Document K6Nv0ZKxnNYmpow8rxmqwzYy2

- AR 226 -- 0870 BIODEGRADATION (BOD/COD) TEST SUBSTANCE Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-7808B. (1Octanesulfonic acid) (CAS # 2795-39-3). Remarks: The 3M production lot numbers were 1 and 501. The test sample is FC-780B. Current information indicatesitis a mixture of 0.58% PFOS, 14% diethylene glycol monobutyl ether, 76.7% water, 5.5% urea, 1.17% Hydroxy foamer, 1.15% sodium octyl sulfate, 0.8% polyoxyethylene monooctylphenyl ether, 0.05% sodium lauryl sulfate, and 0.05% benzotriazole. The following is anabbreviated summary ofmultiple biodegradation studies on FC-780B. These studies applyto a mixture with incompletely characterized concentrationsof impurities. Data does not accurately reflect degradation potential of the fluorochemical component ofthe test sample. METHOD: Method: Specific methods not noted. Type: Aerobic BOD and Dichromate reflux COD GLP: No Year completed: 1978 - 1982 Contact time: 20 days Innoculum: Seed was from various sources. RESULTS `Chemical Oxygen Demand (COD) range: 292,60--0 377,000 mg/kg Biochemical Oxygen Demand (BOD) range: 5-Day: 23,000 -- 165,000 mg/L. - 10-Day: 44,000 -- 290,000 mg/L. 15-Day: 192,000 -- 380,000 mg/L 20-Day: 205,000 -- 490,000 mg/L. Remarks: Testing was conducted on the mixture as described in the Test tShuebsftiuaonrcoechReemmicaarlksprfoipelodr.tiTonhealvoanel.ues reported applytothat mixture and not _ conclusions 000000000 No reliable conclusions can be derived from these studies. The indication is that the majority of the product components are readily biodegradable. 002498 Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 DATA QUALITY Reliability: Kiimisch ranking = 3. The studies lack description and records of the method followed. The values for the study conducted under Lab Request number 7685 are from a summary sheet onl--y raw data not found. The inoculum was not properly characterized. The sample purity was not properly fclhuaorraocctheermiizceadlapnrdoptohretisotnudiyn lacks analytical the solution. confirmationof the amount of REFERENCES Testing was conducted by multiple laboratories atthe requestofthe 3M Company, Lab Request numbers 4461, 4653, 4657, 4673, 5598, and 7685. OTHER Last changed: 6/28/00 002499 a' COD AND BODTADBLAETA1FOR FC-780B : LAB REQ. # LAB. SATE Ed 300g 300, 300, 30D, 80D,,/COD 501 4673 SERCO 3/28/79 377,000 140,000 290,000 300,000 320,000 0.85 501 4673 Haller 3/28/79 293,000 165,000 190,000 192,000 205,000 0.70 s01 4673 Babcock 3/28/79 345,000 27,000 14,000 220,000 230,000 0.67 Lor LAB REQ. # LAB 03 cop BOD 80D BOD.1s BOD, BOD, /COD cop BODg BOD, BOD, BOD, BOD, /COD 1 4461 3M ENV. 11/10/78 360,000 140,000 260,000 . 280,000 280,000 0.78 AvEg. e 346,000 93,000 202,000 245,000 264,000 0.76 1 4657 3u ENV. 4/23/79 353,000 53,000 220,000 240,000 280,000 0.79 = 95% C. I. 326,000-376, 000 28,000-158,000 113,000-202,000 204,000-28070,0 221,000-307,000 0.69 - 0,83 1 4653 3u ENV. 5/29/79 348,000 34,000 210,000 240,' 000 Far 270,002 0 0.78 - WNaasvhailngRteosn,earcDhC Lab 387,000 - 0.96 002500 CURE sox aon ---- . . PRODUCT ECOLOGICAL ASSESSMENT net; Envin, assess, ino. #a 720L 3R7EQUE(S7T8F3O0R9)LABORATORY