.006 247 DUP050307490 RUM MAHEs 9686903F01 PAGEs 3 ANALYSTS a9 TUBE s :l. A SAMPLE as3389 09/85/96 13*10 GLASS TVDL/0T U A :l 08 ZZZZ2Z AUG <ppb> y-RPD AUG aba "0.0100 0.5 0.181 '/RECOVERY = 94.6 l $n ' $o l $X u ' $ i $r il s INSTRUMENT IDs 08303 OF AA ELEMENT,: TL FVDL DF BATCH...HUMBER 100 1 968631056001 BURN l 0.180 BURN 0 0.181 TUBE: 15 SAMPLE 8533330 09/85/96 13 s 1."5 ci. $s s iv o l /w t )( 100 FUOL DF BATCH HUMBER ~10@ ""l 968631056008 3i AUG < Dpb> /RI-'D AUG ab-A BURN i. BURN 8 RR Rl) 8.1300 16.4 0.014 0.016 0.013 ___ TUBES 16 SAMPLE isaiaib '09/85/96 13s17 ' Cl. ASS TUOL/WT ** a - . 100 Q ["'>> TS,A AUG (p? b) y-RPO AUG abs 80.5900 1.0 0.184 /RECOVERY * 98. 3 FUOL DF BATCH HUMBER 100 1 968631056008 BURN I. 0.185 SUNN 8 0.183 TUBE; 17 SAMPLE 8533331 09/85/96 13 X 20 Cl ACC TUPL/WT KS#K .100 AUG (ppb) ZRPD AO 0 (A i.js:-. "-0.3700 99.-9 "-a.sea" FUOL 1>F BATCH- NUMBER 100 1 968631056008 BURN 1 BURN 8 i!R Rj). 8.,083 -0.003 ___ ___ TUBE; 13 SAMPLE 853333.1 09/85/96 13s84 Cl. A SC IUPL/MT k k A ~ 108 ' FUOL 100 DF BATCH NUMBER 1 968631056008 5S5lsA AUG (ppb) XRPP AUG &br 80.1108 0.8 0.181 /.RECOVERY 100.6 BURN I. 0. 188 BURN 8 0.181 TUBE ! 19 09/85/96 13 s 8 7 SAMPLE 8533338 Cl. ASC 3 VOL/W.I :$' n $;$r h : 100 ibCXES AUG <ppb? /RPD AUG 1.'. S ,0 0.005" FUOL 1HL BATCH HUMBER 100 1 968631056008 BURN I. - BURN 8 RR RJ) 0.003" "0.007' .............. 248 DUP050307491 o pr u n $ ; ; 9626y03F0i PAGE: 4 ANALYSTS 689 t u X ; s aa SAMPLE 2583832 89/25/96 13s31 Cl. ASS IMQL/WT 188 'ICiCiXSA AUG i ppb) /RPD AV.G aba *18.7300 4.8 """0.114 ^RECOVERY = 93.6 I..ANCAU fi .;< uifUKH i u k .t t.. INSTRUMENT IDs 82fcKS GFAA iT.UT.HLN E' : 1 L FMOL HE" BATCH NUMBER *100 1 962681056002 BURN 1 0.116 BURN...2 0.111 TUBE; .SI ' 09/25/96 13 s 3 SAMPLE2563633 Cl. ACC IVQL/MI MMMKK-KM 188 ^Sbx.s /Ur.PjO AMO.. "eTsii? 9 9 ".9 ' 0.004 FMOL DF BATCH NUMBER 100 1 962681856002 BUNN 1 BURN 2 r<R RjD *0.806 0.801 TUBE; 22 SAMPLE '' 2583833 09/25/96 1,3:136 C ACC JMOL/WT K-X >:--}C k Ax- 180 lSBxs,Aj AMG < pta) XRPD AMG atas 19.7100 5.1 0.119 ^RECOVERY = 98. 6 FMOL DF BATCH NUMBER 108 1 962681056082 BURN 1 0. 115 BURN 2 8. 124 TUBES 23 SAMPLE CCM e . 89/25/96 13:41 CLASS'; TMOL/NT 8 AMG(cob) *RPD AMG aba 48.6100 1-2. 8.238 itfRECOVERY = 181/5 FMOL BF BATCH NUMBER 81 BURN .1. 0.232 BURN 2 0.228 TUBE s 24 SAMPLE CCB 2 " 09/25/96 13 s 4 4 CL ACC- 1 VOL /MT 0 AMG (ppb) !