Document KJz0Je7zBZOVpREVGDgNXrg5w

To: From: Sent: Subject: Hupp, Sydney[hupp.sydney@epa.gov] Chris Tytanic Fri 5/12/2017 2:56:52 PM Fwd: Response for Administrator Scott Pruitt Sydney - below is the completed form as requested. Please let me know if either May 23rd or 24th works for Scott and Ryan. Thanks for your help! Chris --------- Forwarded message---------From: Anthony Feezel ___ ^mail/E^ 6____________ Date: Thu, May 11, 2017 at 6:07 Pm' Subject: Response for Administrator Scott Pruitt To: Chris Tytanic^ Personal Email/Ex. 6 i i_______________________________________ J External Meeting Request Form for Administrator E. Scott Pruitt U.S. Environmental Protection Agency To request the Administrator to attend and/or speak at your event, please complete and submit the following form. Today's Date: 5/11/17 Meeting Date: May 23rd or May 24th, 2017 Meeting Time: Time is flexible Requested Location (if offsite, please list address, parking instructions, etc.): Administrator Pruitt's office Requestor: Anthony Feezel, President of Reliable One Resources, Inc. (hereafter 'ROR') Purpose of the Meeting: To assist ROR with obtaining contracts to clean up aquifers and discharged contaminated mine water on government properties. Background on the Meeting: ROR has been developing its water treatment technology to remediate contaminated groundwater, clean up acid mine drainage water, and produced and flowback water 17cv1906 Sierra Club v. EPA ED_001523B_00005615-00001 from exploration & production (E & P) operations. Role of the Administrator: To provide ROR with the appropriate contacts and or introductions to the personnel responsible for awarding contracts to do business with the Federal Government. Attendees: Anthony Feezel, C.C. Cravey, Chris Tytanic & Sharissa Ward Point of Contact: Chris Tytanic (405) 406-1394 Anthony Feezel P. O. Box 1371 Ada, OK 74821 580.235.3557phone 17cv1906 Sierra Club v. EPA ED_001523B_00005615-00002 TCEQ Public Water System ID: V..' it 'if "toi.K - MICROBIAL MONITORING FORM ENVIRODYNE LABORATORIES, INC 11011 BROOKLET, STE 230 HOUSTON. TX 77099 (281)5687880 NELAP CerUfeate # T1O4704265 Public Water System Rame: .. .. ..: TCEQUblD; TX-288 Test results meet all requirements of NELAC unless stated other*iso County: Name: Address: City: State: NV NA Reliable One Resources, Inc Sample Iced? Received No By: 297 Kingsbury Grade Suite 1038 It no,WW** wtrwolpt? Tested By: .. Lake Tahoe ... .. Reported Zip: 8 9 47 4 9 ** 4 4 7 0 By; Date / Time Received: J Date I Time Tested: Date/Tlme Reported: [Phone #: I 'S -, it, PubiicTf 303-350-7209 Be Fax#: I X Operator..| 5 - Groundwater Surface Water Report Approval Slgnatore/llUe: ....77 . Approvino Technical lb/l^ Director: D Other Groundwater with Surface Water Influence Free' Use Specific Address/Location Date Time [< gggd j IJ I not she * ittt Raw Wells Use Source ID for Well Sampled Er I 8 g G1234567A | 5 | " F h q" I muuiiiTfoiuo' - S_ ? 't ( lb I oa al Rcpcm 1 ar n..,TM. ,, mg/L 1 7 Rejection Criteria Presenti - Absent Datoof Approval -Escati- .. Present Absent Raw Ground A Treated Ground TCEQ Form' 10525 6/2009 s y ;y <9 n ri n s a______ pm CJ o a o uo alwm o o w pr- o o am pm O am pm D O o o H pm O" O. 31Excessive li S uiwh. 1<-o olii Ari', .1 ml imli.it'd v.,mni 30 lime, of ccie< tor Quantity insuftrarnt for .nnalyto (iOlimi lequimll 4, Hcm.S.r/tiimd.i/rr.-.m: | Ei' D ny foie, 9 ` j i Ki lS > i n o O Cl n ci n o Q n o a n nn n n n I 1 [~l D Cl P] Q n o 5> f omi hK'i.np. !,, 'Mie "w; i-ry >> ir.r r,.-:: di 17cv1906 Sierra Club v. EPA ED_001523B_00005616-00001 03 May 2016 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reliable One Resources Inc R McElroy 707 W. Corsicanna St Athens, TX 75751 Reliable One- Water Enclosed are the results of analyses for samples received by the laboratory on 29-Apr-16 14:08. The analytical data provided relates only to the samples as received in this laboratory report. ELI certifies that all results are NELAP compliant and performed in accordance with the referenced method except as noted in the Case Narrative or as noted with a qualifier. Any reproductions of this laboratory report should be in full and only with the written authorization from the