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Cian GEER Te h[eM:S MveraormaAscsquQtuyaUtrtomPicerrooArPmancLoC | |EenrnomatonraoRtiec cyonUgPtLonsBe sviidv5, , 17pm 21 100mm EspxapnoFsulsScnan(a215c-90t0 a:m) i Moe has:S5oic(32c50%2H0HOoWOHAC1N0) WAhKH1DOmRMNHOA: CoC Snoeuv:rVEoonatcaaop(rg=e18y0e=0y20a6a0 a) i| TRoarpt: 1o0nmien SGanoe Gars Foeloswv(oUaw(H=Ut5)h0)o=0n50 J RiFofefs 0pmior srei 45 Sse 31. GO 1G 45 GANDA wprosouseels) [E2i0g[uarne2020i6_LPFOSL_-0P0F5OS; Selected MRM Transitions ZoJan2008 98047 5p00 ppb Pros 9 49915>099] 020 0A 080 080 180 120 140 @ 160 180 200 220 240 = 260 foc Prosi 483>41`9")l 020 I 080 u 107120 140 \ 180 200 | 220 240 260 100 PFOA 413>36t9o) 020040 080 080 180 1.50 140 180 180 20 220 240 260 Tine ; (locCioon:ndfoirDFoeiunlros2ope:jecctiton 1PSanmeters !i 104(500 2L-PFOS) [Molophase:I1so0caMtc 85m% (m8:a20 MreetOaiHtIoAuCtNmrY)3ST% HO `CCoolltsoonnGVaosl(gmeba(r1) =#4304603 ( m a ac u | [owe 30min | ime Wellington Laboratories Inc, 345 SouthgateDr. Guslph ON N1G 3S CANADA (pFOSUOS (ot3) p10 IWAEBLOLRIANTOGRTIOENS CERTIFICATE OF ANALYSIS/DOCUMENTATION BCROOMDPUOCUTNDC:ODE: STRUCTURE: L`-SPodFiOumSperfluoro-1-oclanesuffonate. N" OKNFA THK R"NTN jo ANI LOTNUMBER; CAuSmHes ~LPFOS0405. ease Not avaliable M`OCOLNECCEUNTLRAARTFIOORNM:ULA: SHEHICAL PURITY: LASTTESTED: prsssort ERXEPCIORMYMDEANTDE:ED STORAGE: CF,SO;Na S50o+h2.5 pgm 0172012008 (LC/MS/MS) SSttorbeilayt 4stCoiporsogtoencfgtreodm ight MOLECULARWEIGHT, 622.11 SOLVENT(S) Methanol DETAILS: + + + OSUninceuecprlrtouadriuenctcIosunnthfaemibmmibaegxyduioNmuMusmRscy('onFms) bised rlativ uncertainty of welghs and volumes AMLlRvMeMSlgoh(ntTsiCoanandnsdvsmohlaouswmsienssgpaorLcoItPturFmaO)cSedaabatlageroaeatNcaIhrSehTda,nse9o8%Figpuurrety1 and the absence of common Impurles are shown n Fgura 2 ADDITIONAL INFORMATION: additional Information is required please contact Wellington Laboratories (www.welkiabs.com). |i PNOTOETNTFIOARLLHYUTMOAXNIICDTROUHGUUMSAENS =2xR | comin, RE. owe pn > | 5.6 Gitlm < || me Wellington Laboratories Inc., 345 SouthgaDtre. Guelph ON N1G IMS CANADA LPFOSONOS (1 of) | i S p--T == @) Accustandard, Inc. Z < CERTIFICATE OF ANALYSIS ptt as=epi "EE Lor. saoioots (CATALOG NO. PFOA-001S DESCRIPTION: Perfluorooctancicacid EXPIRATION: Jan 10, 2018 a sow; SMoonorkovers for aon catfcation informatione . e fa o emppconneern)t - ase puiye pRrapao red . -- GMAT [-- . MFG ot1070(pgzimsl) me(g/mL) . {a bn Hi Fsg.RBed pie, Seed [---- ng Ltaey i cs lno.ycom rns EAwehighC eeoscd rFs i rf Snsetee.c | FE a os TTbIabieissp, e: ee 8who ila. | iretvo encryoOp TE 0dt 80 i nz vasLp @ Acycustandard, Inc. C[ai | ensuite CERTIFICATE OF ANALYSIS [WE DESCRIPTION: Perfluorooctanesulfonicack) EXPIRATION: AinEiE If souvenfto,n Ss MeeoorHw eversefo adlonal cartfcation formation. Comers [Lr ---- imaast MFG eiod(usgemLo) F po m Topte pared we 046.53 fb -- wos(ng/mL) | Eaa y, St | ES 7%, : ' a HB | - | II | f : ! Fos Acvt s 3.coma pie | A AaimdsmeinustikGoh ns Elf AANA ARASH T CAnght Caytty PpepdCCoomceattn I a i era wb be deen] ! This product was manufactured 1o mea! the quality system requirements ofISO 8001:2000 and ISO 