Document KRa5bejLa87BwqbvrXJXRw7e0
c.v. io s ^io I)
OG 46
CODE YC-5-A
PKG
OCT 26 1982
( DATE )
L2H53
(LOT NUMBER)
EST. WT. 2131 * 'LBS. Ati
PREPARATION NOTES: _r
D.V.f 30^(315)317,322,232
PROCESSES
.
(E)YC-5-A
()
<) <)
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TYPED BY: JMH
STANDARD HRS.___________
APPROVED BY EWK 10/23/81
TIME
BLEEDING
EQUIP II MENT | | NAME: "DALAMAR' YELLOW
03 PAGES
PREP 1
I 1 I OBTAIN FOR S6 (5-NITR0-2-AMINQ ANISOLE) I 2 | OBTAIN FOR S23 (ACETOACET ORTHO ANISIDIDE) I 3 ! CLEAN, DRESS, CLOSE 24* CLARIF PRESS - 15 I I FRAMES.
DV \^r\ RUN 17* (595 G) WATER INTO V-_. o EIGH IN FROM V-324 (HYDROCHLORIC ACID)
m_,,.J2l ______
DUMP & RINSE IN DRUMS FROM SI (5-NITR0-2-
AMINOANISOLE)
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USE | N-CODE | ACCT
LBS I
I LBS
I557-C |
46-C |
1,
I Ht&k'
,1. I 28-D ! 441
I I
#&J\
557-C | I
I
938
I 3JJL__I
I
I
I I. I
_______ I.
IR 1' MIN OR LONGER TO WET
\
0 DV TO 37' <1295 G). AT 28-32* F (ICE)
SIPHON IN IN 12-15 MIN (SODIUM NITRITE)
M___
STIR 38 MIN AT 28~32F MAIMTAjl^G -fCRj +KI
FOR SI 3. RECORD: TIME START..
CR,,__J^, KINOTE:
(1)
IF CR-, KI- ADD 204 (HYDROCHLORIC ACID)
'lJSA*S>SUINMCERE3M2%ENTS
RECORD: CR____ :___ ( + >;
_______ (+)
(2) IF CP+, KI- ADD 2 fi;s> 3IS' INCREMENTS
So d iu m n it r it e )
---------
RD: CR,,:.( + >, KI_...
f -VL'i 10X3301 57-A
I1 I 725-A }' 398 I4
0CT1291982 !
______ I 28-D V______
______ I 725-A I___ I1
RY IN 50/GAL WATER IN DRUM 4, PRECOAT RIF PRESS WITH (DIC^LITE FILTER AID) LyRRY IN C GAL WATER IN-DRUM FOR S 20
SULPHOIL SOAP D)"
"STIR COMPLETE, DUMP IN (BS'CY&LITE Et&fjID) * jl' (ACTIVATED CARBON) '
Ii 5 | 777-A | 5
82 I 39-A l 82
I` I
-I. 10^ | 777-A I 1
. ' !
I
15 1 1 M3-B I 1
. CfltfTYP JOB
46YC005AME PAGE 02
DATE PRINTED: 3/22/JS2 *.
fQUIP I Se n t ., i
1 J PAGE 02 OF 03 CG 46 CODE YC-5-A
1 USE | N-CGDE'1 ACCT
(E> 1 LBS 1
LBS
tiv. 'i
G +CR: i
i
4 1 i1 +KI FOR S21. RECORD: TIME START_iI
11
CONT. | i CR, KI* NOTE:
1.... 1 57-A
i1i (HYDROCHLORIC ACID)
!1 ASSUME 32% 1....... I 28-D
i RECORD: CR< + > KI( + )
1
-* | 1I (2) IF CR + , KI- ADD 20# * AS IS* INCREMENTS !
1 i
I (SODIUM NITRITE)
ASSUME 33%
725-A
i CORD: CR( + ) KI________________ __( + >
1
(
CV | f6 |I . RUN 10* (970 G) WATER `i NTO~V=]L^III"&
1|.
51
.INSTALL TEMP CHART
-^
POUR IN (SODIUM HYDROXIDE) M_/J?1_,
.
\SlL\
7-D
TO 37* (3611 G) AT 66~70*F (ICE)
13X330 1 57-A
v WttteBSE STACK DAMPER
11
IJMJHPOUR IN N-39-A SLURRY FROM SI 2 6 STIR FOR
%
S23
11.