client. The total number of pages in this report is 10 Thank you for selecting ELI for your analytical needs. If you have any questions regarding this report, please contact us. Sincerely, 5 r'" Itzel Dominguez For Monica Smith Project Manager Certificate No: TX104704265 17cv1906 Sierra Club v. EPA Page 1 of 10 ED_001523B_00005617-00001 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3258 ANALYTICAL REPORT FOR SAMPLES Sample ID Laboratory ID Raw Ground 16D3258-01 L-Analyzed by NELAP accredited lab T104704231 Matrix Water Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:46 Date Sampled 28-Apr-16 00:00 Date Received 29-Apr-16 14:08 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 2 of 10 ED_001523B_00005617-00002 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3258 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:46 Analyte Wet Chemistry Alkalinity (m) as CaCO3 Alkalinity (p) as CaCO3 Total Alkalinity as CaCO3 Ammonia-N (NH3-N) Ammonium (NH4) Chloride Conductivity Iron (Ferrous) Iron +3(Ferric) Nitrate Nitrate-N Nitrite Nitrite-N Sulfate Total Organic Carbon (TOC) Total Metals bv ICP Cadmium Calcium Iron Magnesium Sodium Result Raw Ground 16D3258-01 (Water) Sampled: 28-Apr-16 00:00 Reporting Limit Units Dilution Batch Prepared Envirodyne Laboratories, Inc. Analyzed Method Analyst Notes 340 20 mg/L 1 B6D3303 02-May-16 02"May~16 15:30 SM 2320 B KCT <20 20 mg/L 1 B6D3303 02-May-16 02-May-16 15:30 SM 2320 B KCT 340 20 mg/L 1 [CALC] 02-May-16 02"May~16 15:30 [CALC] KCT <0.10 0.10 mg/L 1 B6E0089 02-May-16 02-May-16 14:35 SM 4500-NH3 D JAS <0.13 0.13 mg/L 1 [CALC] 02-May-16 02-May-16 14:35 Calc JAS 140 3.0 mg/L 1 B6E0016 02-May-16 02-May~16 07:35 SM4500-C1 B JMM 1320 10 uS/cm 1 B6E0025 02-May-16 02-May-16 11:00 SM2510B KCT <0.0500 0.0500 mg/L 1 B6E0024 29-Apr-16 29-May-16 18:52 SM 3500 Fe B IZW L, n <0.0500 0.0500 mg/L 1 B6E0238 03-May-16 03-May-16 12:21 Calc JMM 266 0.32 mg/L 1 B6E0198 28-Apr-16 28-Apr-16 08:00 SM 4500-NO3 D JAS 60.1 0.10 mg/L 1 B6D3446 29-Apr-16 29-Apr-16 15:00 SM 4500-NO3 D JAS <0.16 0.16 mg/L 1 B6E0198 28-Apr-16 28-Apr-16 15:25 SM 4500-NO2 B KCT <0.05 0.05 mg/L 1 B6D3448 29-Apr-16 29-Apr-16 15:25 SM 4500-NO2 B KCT 30.0 4.00 mg/L 2 B6E0026 02-May-16 02-May-16 11:30 A STM D516-07 KCT 2.74 1.00 mg/L 1 B6E0091 01-May-16 Ol-May-16 23:17 SM 5310B IZW L <5.0 181 22.3 14.2 73.1 5.0 ug/L 2.00 mg/L 5.0 ug/L 2.00 mg/L 2.0 mg/L 1 B6D3175 28-Apr-16 02-May-16 12:00 EPA 200.7 ACB 1 B6D3180 28-Apr-16 02"May~16 10:27 EPA 200.7 ACB 1 B6D3175 28-Apr-16 02-May-16 12:00 EPA 200.7 ACB 1 B6D3180 28-Apr-16 02-May~16 10:27 EPA 200.7 ACB 1 B6D3180 28-Apr-16 02-May-16 10:27 EPA 200.7 ACB Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 3 of 10 ED_001523B_00005617-00003 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3258 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:46 Analyte Batch B6D3303 - Inorganics Blank (B6D3303-BLK1) Alkalinity (m) as CaCO3 Alkalinity (p) as CaCO3 LCS (B6D3303-BS1) Alkalinity (m) as CaCO3 Alkalinity (p) as CaCO3 Duplicate (B6D3303-DUP1) Alkalinity (m) as CaCO3 Alkalinity (p) as CaCO3 Batch B6D3446 - Inorganics Blank (B6D3446-BLK1) Mitrate-N Blank (B6D3446-BLK4) Nitrate-N LCS (B6D3446-BS1) Nitrate-N Matrix Spike (B6D3446-MS1) Nitrate-N Matrix Spike Dup (B6D3446-MSD1) Nitrate-N Wet Chemistry - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source % REC Level Result %REC Limits RPD RPD Limit Notes Prepared & Analyzed : 02-May-16 <20 20 mg/L <20 20 Prepared & Analyzed : 02-May-16 58 mg/L 50.0 116 80-120 46 50.0 92.0 80-120 Source: 16D2577-01 116 20 mg/L <20 20 Prepared & Analyzed : 02-May-16 118 <20 1.71 20 0 20 <0.10 Prepared & Analyzed : 29-Apr-16 0.10 mg/L <0.10 Prepared & Analyzed : 29-Apr-16 0.10 mg/L Prepared & Analyzed: 29-Apr-16 26.1 mg/L 25.0 104 90-110 Source: 16D2938-01 25.3 0.10 mg/L Prepared & Analyzed: 29-Apr-16 25.0 2.13 92.7 80-120 Source: 16D2938-01 Prepared & Analyzed: 29-Apr-16 25.3 0.10 mg/L 25.0 2.13 92.7 80-120 0.00 20 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 4 of 10 ED_001523B_00005617-00004 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3258 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:46 Analyte Batch B6D3448 - Inorganics Blank (B6D3448-BLK8) Nitrite-N