WORK Le eavesro,_ZG 7S Compte larsSo! neovesren LasonaTony `Name: oA See neo Phone No, SOZF |Date Received Sample: Analyst: 1a TC CSPoornoodjelecetsNio.:e. ZL =77 TT -- Pio-- op------ Prob.No._______| DateCompleted: 3-25-77 DPuerpsoscgriptioofn:Test_s:CaLnedbist7T2u hfaslflesruieilyin8e 1I0FtTehait oDfs3ad0doifasdl@| PleaseCall RequesterItDelays Are Encountered. PRS Vagasiimets of MIL-F-243858 anteCombustion CalG (BTUILD) Density Ash = Other i -- or 30> s0o0.o oor BOD ms wP 300= 7 B00 Srey / PaDehydrogenase Other Activity (TTC) B10ASSSoAcYrssndMa ethod omer a cob. B00 B00, Untimate. STcoc Bioway. Other igSesmumtion \ Persistence DegradationProducts. Lot sol TD -- py = ry er TE T tT t T" 1 1 r Tr T T1 rrr 1 1 X I T 1|12|7f7 #o0 je000T =[291265,,400000|_c| uilizzB7S,,.C IX Sx T T 1|1[Z 1132076,z 000000 8[1Z0 og17sz0,,.o0 00m00w6|0 | || 44, O. 2230,000 Tr Tr 11 r rr r rr 1 1 rr rr 1 t Tt t 11 F111 [1 || |] TT rr rr rr rr 11 Tr T1 T r r r rrrT 1 1 Tr rr 11 rr 11 r rr T Cr 1 1] | | fe AE -- rT T rrr T 11 Tr cebet 1 Fer roW If[ roTS onO 0 Gs-- -- -- 0ReS w to Ree rw Yom X.Y. movimicE. 1 ostox.Mass. ew HAVEN, CoN. sorEaLo, MT. PLARamD, N.J. BEE THE HALLER TES`cToIwoNmmGm LABORATORIES -- J . P3l3a6inLefliaenlNdd.,AvJ.e0n7u06e1 P.0.Box consuLTATION , -- Client, Project Sublet nt ThimsraeyponrotitsbtehpecuobnlfiisdehnetdioalrprreopperrotdyuocfetdwhietClhioeuntt,oaunrdwirniflolremnapteiromnicsosiionn.ed Minnesota Mining & Mfg. Co., St. Paul, Minnesota Purchase Order No. 711707 - 400 z Laboratory Testing for C.0.0. and B.0.D. Report No._P-79-4611 Date March 15, 1979 -- Tw. el TThaebofroaltloorwyinogn aFreebrtuhaeryte5,st19r7e9s.ults of Sample No. 7901 delivered to our TEST RESULTS .0.0. 292,600 ng/1 8.0.0.5 165,000 mg/1 8.0.0.39 8.0.0.5 190,000 mg/1 192,000 ng/1 B.0.D.20 205,000 mg/1 * THE HALLER TESTING LABORATORIES, INC. Rt opel ger W. FaTTer Vice-President RH: 1g -- MRienpnoerstoetdatoM:ining & Mfg. Co. L BSlt.dg.Pa2u0l,, 8M8i1nneBsuosthaA5v5e1.06 Att: Mr. David Seely -3- z 002502 " HE em wi . 1 ELY +ROSEVILLE, MN 2S0A8N21I.TACRaYvlaEnNdGAIvNe.EERR"oIsNiGe,LMAi.BO$R5A11T3O8R1I2E)S6,36.I1N1C7.3 ' PERU, ILLINOIS _ ` REP(ORMTeOtF hLAoBdOREoAPlTAOoaRpgYpriAoNveAeLdsY)SIS. REPOR0T2/W2O1./19 205 PoE 20r 2 CDDLAAITTEEENTCR:OELCLE3EIMCVTECEDoD:m:pa0ny2/01/19 CPOILCLKEECDT-EUDP BBYY:: CLIENT ~ SAMPLE DESCRIPTION: WASTEWATER 7b [ee Ch i enes ewrg M eBRE RE 8 . AmLrsis: ConSBEe: VTie SS H A WSTIRD) CRETE AE SYETE Ea ATE Ci OD, Chemdoe al Oxygene Demand, wmsee m/e1n in S31E70E00 1 3 BOD, 5-day, mg/L wooo BOD, 10-day, mg/l C 0D, B00, 15-day, 20-day, mg/L me/1 290000 300000 320000 BEST COPY AVAILABLE 113 i prs COREPSE A ne eR OREA CS Spide e $i hate 3 Sh A fR a SE aEhr Ld a in|; RyE ay TREE A E XR E REELEEak : 3 oR anion i" iy Tae SR L Approved by: : DFS.TriCtmeaane ns "leeesds sethannt 4 : Ea Miovipieb i@adil LoabsTnaea A yoC u N SOMATA somsom BESTaC.OmPeY wAeVAILABLE La am EDWARD 8.rBomAaBC&OSOCNSK,: Inc. 0Cacaoaman so 10 3 X Company Lov. Luaeh 2A3venxu St. Paul, 35106 Lab No._R _790205e -3 le gana%s Atti David Sealy ; 901 Ci vi owe 33/18 La CoE ee Te WE Lage C- S Day * 10 Day . 15 Day 20 Day : EiL na Ba 0D ug/l 22,000 44,000 230, 000 23000 WEL ARLsi Eh "x8 He con mg/l 34s, . 