Document KRrXbJz1VQ11q4bNw807nqw6Q
Nelson Mullins . '
Nelson Mullins Riley & Scarborough LLP
Attorneys and Counselors at Law 151 Meeting Street / Sixth Floor / Charleston, South Carolina 29401-2239 Tel: 843.853.5200 Fax:843-722.8700 www.neIsonmulIiits.com
.
August 11, 2004
Michael T. Cole 843.720.4325 Fax: 843.720.4355 mike.cole@nelsonnmlltns.cora
Randall Bono, Esquire The Simmons Firm 301 Evans Avenue Suite 300 P:0. Box 559 Wood River, IL 62095
Re: Durez Division of Occidental Chemical Our File No. 04716/01604
Dear Randy:
Pursuant to your request, I have enclosed documents dealing with molding compounds produced byBlenco and Rogers.
MTC.ras Enclosures
SC-EEI-0750
Atlanta Charleston Charlotte Columbia Greenville Myrtle Beach Raleigh Winston-Salem Washington, DC
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MOLDING COMPOUND REPORT
.
Pioduo^gy-J-^ ... / ^
/ /Us+p)
Color
________ f6m3!&*+*'*4liSv
1 From
-A/*/*/+/*' f
dfe *SQ>
Dotegec'd S&Ss'tr/Z?
CompeteswithDurez
AppBcoHon /zie~ -3 +**S *
t"*!
/*y. ^2-
Cmlomef'tCemmenb y^VT ~
jTrre:/.
&e ffe' *r`"
^ / cdr /ge S ft-
Bleeding ( )
Non-Bleeding ()
^_____ ____________________________________ _
Comments After Teat /V~ SS% y>
r/>r / /Cf> C
<A//r /> /iV/j'f a.
Pj? t?. /rtufyS"^
/^Z5y?
?* . ffc-ferre .
/<>
i- /f/t. /g/<ygtf/'
e
//L <r ^ .g /i/> /^e </ r'ef/Ptrc `w-f <.
/>^<j ^1rt^?e.+~
pdjpez- ??Z'7 / s-rcr^ -n't- &pt/st'~/e*rf` y*
/? S'S'Z,
___ ______________ ._________________________FOR INTRA-COMPANY USE ONIY DUREZfOKM 1*13.
COMPRESSION MOLDING: PROPERTIES
SCup'Mobilily
"<* 9
.. '3/ -- f'** SCupcure.ot__________
Flexure-
____ .... Uvbor
Impod/inch _________ .in::bcr
:
Tensile:... Hot. Deflection
.
<
.*
M. Gravity Shrinkage-
^ -7a**
Coverage
ft-Cup:
-Rf Preheat
Gosefime .
Cure
Timer)
Gloss &-Cup Remark*______________ .
POWDER PROPERTIES
^//g- g
o/,3 6
ApD. Density
7^./
w'/ 9- 6 'ao/ g. 3
funnel Flow
/ 9% * SO *
Preforming
7.3SV
. 77V
Screen .Test On
M _ ______ %.
9227
.
M_
?S-f/3e>r*r)
M
X?*2,
M%
-<3c?/7
M %
M%
. sec sec. '
M .% M M%
M%
Total
Cop cute I80C.30 mm Torque_________________________________________________________ Cop. App.
PLUNGER AVOIDING PROPERTIESMold Tempeiolure Aux. Rom Pres. lmlrO .
Flexure (____in bor) hnpoct/iru (____in. bar)
Gale ` Vent
Shrinkage COMMENTS ON MOLDING
Cure (___ __ Jn. bor)
wr r.ffw?.gry7rf
ELECTRICAL TESTS
Dielectric Strength (Compression) DielectricStrength(Plunger) VohimeiReststtvity
S/T . <?6.. %n------------ ----------
v/mil v/nul
s/s. y??.;. r-
s/s................... ..
.v/mrl v/mit
Powersfactor:orta Dielectric Constant ( . .
cycle)
.
Dry(Cond;B) W 24 bn. WeliOOOhrs. Wei 400hrv Wei 1200 ho.