*RPP AMG aba --0.3800 69.4 -0.003 FMOL DF BATCH NUMBER 0 i~ BURjbLi. . BURN S -0.001 ' -0.004 TUBE: 25 09/25/96 SAMPLE CLASS; 2583834 re> \ AMG < |3tab) %RC'JD '0.2700 99 .*9 13: 43 TUOL/UT :l 88 AMD aba 0.i"w2 FMOL DF BATCH HUMBER 180 1 962681056002 BURN L BURN f? RR RJD 8.088 -0.004 249 DU P050307492 t- ~ RUN HHHI:.: 9626903F01 PAGES Li ANALYSTS 609 IU.BE.S. 26 SAMPLE 3583634 09/25/96 13:53 a, IVQL'WT A-x 300- P&mSA A VG < pjrb> ZJgPft 0VG bs 20.6300 6.8 0. 124 34RECOVERY ~ 103 .2 ... ...... .................. - - ~ . ------ ---- ----- ...... TUBEs 27 ifiNFEE CCV 3 .'09/25/96 13 s55 QLMSL IVGL/.WL 0 AVG(piPb) gRPD fiVG..^b.5 40.5500 2.9 0.230 34EECGVERY = 3 03 . 4 .... _ .... ....... .. ______ .. ------------ ----- . . ..... . .. . TUBES. 28 SANfikE COB 3 09/25/96 13 e'SA CLASS i VOL./WT 0 AV(3'CDPb> 34RPD .AVG_ a ba 0.5900 99.9 0. 004 I ..A MO ACT I.ASlJUl-l luli .1. 1M ST RU ML N T 11> : 0 2 a W GFAA ELEMEH T TL FM.OU JBE... BATC-H....NU!l!Bt::R. i0 1 962661056002. BURN 1 BURN J1 0.3.30 e.na Eitfik J8_.^J2JM3S& 0i BURN i. 0.235 BURN 2 0.225 FWL _2E_ BATCH_MUMBLE 01 BURH...3, BURN_3 0.000 ' 0.008 DATA REVIEWED BYs 5Cg>P DATA VERIFIED BYs qftfhL 250 DUP050307493 Mercury Data DUP050307494 q r s t uv w$ ui:ic> r; $ $ u k .i. l >> MERCURY ANALYZER DATA REVIEWED BYt DATA VERIFIED BY a* FS-3 DATA FILE NAME 8 '36T'&93.. f`RN RUH NAMES '36S6903M03 ANALYST:: eC3 "3S> INSTRUMENT NO: 0S2S0 ELEMENT: HG 252 DUP050307495 HU IS HAHL s. U626903M03 PAGE 3 i ANALYSTs a*: 3 TUBES 1 SAMPLE BO 09/25/96 17s14 CLASS JMGl/WT * *** 0 AUG < ppb> 0.0000 Intensity 773-. 0 Lr Nu v ."i rr-H l A HR M l UK 1 My 1 KUl'iEM 1 i:i.>3 00 cu ; x: .. I'l: . IS 1 : 116 FUOL .0 j u f __ 1 BATCH NUMBER TUBES SAMPLE S8.2 . TUBE s 3 y$z{|; : SO. 5 TUBE i 4 SAMPLE. 81.0 . 09/25/96 17.: 16 . CLASS :i UOi. /MI *** 8 AUG <ppb> "0.2000 I when si'by 20160.0 09/25/96 17 3 10 Cl. ASS. :f v u l /w t K****** 8 AUG<ppb) (3 .'3000 tntwftljsy. ' &1 " 0 09 /2 5/96 3.7 i i'.? T Cl. ASS lUOL/WT . {; -**:*:- 0 fiy.S-lUvUl.tL?.. 1.0080 1033&i.0 FUOL .0 FUOL 8 FUOL "0 PF 1 BATCH NUMBER DF BATCH NUMBER 1 UK r BATCH DUMBER TUBES 5 SAMPLE S t-i - s 09/25/96 17 a23 Cl. ASS IUOL./WT K-*XK')CK4C- 0 AUG <ppb> 2.5080 Intensity 49425.0 FUOL 0 PF 1 BATCH NUMBER TUBES 6 SAMPLE SS.8 89/25/96 17:: 26 CLASS TUOL /UIT FUOL * ** ** 8.0 PF 3, BATCH NUMBER AUG <ppb> 5.8000 Irrfc&risi-by 4 3 {? 2 36,. 8 C<: r e 1 a 'bio n Ca e? f f 3. c i @ n t. - 3.39996 TUBE; 7 SAMPLE :r.cu . 09/25/96 1? 3 2ft CLASS IVOL/WT X ->C -X at X X- -JO @ FUOL 8 PF 1 BATCH NUMBER AUG <mib) 2. 