Document KJ88Q212XvMxvrOvv99k7pjOQ
(105;
CO ^6 CODE YT*868-D
A- " FEE-1 34154
EST..WGT.
wmu/L%%.
STD. HRS.
^
. Time
.
pkg.
7/9*
it -.
MAKING INSTRUCTIONS: BATCH UNIT
,T,iL,.r.r.v\g3aL>?*z w*p*
PROCESSES
APPROVED BY
' *
{ J YT< 868-D a>
() ()
( ) <)
t) . ..'_____ (1
EWK 10/23/76 EAS 5/26/78 DCG 5/30/78
MW 5/30/78
.
TYPED BY
^ t ft m rj 6/6/78
'.
,,
EQUIPMENT "PEEF 1
303 2
DALAMAR YELLOW
aitri -ferizr..UP*
/&,% m, 17'trtrr
- rtain far s-s 6 5a~bnj.r aig t t i*
Clean* Press, close 24*g].&. jg.framlir
J? $Sr% "(2536) Water 1nta V^303~
V 2m.r..f.i.lr..i............................. . ' " ; . ie^KlGri:'';PttSi.ial -^cale 'ft.rdurojpT 'In'
Note* Break ip lunins Lot
M ^ , <4.Q. J&yfc
' ' ~ 3
Stir 45 min to dissolve for 311
W Daring S7. Run tn 10** (323 G) water Into
3
Btamip -1nl& stir 5 intn
. ;
303 3$^1jjhenS7 stir complete weigh on postal ' M
4 jteal e^ pour 1.1 n &~stt r- 5 ml n 'AdUkto 60>62QP ' Recordr
op*
3hon. .1n:'4n.4*6 min
to W 1395 :6) at 66-TIFf
>Z..'.'"MT
:
"5 min a Record; ~ wLff,(4.1-C5T
" Assume 50%
LIT 3 Wrs inlntffluW:fon^44 maintainingat 66*-7QPfF
Record; Start
Total fflffr
USE LBS.
BLEEDING
N
CODE
ACCT. LBS.
46-C
HL 7T
T vr 46-C
7Z7-A,
725-A
"-....... ' ......
321
30-D 57 A
30-0-, 7-D
37.t L
y m
4^ ."/ '-r 4
EQUIPMENT
PAGfy 2 co 46 c o d e YT-868<d) es t . w g t . 2253
l bs.
USE LBS,
DV ML '.sift*' 10 min or longer to wet
.............
5 Coni.
JSC
M to Stahorrti
37" (12|5j |) 1rf 12-15 min
at
20;22qF
^ v , . ^ /^ W$T&% 'WJjgSPfoCf
T%..
18x330
SkL "Stir 30 mtn at 28-32P maintaining + QR'J + Kf for S 27 .......
'.
iecofds Time Start //.'HO-mil CR' 4> , t+T 'Kl ' /*'.. (+.
NOIL:
.......... . ' - '' . -J- 1
..........
(1) . If CR*, KI-, add 20# "as is* increments . Assume 3256
___* ^ecQr<jj c r \ > PFT7TF " (+)
`
:
N CODE ...57rA. 725-A --57-7T
..
28-D
ACCT, LBS. i
(2) if CR+, KI-, acid 20# "as is* Increments
Record? CR n (+1. KKn
C+)
Misc ML 3tafing S 24 stir welghiin 'drums for S31 M P,
6 J&L Weigh in Buggy 'for S 41
....
M 'A.
Assume 33% ,% , V4M %
725-A
' * ry&4 `s
wV. 7-D 4ST |
30-D.
..jj
DV .When S 24 stir ccmiDlete. dumo in
15 113-A ' 15 ii
7 "^l^tcTmiri at: ?832eF maintaining +CR, +KI for S 34
' in
7/7-A b/^A
1fl ',
..
|hPi
.......
Cl) If- CR-, add 20# *as is* Increments
Assume 32% -
28-D
Record: CR
{+) Kl >/- {+)
": `
-
(2) If CR+, KI*, add 20# *as is" increments
Ii. Records CR v ,
(+), KI v ' '= f+T
Assume 33% . ;"
. ...... "72F-A' -:slu" 1 1 1?i
CV During S 29 stir, run 10" C970G) water into V** /flfs &
8 temp chart
JW&rih N-7-D from $25
\.
--3ZS to 30" (2928G) at 66,70F
ijr Close stack damper
'
.................
