Document KRra1kBDKkZLdxpQq62EEZgqN
C.V. 260
f 00 A
CODE RT-531-D
JUN14 m < DATE )
fZKZS
< LOT >
PATE PRINTED D.V. 303, 315, 317,
t4>3^8? ./323,
PROCESSES
APPROVED BY
( JRT-531-D (N) EWK 11-24-81
COMTYP JOB NAME: 40RT531DMN
TYPED BY: JMH
EST. WT, 643* LBS:,
STANDARD HRS. ___________ TIME_______ M
PREPARATION NOTES: SUPV'R NOTE; DO NOT USE V-303 FOR NAPHTHANILS WHEN
CAMPAIGNING DALAMARS YC-39-A, Y0-40-A, YT-839-P, YT-B40-P, YT-8S8-D, AND
YY--868-D.
-------- ... ..
A
.- JEcrJl$ksSuT*--- Lj&e.&--<
.
SEMI-BLEEDING
EO'JIP KENT
| _^N'^ME: NAPHTHANIL RED LIGHT
USE | N-CODE | ACCT
LBS I
| LBS
4-NITRO-2-AMINOTOLUENE FOR S6 r UOBTAIN 3-HYDR0XY-2-NAPTHYLAMIDE FOR Si 8
CLEAN, DRESS, CLOSE 24* CLARIF PRESS -
15 FRAMES
(486 G) WATER INTO V-J^llSL
RUJsL I N HYDROCHLORIC ACID FROM V-324 A
M_,,___ J_______ ______________%
I DUMP IN FROM SI
UQL
ss-2-AM I NOTOLUENE
i 504-C I I 150-C |
28-P I 126 504-c 4^-am
i <57/
i mmm
___STIR 15 MIN TO WET '
__________
_______ I
'J TO
<1020 G) AT 40-45 DEG F
3X330 | 57-A I
SIPHON IN SODIUM NITRITE IN 7-10 MIN
M %______________ Jk.J*
fe#5L_ l , 725-A I
STIR 5 MIN & RECORD: CR_5E-_( + ) / KI_*qpL_< + >
I
I
95
NOTE: (1 ) ' IF CR-, KI- ADD 20* "AS IS'
II
INCREMENTS HYDROCHLORIC ACID ASSUME 32% ______ I
28-D I______
RECORD: CR______< + ) KI__,,_____(+) I <2) IF CR+, KI- ADD 10* "AS IS" INCREMENTS
II
I SODIUM NITRITE
ASSUME 33% |
725-A I_____
^RECORD: CR_J____ ( + ) KIJ( + )
'I
I
1-TTs TIR 10 MIN AT 40-45*F MAINTAINING +CR, +KI|
I FOR SI3 RECORD: TIME START ______ *
|
JUS? 181982 i
MISC |1
SLURRY DICALITE FILTER AID IN 40 GAL WATER I
3' . b a I, IN DRUM & PRECOAT CLARIF PRESS
I
5 1 777-A | 11
5
DV 11sjPTjmriSi 1 STIR COMPLETE DUMP1IN ACTIVATED
15 1 . 113-B | 15
I ^rXARBON
11
1<J^DUMP IN DICALlTE FILTER AID
10 1 777-A | 10
H5H STIR 30 MIN AT 40-45 DEG F
ASSUME 33% ___ 1 725-A )____
| | MAINTAINING +KI FOR S23.
____1 57-A |___ _
I I RECORD:START, ___ J___KI_.___ < + >
11
7^N 13" (177G) WATER INTO-V-SS^i
11
5
|1>-TSLURRY TRISULPHOIL SOAP D IN 25G WATER & 1
1
! I MWJR IN
I
I 1 a^r&UMP IN 3-HYDR0XY-2-NAPTHYLAMIDE FROM S2 & I
16
||
39-A 1Ij 16
i i STIR 30 MIN OR LONGER TO WET. I i RECORD,:
LOT
| I
Lhc.\
150-C J 370
I I * csyUy
--4?