LOS (B6D3448-BS1) Nitrite-N Matrix Spike (B6D3448-MS1) Nitrite-N Matrix Spike Dup (B6D3448-MSD1) Nitrite-N Batch B6E0016 - Inorganics Blank (B6E0016-BLK1) Chloride LCS (B6E0016-BS1) Chloride Matrix Spike (B6E0016-MS1) Chloride Matrix Spike Dup (B6E0016-MSD1) Chloride Batch B6E0025 - Inorganics Blank (B6E0025-BLK1) Conductivity Wet Chemistry - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source % REC Level Result %REC Limits RPD RPD Limit Notes <0.05 Prepared & Analyzed : 29-Apr-16 0.05 mg/L Prepared & Analyzed: 29-Apr-16 0.10 mg/L 0.0997 99.3 80-120 Source: 16D3170-01 0.10 0.05 mg/L Prepared & Analyzed : 29-Apr-16 0.0997 ND 96.3 80-120 Source: 16D3170-01 Prepared & Analyzed : 29-Apr-16 0.09 0.05 mg/L 0.0997 ND 93.3 80-120 3.17 20 Prepared & Analyzed: 02-May-16 <3.0 3.0 mg/L Prepared & Analyzed: 02-May-16 102 mg/L 100 102 80-120 Source: 16D3170-01 82.0 3.0 mg/L Prepared & Analyzed: 02-May-16 20.0 62.0 100 80-120 Source: 16D3170-01 Prepared & Analyzed: 02-May-16 80.0 3.0 mg/L 20.0 62.0 90.0 80-120 2.47 20 Prepared & Analyzed: 02-May-16 <10 10 uS/cm Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 5 of 10 ED_001523B_00005617-00005 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3258 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:46 Analyte Batch B6E0025 - Inorganics Duplicate (B6E0025-DUP1) Conductivity Reference (B6E0025-SRM1) Conductivity Batch B6E0026 - Inorganics Blank (B6E0026-BLK1) Sulfate LCS (B6E0026-BS1) Sulfate Matrix Spike (B6E0026-MS1) Sulfate Matrix Spike Dup (B6E0026-MSD1) Sulfate Batch B6E0089 - Inorganics Blank (B6E0089-BLK1) Ammonia-N (NH3-N) LCS (B6E0089-BS1) Ammonia-N (NH3-N) Wet Chemistry - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source % REC Level Result %REC Limits RPD RPD Limit Notes Source: 16D3261-01 59.8 10 uS/cm Prepared & Analyzed : 02-May-16 59.7 0.167 20 Prepared & Analyzed: 02-May-16 179 uS/cm 180 99.4 0-200 <2.00 Prepared & Analyzed : 02-May-16 2.00 mg/L Prepared & Analyzed : 02-May-16 20.4 mg/L 20.0 102 90-110 Source: 16D3170-01 23.4 2.00 mg/L Prepared & Analyzed : 02-May-16 20.0 1-76 108 80-120 Source: 16D3170-01 Prepared & Analyzed: 02-May-16 25.4 2.00 mg/L 20.0 1.76 118 80-120 8.49 20 <0.10 5.11 Prepared & Analyzed: 02-May-16 0.10 mg/L mg/L Prepared & Analyzed: 02-May-16 5.00 102 90-110 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 6 of 10 ED_001523B_00005617-00006 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3258 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:46 Analyte Batch B6E0089 - Inorganics Matrix Spike (B6E0089-MS1) Ammonia-N (NH3-N) Matrix Spike Dup (B6E0089-MSD1) Ammonia-N (NH3-N) Wet Chemistry - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source % REC Level Result %REC Limits RPD RPD Limit Notes Source: 16D3045-01 4.02 0.10 mg/L Prepared & Analyzed : 02-May-16 4.10 ND 98.0 80-120 Source: 16D3045-01 Prepared & Analyzed : 02-May-16 4.11 0.10 mg/L 4.10 ND 100 80-120 2.21 20 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 7 of 10 ED_001523B_00005617-00007 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3258 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:46 Analyte Batch B6D3175 - Metals - EPA 200.2 Blank (B6D3175-BLK1) ron Cadmium LCS (B6D3175-BS1) Cadmium [ron Matrix Spike (B6D3175-MS1) Cadmium [ron Matrix Spike Dup (B6D3175-MSD1) [ron Cadmium Batch B6D3180 - Metals - EPA 200.2 Blank (B6D3180-BLK1) Calcium Vagnesium Sodium LCS (B6D3180-BS1) Calcium Vagnesium Sodium Total Metals by ICP - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Prepared: 28-Apr-16 Analyzed: 02-May-16 <5.0 5.0 ug/L <5.0 5.0 Prepared: 28-Apr-l 6 Analyzed: 02-May-16 240 ug/L 250 97.9 85-115 248 250 99.4 85-115 Source: 16D2848-01 460 5.0 ug/L 515 5.0 Prepared: 28-Apr-16 Analyzed: 02-May-16 500 ND 92.0 80-120 500 3.21 102 80-120 Source: 16D2848-01 Prepared: 28-Apr-16 Analyzed: 02-May-16 506 5.0 ug/L 500 3.21 101 80-120 1.59 20 450 5.0 500 ND 90.8 80-120 1.32 20 <2.00 <2.00 <2.0 19.7 19.6 19.0 Prepared: 28-Apr-16 Analyzed: 02-May-16 2.00 mg/L 2.00 2.0 mg/L Prepared: 28-Apr-16 Analyzed: 02-May-16 20.0 98.7 85-115 20.0 98.1 85-115 20.0 94.9 85-115 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 8 of 10 ED_001523B_00005617-00008 