245,000 F fonRt ana C . \ : ei . a 0i0j2do5o0m4Tie? DEPT. CHARGE - S-eere--wonron 0535 PRODUCT ECOLOGICAL ASSESSMENT fet; E|NVI6R2,0As2seEssN,GwRa # 783o0viR7Es1QUEST FOR LABORATORY WORK wencavestvo_ Z(G 3S ROS oor rk wane: Erie A LBun~eSeEouesTen roti, 5025 oustcsaasinsLsso[nEatConUy 2D m Re On SPGeroortjeiocetNoN.Oo.s: Sho FOO Prob. No. Doe Rewind: Anas DHP aovuersCSoprepnto:r 2 2e 222 -- oncipton, lige Jaf 501Only SfarsOla IF pass Call Requester I Onays Are Encoune- Purposeof Tests: n7ialiCtily k57aCgaiOnr ibfeiPdeoydnidlipf anukl Agestis. frat Essenos | | fg op | [oo | rey | 2 PHYSICAL & CHEMICAL PROPERTIES FC7906 Fern ~rm T F TA Tae)T rrake) | TT g) O--the--r -------- r [--&F-- T rT r1 == : |[Fee|[E [Be E [eT WATERPOLLUTION = rrr to 1 5: Sg T(Roptiata) |X| sshee0||asi.oc0 |1343000 Aud S8o0o0.;vis Soedeeds gets |[XX[T|F 7p#keeacldeuzdkw,e[ et nape]| -->see 1 351000 Wrtacses sTcoc C o e r e TTS 800TES LL tl hncn dl He meerepsAy 761 N BOse ak Bob/se Nudclg inagh wrens Fader) [NZ7a arcor 3 se edel ,kan nea ssdai d]an cd, YA BIOASSAY. Spuciy Ogi ndMethod: [{S 0ee nee \? Bopri, CFR [p1tr10 11 gobs|Basic, Borys - FhunedE Pak e faclits --Li-- d N -- TT d-- ds, . som | se od Ah er || LEAGHATE FROM LEACHING TEST i op rrrr] 2o0o0.5 Uris T eetelusO oOjie adel 1| fTrzorece ECEeEaLgRRE ZlU7t3e.rFSoekl| AADDITIA ONAe L" UiOEKT oN||| Other r rr r rr r1 en |[BESTOQPYAvATAS[E|T] omHR B \ SPRearassiysyteencre rots Beurnnianbgy r r rr r r rr ] 1 1 T Tr T _O0Rs1 Dh 74al --1 [1 J=--g rd Boo: Ea LEBER |Em leu] me GE VERVE ie | = NUN seeosl-tus eve oly" I DK [ott se2-cx ucwos nirc eT BESEGOPYAVARABLE |secph cicmureC~\V | Frey EFPLEOT | SehLe wsistsaStak Sce aSvers TSpai uIsEaCAUTsEeDMoi|xedSiogunso ot) TED | SE | FE| Gi [42cee | Eile SE |Ren SoImdf 13500 2s, 25. 0| ps peed GE EE| 3B BEBE Biel pr. Test*2 00! mie BEE Ee aR eE a oo3 TEsT*3 ool ifs padiest BsomE SREO PED, | imo BEPomsWmqmem)|| = BzE sasmea aweE~en we:r | mse | Sshoaors 10000 T1teEcs| | SENS ne LweO:eRn|| SSPhEeeEprS HRT NERS Jume| 4g SdUWeoEemS)d ez, - SEwonS SiMomEomtSe a : EE 1G00000 ,: SE RE | dE IR dE BE BE WER0KGEs | ropmoesy HDe8b0e0+) FIU~SE 20a pagney| 11900) 0 z| = A = SSAViEyeRAnGaE ~% | 3% eo ae 225(0) we 235 (3) 2a me 185G) diez m | >Caadfeo0os0s+ MSL 2300000) B FE E2 me 2008) 2w15n ntohAmese| uNeA sS gnomes] 2osesay EB ER y BE 255G) NMoDw edrriems13 33505 oBrE We 23000 MERGE = he ATEASEOFPIuTolS rH AT LTAST 2.0mg4 DO DERE +) ; CiigE ar B R y i. K TH a Ee re Zatz SA H ro n IN C2oRyCd r L A! NNE Hed doh At ade) | ininel 47 HBTs - L i | H [| HSELEFed HH Al od a Le at a TT] Re | HEA elgd Ld LL ohd aar pn T Dyaklat|P e ae eayIdaSl pGHiEOlTs]] HTT TTT 11112 ie er CHEESE Re A Bg AZyliz a | . LASI op ppiiar d yo di a fold re ST I Peh r HARE A AE LTBRIBE Lp puisnteog Cade GUI E2P p rs r s BEA iC]lad dC eTebLBee ddLaro Ipad Sr tests) [LT Lt ra rae al ae H BEr CEa B)s Tedsa=tsgf papoLrT HOR eeApit n a TET rH A Liat ee SITET LL flfo acto pTeE tal)1 oreswe D J 2 "rn - Bo oA ENVIRONMENTALLABORATORY "Ib 80D WORKSHEET BEST COPY AVAILABLE Fu Hes3s ow 2144d-,So1f DiWatrr: 1t38on seo: APTA)Bnd we [omen| oe [1 = linsadid [CHE Tulle] eee] 22 STD. NETH.