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3 Golambia Analytical Services"
Created with Analy1Reporter Printed: 15/02/2010 2:34:00 PM
Quantitative Peak Review
K1000911-013
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315130C2-P7F0H0XA0a
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Page 99 of 265 157
8 Solum Analytical Services
Created with Analys2t Reporter Printed: 15/022010 2:34.00 PM
`lonRatio Confirmation
K1000911-013
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Page 100 of 245 138
4 ACnoalluymtbiciaal Services
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8 fohumbi Services:
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Page 104 of 242
PAS Columbia Analytical Services"
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Printed: 14/02/20106:41:00PM
lon Ratio Confirmation
K1000911-014
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Page 101 of 245 13
PAS SolubleServices"
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Printed: 15/02/2010 2:34:00 PM
RCSUmmary
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Page 103 of 245 145
4 Anoalluymtibciaal Services
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O Before OJ After
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Page 104 of 245 146
4CAonlaulymtbiciaal Services
Created with Analyspi1R1eporter
Printed: 14/02/20106:41:00 PM
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Page 106of 242 147
8 Solumbia A
Analytical Services
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Printed: 14/02/2010 6:41:00 PM
RCSummary
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Page 108 of 242 149
4 Solmbia
Analytical Services
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K1000911-015
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Page 105 of 245 151
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Page 107 of 245 153
[8 lmbia AnalyticalServices"
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Page 108 of 245 154
Columbia LS Roti services:
Created with Analypst.1R9eporter Printed: 14/02/2010 6:41.00 PM
Project
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Instrument Name__ API5000
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Page 110 of 242 155
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Page 111of 242
156
3 Solus Analytical Services
Quantitative Peak Review
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312200 No | 214238) 1980500 No | 138165017) No
600
No | owas
No
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28001 no | 03032) ves
st0s700 No | moze
No
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No | 000015)
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1 vo | owe1 | te 118220 | No | 33400186) No
wee | No | 027032)
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Page 117 of 242 166
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Page 114 of 245 168
PAY i ColumbiaP
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Page 115 of 245 169
4AnSaollyutmibciaal Services-
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Page 116 of 245 170
L850 Ssoleumrblvaices
Created with AnalyS:3R5eporter
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Page 121 of 262 174
3 AlnaulymticialServices"
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|
|
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|
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Page 12201242 179
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Page 124 of 262 181
Columbia
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4 Golam Analytical Services
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Page 121 of 245 183
4 Skmbia Analytical Services
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Page 12201 245 184
Columbia 4 Analytical Services
Created with Anahi4R9eporter Printed: 15/0212010 2:34:00 PM
`Quantitative Peak Review
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Page 123 of 245 185
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Page 124 of 265 186
5 ambi Analytical Services
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Page 133 of 245 187
Lo Smbia AnalyticalServices
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Page 134 0 245 188
Columbia 4 Analytical Services
Quantitative Peak Review
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Page 136 of 245 180
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Page 13701242 104
4CAnoalluymtibciaal Services:
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Printed: 14/02/2010 6:41:00 PM
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4 Solumbia Analytical ServicesTM
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Project Data File Result Table Instrument Name
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Page 1101262 221
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Acquisition Method _prCiinetoxtong dam
ARlegosriathTmavUissed nCtEeEliTQuOanSamoensg ab Instrument Name__P1 5000
[SempleName TP2C26a1o0p6m2256 7 I
[sampeo | PLFoCvKsizneetseaxong dart [Ditwion Factor [100
|
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Results Summary
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2771300
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Page 15 of 262 25
4 Solum Analytical Services-
Created wih Analyt9R0eporter Prined: 14/022010'6.41:00 PHA
`Quantitative Peak Review
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Page 16 of 242 22
A Columbia sora
PriCnrteead:ted14w1i0t2h2A2n0a1l0ys6t:p49R1e:1p00orPeMr
fon Ratio Confirmation
-
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Created with Analystp5Re2porter Printed: 14/0212010 8:41:00 PHA
DaPrtojaecFtile
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Acauisition Method __PFCKnetextong dam
Result Table Algorithm Used
2I0n8t1e0l8iaQumapnIesLong rab
Instrument Name __API 5000
[Sample Name TPC 05ppb
[injection Vial ___To
1]
Acquisition Date 2/8/2010 6:30:24 PM
[InjectionVolume [5]
[Samp|lcPuFeCsiiznse>t5e5xLong dam
Sample Type [Standars
[sampleComment |~~ [WeighttoVolume Joo
|
Results Summary
nate |Anaiyie RT
roa | Ante | ExpConc | Gale. Cone| Accuracy
Name (Erpeciaq|y `Shame | 1sarea |AR
[pron1 | 137 | 16 acP) ron|asssaoo| sos
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| oso | oss |
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|