-Arc*Resistance
Method
iMox. Min. Ayg.
.
Remarks
sec. sec set.
...
4 fL\f. / d'eerf > . / tC<rct{ f__.3,.^. ,/r >/?.
. sec sec. see.
. CHEMICAL RESISTANCE TESTS
96 hr. Boil. HlO 96 hr Boil 10% HSOf 96 hr Boil O.S% NaOH 24 hr. Boil Soap
__ A
- iU
Weight
Thklt
Width
Water Absorption (A5TM)
Length
Appearance
%% O/Of % % ' %
%% % . %
%*
Cop Bleeds 4 Solvents
Appeoronce
Alcohol
Phenol
mg.
Comments on Chemical Resistance
Transmission pH NH3
CHEMICAL ANALYSIS TEStS
Aih c?. 57' % -N. /.3Z % TypeResin
.
Tis?-r> t~.*. Furforal_
CoO _______ %- HexoonResin /1 *> .%
n--t1**'
"
Acetone Extract
</jr %
. Color,of liquor
Color olresidue
___________
Coloring ogenl __________
. B-Nophlhol Extract__________ % _____________"
__ ___ _____________________
Filler Conlenl (Microscope) On Acetone Residue--
/^Jl^<e. f-<r
t/a/e^A.
On Molded Surface
Hot Plate Odor at IA5?C Comment on Chemical Analysis
c;^// Ct.
MISCELLANEOUS TESTS
. <e-.c4. Rockwell Hardness
f- 7XZ
.
y - .?/, 2________ Nigrometer_____
________ Heat Dctorlion
flame Resistance: Ignition Timesec.._________________________
Burning:Time
Remarks'
Modulus of Boslicity in Tension___________________ ________________________ _________
_______ sec.
Heat Resistance
'I
Dale
'i }
1
I
?L.
MOLDING. COMPOUND REEORT
Product- pc ^ ^
From
fiii,
Competes with Puree
>7 - ? />/-
Applicotion
Color / W,v
. Form Dore Kec'd -
A i~*~
li_!
_____________ ____________ .________________
__________ ______________ ________Bleeding ) )
Non-Bleeding 1 )
Cwhyner^sComments ^^
,*** ( /V SViKt*____
. -ill?!1
Lt-
( .< > i S __
i^t 'J-ur* -~f~
Jud L o--
L<-->Comments AfterTest
f sr*i
^-ris
_____________________'; ,
J * 7J 7;//C
DU8EZ FORM UM3
FOR INTRA-COMPANY USE ONLY
Cop cure 180PC
30 mm Torque
Cop. App
PLUNGER MOLDING PROPERTIESMold Temperahire
Auk Rom Pres (min 1 M. Gravity Shrinkage
Flexure (__ in. bar) !~p=c.','in.! .. i.v bai! Tensile Cure (in. bor)
COMMENTS ON MOLDING
Gate Vent
.
ELECTRICAL TESTS
Dielectric Strength.(Compress>on) ' dielectric.Strength (Plunger) VglumeResistivity
PowcrFoaorondDielKIric Corclonl (
S/T . ... s/t................... ...........
v/mil
s/s. .. v. . s/s. . ..
. v.rnwl v.-rml
cycle)
Arc-Resistance
<
.f
Dry (Cond. B) Wei 24 hri. Wet lOOhra. Wet .400 hu: j Wei 1200 hn.
Method . Mox. Min. Avg. Remorks
set'- . . .. ' sec. sec. '.\set sec. sec.. '
CHEMICAL RESISTANCE TES1S
Weight
Thick
Widlh
Water Absorption (A5TM) ^
length
Appearance
96 hr. Boil. HK>
%% %%.
96 hr Bal lO%HJSO` 96 hr: Boil 0.5% NoOH
%% %% %l
%% %
24 hr.:Botl Soap
'%
.
Cop Bleeds 4 Solvents
Appeoronce
Alcohol Phenol
mg.