17025 hg Inlet Method Report HLoatshtoMdotFiileirod: Petnteas p.13 Masslymx 4.1 CT1od\ nasdH ey, a NPoFvOeAss .beBrROa \3A3,CQL U3D0B0\6Py F1O0N1I2T\ 3e180t.3 Mountain Standard age Time 1 of Wodnesday, Novesber 29, 2006 10158153 Yountadn Standard Time Waters Acquity 808 Wathod CSSooomllmvveeennnttt: SSeelleeccttiioonn A8:: BAZL SiLooglvhvePnrPtersesNsuasrmueereAL:iLniinMtie:tt:ha0n1op5ls0i00 pai SSSouuliivtteeenhht21::MemXNeoo CCB:hhaann0.gg1ee% aq Formic Acid CSSauhaialtretWnaOsu3h1t: N1:o3.0SCyrsaAtniegnae Pressure CSShiyaosrwttenROautPtereD2s1astuaz3e8chDaancnaelC:hanYneesl: Yes NS3Aer8'ciDunDamaatirtlayaatACCohhraaPnnrnnAeeosllsP::urreesYTeosssuDraetaDCahtaannCehla:nneNlo: No NDDeaecgiuammsaisrleyartBoPrPrerBsossuPsrrueaessDuaDztaeataCDhaCathnaannenCleh:la:nnNeNolo: Xo 31t.7TGirn1Iaen0dii.(to0ain0iant)l0T.a0P3b.l0l30oe0u]010R0a8.t06e.(0n0i20/0'n.Si0n)IniWtAia8l8 Curve R3.im3E0v0e1nts0:13y0e0s80.5 20.0 Waters Acqulty Autosaspler Method TTCooomsondpanOAth.p:etaido:n: DiFsualblleLdoop HWLoaeaaapkkofWWaaissihhneVS:oolluvDmeisns:tablN1ae0m0e0: uWlater TSSattrrrgooenntgg Cotten HCTHaeoasmlshpuhemVrnSooalltTuvuememrenpe:terAaNl1taa0um0rre0me::BulaW.naOdtE:eErCDisabled TaSaa1rm}gpelteLoToSepemmpopevlreeartfTuoirrlpelerAFalatcautrromer::Ban11d.5;0.0DiCsabled NSPyorrooid-nlagseepiPzlbaartcaeewneRAnartte::Ga2p.5:00 2.0 FCSSooRaslbmtuipmelannestpTTieeTrmmeapppteeeerrcaaattAtuluurxrceeeGaDDpaDa:tatataa3.CC0hhCaahnnannneenlle::l: NNooYas . B SSSaiummlpptlloeen OP1r:rgeaNsnosiuzrCehearnagTete.ampeCrhaantnuerle: DaYteas Channel: Wo SSuuitcteenn 32!: NNoo CChhaannggee | CCSSowahTimautpsmclnheouTT4t:ee:mmNppoSaAMlCmaahprralmane::gePDDrieisssasabublrleeedd || enRdunofEveRnetpso:rtyes | ps FQiu:atio PromoCTiuMnaesPsaLryammePtFeOrAsPROACQUDpBIPrFOAyIPR Page 101 Printed: Wodesday, November 2,200 11:0:15 Nuria Standard Timo US AU | . n rel rie f ne Fan TBeBeeterscan ESSates aa EEnSamass hSeatass fiat] `Source(ES-) iSettings Ta Roadbacks : Cone(V) 20.00 26.25 f`EoSxtcraacntosr((V1)) 5ot.hao00 574 11 DSeSsoeatlrmvvaaattnioonnHGoToewmp(FeLirHa)tu(rUeH()C) 3Ei0S0 204 JOirh RReesnoauittoonn Sau3teings Readbacks lGeolamneos faGo i1 FEiixr RRuessttoonn i23s 2 fWoniEnnoo i3 ws I `Syringe Pump Flow (uLimin) 500 ! eso) Pressure Gauges 5003 | HMeux Contguraton Sindars | SouercorTaWAsVE Parameters | GolnsondCol TAVE Parameters p15 Exporiment Report MassLynx a1 File: cimasslynxiploa.prolacqudblpfosiong.exp Printed: Wodnosday, November 29, 2000 10:56:00 Mountan Standard Time Pago tof 1 CrNoaamtoon Timo VIenrssiiuomnenNtumKbeenriier CDaulabtaotno(nmFiin)ename `NSucmvbenetrDOelfaFyuDnicveirntsValve Enabled WDeefdeu2t0NExopve2ri0m0e8nt07:02:14 11020 C0lassLynxHexachorophenePROWCQUDBIPEG100306 cal 1 Function : MRMof mass pals, Time 0.00 to 12.00, ES- TloyneWad EwS.R Inter ChannelDelay (sec) 0.010 InterScanTime (sec) 0.010 Span (Da) 00 SEtCnadhrTtTiPimmmioe((D(rami)inn))Dau(Da) Dwel(s) 01020 Cone(V) Col(eV) Dely(s) 21 4411227700 2316889%0 00330000 22000000 11080000 00001100 43 441843700 370999900 00220000 62000000 41000000 00001100 5 49800 980 0.400 6000 4090 0010 i : ~ 3 . 3 lo . 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