| Submtactis | 22[29s| 1 | Cseepl RTTr] | Ze2c lis | toed IrcontodlarsSAT |lsfiake. tend of dilitichlume | i. | Hf ltr NTT T -- --T7 1 777 1" 7 1 o2 | 20 T =~ Tago <os|= T= |A| 1325[os [= T= _ (1 1 1 --T | 3:0 [Fc-1308i079| ~ 1565 [320000| 350,00: 23 [6:0 [Cnitil tamplumo=| -- |3.70|3ci000 [220,008 |90[230|m=g12r .40e[2d 3000' 0 | 95000 1 ---- T 1 71 : Tar |20 |dplcat. | -- [sy [320000] 2560 Q |o | fosabrve) |- 1330 [330.000 | 29900 ag |90| 1 1i90 230,000 | Jie {4 |6.0 liitnifasmptdo-5|5 [23| 9,0 |mf jiton/-->jaomd] es]|220,000| 30,0 |26s [30.000 | (90,00 |20|30 | Adglhigt,, | 39 60 |Cascatne) |- |- [|S3o.8s5'||33<o&000o0o0o|| 203,/0000000 NL 1 20| T= Ta40 |220000| 130,000 - 8 |do|SND |-A 14R 4s |D 390-| ado |So [img luce | ~ |420|380 | 240 $1 | 6:3 |isorg Bolimiincil|- |3,30| 280 | ode oamplt00 =9.2) 00 U8 YD ovanbnsims - 20E7oLf,S Jf Boks ZL Dun nam LABORATORY BESWePHAt AB WTIAL 7 wR e535 oOimkaetodnoWwV:][984.0.5: SetQEXA100) 000 Aw STD NETHO RACT? lL Pe2 201 eedhsaediallmoalalr7)2 IV=V7 NN OW sv 1 1 TT Teer] 5 20 |25 V<erp satis|20. [690 | 7} - | wadstrmont(Liitildlticiod ohmal 4n2lbd Had] r rr 1 | rr SIT 1 ze| eds |370,000| 795000 28 |Go| dugloate |= 1cup| 190,000| isnp00 [90[ 7 TT - T390| 30000 | i52,00% rr rr TT Tr rr r T 2 | fo |B srampper |~ [Sor|sjo | eso |Sto ison lucaeed] - [Hig|270 | 130 23 |o 50nd alonideall ~ |3.75| 370 | azo | Wp=| t2ags) 1 -- vv Tr rT r r rr Tr rr r r rr r r rT rr r T -- +rr rT r T rr rT TT ao2sad] NE Don he_os3s : BR, 9 --LABORATORY Dnrt:l6d:2-.739k Voa .. BBEODSWTOCROKPSYHEEATVAILABLE OtWetr:(i80on Baa lr... Fehon eI CT ho nil Za tT pli ll J1]thn dlJlsTpE eTold 2 | CG | -- Tas [cae]RAs nflecritin |30 | |= Teo| = _ 1-- 1 asad [30 |w = T T%5 370000] 195000 |00 | Ziglicate |- [Ge| 7 T= | Goo | i000| T38 | 50.000 | rn 000 Joon Er mr Terete |60 l Rultbom~ic | 3c .86a|s27d 0 d| a3e rrTT rT TT --| 11] rT TT | rT _ | rT . rr T [1| [| 71 | TToozsio 7 ee ee Foo.S pS fn$A Tee, = .f ENVIRONMENTAL LABORATORY Ow 214td-So1f ua sod oa oe a be ___ I Jue Aw =r rh tine] coscutre " [oie | on[#2][1s] ree] SUBTRACT -- en~ t -- 1 Isla hitrlINe g dp lede Ee at oa ttre Tpi punt ts -- | 140.7 peper fel] | BES COPY AVAILAR oz |2 zo rite ar teear eTT z -- -- - I---- [20[tft|= m|gCoas[e0y To Bhfoe [Todd pee Feet =T1<oocr 5 > Ta I 1| I 7 a A [Cheo [ T Cao T s= lT Ie cob] n ~d --T 3 I 8 | do|sm|b = 1h 3%s |=- T= 7 [150 Blomar2s | =|Fs] wb00 =9.2) 2_ 9 a BEST COPY AVAILABLE Ane. PASE oun=1~79 /.@. OD 7 wo ron wrt or Suton: [RL 0a OERu wan al Cl[ ee Fp r T(ruo se t ed 77 W Re Vn575i 71 MP aGFdWhoapr= d >. ie i ar oa 30 |35Tsar mus[27 [IoSlates 1 5 T-- r] om=ar5n 0 T-- om Th~i~ =T T |bioa |t deT glimte [= licv os temt 5 et------] Te ---- Fetes =T77 Ts% 1 225 ||CS1o0 J[7i50nmdgt4iLlgicmeeatrae=a)| d =TosTo = [| 735| deo | 390 [ r T eI lyT T A-- T ] ] T T 1 T 1 T T ] T T T T T T T T T 1 ] ] T T -- T T 1f T a T m ] a CURES soox con PRODUCT ECOLOGICAL ASSESSMENT fat ENVIR. Assess. Na. 75309RE--QCUEST FOR LABORATORY WORK LAB REQUEST NO. CS ommerc. Er E F> am ors DIVISION Fe Hes 77S Name: _E27e ReineArEouesTCR Request Ont: 7229-57 PhoneNo. S077|| Doe Recareasoimapsioin_w_o{n~v2A7=R7D7 Ansys: [A= F134] FPSrojectNo-- : 33700)20-- 60 ProbAN-- o. ---- | Sample