0-480 8424.7. 8 ' SSRECOVERY 102.0 253 DUP050307496 RUN NAME t 9&2O903M03 PAUL : j. * ANALYST s 023 TUBE s 6 SAMPLE ICB 89/25/90 17s31 Cl. ASS 3UOI. /WT xx-x-x 8 AUG < ppb) . -0.0170- I,v>.t<2nsi ty. 539.8 FVOL. LAHCA'-S l ,R . A UK A l OR .i ' - I Nut RUMEN I I u : wfjt-:t> CV LLLML'.M i . MG I)F BATCH NUMBER 1 TUBES- 9 SAMPLE CRA 09/25/90 17s33 Cl. ASS :i UOl /WT K-!<* flVG'tppb) "TM 0.1908 Intensity 218SS.0 FUGL. 8 1)11 BATCH NUMBER TUBE: 1 SAMPLE CCU I TUBE: 11 SAMPLE CCB 1 a / p/ o $ 17;. y< ;-j et, $s s :i v o l /i/t x x -k k -w k * 0- f uol 0 ?f i }~X $t ' h ... X; r AVG <pb> 1. 0488 I.i'-kg-GisA.ix 105717.8 StRECQVERY 104. 0 09/25/90 17:30 CLASS - IUOL/WT #***** FVOL 8 DF 1 BATCH NUMBER AVG < ppb> - 8. 0200" Intensity "i 29~."i iysi: IS SAMPLE PBW Z2ZZ2Z 09/2S/96 17.; 40 Cl. ASS - :i UOL/WT xxxx *; ~1\ AVG<ppb) 0.0100 IllfelvllLLklGL 3 1 &"(3 TUBES 13 SAMPLE LCSW / X zzzzzz 89/25/90 17:42 Cl. ASS IVOI../WT !;-!;x-3;-)c-K)( :i AUG<ppb) 0.0020 01022. 0 FUOL S FVOL. 1 DF 1 BATCH HUMBER 902000021081 RI> 1>F BATCH...NUMBER S&B6&0&l00i RD TUBE s 14 89/25/90 17:: 43 SAMPLE C:L ASS 3UOL/WT 2503205 zzzzzz . ****** k . e 1/ AUG <ppb) -I.8020 Inteu-iii ty 2080.8 FVOL 0 DF 1 BATCH NUMBER 902030021001 RA R 254 DUP050307497 RUN NAME: 9626903N03 PAUL;: ANALYSTS 623 t uX ; : X5 SAMPLE 2563206 zzzzzz 09/25/96 17 s A? CL ASS I VOL/LIT k i' k t\ I AVG ( ppb)' 0.0060 i n Ljvvj i. by 8767.0 FVOL a I .HI'ICMC (': >: I. RHivH ui*. -I 5 IHoTRUMLNi ID: CV LLLi'IO-n ; ut; DF i BATCH . NUm.iLk 902660621001 KD TUBEs 16 SAMPLE: 2563207 ^ ZZZZZZ 89/25/96 17;; A 0 01. ASS IVOE/WT . K -K K -X $C-)C-*K 6. . FVOL a V/ A^lLLlllikL ~~ 0. 0110' Ivitevi-i i 'ey 3243.0 DF 1 BATCH NUMBER 962660621081. ;<R i<c X ; : a t7 SAMPLE aaasasa ZZZZZZ 09/5/96 17.: 51. CLASS i: 1V.QLZMI a AVO tppb) a-*050 Int;t by 670-0 FVOL 6 DF 1 BAT Chi N UMBER 962660621001 NR BP TUBES 18 SAMPLE 2503269 09/25/96 17 :: 51 CLASS TVOL/WT U-K ) 6 zzzzzz v AUG < ppb> 0-0030 In fay 2494.0 FVOL a DF 1 BATCH NUMBER *3 &cl t> 8 tjft cf 1 t'K'J 1 RR RD TUBE s 1 9 s $mp l ; : 2563209 ZZZZZZ 09/25/96 17 s 56 CL ASS IVOL/WT **' is a FVOL a DF 1 BATCH NUMBER 962660621001 */ AVG <ppb> 0.0040 by 631.0 1- ' RN RD A TUBE: 0 SAMPLE 2563209 ZZZZZZ 09/85/96 17 .; 5:1 Cl. ASS :i VOL /WT :a ,/ y AVG <ppb) 1- 0980 In b:.rn-i i. i;y 110152.0 FVOL . 