. 3x330
DV y *' ' 9
When S 29 stir complete, test DV & Record:
Record: CR
(+). KIn V"' (+), temr\ : WF (28-32"F)
NOTE: 1 ' " `
.
l~
11) If CR*. KI- add 20# *as is* increments
Assume 32%
Record: CIV =
I+). Ki
(+)
(2) If CRt, KIw'add 20# "as is* increments
Jr Record: CR . f+). KI
(+)
Assume 33%
Pump DV thru clarif press into Temp at 28-32&F Record: time start
..maintaining ,, ..y-P 2x330 Total min vW
-jmxr
.'1^._______
- .
'^asfaKrflgl^^^
....
.
.
.
-4-
ip ,,3r 'DissojVe in 20 aal water in drum for 059
.'
--tr Wmp In from S2
Lot
n%,
" 67
..
n
' \
Note: Break up lumps A'
, j <:%.............
.QmQ WwLr> Q/<?/n
......&00..... .MS /J:
y,sm. q s t . ^
:..............
G<Zmn. L&ho
2^. __
'
w
~W :`jt
Sti^ Jpen
lO min to dissolve stack damper
.............
afP Bur in N-30-D from 526 undersurface in'20*25 min ~
$sr S.tTr 5 min & Record:
(5.8*>6,3)
........
LJ&L If necessary, ad.i to pH 5.8-6.3
. Assume 50%
Accord: d H
Assume 77%
W When S17 stir complete, run in V-303 on surface AFAP
57-A J^T\ 1 . i j
57-A ' -. t t [
28-A
I1
725 A
57-A 4^ i
..... ' M,; 979-D 67
46-C. sam 16&JL
:--"t t t 30-D
. .
...
.-
:3i1
i
* -.
* ' S. 13830 FtSV*
.............. * . '
'
''
w " '
r- _ ...
....
.....
-.
*
-' , * :
;. v:,t
.............' '..........' '* `
/ '
' '
''
'
" ' ' .
'
......
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DUP050292978
;..........
EQUIPMENT r-;, ' pag e 3 co 46 c o d e YT-868-D
es t . w g t . 2253
l bs.
_ gy-But men 535 complete, wash DV lines,.pump & press for 20 inin
USE LBS. ............
N
code
ACCT. LBS,
12 or to a - CR test on a sample of total press effluent. .which ever comes first * collect washings in DV (535)
....
^Stir 5 min A'records' Temp SIT (28-32<>?) & if ^ ...........
necessary, adj to 28-c32F iRecord:
YY "
'
~~W=t
'-
Weieh in rubber bucket & wash, into 0V
.....................
ITT" 395 D 10
min & Record; KI'
(-)
W* If necessary ad.iust to KI & Record; KI '. * * ; . ' '
'....... /.,,______ 395-D *TO
CV 5iH*' -When S49 complete, adj CV to 38" (3708G) at 80-84?? ! !
% 13
HTife?
REC
QF _ ^ I
'Immediately run in DV thru unoersurface distributor
< in 60-65 min. Maintain CV at 80S4F. Record: Time Startle A'A
.................
> Total min ..io& r
nmr
' 44
SZmOammUh unfitiliua
nriimJSSBg?Spi*.
', .
; ..................................................
.
.....
CV ^5P ""When $51 cdmo'lete, stir. 10 min
.
15 Sfi^ `"Record:. Diazo ' 't v . (* ) Base
{+) pH if,3 (4.3-4.7) `
Note;
'
(1) If Diazo +. Base and pH below 4.3;
(a) ad.i to pH 4.3.4.7
Assume 50%
. . .(b). record: pH
,,
(2) If Diazo + , Base -, and pH 4,3 or above;
(a) add 8# 100% N-7*D to a 55 G drum
(bj ad.i with water to # 25 G
;
jc) add 20# 100% H-46-C
(d) stir to dissolve
. tel oour Into CV
'
'
(f) stir to min
........
(3) Repeat (1) & (2) above as necessary to - Diazo, + Base
' 3*-
BP* JUammSCL^T) P-
5P , t -f aags^jijaii^a4ii tn
ff rTiffggpaiM
, AJ'JiHWjF1 COfit
,
'
7*0
7*D . . ..
46-C
_ - ____ ____
13830 RRV
DU P0502 92979
N 31970.01
DUP050292980