Date, Dane Nenad: YDT.Taw Copied8 :J% --- 23=-- 98 PDuesrcproispetioofn:TotIs: 2_2OSceFicmmief,PraoMdiumteitse,Smi0l0esFo FOL. PleaseCall RequIefDseltayseArre Encountered. om meres |[SF[su|e] TT HeaamtiofsCombustion Cal/G (BTU/L.) oxer -- wren I I o a g S0000. Uimsts 74D, Toc sOcr. nate Domerogree AST(176) ver BIOASSSoAuYc.yOrgani and Method: Fz ? efey 1 r rr rr r rr [X[352600 [W[s|e3oe0 XXTT waaorrplhadzblfeaodtesddet1 a shedar0 1 RI] D| rr 1 rr r Irr TTr 17 r rr rr r r rr r rr r r rrr RN 1 I a05 86050.;Dimers Tsocc Bow form - EN A PBroercsceunmcueinion DeamionProsumy rrrrr rrr r Tr Tr T r rr rr r r rr rr r r rr rr r r rrr rrr r rrrr Tees WP Pee em EeTee he Ee|te e1e| fr 3 ro aia Go) BEST COPY AVAILABLE ~~ Se fess La\ sh mmm een Soni Duter-lg=" 9. wr -- AZCun Cs woe[en| [PRe [pe[re Pe Telieintddalat l{nadb henn pdreaayt7nsd i x SauddGGodtelo 7 al |7 G S Et TE Er = Coto aad? =TGs T Se 7 q TsifoaeT glb ww aslag Tx Er GFro a [opea T 2a ry [5:t0aTnitmgaMlmucesraend]|-- I2gT|ETwx T [retm=T r2nd ] Eppa ge teraatif cia : -- r T ] T T 1I T ES] T T TT T T T ] 195 BEST COPY AVAILABLE ie Bi sao u foe -4 Ee SETATT bHATTTT SesAsRT BOY |E siem e scmemE Se PIEmOmFme C AVe e e EAe ERe F E E e ETee e e E EA m CEe GEe hL er ePREEe ee e e e EEe ee B1 m EE R aE i e me Ee e Ee e e EEe Eeen et ee !i| i|i e E C r e EE E ie e En eE e ea a e e E p pe e e ns e eee E e e E ee y e u= A |i ESC CCeCe r EEe m se Eeee e ee eE Eee e mE e pe e e e E ee eP ee e EEE E rrm mmayae e tE eea e e m e e ee e e eCe SEeAe Ee e EEeEEEEEEEE E B Be e Ee mEeSm F m ee ee a r Em e Se bSaI m GzECTe e LEEELR e eIet E ee eleer 4 it 2g885ExE t P TEkEt e EP E rS eel e e e ab r Eebe e B5 B E a e l oir nsf wnnRB lerae eteLstebhndaPlEaT,TRootry titi G BAb E eeT d bleAs1an]ti EL cnt len weSE BODWORK SHEET EN o Pr ww a Teo PA r Wge 17 y 7 I yAET myTT [ loasw |l| S1 oswe1 [1 $=pe0 7] 1 re | 790 820 lege |jeswF|/95000 7 130 |D400)800 [0 1sso0 xs | 55000 7 T[ s--o Jewies | srbisg[deaf| 92,000 120 1 144] 7.60 |30135]38.5 F | 3g500 [40 = Ara O00 Agading Toforact "1 H rucord (eb [TU [ r=" z 71 I TT Hd L/efo hoddim | [NT Olelda, [NC 2X To07 [ ze [| Tg [71 s1 o [ao[Te | 1e 17 |so [19. [4205 004 370 .000x| 37,000 [| Le [ T.ce [29] 0% 2500033 000 [20 F--"""% " sub" tat" nd-- P--b| rr | TT (Srapnmd[ n TN I 7 Tee Ti Tr TT er | Tr] 002516] /-2 -- . op desis --- IR mle avinonsen: LABORATORY onWN a BODWORK SHEET EW) , er T r Tieh ra s e Ih r g d ] 7 ldo [kL id vore rompefT r| a 70T TE [Foee Tloaoes[Tnamncodmlaosseeosmsnklzcopa Ret f TT F2 reeA coe1odpleectaJo-- t--oo-- o1d s-- o00] eil sio00 P TT T r T r T 11 r rT T r TT T r 11 T r 1 T 1 f T T T ] rT I -- T +------ r --F---- e +--+ 1 : I rr yy 2% roma supers 20 R gis weJagr|oem [on [oweJisoren| : ENVIRONMENTAL BODWORK LABORATORY SHEET J Srl switionbiWater/r: t We ga | Jeccagem | Teorgo) || | 1] TTast | leakiboertonje]-- [WWFTEEF-- "Fh 1 ro 0 lBeee Ts os LemTb= o eas : 174 550 [260 000 [29' 00 a 126 [| Toy[ = | goncallie [330,000]560000 [24500 - | [ I F rr T r ha rT1 rr T r1 rT rr rT rT rT rT rT -- r r r r r |T T T T ) 7 = T -- [ T re 1 1 rr ne ENVIRONMENTAL LABORATORY Dilton LT woe [apn[m Tooe [oneoe om | --__ BOD WORKSHEET 3p oanLgeVowr: ty/e 