6 I)F 1 X $t ' h n u mX ; r 962660621001 RR RD. 255 A DUP050307498 RUN NAME s 9626903M03 PAGE s ANALYSTS 623 TUBE s El SAMPLE 2563210 zzzzzz 69/25/96 161 tit) ' :; $s s :t yen., /wr flW(ppb) 0.0170 3666-0 Li-INCh C I LiibR'H l ul. 1L in s t R; ! iu; CV ELEMENT ; HG PVOL ' in-61 BATCH NUMBER 9t>2o60621 001 i'll) TUBEs 22 SAMPLE coy 2 TUBE;; 23 SAMPLE COB 2 " 09/25/96 1.8:: 03 BLAGS :i vcn /w t S-S-SKS-1( 0 pvg l . 0 DP 1 1 BATCH NUMBER AVG< cpb> 1- 0500 Iwbenssiljy 106169.0 *RECOVERY ~ 105. 0 09/25/96 16T05 ct. $s s t v ' h . /wr ** 0 f vol . 0 1>P 1 BATCH NUMBER 0- 0280 TUBEs 24 SAMPLE 2563623 S' \y // 09/25/96 16 3 07 CLASS :i VOL/LIT tt-K-x-Ji i -a ZZZZZZ AUGEppb? 0.0090 I-jl'J-iS3086.0 TUBE s as $; ; 2563624 / ZZZZZZ 09/25/96 16:09 ca-$s s :i voi /wr ** as a v Ayj3jLBili2.iL. LllkSlJlCLfeC. ~"~i70010" ~ 2252". 0 FVOL 6 PVOL 8 DP 1 BATCH NUMBER 962660621001 I>P 1 BATCH NUMBER 9626606210B1 ED TUBE s 26 SAMPLE 2563625' 09/25/96 16 a.12 CL ASS ilVOL/WT ZZZZZZ ****** 8 V/ - AVGEppfcC 0-0010 1 n i. Lv 2203.0 TUBES 27 SAMPLE ri? Ill; & 3 tiJ. / ZZZZZZ 09/25/96 His 1 1' CL ASS; :i yen. / wr ****** 6 AVGIppb) "0.0010 X r\t; >.-'Vr >i ty 2079.0 PVOL 6 f vol 6 DP 1 BATCH NUMBER 962660621001 RR RD DP 1 BATCH NUMBER 962660621001 EE KD 256 DUP050307499 RUN Hi U'lL r. 9fe<i6903M03 PAUL :: ANALYSTS 823 TUBE: aa SAMPLE asssac? 09/25/96 18:16 Cl ASS :i MOL. /WT ;; >: :: 8 zzzzzz AVO <ppb> ~ 0,,0030 , 8466.8 FVOL a i.i-it-li,i-v . l !: i i ii.i.M i i i;;< I.: . i.HS ! HlJhi N 1 ID; I'l *.* L..' l-' CV ELEMENTi HO DF 1 BATCH NUMBER 96268082101 RR RD TUBE: 29 SAMP LiE PBW PSu3 09/25/96 18:18 . Oi. ASS TV01. /WT v iV \l / AVG < ODb> Inbtnvri. by 0.0000 2237.0 FVOL a I) F i BATCH HUMBEL 962 6888c.' 1 08 si K X> TUBE: 30 SAMPLE LCSW 09/25/96 18 s 21 C:l. ASS :iv o l ./w t :i FVOL 1 fiF 1 BATCH HUMBER 962688821082 V/ >y AV6<oob> 1.8780 I vi b-.in-v i. by 108785.0 RK KD TUBE: 31 SAMPLE 2583222 .09/25/96 18;: 23 Cl. ASS S LH.il. /LIT *** ~8 FVOL 8 DF BATCH HUMBER 1 962680821802 / USS^F A V AUQtPPb) Intensity 870030" 2489 .*0 ><r< r ? A TUBE: 32 SAMPLE 2583223 89/25/96 U Cl. ASS - ** J VOI. / WT 8 FVOL 8 DF i BATCH NUMBER 9(62680821082 AVO <ppb) 8.0010 Inb=-?nsl by 224470 RB A TUBE.! 33 SAMPLE 2 5 >836? 2 4 09/25/96 18:27 Cl. ASS JVOl /WT FVOL a DF 1 BATCH NUMBER 962680821002 vX Y AVO(nob) 0.8070 In tsn-j L by 2988-0 1 < < RD 257 DUP050307500 RUN NAME): 96269031*103 PAUEs c ANALYST s 823 * s.4Wy:^l|v.'--:-- ...JS ...... ; .: .. l- ...... LAN' $ 1 L;< LA v.