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3258 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:46 Analyte Batch B6D3180 - Metals - EPA 200.2 Matrix Spike (B6D3180-MS1) Calcium Magnesium Sodium Matrix Spike Dup (B6D3180-MSD1) Magnesium Sodium Calcium Total Metals by ICP - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source % REC Level Result %REC Limits RPD RPD Limit Notes Source: 16D2848-01 94.2 2.00 mg/L 30.9 2.00 156 2.0 Prepared: 28-Apr-l 6 Analyzed: 02-May-16 20.0 72.4 109 80-120 20.0 10.3 103 80-120 20.0 132 121 80-120 Source: 16D2848-01 Prepared: 28-Apr-l 6 Analyzed: 02-May-16 29.2 2.00 mg/L 20.0 10.3 94.2 80-120 5.67 20 154 2.0 20.0 132 111 80-120 1.32 20 92.5 2.00 20.0 72.4 101 80-120 1.79 20 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 9 of 10 ED_001523B_00005617-00009 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3258 Notes and Definitions n L DET ND NR dry RPD CLT Not accredited for this analyte Analyzed by third party laboratory Analyte DETECTED Analyte NOT DETECTED at or above the reporting limit Not Reported Sample results reported on a dry weight basis Relative Percent Difference Client Representative Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:46 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 10 of 10 ED_001523B_00005617-00010 KNL ZJXA ENVIRONMENTAI. TESTING DOH Certification #E84025 Cert.# T104704527-14-1 Report Date-. May 10, 2 016 Envirodyne Laboratories, Inc. 11011 Brooklet, Ste 230 Houston, TX 77099-3543 Field Custody: Client Client/Field ID: Reliable One Resources Sample Collection:4-28-16/1700 Lab Custody Date: 5-3-16/1035 Sample description : Water CERTIFICATE OF ANALYSIS Parameter Gross Alpha Units l/fijljjll Results Analysis Date 5-10-16/1124 Detection Method Limit EPA 900.0 lllllllslllill IBBJl +1 --, Gross Beta 5-4-16/1658 EPA 900.0 'SSIglS Radium-226 5-5-16/1610 EPA 903.0 Radium-228 :fSc^ 5-9-16/1159 EPA Ra-05 Uranium pCi/1 5-10-16/0921 EPA 908.0 lllilllliligllllll Uranium Alpha St 'i: Th-230 Beth Stdud.nd: Cm 1^7 C^M^ llllOOilBIIIIIllllllllO c^ James W. Hayes Laboratory Manager Test results meet all requirements of the NELAC standards. Statement of estimated uncertainty available upon request. Test results refer only to sample(s) listed. KNi r id'IPOMi IMA! I A.;.AA LL | DO? ; y nd H H u Al : a A V f 111 ! I A td'A r I ( ADA 813.229 28/9 | K NL EN VIRONME N i A L .COM 17cv1906 Sierra Club v. EPA ED_001523B_00005617-00011 17cv1906 Sierra Club v. EPA Comp Temp. Analysis Time Envirodyne Laboratories, Inc. 11011 Brooklet, Ste. 230 E A138697 TCBQ Certification # T104704265 Houston, Texas 77099-3543 Phone (281)568-7880 - Fax (281)568-8004 Page Of Name: Address: City: Reliable One Resources, Inc 297 Kingsbury Grade Suite 1038 Lake Tahoe. NV 89449-4470 Analysis Request and Chain of Custody Record Ce I -303-3 Office-775- Project No. No. ........ Field Sample No./ Indentification Raw Ground Treated Ground 1 Date & Tim .7 ? Client/Project . . _ !- I Sample Container Sample Type ( Liquid, (Siz/Matt Sludge, etc) Preservative ANALYSIS REQUESTED 1 Gal/Cubie 1 Gal/Cubie Liquid Liquid lce,HNO3 Jce,HNO3 Gross Alpha/Beta,Radium 226-228, Uraniu Gross Alpha/Beta,Radium 226-228, Uraniu X d iSt JJIIf fV: ... (OB liiilBil BSWiB c 11 At ' cy: ~ J B I B - .............................. . .. ---- .lu iWssSygO ...... ....... ......................... X. J 5s . ........................... ................. - - / - ED_001523B 00005617-00012 Samplers: (Signature) Affiliation Remarks: fl"'-' I *. Relinquished by: (Signature) j.J?..,.. d... b . Relinquished by: fl (Signature) Relinquished by: - . (Signature) ! J;.; .. . FLOW:_________ i Meter Reading:_______) - r: CI Residual:_______ Mn Correction:_______ Cl2 Corrected............................ : ............... ....... . Date: Time: -, Date: ) : Time: Date: Time: Received by: (Signature) Received by: ( Signature) d 1 : Arrival Temp. -v x fl Site Representative: , B Date- < .. . Seal Intact? ' ' . Time: - - Date: Time: Seal Intact? : Date^fl^y^ Seal Intact? Time:.: Time: Comp r ornp. Analysis Time TCEQ Certification # T104704265 Envirodyne Laboratories, Inc. 11011 Brooklet, Sie. 230 Houston, Texas 77099-3543 Phone (281)568-7880 - Fax (2.81)568-8004 Page E Al 3 7624 Name: Address: Reliable One Resources. Inc 297 Kingsbury Grade Suite 1038 Analysis Request and Chain of Custody Record City: Lake Tahoe, NV 89449-4470 . Contact: Philip McElroy Project No. Phone' (Client/Proiect Ce I - 303-3 Fax: Office - 775- No. IJJIIIJI Field Sample No./ Indentification Raw Ground Raw Ground Raw Ground Raw Ground Raw Ground Raw Ground 1 Sample Container Sample Type ( Liquid. ( Size/Mal'O Sludge, etc) Preservative ANALYSIS REQUESTED Jo Q 1 Gal/Cubie Liquid Ice, HNO3 Gross Alpha/Beta,Radium 226-228, -10 Uraniu g 500 ml/P Liquid : fee, : H2SO4 TOC, AMMONIUM j Jir M0ml/p Liquid Ice. HNO3 Na, Ca, Mg, Fe .0,. Ice Chloride,Aik,SO4,NO3-N,NO2-N,Cond A nc-c7 i.liY 250 ml/P : ' Liquid Ice. HNO3 Liquid 1 y a i 1 J c Ice, HCI --. '3^*^ > Ferrous Iron :SWaS;5ii?:^ 7 : L Remarks: 17cv1906 Sierra Club v. EPA Relinquished byi 7 HliBiiiflk Relinquished by: ' ( Signature) --c FLOW:.. Meter R ?adir g: CL Resi Jual: Mn Corr JCt>O n: . .. CL Coir S ate Received by: iiiBSiiaafiis Date: Time: Received by: ( Signature) Date: ) Time- Arrival Temp. 't-J n-.y : Date: Date: Time: Date: Time: Seal Intact? Seal Intact? Seal Intact? 222n 1 ED 001523B 00005617-00013 Gold King Mine Reliable One Resources, Inc. (hereinafter "ROR") has tested the water at the Gold King Mine in Silverton, Colorado. The states that are being affected are Colorado, New Mexico & Utah. We have been successful in cleaning up the water that the mine is discharging. This is polluting the water flowing into the Animas and San Juan River. Groundwater Remediation ROR was asked by Argonne National Lab in Chicago, Illinois (David Surgnier) to pull samples from the North Kansas aquifer. We were asked to remove the high levels of Nitrate only. The before treatment results for Nitrate-N were 60.1 mg/L. After ROR treated this water the Nitrate level was reduced to 1.26mg/L, resulting in a 97.9% reduction. Attached you will find the water sample test results for the North Kansas aquifer. Produced and Flowback Water ROR has the capability to provide their customers with a process to recycle or discharge their Produced or Flowback Waters back into the streams. 17cv1906 Sierra Club v. EPA ED_001523B_00005618-00001 03 May 2016 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reliable One Resources Inc R McElroy 707 W. Corsicanna St Athens, TX 75751 Reliable One- Water Enclosed are the results of analyses for samples received by the laboratory on 29-Apr-16 14:11. The analytical data provided relates only to the samples as received in this laboratory report. ELI certifies that all results are NELAP compliant and performed in accordance with the referenced method except as noted in the Case Narrative or as noted with a qualifier. Any reproductions of this laboratory report should be in full and only with the written authorization from the client. The total number of pages in this report is 10 Thank you for selecting ELI for your analytical needs. If you have any questions regarding this report, please contact us. Sincerely, 5 r'" Itzel Dominguez For Monica Smith Project Manager Certificate No: TX104704265 17cv1906 Sierra Club v. EPA Page 1 of 10 ED_001523B_00005620-00001 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3261 ANALYTICAL REPORT FOR SAMPLES Sample ID Laboratory ID Treated Ground 16D3261-01 L-Analyzed by NELAP accredited lab T104704231 Matrix Water Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:48 Date Sampled 28-Apr-16 00:00 Date Received 29-Apr-16 14:11 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 2 of 10 ED_001523B_00005620-00002 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3261 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:48 Analyte Wet Chemistry Alkalinity (m) as CaCO3 Alkalinity (p) as CaCO3 Total Alkalinity as CaCO3 Ammonia-N (NH3-N) Ammonium (NH4) Chloride Conductivity Iron (Ferrous) Iron +3(Ferric) Nitrate Nitrate-N Nitrite Nitrite-N Sulfate Total Organic Carbon (TOC) Total Metals bv ICP Cadmium Calcium Iron Magnesium Sodium Result Treated Ground 16D3261-01 (Water) Sampled: 28-Apr-16 00:00 Reporting Limit Units Dilution Batch Prepared Envirodyne Laboratories, Inc. Analyzed Method Analyst Notes <20 20 mg/L 1 B6D3303 02-May-16 02-May-16 15:30 SM 2320 