8LLa | Teorgoy 11 [Eo TTApA] leiaiboeac[to| m [5 & ] ; Mette / lo | [Be | 1%[2000 159cTdoommyostpoe oes pg [eA Pte| TT { T TT T t Tov uagw T TT TT T ve] TT TT] TTT] rT TT TT TT] |TT --1 rr I TTT |Tr x | r rT T 17) 1 pie. 2 7Por - 53S ENVIRONMENTAL ABORATORY B00Wonk su Blanks: ' y3 ' ai --_-- Srl Lug. 54F0o VowsLiga aye Fe [Sed |y S d yo |n T T ontfea 1d s SANT Drosel oss -- 1Ar i PERT E-- f=I--eexd-- L Bl Ta [l ol up r [Late 23 Jr rrp I r rar e1 TA] rr 1 2833 I llooaessool]eeawee [|] _ T I I ------ T ---- br T Th r re t e I v r r e r I 1 E-- E -- 7 -- -- -- -- 1 -- | Je D2 nr nomena Sell onEo BOD WORK SHEET FlomDioLn Waaer: Zye8-R8a Blanks: PE -- | Pet lL TThaSolbbtaangmer[[NyN Jag JASE LTomtfe 17 J& qq ee g Toda 1 I Ga=T ge TF TTT Trot I Th al 7] Ta 7T = Ip eh] hag =]pS 2 _ 70 Cll i TT 2S [eo 0s= Teta Dlr La ay TES ates rTTTT 3 FE) LT Teac iatdaTE geTyotf Lr T avaT TnJT] -- TTT TT [ -- 1 1 bras Ze| [BESTCheyAvaiABLE| [LIVI $8] = TTEe Tr rT TT rT 002521 3 oe regen : J 5 Vly lun ps3 4. ENVIRONeMeENeTA.L T3 hso0 n k ovu:on2 ne15.8- Bless: Logs 50 - R. [ zd ye TTorfe C Ss SN TrTew TT t T 75 al To T 3d [CF pga dar] re Pe Tr ee t da r Trre eeme[aseye-- TT AS SS NE a T T I -- h -- v re A yA e r rr + r T Tt T ts mu rareis ua ' rd 7s ENVIRONMENTA2 L 0 for One: 3716-79 BODWORK SHEET gf ih . eede A D7. Too 3 ae 1 TT 1 Tm gooLE f Eg e har Sr 23 -- rr ogy TT TTT rT--7 Trew i Tv rT I 1 TT 002525 SR .: - ENVIRONMENTAL 32 unr C53 one LTE BOD WORK SHEET 3 wp -- rh i Bk. Avg. rrTTT T 2 I T2oe 0 [I | RA EVaelaIC gpTR |We 2Po .s 0B | 3rJe] :l3.] 335 Zi P | =Caa el er T| agu0sT|soeasstto]n HA ------ Tr |H VL ZiD20 Hr P d 1 T 1Pp 0 =Fo1 v| z N rr r t r ] Ne ITaw ajaeo Sen [2T0IT77= |1 w92008 30 a 00--x| 5 200: Ae 1 as TT ao= ,a TE LT LT apa bofooFtehde ) [ =|34 2043100]| 30, -- r rr rT T] rT pT a I [ [ 1 r rT T T | T 1 Too=sz }9-22 mri ,: 20d "ssz ENVIRONMENTAL LABORATORY ou iil BODWORK SHEET tion Water: [5/__ 3 wt/R seus fl, = TTT] 2A Lg | eT TlVe 7zeTe |eam r|o1 m 1 og p]1 2 7) l[23o0IT 4aT [rJoo0x%]]352300 xX]Z] 50% 320% - 4 B T d 2acT T | 390%] 320 se] slo | ava ofx veliee ~ |ool] 555 Tl ng) 1 310. IT LT L TT TT lTT rT TT TT TT TT] TT] rT TT [rT rT -- TTT rT TT r" Ta] 2 r TT r Sv rT | rT TToozsey] rmavanes 0 yw "ss 5 ---- 2 lpips ENVIRONMENTAL BODWORK F SHEEaT l oaetio-- n aw:-- 5 3 tf su = lL AMT3WP To [SF Item ze [7 [SOToo8T . UL go TV 5 o [2.0 1 dh 13.0 Tr|Sdox] 330x] 2.503 TSs dgow]330 4] 00 weit 4.8 ------Fe[sox]svi] - 1 rT =H 0 | aon I allie= | F000 330.7] 00 I 7 TT TT TT TT rT TTT TT l rT lr rT rT TT TT TT TTT TT ny TrSe TT lrT rr1 FYRY omens iy com a I: BODWORKSHEET 3.0 Binks: . ` . om SH, YES3Ss pt LE Te ae Izmir pa ATHC TE [77 Ty 21 Lge Tm 5 Fee V7 e Tags e [|e7of1= 520] 5] 30% o 13.0 | "el Rdsi |33r 0a] 310% Tie 4m 35437. LT |algeml opY ep) boo =||3T 0,3d 4 30.0 71 Sic, J" rrrT TT . r rT T TT rT TT TT rT r T rT r r rT r TT T T rT rr T Tr a Sea] - rT -- T r T T Tozsz . 