<.i < t i 1 UU .1.' INST RUM EM'i 1 i;is A CV ELCMEH ri Hi.. TUBES 34 SAMPLE CCV 3 09/25/96 IS: 30 Cl. ASS TVGL./WT K-tt-K 0 FVOL 0 F 1 BATCH NUMBER AVG <ppb> 0.9660 Intensity 96044.0 3CREC0VERY = 96.& TUBES 35 SAMPLE CCB 3 09/85/96 1S s'38 Cl. ASS :i VOL /WT 0 FVOL 0 BF ' 1 BATCH NUMBER AVG <ppfa) -0.0310 Intensity -670.0 TUBEs 36 SAMPLE 2563885 RiAH'SF 89/85/96 16.: 34 CL. ASS .1VOL/WT 6 xl/^ \s AVG < pp.b? 8.0470 I vi Biswiity SS>'j 3* 0 ' FVOL 6 . BF.. 1 BATCH NUMBER 968660681088 RR________ K TUBES 37 SAMPLE 2563226 R.C^S>bF '09/25/96. 16 a 37 Cl. ASS 3 VOL./k)T FVOL I)F ' U***K 661 BATCH HUMBER 962630621W02 v AWL<J2b2. In t;y " -0.0810* "2896."' RR RjO TUBE a 38 SAMPLE 2S6328G 09/25/96 18 39 . CL ASS 1 VPL/MT D >( ** & AVG(ppb? 0.0030 Ili!2*liLLUi:.5i FVOL & 1)F `1 BATCH HUMBER 962680821002 m e t RP TUBES 39 09/25/96 . SAMPLE Cl ASS 8563886 R->; / FtFsbF'S 18 s 41 IVOL /WT ft <V7 AVG <PDb) 1.0600 IlLi'I-.lLiJLk/. 107861,,8 FVOL a BF .1 BATCH NUMBER 968660681008 RR RB TUBES 4 0 SAMPLE 8563827 ^2>SF 09/85/96 16.: 4 4 CL ASS 1 VOL /WT >= 6 & y. fiifiLtaafel In tH'Vi'i 1 'ey -0.0010 8128.0 " ` ......... ----------- --------------------- FVOL 6 BF 1 BATCH NUMBER 96866 8621008 258 RR. RP DUP050307501 ft UN Ni'-lHI:..96269031103 PAGE t ANALYST; 653 TUBE; 41 SAMPLE 2563630 09/25/96 Id;46 ci $ ? uoi. /ur k k ): >: 8 d?JM3X AUG (ppb) .0070 ' Inbornl by-2698.0 Lh NCAS < Lft < .i-iiJKH i ui;.i. I MSTkUMEM1 U>: W522I CU ELEMENT ; !!G FUOL 8 _JDF_ 1 BATCH NUMBER 962680821002 RR RD IUBE: 43 SAMPLE 2583831 eDSCSXS 9/25/96 18;: 48 ci. $s s :i uoi. /m ->c x a AUGEpp b) ". 070 "a a si. s FUOL a DF BATCH NUMBEH i . 962680821002 ? TUBE: 43 SAMPLE 2583832 09/35/06 13,: 50 C:|. ASS lUOt/WT >: 8 . FUOL a DF 1 BATCH NUMBER 9 6 3 6 Ati 831003 AUG(ppfa) 0.0830 Inbnva-1 by 3466.0 ftp RD TUBE-: s 44 SAMPLE 3583833; /'btSXS 09/25/96 18:: 53 Cl $ ; :; $' -k ;:-x TV0L./WT a vy t/ . AVG<Db> 0.006 IVi b<r)n-> i. fey 2826.0 . FUOL a DF 1 BATCH NUMBER 962680821002 Rft RD TUBE s 45 SAMPLE 2583834 fS\ JbS 09/25/96 18 s 55 CL ASS :i VOL /W"i ft : 8 AUG i ? o b) 0.0030 Inb**:wi. by 2469.0 FUOL. a * DF 1 BATCH NUMBER 962680821002 RR RD TUBE; 46 SAMPLE CCU 4 ' 09/35/96 IS;: 57 Ct. ASS KKK*-* :i uoi. /ur & FUOL ?f 0. 1 X $t ' h HUMBER TUBE; 47 SAMPLE COB 4 AUG < ppb? 1.0300* Ivrbe'nsl'by 1049:107. ^RECOVERY TM 103.B 09/25/96 18 s 59 (.L AJJt* :ruoi../WT 0 FUOL 0 I).F 1 BATCH NUMBER AUG < p pb> -0. 0290 IvrteriBi by -662.0 259 DUP0503 07502 Extraction/Distillation/Digestion Logs 260 DUP050307503 1151 Re/. 