Document K2zwdaRa3Bn2w8V4RbDYXEGQ
' REQ 41220
AR226-0265
R. Howells
GC/MS analyses of these samples were accomplished usinag 25m X0.32 mm HP-1 GC column to introduce the samples into the Finnigan SSQ-70 mass spectrometer. The sample components were ionized
ruastiengofc1h0emdiegcraeleisopniezramtiionnutwei.thTmheetrheasnuletsasofthteherseeagaennatlygsase.s TcohmebGinCedcowlituhmnthweiarscooprerreastpeodndfirnogm4GC0/tFoI3D0a0reCa ata percents show the following:
A PT I `ompon:
N.R. N-EtFOSE Lot
W.R. N-EtFOSE Lot 547
lorsonmoowns olnouo s n|
lomsonmo{ouns o|nimo s r|
lomsomes
Lome Lows |
lemsonmoocwsm| an xor|
lomsonme[on an cnano s s|
lomsoseoe menc lowrs a|
lorssonem one s e|nwwor|
lomssonao[ocmemelnowor| lorsoneaJc onm e e|n.os|
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' [Component ID.
ettcstounites Become --
11276 |N-MeFOSE Lot
lomsonomon|e0non|
lersoommscrsconosomealnnosesne||
PE N-MeFOSE_ CgF17S02N(Me)CH2CH20H
83.88%
olmsoonowsn sompnc[ognuusnon||
loswnpse
[i]
dtFeruisrfitlghuenorerodwatocoertkiinchvaeanssthbiyegdearntietddehoe(npeToFtbeAynAtG)iCaalnopdnraotgbhaleisenemwssiattmhhpatlBecSsoAuwlh(diobceghioivvneevtrohllevoeotskreidmdeerbtihyvyaltsiizlaytliootnohefrtsh).e Tahlicsohwoolrs kwistahs
dAPermreiilvdiaemtiiunznaecddyewrritethshuelTCt-sF3sAhAaolwscohthohoawltspatenhaaaklyizninwgidteherEaXngFeOmSaEteurnidaelr.ivHaotwiezvederc,oualndalhyizadinenyagostnihegenmisfeaitmchaeontmdaatomefroainuaanlltytsoihfst.hNa-eEbGeFaOnS
fbiyptehcetedderbievcaatuizseeod Cf-t8healncuohmoble.rTohtfedainBfyfSeEArXeFdnteOrSciEov-mactphiolvneoerhniatdssenitonhtattbheeiesnparmeepvslaeela.utaitTnehdtehyeesrsa,ambmeuptsloesriitmsoiflnaoprrw`opcbrolomebplmlesemtwsieallrlyemmoasked
likely exist with MeFOSE and will be even more complicated in the analysisofMeFOSEA.
st
702493
003107
--
' REQ 41343
J. Grant
uisnitnrogdcuhcGeeCmti/hceMasSlaiamonpnalilezysasteiisnotnoowftiththeheFsmieenstnahimagpnalneeSsasStwQhe-er7re0eamacagcesonsmtpslgpaiessc.hterTdohmueestiGenrCg.acToh2le5ummsnamXwpal0se.3oc2poemmrpamotneHedPn-t1s wGeCrecofolnuimpend.to
rate of10 degrees per minute. percents show the following:
The
results
of
these
analyses
combined
withthircorrespondfirnogmG4C0/tFoI.D30a0reCa. ata
Component 1D.
PrWecRutN-EFOSE
|WR. N-EFOSE `main cut
ocrmeconmmn osname
97900-112-1
Jens [ine
| ins 97900-1122 | age |
ossormo[e uw cnpwon|
Fp --
loans [oe |
lomsonme [inne cn louos r|
l eo om ss oo ss mm o[woo niesm oo n [laaewo o ss n n|| l eroo s _ncusos neuco reronsmolLl oien ossuemrwueos ] r|
`Component 1D.
NR N-McFOSE BP.132 97900-1072
003108
ome13n7 possivy oSpnE momn[p[euososxn|] nar csoavecneron
crssoNecczon
osovomicn|epnon| l[ osers py]
Component LD.
yeti (ecto:
'W.R. N-EtFOS
Amide
loss| 97900-111
f[ omsonen 0|
oE so E [py |
NEFOS Anite (uFrsONE:
lass|
`numerous other impurities of most homologs
thatinclude hydrides, chlorine in the backbone, and unidentified high boilers
003109