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AR226-2715 2 AR226-2715 DRAFT DuPontWashmgton Works Occupational Blood Monitoring Program for PFOA Preliminary analytical results from new employee serum samples. Final Report pending. November 15, 2004 Project: P642 Preliminary Results, Not QA'd Summary of Residue Found (ng/mL) for PFOA in Human Serum Samples SSponsor ID WW f^r- WW; WW WW WW WW WW WW WW WW WW WW- WW< WW ; .. WW WW ! %/% SBS^^, S,ja %-5@1 fesr-as tr^ ISS^d Br-?3 ^ SSE^py ^ : ; . . ^ eBsaasaeiaMsSsvCsQi ite8 ^S WW WW j J WW i WW J l WW WW PFOA (PPb) 96.1 98.2 35.5 15.1 203 14.2 69.1 20.4 63.5 28.6 23.6 66.4 68.1 27.7 19.8 NQ 15.5 36.4 NQ 85.1 68.3 27.2 Project: P642 Preliminary Results, Not QA'd Summary of Recoveries (%) for PFOA in Fortified Serum Samples WW WW Sample ID 0301028SpkA 0301028 SpkB L2676-1 Spk C L2676-1 Spk D Matrix Spk , Matrix Spk MATERiALEXOISED PFOA (PPb) 9.84 97.7 17.5 1040 1140 1100 Summary of PFOA (ng/mL) in Rabbit Serum Control Samples Sample PFOA 0301028 ConJtDro_l _A _1_0/_06_/0_4__________(ng/mNQL) Amount Fortified (PPb) 10 100 10 1000 1000 1000 AVERAGE: STD DEV: % RSD: Summary of PFOA (ng/mL) in Human Serum Control Samples Sponsor PFOA L2676-1 ConJtrDol_B__10_/_06_/0_4__________(ng/7m.54L) Recovery (%) 98 98 100 103 104 103 101 2.7 2.7