08/22/95 rV rrArti s co DUP050307504 DUP050307505 5cn ! i =* o w 01 >r cn gs < sre 3 1 ii i s DU P050307506 DUP050307507 DUP050307508 5-157 X3, 10-91 LAB FILE COPY AQ VvJ =i iw t iv l ______ DUP050307510 5-167 X3. 10-91 LAB FILE COPY JMSNwH<l<1artf W*Lntter, PA 17601-5994 Sample Administration Receipt Documentation Log Client/Project:________CO//O ^_______________ COC Sea!: Pre^t / Not Present on cooler Date of Receipt:_____l -- / *?- G______________ Time of Receipt:^ f?^L 0Package: Ci^d / Not Chilled Broken / Irj^ct Source Code:_______ _______ /~~~ I Unpacker Emp. No.:______________________V*V~7' #1 Thermometer ID: /6 (0 3 Corrected Temp.: "7 B^tjsle / Air W^jjee / Dry Ice / Ice Packs Ice Present? ]N . #3 Thermometer ID: Corrected Temp.: Bottle / Air Wet ice / Dry Ice / Ice Packs Ice Present? Y / N Temperature of Samples Thermometer ID: #2 Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / Ice Packs ice Present? Y / N Thermometer ID: - #4 Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / Ice Packs Ice Present? Y / N Paperwork DiscreDancv/Unpackinp Problems: Name ir ----- -------v -- p Sample Administration Chain of Custody Date Time Reason for Transfer Cf~/IT-'W f'/t- ? C Q'ir-9L 1 c 1 c] II 00 1^0 0 Unpacking----fejace in Storage_J)or Entry Remove from Storage^ Place in Storage or EntQ/ Entry Rev. 2174 09/09/96 DUP050307511 ^Lancaster Laboratories 35 New HolldP*e*Unc**tW,RA 17601-SOW Sample Administration Receipt Documentation Log Client/Project: C'V,-A/C CO___________________ COC Seal: Pr^sjent / Not Present on cooler Date of Receipt:_______ ^ ________________________ Broken / inject Time of Receipt: 0 1 *pT~ Package: Ci^led / Not Chilled Source Code:________ P1 1________________________ Unpacker Emp. No.: Thermometer ID: #1 } 0 i O'3} Corrected Temp.: li 1 Bc^le / Air We^ie / Dry Ice / ice Packs Ice Present? (Y^/ / N #3 Thermometer ID: Corrected Temp.: Bottle / Air Wet ice / Dry Ice / ice Packs Ice Present? Y / N Temperature of Samples #2 Thermometer ID: Corrected Temp.: Bottle / Air Wet ice / Dry Ice / Ice Packs Ice Present? Y / N #4 Thermometer ID:' Corrected Temp.: Bottle I Air Wet Ice / Dry Ice / Ice Packs ice Present? Y / N Paperwork Discrepancy/Unpacking Problems: Name \ljb Sample Administration Chain of Custody Date Time Reason for Transfer 9-/9-% f&n Unoackino Vd6 < Place in Storage^ or Entry q-19-qL 1206 Remove from Storage^ Place in Storage or Entry Rev. 2174 09/09/96 Entry M5 DUP05 0307512 Chain-of-Custody Record 270 DUP050307513 % X2S New Holland Pike Laneasrer, f 17801-5994 Locked Storage Chain of Custody Original Sample Client/Project: P) u iPfthT" fTnlu ? f rvu taTT ft A .