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6 | No
[PRUNAT | 412|01C0PF6UN)A | tesa| 75138 | 0500 | oan | 82 | No |
PFDS1 | 4134.10)| 13C.PFOS| 6831100 | 378480
No |
| PFDOA1 | 477(|143C6-P3FD)OA| 197730 | 59384 0s00 | 0518 104 No |
I[Prim1 | s29s1e | 1ice|roamomon| 4mm | oso | oss |e m3e| d he
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4 ASnaolyltuicmal Services
Created with AnalystR9e3porter Printed: 1410272010 6.4100 PM
RCSummary
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259
50.25
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2)
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1
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Page 19.01 262 20
4 ASnoalluymtibciaal ServicesTM
Created with Analyspt 9Re4porter Printed: 1610212010 6:41:00 PM
Quantitative Peak Review
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|
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250
Page 20 of 242
La Sumbia
)Analytical Services
PrCinrteeadt:ed14v1i0t2h2A2n0a1l0ys6t:41f:0o0rPeMr
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51P3F0D2A629D0a BaseclMiisnseed
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663P0/E1T69A20 0a BaseolMiisnseed
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Page 21 of 242 2
4 lambs Analytical ServicesTM
Created with Analyspt.R9e6porter Printed: 1410222010 6:41:00 Pt
DPraotjaecFtle
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Acauisition Method _PFCKinelextdoanmg
ARlegsuolrtitThamblUesed 0I2ne0l6i7Q0u5aanmpiesLong db Instrument Name __AP15000
[SampleName [Pe Top
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2812010 6:37:56 PV
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[Sampled [iPoFuCisizneetesxcLong dam
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[SampleComment || Weightto Volume [000
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nNaamtee
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| 1aa|nncarrnon|
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PENAT | 2310.4|7 13CPFNA| 220300|za0|ttsow0| oss | ss | Ne
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PFOA1 | 3.92034| 13CPFDA | 2118100| 222700 | 1000 | to20 | 102 | No |
[rum1 | 412008| acorUna | tsste0| asm
2 | Nn |
[PFDS1 | 4120410)| 13cPFOS | esso30|0 sooss|0 1000 | 100 108 No |
PrDoA1 | 47 | 19GP5 rDoA |d zaam0| rz| tom | oss | wm | No | PRAT | saws| 1aCerdon | woo| sz | tow | tem | me | we
PFTeA1 | 574(574| 13CPFDOA | 234070 | 58420 | 1.000 0.928 93
No
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Pa22g0f2e42 252
5 Solmi Analytical Services
PriCnrteead:ted14w1it0h2A2n2a0l1y0st6:R4e1B:0b0rtPeMr
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e Anatye peak Name e || Rimee s !| Ae
|proaz
1.35 (1.36)
70
[s.rron
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[oraz
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[5.1.0
[ T ae
2000
| PFOS 2
II'ss 13ceros
| 2300283
228880
231283 | 6650300
PFDA2
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29896
wee
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| at3@0s | e1151
[Se_r1o3sC2-PFUNA
| ars
155180
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|
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42824
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24
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237
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8.98
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013
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023
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0.87
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| No
01.3e 830 d1
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| we
033
|
Page 23 of 262 233
8 ASnlaulymtbiciaal Services
Created with Analys9t 8Reporter Printed: 14/0212010'6:41:00 PHA
`Quantitative Peak Review
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Tozm PFC1.0ppbery oT
1 : A iIno A | a-
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41137C.-0P37F2O0A0a Baseline Missed |
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461830C4-2P3F0NADa Baseline o Missed
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499P0F1O80S01 Da
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61135C0-1PF6D9o0.A0a oc Baseinec Missed
713.P0F6T6E9A.01 Da
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0 Before 0 After
234
Page 24 of 262
Columbia LS Ss services
Created with Anaiysx P&Eponer Printed: 1410212010 6:41:00 PM
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=T
ARAN 'A
Tl Il =
4130P/F3O6A9.20 Da
463P0F1N2A120 Da
459P.F0O9S920 0a
513.P0F26D9.2A0 0a
_BWarsoenglcMPieiasnkseed | c BWaisonegolPMieiasnkseed |<B=aWsroenglcPMieiasnkseed |<BWarsoneglcPMieiasnkseed
| 4 og fg fo 1
563P.F01U2I6A902 Da
509P.R01O9S92. 0a
613P0F1D6OA802 0a
563.P0F/T16I9A.Z0 0a
BaseWlrionneg PMeiasksed | BasWerlionnegcPMeiasksed | c BasWerlionnegcPMeiasksed | c BWasreloinnegcPMeiasksed
3
iT
713P.E01T6A29.00a B<asWerlionneg PMeiasksed
O BeforeOJAfter
Page 26 of 242 25
4 Solana Analytical ServicesTM
Created with Analy AS1P00oner Printed: 14102120106:41.00 PM
Project
Evan's Poec PFCs
Data File
0208100\CalLong vif
Acquisition Method _PFChinetexLdoanmg
Result Table 0208108amplesLong ab Algorithm Used InteliQuan Instrument Name__API 5000
[SampleName--TPFCSOppb _____ [imectonvial [5
|
[AAccqquuiissiittiioonnDMaettehod _||P26F20C10k64n52c6PlMexCo||nSiganjmepdcltieoaTnVymopelume [5
|
[Sample
TLCMS285D
[DilutionFactor [100
[SampleComment|
|weighttovoume [000
|
Results Summary FNnaamlyeie || A(EnxpaectieRdsT) | SN-- avos | AnAarievsie | ExgpiClon)e|| Ca(incgiCmotn)e|| Acc"auyrac||y M9? [Prot | 1asia|e raceroa | arestoo| estes |so | saw mo| ss No | [Penat | 230242| 1aceENA | 215460|0 1218400 | soo | ase | ss| No [Prost | 23@sy| raceros [erento | aoso|o sow |sie | 103 | No |
[proAt1 | 3.3433|4 1acproa | 211150|0 toat80|0 so00 | 4700 | sa | no |
PFUNAT | 4.12406| 13CPF|1U72R74A0 | 848100 | 5.000 5.130 04 | no |
[Prost | 413410)| 13cprOs | 676110|0 3ss7300 | 5.000 PFDOAT | 4764.63 | 13C-PFDOA | 139680 | 578350 | 5.000 PFTA1 | 5296.14)| 13C-P|F1D99O68A0
[P[FPFTreeAatt|| S5767.764 ||51133.cC--7pPFFDD4ooa||1919s638608||0 227768534000 || S0so0oo0
5060 01 | ne
530 | 106 | no | ss | 16 | No | || 5s1s%o |11404 || MNeo ||
7
AeA
[Zaid
Sialic
Pa26gof2e62 23