B KCT <20 20 mg/L 1 B6D3303 02-May-16 02-May-16 15:30 SM 2320 B KCT <20 20 mg/L 1 [CALC] 02-May-16 02-May-16 15:30 [CALC] KCT <0.10 0.10 mg/L 1 B6E0089 02-May-16 02-May-16 14:35 SM 4500-NH3 D JAS <0.13 0.13 mg/L 1 [CALC] 02-May-16 02-May-16 14:35 Calc JAS 8.0 3.0 mg/L 1 B6E0016 02-May-16 02-May-16 07:35 SM4500-C1 B JMM 60 10 uS/cm 1 B6E0025 02-May-16 02-May-16 11:00 SM2510B KCT <0.0500 0.0500 mg/L 1 B6E0024 29-Apr-16 29-May~16 18:52 SM 3500 Fe B IZW L, n <0.0500 0.0500 mg/L 1 B6E0238 03-May-16 03-May-16 12:21 Calc JMM 5.58 0.32 mg/L 1 B6E0198 28-Apr-16 28-Apr-16 08:00 SM 4500-NO3 D JAS 1.26 0.10 mg/L 1 B6D3446 29-Apr-16 29-Apr-16 15:00 SM 4500-NO3 D JAS <0.16 0.16 mg/L 1 B6E0198 28-Apr-16 28-Apr-16 15:25 SM 4500-NO2 B KCT <0.05 0.05 mg/L 1 B6D3448 29-Apr-16 29-Apr-16 15:25 SM 4500-NO2 B KCT <2.00 2.00 mg/L 1 B6E0026 02-May-16 02-May-16 11:30 A STM D516-07 KCT 1.17 1.00 mg/L 1 B6E0091 01-May-16 Ol-May-16 23:28 SM 5310B IZW L <5.0 <2.00 <5.0 <2.00 14.9 5.0 ug/L 2.00 mg/L 5.0 ug/L 2.00 mg/L 2.0 mg/L 1 B6D3175 28-Apr-16 02-May-16 12:00 EPA 200.7 ACB 1 B6D3180 28-Apr-16 02-May-16 10:27 EPA 200.7 ACB 1 B6D3175 28-Apr-16 02-May-16 12:00 EPA 200.7 ACB 1 B6D3180 28-Apr-16 02-May-16 10:27 EPA 200.7 ACB 1 B6D3180 28-Apr-16 02-May-16 10:27 EPA 200.7 ACB Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 3 of 10 ED_001523B_00005620-00003 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3261 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:48 Analyte Batch B6D3303 - Inorganics Blank (B6D3303-BLK1) Alkalinity (m) as CaCO3 Alkalinity (p) as CaCO3 LCS (B6D3303-BS1) Alkalinity (m) as CaCO3 Alkalinity (p) as CaCO3 Duplicate (B6D3303-DUP1) Alkalinity (m) as CaCO3 Alkalinity (p) as CaCO3 Batch B6D3446 - Inorganics Blank (B6D3446-BLK1) Mitrate-N Blank (B6D3446-BLK4) Nitrate-N LCS (B6D3446-BS1) Nitrate-N Matrix Spike (B6D3446-MS1) Nitrate-N Matrix Spike Dup (B6D3446-MSD1) Nitrate-N Wet Chemistry - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source % REC Level Result %REC Limits RPD RPD Limit Notes Prepared & Analyzed : 02-May-16 <20 20 mg/L <20 20 Prepared & Analyzed : 02-May-16 58 mg/L 50.0 116 80-120 46 50.0 92.0 80-120 Source: 16D2577-01 116 20 mg/L <20 20 Prepared & Analyzed : 02-May-16 118 <20 1.71 20 0 20 <0.10 Prepared & Analyzed : 29-Apr-16 0.10 mg/L <0.10 Prepared & Analyzed : 29-Apr-16 0.10 mg/L Prepared & Analyzed: 29-Apr-16 26.1 mg/L 25.0 104 90-110 Source: 16D2938-01 25.3 0.10 mg/L Prepared & Analyzed: 29-Apr-16 25.0 2.13 92.7 80-120 Source: 16D2938-01 Prepared & Analyzed: 29-Apr-16 25.3 0.10 mg/L 25.0 2.13 92.7 80-120 0.00 20 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 4 of 10 ED_001523B_00005620-00004 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3261 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:48 Analyte Batch B6D3448 - Inorganics Blank (B6D3448-BLK8) Nitrite-N LCS (B6D3448-BS1) Nitrite-N Matrix Spike (B6D3448-MS1) Nitrite-N Matrix Spike Dup (B6D3448-MSD1) Nitrite-N Batch B6E0016 - Inorganics Blank (B6E0016-BLK1) Chloride LCS (B6E0016-BS1) Chloride Matrix Spike (B6E0016-MS1) Chloride Matrix Spike Dup (B6E0016-MSD1) Chloride Batch B6E0025 - Inorganics Blank (B6E0025-BLK1) Conductivity Wet Chemistry - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source % REC Level Result %REC Limits RPD RPD Limit Notes <0.05 Prepared & Analyzed : 29-Apr-16 0.05 mg/L Prepared & Analyzed: 29-Apr-16 0.10 mg/L 0.0997 99.3 80-120 Source: 16D3170-01 0.10 0.05 mg/L Prepared & Analyzed : 29-Apr-16 0.0997 ND 96.3 80-120 Source: 16D3170-01 Prepared & Analyzed : 29-Apr-16 0.09 0.05 mg/L 0.0997 ND 93.3 80-120 3.17 20 Prepared & Analyzed: 02-May-16 <3.0 3.0 mg/L Prepared & Analyzed: 02-May-16 102 mg/L 100 102 80-120 Source: 16D3170-01 82.0 3.0 mg/L Prepared & Analyzed: 02-May-16 20.0 62.0 100 80-120 Source: 16D3170-01 Prepared & Analyzed: 02-May-16 80.0 3.0 mg/L 20.0 62.0 90.0 80-120 2.47 20 Prepared & Analyzed: 02-May-16 <10 10 uS/cm Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 5 of 10 ED_001523B_00005620-00005 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3261 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:48 Analyte Batch B6E0025 - Inorganics Duplicate (B6E0025-DUP1) Conductivity Reference (B6E0025-SRM1) Conductivity