$<f/''O S Pvv I /Varli 'Son Preservative: j-j-iOft 'o _________ Matrix: ~l i)! a ) SDG: FMb'OSu Sample # Range of Entry Group: _____________ Bottle Type: SOOrJL Sample Number(s) Released Received Date of Time of in Custody By By Transfer Transfer Reason for Change of Custody Dist., Extr., or Digest Chain Created (X) --- 7""^"" ,CXf- WA fc ISlb yh' JTPr ifykl. A 4 az&S SfaCCXfSs /ej >is" jf&roserwt'on, cJ&cU ytolT ^/^T4 Sfor^^e* 2 <gS Ssi.2^---2-? "7* d|d|^L3 9/2^ m $u zj O ^Ts'rfn*'--V___ 3339 -a"1 C ^/pit-u 0^00 0f.nun.s3u CovtXeA. ?>v .. ""'.T"9`Ji-WVu&' *4'! o/- 3>^ Pden Sty)&**rt^ &3-P lisrtftip mo /3b M<*zdUi oruX) /~Cg <2^2 3HZJL-2.'? az&3f< &/ PzP 2016 Rev. 09/05/95 271 Page of DUP050307514 1% 2425 New Holland Pike Unca5ter, M 1760VS9W Locked Storage Chain of Custody Original Sample Client/Project: Du Pon~T tsm). R-ffapdiiTT, AsoS CS, Pari Preservative: Ift'h)0 3_____________ Matrix: _____________________ SDG: D M fc>) 3--. Sample # Range of Entry Group: Q.Sft 3? 30 -j?*/- Bottle Type: CE- Sample Numfaer(s) in Custody asf3?3o-w Released By Received By SA . Date of Time of Transfer Transfer 9-/M4 /300 Reason for Change of Custody S ft Dist., Extr., or Digest Chain Created (X) / 3s"f.3i3()DV S8 'SSSO-Srt- 259-3^0-BH ' ?5^3>S30-3H yfoT*. Jets' pff^jcrijqftort <^lrzci<L ctftd* /OS `f-oo-X coS' S-for^y&s m PP 4&b- <H-blU $ />.. _T ^Ut iiU$$ , d ion < Sy ftfhnrs\ ,, r 3>^r -f JjHllfc. #4.i-do fwJLaJLci p T-cp 330> HOD rV. >76 pjhm V&OSrU} ?2-3 lidHhu /S5d 5-<st^Cuc s A^f $Lh$ 3^3 ^??74iA^ $2-3 2016 Rev. 09/05/95 272 Page__[_ of DUP050307515 /A^\ ^ncasterLaboratories ^ 3C25 New Hoftand Pke * Unautrr. PA 17601-599* Locked Storage Chain of Custody Metals Jlient/Project: iXu__Q.cr*OL. Sample#: ^ST3gjQ-3if Digest Type (circle one): Hg ^Aetals?) GF Hydrides SDG: P>V) n <3 3- Trial No: (If not 1, fill in) Batch No: 3- u T _S X o o Sample Number(s) in Custody Released By 3.5x3*30 '3*-/ c?So3^sSi-'-^-V ssT3*S3o~ */ ^p^SCaSL-.^-? S"53o- V , 35- (C^ Received By Date of Time of Transfer Transfer ]<3P S't-an-ew^jt. ,/__________ /#r t M- d /-?recs (CP STC01& 9i/.9L o.-s^ Reason for Change of Custody t 0 CU^d > f O'K^tyS_ /> \dAJ/&u&< 35V&32.-3BT1' -> 'v^ST3d> ~<S'3 *-/ jJMJJta 11?A]Jd4M 9/^ 5a/<r 0 MtMiKW J J' A A- A K 2231 Rev. 09/21/95 273 Page _J___of / DUP050307516 a I\.