Document Jvd08qp0wR9qB58NnzMZqnnYv

APPENDIX I PROCESS EQUIPMENT FUGITIVE RELEASE DATA AND CALCULATIONS SARA TITLE III, SECTION 313 1990 TOXIC CHEMICAL RELEASE INVENTORY LAKE CHARLES REFINERY SAL 000004284 Process Equipment Fugitive Release Process equipment fugitives were estimated as follows: 1. Obtained attached fugitive equipment VOC emission data from 1989 FORSITE Corporation fugitive emissions survey and 1990 changes to 1989 data. 2. Divided die total VOC by the number of "major" streams for each unit. Heavy streams contributing little to total VOC and have no 313 reportable chemicals were factored out. (See attached "major" streams.) 3. Multiplied the VOC per stream by the liquid weight fraction of the specific chemical. (See Process Stream chapter) 4. All relief valves servicing streams with toxic chemicals were considered to be tied into flare system. Process drain emissions were estimated as follows: 1. Obtained attached process drain VOC emission data from FORSITE Corporatation. 2. Assumed 1989 composition. (See 1988 and 1989 documentation) 3. Used Raoult's Law and the liquid weight fractions to estimate release of specific chemicals. Cooling tower emissions were estimated as follows: 1. Used cooling tower circulation rate and AP-42 emission factor to calculate total VOC emissions. (See 1988 Documentation and Emission Factors chapter) 2. Assumed 1989 composition to calculate release of each chemical. The emissions calculations were placed on computer spreadsheets. These spreadsheets are attached. 000004285 SAL GRAND TOTAL FUGITIVES BY UNIT M3 CTU & VAC M2 CTU #4 HDS #3 CRU & HDS #1 COKER M2 COKER GRP #6 HDS FCC FEED PREP FCC UNIT M2 CRU & HDS THERMAL CRACKING CASINGHEAD (pbc) MOLEX L-SHAD & L-VHAD TANK FARM M7 HDS #5 HDS BNZ ------ COMPOSITION LOSS (TAR.) TOL ETB XYL -- - - - ------ ...... CYHX CUM ............. PCUM ............. NAPH .......... 0.456 0.360 0.183 0.641 0.018 0.009 0.055 0.043 0.014 0.156 0.687 0.058 0.143 0.032 1.855 2.196 0 0 0.740 0.573 0.312 1.975 0.720 0.363 0.403 0.040 0.043 0.528 1.625 0.232 0.505 0.030 0.795 7.696 0 0 0.098 0.076 0.041 0.631 0 0 0 0 0.012 0 0.451 0 0 0 0.212 1.904 0 0 0.394 0.30S 0.166 2.076 1.171 0.590 0.655 0 0.057 0.978 1.482 0.377 0.279 0 0 8.948 0 0 0.710 0.550 0.299 0.200 0.180 0.090 0.100 0.070 0 0.195 0.515 0.058 0.279 0.0S3 0 0.521 0 0 0 0 0 0.682 0.180 0.090 0.100 0 0.018 0.998 0.486 0.058 0 0 0 3.365 0 0 0 0 0 0.170 0.540 0.272 0.302 0 0.008 0.606 0.121 0.174 0 0 0 1.565 0 0 0.592 0.458 0.249 0 0 0 0 0.040 0.026 0 0 0 0.075 0.030 0.318 1.565 0.068 0.117 SAL 000004286 LAKE CHARLES FUGITIVE EMISSION LOSSES PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR. ) BNZ TOL ETB XYL CYHX CUM PCUH NAPH STY REG. GASO. 1.8 9.1 2.2 10.6 BO 4.3 2 BO BD TANK FARM 26.09 0.47 2.37 0.57 2.77 0.00 1.12 0.52 0.00 0.00 TOTAL GRAND TOTAL (LBS/YR) 26.09 52180 0.47 939.2 2.37 4748. 0.57 1147. 2.77 5531. 0.00 0 1.12 2243. 0.52 1043. 0.00 0 0.00 0 PROCESS VOC LOSS COMPOSITION (T/YR.) BNZ COMPOSITION LOSS (T/YR. ) TOL ET8 XYL CYHX CUM PCUH NAPH STY U.L GASO. 2.5 6.1 1.6 7.7 BO 4.3 2 BO 80 TANK FARM 26.09 0.65 1.59 0.42 2.01 0.00 1.12 0.52 0.00 0.00 TOTAL GRANO TOTAL (LBS/YR) 26.09 52180 0.65 1304. 1.59 3182. 