Comments on Chemicol Resistance
Transmission pH
NH3
:3JMt
#
CHEMICAL ANALYSIS TESTS
Ash W oC % N ) \ ^
% Type Resin
CoO
% Hexoontein- V.2.
Furfural
lI. ife. t i '>
V, .. ,-I
AcetoneExtroct.
\.l~ % _____ Color of:liquor- ; n . t ^___________ _________ '
`
C--o--lo--r-o--f-r-e--s-i-d-u--e---- .-.----^- --.-----------
B-Nophfhol Exfroct V/t I-y
%
Cdorirtgogent
FillerContent (Microscope) On Acetone* Residue
vc*f
On Molded Surface
G-m.
ft
Hot Plate Odor ofl65aC Comments on Chemical Analysis
MISCEUANEOUS.TESTS
t'f r
JLRockwell Hardness
sj
Home Resistance: Ignition Time
Ntgrometer
Remarks
Modulus of Elasticity in Tension
Heat Distortion Burning Time
Heat Resistance
, 'l
^
'
.
'`
i
I
1
vvjeg *#$0
i
ote 2- /</- (, <S
Competevwith Durez Appltcofion'
Customer* Comments
Bleeding (4^-^ NonBfeeding Q
Comments After Test
_____ _____________________________
xyi- .."Xe^td,
~T^>
A-i-
%sC*3
.^TT'-V^v- /t^-4
')^ /Lht*-S
l*~cX+S* .
O&C? <y^_c, JZL>n y>Lr^
^ ^ 7 j_ *_________________________ _________________ __
DUSEZ fORM UM3
FOR INTRA-COMPANY US ONLY
* 'l i
Cop cura180C
30 mm Torque
Cap. App.
PLUNGER MOLDING PROPERTIES Preheat Amc. Bam Pres. (min.) M. Gravity Shrinkage
COMMENIS ON MOLDING
Vf 4*1
Mold'Temperolure Flexure (_ in. bar) Impoct/in. (. ___ in. bar) Tamila Cure {______ jo. bar)
Gala Van*
/r'4 Tip
/s- 'A.'/'< /O/ie-e
/ ' 3. O/X^-K.
__ .S~ 5~~/Pef____
- /
.
j !
aECTRtCAlTESTS
Dielectric S/rength(Compeuion) OtelectricStrangth(Plunger) Volume Resistivity
.JifiXXu___
S/T--
--__ v/rwl
S/T,.
.v/mll
S/S-_ / ~2-^> __ .v/mil
SA-------
v/mil
Power Factor and Dielectric Coretont { . cycle)
.
Dry (pond. B) Wet 24 hre.Wet lOOhra. Wet 400 hn. Wetl200 hrs.
1
'
Afc'Rojiitonce
'
Method Von.
lf&~t-
Ifat- sec.
. C.
'Min.
/>" 1--see.
Ce
Ayg; .
set
sec
Rtmorks
CHEMICAL RESISTANCE TESTS
94 hr. Bolt. H3 94 ht. Boil 10% WSO 94 hr. Boil 0.5% NoOH 24 hr. BoilSoop
Weight
Thick
Width
Water Absorption (ASTM) ^ 0. 2*-/ s
length
Appearance
% .%
.% '` % *%
* %
.*
*
%
%
*
Cop Bleeds 4 Solvents
Appearance
Alcohol
Phenol
_____________ mg.
Comments on Chemical Resistance
Transmission '
pH ,
NH3
*1
CHEMICALANALYSIS TESTS
/<9 7Ash % Kl.'l'l' N %
Type Resin
CaO
%
HexaonResin/*/ 0%
Acetone Extract
% UO.H f
Color of.liquor
CoJorof residue
Colorinqogent
B-Naphthol'Extract
RltefiCont&nt {Microscope) On Acetone Residue
On MoidedSurfoce
Hot Plate Odor at I65'C Commentson Chemical Analysis
MISCELLANEOUS TE5I5
Rockwell Hardness
Nlgromcter
Flame Resistance: Ignition Time__________sec
Remarks
Modulus of..Elasticity in Tension
(La c^/
Furfural
Heat Distortion Burning Time
-A:
l.r'