\ anr^prl atoratories 2S New HoCUnd Pike * Lancaster. PA 1760J-59M Locked Storage Chain of Custody Metals Client/Project: ____Q. P<*ydt:.............................................. .. ................ Sample#: ~>T ___>5^3^30"3H__________ Digest Type (circle one}: Hg Metals ,/g P) Hydrides SDG: _ Fh^b a a. Trial No: _____(If not 1, fill in) Batch No: a iff 2- (a SL l O s Co o 3- Sample Number(s) in Custody *3*/ <^5833^ c35<B3as^f^ as 5?ss3^ap -a> S^3R3(V34 Released By L-0'^6^1yV' 3>-y Date of Time of Received By Transfer Transfer (Slf St<njexc^ niVAl%. D-HS Reason for Change of Custody looked &s-eyi^?Y---' -rihv'^fin 3ALJ^ Hi 4^ Mco diflA -i? j /Ls ) -- ^'AJLj3^ vMxn, 'OtV^CLPvp 9-2^b d :o $ Sttw~azy? Jd--------- -- -7-^ .. 9-t A He pesos' ]?^Y\ O-Il aA/i t 4s ^Sk-ca, 30. lO , < > aA (Aj- . J^Shi^cu 2CM^ Af\cJ+jA~ Pb fnr,-- i'W'Sb 3D\ Sb -A4" ^B22Z-njft3Cr3H- ^StoniSjo f \ sv \ \, : ^^oi0Y~ 1 41261QL 05/O _r^<r^ C6lS 3l%TOS2. (\(\ 75TS(3( c Chae x/?? (2X^3^y3l?V) 75^3^31 7 <5-5^ .? r5k? --^'7 c 3Y p.sir 3^30-3Y SSS^S^3o"3S & C5J7 3teto, All tfeh ^fZjT ___J^ //fo j(yluz$SD* /f T^t /vs ff2c? 2231 Rev. 09/21/95 d> i pgge J___ Qf ^ DUP050307517 /ix Lancaster Laboratories V-** HoRand c*xafift. ** `TWV&SfS* Locked Storage Chain of Custody Metals _iient/Project: Sample#: " SH y303 ____ Digest Type [circle one): Hg Metals Hydrides SDG: ____ gmDCCL Trial No: * (If not 1, fill in) Batch No: 1j 2- -3l Jk_ % \ o s op O Sample Number(s) in Custody Released By Received By Date of Time of Reason for Change Transfer Transfer of Custody 2513 ft/V-s 2S%Si3b R5^.( ^5biafc QhifcL 0655 ,J/Y)a()j~*AtsA\kQ j 9tZll% Q ..Q/./..C).... Stm2aJL^ AA Q \ . - < il.... 2231 Rev. 09/21/95 275 Page ^ of DU P0 50307518 _ Lancaster Laboratories ... ^ New HoAvd ^ * Uncisuc, M1760VS994 Locked Storage Chain of Custody Metals Client/Project: Pfr E'r- Sample Mi $'2 33 22.-2,'?, fl5~? 3 3g>-3</ Digest Type (circle one}: mjy Metals GF Hydrides <W- SDG: Trial No: (If not 1, fill in) Batch No: 4 X f > S A ! 0 & JL Sample Number(s) in Custody Released By Received By Date of Time of Reason for Change Transfer Transfer of Custody SL<r8 3 2.2.- 2.7 3X3*?- 3V 2,S& V7 *.3_ Jx\ sTri.). -t. Z&&S0j o - t4* lAf tew 32-2.^ - 5.? Jtr* 32 ~ 3 5^ l Cz # PJL && #2-3 9/W?& <0*730 Ug C *U^rft rtc^C. c/< i stJ^-Y cs^a^Aftx^ dk^,A<yi)f_ &rSPc*>o> - 276 2231 Rev. 09/21/95 Page of 1-- DUP050307519