Batch B6E0026 - Inorganics Blank (B6E0026-BLK1) Sulfate LCS (B6E0026-BS1) Sulfate Matrix Spike (B6E0026-MS1) Sulfate Matrix Spike Dup (B6E0026-MSD1) Sulfate Batch B6E0089 - Inorganics Blank (B6E0089-BLK1) Ammonia-N (NH3-N) LCS (B6E0089-BS1) Ammonia-N (NH3-N) Wet Chemistry - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source % REC Level Result %REC Limits RPD RPD Limit Notes Source: 16D3261-01 59.8 10 uS/cm Prepared & Analyzed : 02-May-16 59.7 0.167 20 Prepared & Analyzed: 02-May-16 179 uS/cm 180 99.4 0-200 <2.00 Prepared & Analyzed : 02-May-16 2.00 mg/L Prepared & Analyzed : 02-May-16 20.4 mg/L 20.0 102 90-110 Source: 16D3170-01 23.4 2.00 mg/L Prepared & Analyzed : 02-May-16 20.0 1-76 108 80-120 Source: 16D3170-01 Prepared & Analyzed: 02-May-16 25.4 2.00 mg/L 20.0 1.76 118 80-120 8.49 20 <0.10 5.11 Prepared & Analyzed: 02-May-16 0.10 mg/L mg/L Prepared & Analyzed: 02-May-16 5.00 102 90-110 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 6 of 10 ED_001523B_00005620-00006 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3261 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:48 Analyte Batch B6E0089 - Inorganics Matrix Spike (B6E0089-MS1) Ammonia-N (NH3-N) Matrix Spike Dup (B6E0089-MSD1) Ammonia-N (NH3-N) Wet Chemistry - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source % REC Level Result %REC Limits RPD RPD Limit Notes Source: 16D3045-01 4.02 0.10 mg/L Prepared & Analyzed : 02-May-16 4.10 ND 98.0 80-120 Source: 16D3045-01 Prepared & Analyzed : 02-May-16 4.11 0.10 mg/L 4.10 ND 100 80-120 2.21 20 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 7 of 10 ED_001523B_00005620-00007 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3261 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:48 Analyte Batch B6D3175 - Metals - EPA 200.2 Blank (B6D3175-BLK1) Cadmium iron LCS (B6D3175-BS1) Cadmium [ron Matrix Spike (B6D3175-MS1) Cadmium [ron Matrix Spike Dup (B6D3175-MSD1) [ron Cadmium Batch B6D3180 - Metals - EPA 200.2 Blank (B6D3180-BLK1) Magnesium Calcium Sodium LCS (B6D3180-BS1) Calcium Sodium Magnesium Total Metals by ICP - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Prepared: 28-Apr-16 Analyzed: 02-May-16 <5.0 5.0 ug/L <5.0 5.0 Prepared: 28-Apr-l 6 Analyzed: 02-May-16 240 ug/L 250 97.9 85-115 248 250 99.4 85-115 Source: 16D2848-01 460 5.0 ug/L 515 5.0 Prepared: 28-Apr-16 Analyzed: 02-May-16 500 ND 92.0 80-120 500 3.21 102 80-120 Source: 16D2848-01 Prepared: 28-Apr-16 Analyzed: 02-May-16 506 5.0 ug/L 500 3.21 101 80-120 1.59 20 450 5.0 500 ND 90.8 80-120 1.32 20 <2.00 <2.00 <2.0 19.7 19.0 19.6 Prepared: 28-Apr-16 Analyzed: 02-May-16 2.00 mg/L 2.00 2.0 mg/L Prepared: 28-Apr-16 Analyzed: 02-May-16 20.0 98.7 85-115 20.0 94.9 85-115 20.0 98.1 85-115 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 8 of 10 ED_001523B_00005620-00008 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3261 Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:48 Analyte Batch B6D3180 - Metals - EPA 200.2 Matrix Spike (B6D3180-MS1) Calcium Magnesium Sodium Matrix Spike Dup (B6D3180-MSD1) Magnesium Sodium Calcium Total Metals by ICP - Quality Control Envirodyne Laboratories, Inc. Result Reporting Limit Units Spike Source % REC Level Result %REC Limits RPD RPD Limit Notes Source: 16D2848-01 94.2 2.00 mg/L 30.9 2.00 156 2.0 Prepared: 28-Apr-l 6 Analyzed: 02-May-16 20.0 72.4 109 80-120 20.0 10.3 103 80-120 20.0 132 121 80-120 Source: 16D2848-01 Prepared: 28-Apr-l 6 Analyzed: 02-May-16 29.2 2.00 mg/L 20.0 10.3 94.2 80-120 5.67 20 154 2.0 20.0 132 111 80-120 1.32 20 92.5 2.00 20.0 72.4 101 80-120 1.79 20 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 9 of 10 ED_001523B_00005620-00009 Client: Project: Work Order: Reliable One Resources Inc Reliable One- Water 16D3261 Notes and Definitions n L DET ND NR dry RPD CLT Not accredited for this analyte Analyzed by third party laboratory Analyte DETECTED Analyte NOT DETECTED at or above the reporting limit Not Reported Sample results reported on a dry weight basis Relative Percent Difference Client Representative Envirodyne Laboratories, Inc 11011 Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone www.envirodyne.com Reported: 03-May-16 16:48 Envirodyne Laboratories, Inc. Itzel Dominguez For Monica Smith, Project Manager 17cv1906 Sierra Club v. EPA The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 10 of 10 ED_001523B_00005620-00010 KNL ENVIRONMENTAL TESTING DOH Certification #E84025 Cert.