Mil
N38984
DUP050047518
i USE |1 N-CODE I Acer
! J PAGE 2 QF^jS^ CG 40 CODE RT-531-D <N> 1 LBS 11
1 LBS
l \s^f^m^&'hmm* w a t er in t o v-302
'C'rM
!2*TFWR in s o d iu m h y d r o x id e
a s s u me 5ox
1 & *
SIPHON IN ACETIC ACID & STIR 3 MIN____
ISTfLl1
I ' j^-
m__/_______ ,4.fJ:_____% I
I
!22n RECORD PHj&A_(6.7-7.5) IF NECESSARY ADJ TO 11I * 1ij
I I 6.7-7*5. / -
ACETIC ACID ASSUME '
___ | I
RECORD PNH_',,/ SODIUM HYDROXIDE ASSUME 5 l-tftf--1
7-D
30-D
30-D 7-D
fm
\ | ise:
TURN ON V-j JKJL AGITATOR i, ADD ICE, THEN IT OFF AGITATOR
I2X330 !1
PUMP DV THRU CLARIF PRESS INTO DV USED IN
S 23* MAINTAINING TEMP AT 40~45*F>*> RECORD;
CT^T:MjwUr
TOTAL MlN_JM___
TE: Du NOT USE V-303 - TOO SMALL
WHEN S23A CLARIF COMPLETE WASH DV <S4>
LINES PUMP & PRESS FOR 20 MIN OR TO A -CR
TEST ON A SAMPLE OF TOTAL PRESS EFFLUENT
! I WyjfCHEVER COMES FIRST. COLLECT WASHINGS. IN
J(*&i <S23) RECORD: STARTif!OlCR__'l(-OR+)
25 |WHp^S24 IS COMPLETE TEST DV<S23) ASSUME 33%
RECORD: KI_^T_< + ) TEMP__<40-45* F)
WEIGH SULFAMIC ACID IN RUBBER BUCKET AND
ff IN AND STIR 5 MIN*
10
r e c o r d : Ki^rrr--* mu s t b e - 6 if n e c e s s a r y To -KL WITH SULFAMIC ACID
ADJ TO
<1925 G) AT 40-45 DEG F
TxiSo"
57-A 1 Jkk<&)
725-A 57-A
395-D
395-D 57-A
10-
<3900 G> WATER INTO V-S- /<% |3|XT INSTALL TEMP CHART S. SET AGITATOR AT 16 RPM
#0FI WHEN SI 8 STIR COMPLETE, POUR IN SODIUM
I I^HfDROXIDE IN 3-4 MIN.
ASSUME 50%
HEAT TO 128-132 DEG F AFAP 4. STIR 5 MIN TO
I I DISSOLVE* STOP AGITATOR.
----------- --------------- -----------------------~~-----------135 | IMMEDIATELY RUN V**30 AFAP INTO CV*. NO
I | AGITATION IN CV. RECORD: START^^O. I TOTAL MIN ___3Z___ _ la^rTpoyR in a c e t ic a c id & s t ir 5 MII^jr| %
!j H*^RECORD : PHJllQ,, < 1 SrS^TOT""' ASSUME 50%
1
I ! IF NECESSARY ADJ TO PH 10.5-11.0
! LfiECORD: PH__________
ASSUME 70%
I35*XRUN IN V-302 AFAP
|S<T>trNP IN BARIUM SULFATE
I3SK] HEAT TO 78-82 DEG F AND RECORD: 1 Lh T___ie.tr._DEG F AND REC__XX-r__DEG F
ISrnWHEN S28 COMPLETE, COUPLE DV UNDERSURFACE I | 1^5-70 MIN. M&INTAIN CV AT 78-82J5EG F
I ^RECORD: START.__7WL^- TOTAL MIN Jz.CL..,,.
!.1 4|I mSiT*IR1a V5 1M14>IPN*,, DISCONNECT TRANSFER LINE AT CV I i & RC80f<D: 1DIAZO.rrtf--. I <:imu s t b e +) PH_*eLfS_<4.2-4.6)
L4T | IF NECESSARY STIR TO - DIAZO RECORD:
I, START.____________TOTAL MIN
I RECORD: DIAZO _________ MUST BE -
) . BASE ___ *_____MUST BE +
1 PH _________(4.2-4.6)
220 |
35
7-0 110
30-D 7-D
30-D
65-A
150 35
DUP050047519
tOMTYP JOB NAME : 40RT531DMN
PAGE 03
DATE PRINTED :MM/lWYy
E*GU^p"'~ MENT
! I USE | N-CQDE J PAGE 3 OF 3 CG 40 CODE RT-531-D <N) | LBS I
.MI SC 11
^ADD 30G WATER AT 130-140* TO DRUM FROM HOT I I WATER MIXER ADD BLANCOL N 6STIR FOR S43 |
30 f 567-B j
ac c t
LBS
30
12 /Oj
UR IN N-567-B SOLUTION FROM S42 HEAT TO 194-196 DEG.F IN 55-60 MIN AND ' RECORD: HT,,L$J^___DEG F AND REC_M_6_DE& F
EN S44 HEATING COMPLETE, RUN IN ALUMINUM SULFATE SOLUTION THRU BADGER METER. NOTE:
fiS'E IN LINE AFTER N-115-D SOL'N RUJLIN. 30 MIN AT 194-196 DEG F t I 3
Fl o o d t o & <79200 a n d s t o p a g it a t o r
VAT I V-303|V-315!V-3171V-322IV-323 S4 (4860 | 20' | 14* | 14* | 14* | 14* SO (10200 1 43*1 30* I 30" I 30" 1 30*
I 20
1 5-D
60
START
FIN OPTR _____m______ -
/
DUP050047520
DUP050047521