Document KGEr70dMpn0g07Q7z9o3rr4vo
LEHR 0800 373
AR226-0%1ls -y
Laboratory Report, Analysis of FCs in Samples of Children's Sera, May 21, 1999
The data submitted on perfluorooctanesulfonate contains analytic data when
certain general conditions have been met. These are that final analytic data is
available and thatif this data is a component of a study, a report exists that
combines the data and other parts of the study. Data that has not been
2
siunbtmeigsrsaiteodn.into a report, or pilot data, has generally not been included in the
22 on
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The attached is pilot data showing results from a limited number of human blood ~~ Ls
samples (pediatric samples from the University of Minnesota). This pilot was
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Analysis of FCs in Samples of Children's Sera
Laboratory Report No. FACT-GEN-011
Wins
------ Testing Laboratory
3M Envir3onMmeEnntvailroTnemcehntnaollLoagb&oyraSatfoertyy Services Fluorine Analytical Chemistry Team (FACT)
2-3E-09
S9t35PaBulu,sMh ANve5n5u1e0,6
--e-- e -------------------------- Laboratory Contact Kris Hansen, Ph.D.
PB.lOd.g.B2o-x33E3-3019
StP.hoPnaeu!l, M(6N51)55717383--63031381
FAX: (651) 778-6176
--eS------------------------------------
Requester
GearyOlsen and Jean Burris
.
3M Company
Occupational Medicine
220-3W-05
St. Paul, MN
REPORTDATE: 032199
94230
|
SA ENVIRONMENTAL LABORATORY
|
BEST COPY AVAILABLE
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| LSrsslo1ds00weur.ioeoxfn naseroeiansgvacuadellaoiSnnae.mcTtyi Rlrtltoeehmveoxluencposwrraru)leysicins | analyze for PFOSand PFHSusingigh pressure udhromatogaphylcloacnieeparsys `spectrometry(HLPC/ESMSMS),andevaluatedversusanextractedcurve.Qualitativeanalysiswas.
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`conductedby comparingpeakresponseinthesamplestothatobtainedfromstandafds,whenpossible. If `standard materialwas notavailable, compound identificationwas basedonreasonableHPLC-retention time
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REPORTDATE 0521
04291
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,anionization techniqueused primarifloyr
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REPORT DATE052199
04232
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BEST COPY AYJAILABLE SMENVIRROeNEoNTnALsLiieBOoRAnTOyRY
5.2 Blanks
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Blanksarecompliantifno targetanalyteis detectedabovethelitof detection or aspecificanalyte. In
thisstudy, allblankswerecompliant.
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53
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5.6. Sample Related Comments
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modifiedmethodusd 0 extrac hseSopls. `higherthan theaverage values observedpreviouslyforadultsandmay be due toimprovements to the
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REPORT DATE 0572159
04293
BEST Copy.AVAILABLE *Bsessseesss:
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BieEEE ae
! br mE:abe FACE Aes 8.1 AttachmentA:Quantitative ResultsofPFOSandPFHSDetermination
|
82 AttBa :Quac litah tivem Sume maryn oft FCsidentifiedinSamplesof ChildreSne'rsa
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85 AttachmentE: AnalyticalDataforPFOS and PFHSdetermiration
|
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SEER |
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Ded (bree
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Lisa Clemen, Analytical Chemist
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fideo Ho
Kris Hansen,Ph.D,,StudyDirector
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