DV 6
WHEN 1-5 STIR COMPLETE, TEST DY. ^RECORD: 1 CR_Ttr_< + ) j KI_r__.< + ), TEMF`_^tHL(28-32#F) 1
I l
57-A
NOTE: (1) IF CR-, KI- ADD 20# *AS IS*
1i
INCREMENTS (HYDROCHLORIC ACID) ASSUME 32% :
i 28-D
RECORD: CR( + ); KI( + >
(2) IF CR+, KI- ADD 20# 'AS IS* INCREMENTS l
l
(SODIUM NITRITE)
ASSUME 33% i
i 725-A
i\L*RECORD: CR_
KI J;_____( + )
il
iiam^ruRN o n v-J&Jat a g it a t o r , c h o p & a d d ic e
1 2X3301 57-A
I IIMEN SHUT OFF AGITATOR
11
123STPUMP' DV THRU CLARIF PRESS INTO DV
11
S i MAINTAINING TEMP AT 25i:32 DEG F
iI
RECORD: TIME START^Sl 40T__TCTAL MIN_4L !
1
|. ! 1
| 447 |
I | i I
CV DUMP INTO CV FROM S2 (ACETOACET ORTHO
7 ANISIDIDE) NOTE: BREAK UP LUMPS
|miL ~\m~- -Jsa_
46-C 1 1240
____ OtJi-p-- _____ At....
t.__ i S "i--;
fTTR 10 MIN TO DISSOLVE
ii
i 38*7U8fEN STACK DAMPER
I2^#rTON**IN UNDERSURFACE IN 20-25 MIN.- T ACETIC ACID) M______ % /_> ..y&L&LgS>,,-.X
\mJ
*27-J-TIR 5 MIN & RECORD: PHL^3^!.(5.8-6*3) i
i
|2^T IF NECESSARY, ADJ TO PH 575-6.3 6 RECORD
r I PH____ (5.3-6.3) SODIUM HYDROXIDE ASSUME 50% i______ i
||
ACETIC ACID
ASSUME 70% i
i
.1 ii
3r DV ia^i WHEN S22 CLARIF COMPLETE, WASH DV (S4)
8 ! | LINES, PUMP 6 PRESS FOR 20 MIN OR TO A -CR
l I } TEST ON A SAMPLE OF TOTAL PRESS EFFLUENT
\
J { WHICHEVER COMES FIRST. C0LLECJ4ASHINGS IN I I DV.(S22). RECORD: TIME START_il_Lt_--
\ i J^i-lrr_-(~ 0R+)
.
N \m\ STIR 5 MIN 6 RECORD: TEMP_(28-32#F) &
| >TP. NECESSARY ADJ TO 28-32*F. RECORD______ *F
. !T| RECORD: V0L_4k___,,'
J1
30-D | 685 7-D i
30-D |
57-A
DUP050061373
;COMTYfrJQB NAME a 46YC005AME PAGE G3
DATE PRINTED: 3/22/82
egy-iP i MENT 1
PAGE 3 OF 03 CG 46 CODE YC-5-A
(E>
/
IZ9r \ WHN S 31 COMPLETE, ADJ CV TO 44 (4268 G>
I JxtfT80 - 84 DEG F ! 3T| CHE^^AfCURACY: HT
ti
DEG F & RECORDER
USE LBS
N-CPDE ACCT LBS
IMMEDIATELY RUN IN DV THRU UNDERSURFACE
| DISTRIBUTOR IN 60-65 MIN. MAINTAIN CV AT
80-84 DEG F
.
iECORD: TIME START_/C_l7, TOTAL MIN
>TIR 10 MIN. DISCONNECT TRANSFER LINE AT
1"* l^C-V IMMEDIATELY
.
I36TT RECORD: DIAZO
BASE
fI
PH .JpjJlC- 4.3-4.7)
(+)
i NOTE: (i) IF DIAZO + , BASE - & PH BELOW
4.3, ADJ TO PH 4.3-4.7 RECORD: PH_.JC.__
(SODIUM HYDROXIDE)
' ASSUME 50%
I I (2) IF DIAZO +; BASE - & F'H ABOVE 4.3 ADD 8* 100% N-7-D TO 55 G*L DRUM ' ASSUME 50%
ADJ WITH WATER TO + OR - 25 GAL. ADD 20*
1 i 100% N-46-C (ACETOACET ORTHO ANISIDINE) &
STIR TO DISSOLVE. POUR IN CV 6 STIR 10 MIN
I i J<^3>) REPEAT ABOVE AS NECESSARY TO - DIAZO,
I + ^BASE. 1-27 >*HTEeAa t t o i ?o -i ?4 d e g f in 58-62 min .
\'yr \ s t ir 3 min a t ,19^ 194 DEG F RECORD:
I IJWffE START___
t3>^rFL00D TO 94 (9174G) *< STOP AGITATOR
.Ms*
FIN--Z.f3
OPTR
7-D 7-D 46-C
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