Document KJ4wjywV79k8jngDk1Mb5B1j6

M S ia -G - * 1 9 BIODEGRADATION (BOD/COD) TEST SUBSTANCE_______________________________________ __ Identity: A mixture containing perfluorooctanesulfonate; may also be referred to as PFOS, FC-95, or as a component of FC-206CF or FC-206CF-X. (1-Octanesulfonic acid) (CAS # 2795-39-3). Remarks: The 3M production lot number was 101. The test sample is FC206CF. Current information indicates it is a mixture of 0.5% PFOS, 10% diethylene glycol monobutyl ether, 78.08% water, 1.375% acrylic foamer, 1.5% sodium octyl sulfate, 1% sulfonated alkyl ether salts, 6.0% urea, 0.5% triethanolamine, and 0.05% tolyltriazole. The following summary applies to a mixture with incompletely characterized concentrations of impurities. Data does not accurately reflect the degradation potential of the fluorochemical component o f the test sample. MET HOD;_____________________________________________ Method: EPA 410.1 COD and EPA 405.1 CBOD GLP: No Year com pleted: 1991 Contact tim e: 20 days Inoculum : Not given. RESULTS_____________________________________________ Chemical Oxygen Demand (COD): Biochemical Oxygen Demand (BOD): 5-Day: 10-Day: 20-Day: 340.000 mg/kg 160.000 mg/kg 170.000 mg/kg 180.000 mg/kg Remarks: Testing was conducted on the mixture as described in the Test Substance Remarks field. The values reported apply to that mixture and not the fluorochemical proportion alone. CONCLUSIONS _____________________________________ ____ No conclusions given. Subm itter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 001855 DATA QUALITY R eliability: Klimisch ranking = 2. The study meets all criteria for quality testing. However, the inoculum is not properly characterized. The sample purity was not properly characterized and the study lacks analytical confirmation of the amount of fluorochemical proportion in the solution. REFERENCES_________________________________________ _ This test was conducted by Pace, Incorporated, of Minneapolis, MN at the request of the 3M Company, St. Paul, MN, Lab Request number J1885-2, 1991. O THER. _____________________ .________________________ Last changed: 6/28/00 001856 r tt m i M i c i i t m u r f REPORT OF LABORATORY ANALYSIS V f% T '] July 02.best copy available Mr. Hade Schell (Ko. cjA ^ . 3M Environmental Laboratory w 7T u J ' f 935 Bush Avenue Bldg. 2-3E St. Paul, MN 55133 RE: PACE Project No. 910522.526 J18B5 Dear Mr. Schell: _ Enclosed Is the report of laboratory analyses for samples received May 22, 1991. If you have any questions concerning this report, please feel free to contact us. Sincerely, Lisa A. Arndt Project Manager . V .'., := 7-'rx?k. -x ./ fess*'>***$ " f e L i ; ";p ^'^vhn^MSNTAL v- ^ p4i'fl^; i ' ^ : s' -v v : *v:-'iA.'* ` '^ K r v -> J7ieBm*0*tlMhj iraiiTuwij oo: m mi iimmci > maun Hr. Had* Schall Page 2 J 1885 PACE Sample Number: Date Collected: Date Received: Parameter INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Biochemical Oxygen Demand, Carb 05 Day Biochemical Oxygen Demand, Carb 10 Day Biochemical Oxygen Demand, Carb 20 Day Chemical Oxygen Demand REPORT OF LABORATORY ANALYSIS July 02, 1991 PACE Project Number: 910522526 H alli -HDL 10 01B5876 05/21/91 05/22/91 J1B85-2 DATE ANALYZED & HETHQQ mg/kg mg/kg mg/kg mg/kg 6000 6000 6000 50000 160000 170000 180000 340000 05/29/91 05/29/91 05/29/91 06/03/91 EPA 405.1 EPA 405.1 EPA 405.1 EPA 410.1 MDL Method Detection Limit \ ~ `.. 'a"-' v> ' BEST CQPffWAILABLE y.v- ': ? <Vf1-r ^ lMBMmiflpUMIMMNMMi*Ml y IOMm ITmmRmUIi.1 Umfla'lMj w LlhnkCanfMl 001S58