22-212 r Mammoyws2a +45, 2AR woo asm Ld en, contain PRODUCT ECOLOGICAL ASSESSMENT ag. 2 o ! Con ee REQUEST FOR LABORATORY WORK 12903Fs70r( 78309): Te g am $ etytott i weneovevsot,EEEF,S 7C7= >2 t No. REQUESTER Prone No. wSl073 7 | AnoDaaletyesCRtoo:cropvieodwS:omerLABOZRATT OT=RTYST.27F]T PrPorjoewcate: 22 201 SomploDna: JZ =JF LLL FronNo DueNod: | vFT 5 ht los Ctl Reais Dees wwEn rr DTap ee e R . fr Seeprmmma ||[17777 [0Ene] [JiR] JdPecdd [P270 Poova ics EE mr Ty A FEEL Ae genPee s 745F%i, REQUAERSTT FFOIRNALLABROERPAORTTORY WORK woafthr'nt.nA gGeielesad phase ! CT emer va. we (*o_veZrReEGURERSTOR=- DATE R--E-CLEAIBVEPDE:RSO.NN2E7L0-1--71979 fa Qi o ~DeR sOcJ:ECTFeWO7.8-98970L0O1T27S0010 ASHMARASTLEYSSPCTEOZNMTPTLDECTSED: ACTION DATE 372871973 27171979 2 > 35 + cToenee TATE B>ei cof ee i TTEHE nn i, ADD. DECLE CLS Ln SAVE a5 liedg aeA d eRL RsRL al A Nl a rest iaRnEpnT ie13g00e0R 03MGI a ETeegl an Tey Crdk ea27lONFHeZLil TALB S HEyAT Eiie E FF Den "BOD B2BO0ODDD 1U105CT (20) 233902000000000000 MMHGEEZZILEL., 121320028000000000 MMHAGGS/ZELL = 32242200000000000HEHHZeErLr" FT ETEER con 377000 MEYL 292800 MEZL 349000 HETL kip yi -- T -- L -- r -- tig mt e--] -- fo=ri pr Nl= Boscumumion Devisionioticn b 11 r t 1 r ----oo--es[py1l r Fr T oe 1d hahaa Sig Vinita-Return 5Requester Can-aarviryor le armrains te P E; o Fiismee t bge ,Lab:a Goidenreas-NloneaJeoDenuiiE , To sno nance asomrony ~suions 2s Ng moro A fC TB [. oGeoraowuoawnreon | Roma 0 0222 - EnGA. WWetarsatndowatar REQUEST FOR LABORATORY WORK Nome DC Reamer were one: _S/=/5~ED 7606 ee, _SSTRS & o Crore = Description: Hold Sample For. `Special Precautions. _ D | = Days Est. Date Needed: ------------. Poles S34 Compose His Spin Home Pthaen Tova] [Ih [T ocoolAs t r tHatrdn.essm,e omtowsc0a,co, -- |H-- --H----H-- --H---- -------- Ee-- [[lrFeo]oT m tncoheiordFme,gmtnoawsoe,r g H r ] ] [Foihmmamrtaeer------------ FH "fe [oF e]nae sn st era t [Elsir fBoeb =ang [H 70,000 H | 757z--m -- H] H] 100 190 or 20571 Sap [is comm --25CT For orSe 1] Ee E e [[o2[0T]Sm sAotimenia mSmgsn,r maraes] -------- [21] HoonNop 1] pee [[[ 22[2]]m sTovohoemoogso h mn myornaryy o ] l 1 on] --g ---- ] 1] foa E ol-- [pre ona-- ouge ss c--oae-- mTnPm-- ngi--o-- r1-- 9= -A 7--74--7p CH-- T] a --A --i --1 -- f[[o2er2]oonnmsvbGenmmopsmgen ---- | fb ee h ; -- [Ceooemo]lmn ipFeeecstcsotpto onr, Neostn oom sr1 m1-- 4TTAPS-- S p-- r ----f IT J----E-- STEC STEO OPYP AVAY RABAEE-- V--A--R--A --BLE -- -------------------- 99-- R5R9-- . . r., ee T--T ---------------------------------------- Internal Correspondence. cc: DD.. RL.. BRaiccokne/rR.- L5.3-B4oNhon - 21-2H-05 pa 3am To J: A. PIGNATO - COMMERCIAL CHEMICALS LAB - 236-2-01 Fon Swix B+ A. REINER - ENVIRONMENTAL LABORATORY/EE MIL-SPEC AFFF BOD AND COD TESTING & PC - 21-74-5 Attached COD test is a Summary of the results on FC-203C, BOD, carbonaceous BOD, FC-206C, and FC-780B and atnedstifnogur woasutsciodnedulcatbeodraattortihees.3M Environmental . This Laboratory variable than I had anticipated. The results were more BTrOheDes2u0lGt/aClObfDrroamirtathpiaosr.tesutTlehtsistsinogon,ccFuCir-.re2e.0,d6Cdtewhseepryietheatdypthiaecavlegraiyotfhittghhhaetir some of this testing inhibitor (the C-BOD was done results) with a nitrification and some of the done using a Of nitrifying seed unlikely to organisms (seed contain a large tests were population from the Knoxville treatment system). their results were While due to I had previously nitrification, waste