# T104704527-14-1 Report Date: May 10, 2016 Envirodyne Laboratories, Inc. 11011 Brooklet, Ste 230 Houston, TX 77099-3543 Field Custody: Client Client/Field ID: Reliable One Resources Sample Collection:4-28-16/1700 Lab Custody Date: 5-3-16/1035 Sample description : Water CERTIFICATE OF ANALYSIS Parameter Gross Alpha Units Results ||||||lji|;|||g| Analysis Date 5-4-16/1658 Method EPA 900.0 Detection Limit Gross Beta IlllllljJIll 5-4-16/658 EPA 900.0 Radium-226 |||||||||||||j|jl||||||||||||| 5 - 5 - J 6/16 10 EPA 903.0 Radium-228 Uranium Uranium A I phu St 'Atari ' -1 : Th -2 50 i Hid u JI d-.'ioi a Cu b/ 0.0 1.3 5-9-16/1523 5-10-16/0921 EPA Ra-05 llllllliljlllll EPA 908.0 ||||||^^ ||||||||!|^^ ggggggg^^ gggggggggggggggggggggggggggggggggggggggggggggggg-^ gggggg^gg::Ky/ulgggggggggggggg- James W. Hayes Laboratory Manager Test results meet all requirements of the NELAC standards. Statement of estimated: uncertainty available upon request. Test results refer only to sample(s) listed. PK f NOkGMfHu.i D pirn iNC ) 'OU/ IrC-m I I < u 11 ;/ /./(-! ; i/o U /.p iorio. T-MM. I roc uvihiUHMrui A! < mm 17cv1906 Sierra Club v. EPA ED_001523B_00005620-00011 17cv1906 Sierra Club v. EPA Comp Temp. Analysis Time Envirodyne Laboratories, Inc. 11011 Brooklet, Ste. 230 E A138697 TCBQ Certification # T104704265 Houston, Texas 77099-3543 Phone (281)568-7880 - Fax (281)568-8004 Page Of Name: Address: City: Reliable One Resources, Inc 297 Kingsbury Grade Suite 1038 Lake Tahoe. NV 89449-4470 Analysis Request and Chain of Custody Record Ce I -303-3 Office-775- Project No. No. ........ Field Sample No./ Indentification Raw Ground Treated Ground 1 Date & Tim .7 ? Client/Project . . _ !- I Sample Container Sample Type ( Liquid, (Siz/Matt Sludge, etc) Preservative ANALYSIS REQUESTED 1 Gal/Cubie 1 Gal/Cubie Liquid Liquid lce,HNO3 Jce,HNO3 Gross Alpha/Beta,Radium 226-228, Uraniu Gross Alpha/Beta,Radium 226-228, Uraniu X d iSt JJIIf fV: ... (OB liiilBil BSWiB c 11 At ' cy: ~ J B I B - .............................. . .. ---- .lu iWssSygO ...... ....... ......................... X. J 5s . ........................... ................. - - / - ED_001523B 00005620-00012 Samplers: (Signature) Affiliation Remarks: fl"'-' I *. Relinquished by: (Signature) j.J?..,.. d... b . Relinquished by: fl (Signature) Relinquished by: - . (Signature) ! J;.; .. . FLOW:_________ i Meter Reading:_______) - r: CI Residual:_______ Mn Correction:_______ Cl2 Corrected............................ : ............... ....... . Date: Time: -, Date: ) : Time: Date: Time: Received by: (Signature) Received by: ( Signature) d 1 : Arrival Temp. -v x fl Site Representative: , B Date- < .. . Seal Intact? ' ' . Time: - - Date: Time: Seal Intact? : Date^fl^y^ Seal Intact? Time:.: Time: TCEQ Certification # T104704265 Envirodyne Laboratories, Inc. 11011 Brooklet, Ste. 230 Houston, Texas 77099-3543 Phone (281)568-7880 - Fax (281)568-8004 Pg E A137624 Of Name: Address: Reliable One Resources, Inc 297 Kingsbury Grade Suite 1038 Analysis Request and Chain of Custody Record City: Lake Tahoe, NV 89449-4470 Contact: Philip McElroy Phone: Ce I - 303-3 Fax: Office - 775- Project No. Lab ID No. Field Sample No./ Indentification Treated Ground m lilil m i1u11! Treated Ground Treated Ground Treated Ground Treated Ground Treated Ground 5:B Sample Container Samplo Typo (Liquid. ( Stea/MafO _ ---- Sludge, etc) Preservativo Gal/Cubie Liquid Ice, HN03 500 ml/P Liquid ice, H2SO4 ANALYSIS REQUESTED Gross Alpha/Beta,Radium 226-228, Uraniu TOC, AMMONIUM ,,0 1 250 ml/F -- Liquid Ice. HNO3 Na, Ca, Mg, Fe Chloride,Aik,SO4,NO3-N,NO2-N,Cond Ice, HNO3 Ferrous Iron 250 ml/P Liquid Ice, Hpl ? p III Remarks: 17cv1906 Sierra Club v. EPA Relinquished by. ( Signature) FLOW: . _ Meter Ru.idin) Cl, Residu.il Mu Cnnc-cLon Date:'l? : >/.. Received by: Date: Time: Date: Time: Received by: ( Signature) IM Site Representative: Date: Date: Time: ( atei ! I Seal Intact? i gi|g|ili|f^^ 'Seal Intimi? Seal Intact? Date: rime: il ED 001523B 00005620-00013