thought that that high I do not know BOD results. why Galbraith gets I must now say suchatypically pqIroeprpleaacrynrintgHoaBluuesrreiaPtlrhoedSuaacfvteetryaEgneDvaitdraaotnaSmheenfetrtaoslm. Juestions all DatIaf of these tests in ySohueethsaveandansinput - contact goncerning these me on 778-5079. data, please feel feos oo EAR/mk oC Attachment 002530... | | BOD, CARBONACEOUS BOD, Lab BOD (ng/kg) 3m Pace CSaeprscuole GSalabWraiStehed GKanlobxrvaiiltlhe 580,000 800,000% 454700,,000000 616,000 670,000 n AND COD DATA ON MIL-SPEC AFFF c-BoD (mg/kg) (mcgo/pkg) BCOODDyg FC-203C Lot 501 600,000 773400,,000000 .79 730,000% 871300,,000000 464200,,000000 973570,,000000 ..660 671,000 776,450 .79 641,000 776,450 .86 PRODUCT cc=oBpoDg .81 6605: `86 .82 :5 3: 1 : = pe {: . 3 i. : As.verDa.ge 57855,,000000 59940,,000000 78820,0,00000.1.273 .a725 * CianlccounlsaistteedntB.OD'sPacferomagdrieefdferteontredpielatutitohniss wweorrek vbuetry diindadnvoetrternetqluyestlosatthtihredirtreestpienagtednortesdtidrweesulitnscluasdewetlhle.se We values in the averages. FC-206C Lot 502 3M 290,000 290,000 338600,,000000 0.78 0.78 SPearcceo 325400,,000000 327600,,000000 435700,,000000 00..7685 00.:8702 CGaaplsbrualieth 246106,,050000 342101,,000000 441007,,020500 01..6032 01..7081 GSal&bWraiStehed 395,500 374,000 407,250 .97 92 Knoxville 3 - As.verbpa. ge 348,1000000 33"587,,00000 33936,0,00000.81116 .a813 FC-780B Lot 501 mn 240,000 230,000 332300,,000000 74 271 PSaecreco 225100,,000000 225200,,000000 325807,,000000 ..7713 7771 ~ -- Caps-- ule ------ 240,-- 000--2-- 30,0-- 00 --36-- 0,0-- 00 --.-- 67 ----6n4r---- Average 8.po. 235,000 17,000 232,000 13,000 329,000 28,000 .71 .03 .71 05 { 002531 fCormUroAczoRsrEo asooEK~SazYem - - : Ref: ENVIR, ASSESNyS. ING * PRODUCT ECOLOGICAL ASSESSMENT REQUEST FOR LABORATORY WORK VISION Mcoron Las neauest no. 4,/ egmmm |-- ] T--11| mgr | [ @ eee | ] T71 Ware: REQUESTER _ ZAa L7J[-- Fy ----Pro-- ne No. F--37--9| wt Recaved Lasoratory ARD Sais: =2-7-7 7A; ilnl7e CoPrdoejeNtorN:ov T7601 2607 SampleOster Prob No | HoDuatresCSopernmtp:e7i1ekg:[=T=1[5674747 = Dre Needed:ATED| Yor gs LO MEE [DescEripAtion:rC 30e7-- ,0 e 0, -- _ ieToR x-- ieg rda v-- el| bless Gall Requester 1DeesAre Ememamered PINE OF SHAE DeerihngCompion ca STU) Soenr ------ r & r Dupceares r re 1 r rr r 1 1 Gi) co QEeEpuSmmRs fTeoilia odeweoe [|e[legees[|af | Se ong voe rr rr LT L TT oOysetopmae A(7767 r E r SS F B r E-- r rr r BIOASSAY rr] Soucy Organana eos: 9% 4LC Aquatic Tor _Blueg e 2S gramal[r Ae e wgmeenmenes || WL[TTF caop 80000,g mer STcoc OmBoesr rrr rr rr 17 r 1T BEST] COPY Tr 11 AVAJLABL r rr rr r rr 1 = TI 11 PBeoissnman Denier r rr rr r r rr rr r rrr 1] TeRw eve T0028 Gay vieEren sOieFieJ PEEEIienEN.Ar GSAcareRceo ieRo eas WT SE oid ANTESPom IC / a Me ite meensem 73s . Gor Bos Bef, es rSrEmn.eLeASoRmEeiGogf .ael|T r455TfT f T f $ we] f SI p {0 ferries= | 1 ---- + b Ee T re e fre he fa armed l a Tash e a ee Dace 3cfinen] A| Wo | o oPeCe3SS IV31 hPT euc=eeeB ] [Y So|0 ayeed [5=8[E=S[| ed= 1 E= i = 1 ---- 5i: .d FeeEE TT] 3 EE EE rA rF rC rr SR2.5Ass rr| 3 i + yr T rr r r t : !1 EBr rr I1ae 2A WT I BESTCCOOPPF Yv A AVv Ae Rr AB] HE i3E2 Hr eee i