0.42 834.8 2.01 4017. 0.00 0 1.12 2243. 0.52 1043. 0.00 0 0.00 0 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR. ) BNZ TOL ETB XYL CYHX CUM PCUH NAPH STY SUL GASO. 2.8 9.8 2.5 12 BO 4.3 2 BO BO TANK FARM 26.09 0.73 2.56 0.65 3.13 0.00 1.12 0.52 0.00 0.00 TOTAL GRAND TOTAL (LBS/YR) 26.09 52180 0.73 1461. 2.56 5113. 0.65 1304. 3.13 6261. 0.00 0 1.12 2243. 0.52 1043. 0.00 0 0.00 0 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR. ) BNZ TOL ETB XYL CYHX CUM PCUH NAPH SOUR CRUDE 0.23 BO BO BO BO BO 80 BD #3 CTU & VAC 9.87 0.02 0.00 0.00 0.00 0.00 0.00 0.00 0.00 TOTAL GRAND TOTAL (LBS/YR) 9.87 19740 0.02 45.40 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR. ) BNZ TOL ETB XYL CYHX CUM PCUH NAPH SWEET CRUDE 0.32 BO BD BO BO BO BD BD UZ CTU TANK FARM 7.64 26.09 0.02 0.08 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 TOTAL GRANO TOTAL (LBS/YR) 26.09 52180 0.08 166.9 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 SAL 0.00 0.00 o0000^2fl7 PROCESS VOC LOSS COMPOSITION (T/YR.) BN2 COMPOSITION LOSS (T/TR.) TOL ETB XYL CYHX CUM PCUM NAPH FCC GASO. 0.8 2.7 BO 5 1 5.1 3.1 BD FCC 19.57 0.16 0.53 0.00 0.98 0.20 1.00 0.61 0.00 TOTAL GRAND TOTAL (LBS/YR) 19.57 39140 0.16 313.1 0.53 1056. 0.00 0 0.98 1957 0.20 391.4 1.00 1996. 0.61 1213. 0.00 0 PROCESS VOC LOSS COMPOSITION (T/YR.) LSR GASO. COMPOSITION LOSS (T/YR. ) BMZ TOL ETB XYL CYHX CUM 3.2 3 80 BO 5.2 BD PCUM NAPH BO BD NO. 3 CTU & VAC NO. 2 CTU NO. 4 HDS MOLEX NO. 6 KOS NO. 2 CRU l HDS 9.87 7.64 4.16 1.02 1.36 7.16 0.32 0.24 0.13 0.03 0.04 0.23 0.30 0.23 0.12 0.03 0.04 0.21 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.51 0.40 0.22 0.05 0.07 0.37 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 TOTAL GRAND TOTAL (LBS/YR) 31.21 62420 1.00 1997. 0.94 1872. 0.00 0 0.00 0 1.62 3245. 0.00 0 0.00 0 0.00 0 PROCESS VOC LOSS COMPOSITION (T/YR.) BNZ COMPOSITION LOSS (T/YR. ) TOL ETB XYL CYHX CUM PCUM NAPH REFORMATE 5.4 15.2 5.3 16.7 BO 6.8 1.7 BO NO. 3 CRU & HDS NO. 2 CRU & HDS 10.03 7.16 0.54 0.39 1.52 1.09 0.53 0.38 1.68 1.20 0.00 0.00 0.68 0.49 0.17 0.12 0.00 0.00 TOTAL GRAND TOTAL (LBS/YR) 17.19 34380 0.93 1856. 2.61 5225. 0.91 1822. 2.87 5741. 0.00 0 1.17 2337. 0.29 584.4 0.00 0 PROCESS VOC LOSS COMPOSITION (T/YR.) NAPHTHA .. NO. 3 CTU & VAC NO. 2 CTU NO. 4 HDS NO. 3 CRU & HDS NO. 2 CRU & HDS TANK FARM 9.87 7.64 4.16 10.03 7.16 26.09 TOTAL GRAND TOTAL (LBS/YR) 64.95 129900 BNZ COMPOSITION LOSS (T/YR..) TOL ETB XYL CYHX CUM PCUM NAPH 1 4.5 1 4 2 BO BD BD 0.10 0.08 0.04 0.10 0.07 0.26 0.44 0.34 0.19 0.45 0.32 1.17 0.10 0.08 0.04 0.10 0.07 0.26 0.39 0.31 0.17 0.40 0.29 1.04 0.20 0.15 0.08 0.20 0.14 0.52 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.65 1299 2.92 5845. 0.65 1299 2.60 5196 1.30 2598 0.00 0 0.00 0 0.00 0 PROCESS VOC LOSS COMPOSITION (T/YR.) 8NZ COMPOSITION LOSS (T/YR .) tql ETB XYL CYHX CUM PCUM NAPH $AL KEROSENE NO. 3 CTU VAC NO. 2 CTU NO. 4 HOS TANK FARM MOIEX TOTAL GRAND TOTAL (LBSAR) 9.87 7.64 4.16 26.09 1.02 48.78 97560 BD BO BO BO 80 BO BO 3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.30 0.23 0.12 0.78 0.03 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 1.46 2926. PROCESS VOC LOSS COMPOSITION (T/YR.) DIESEL NO. 3 CTU VAC NO.2 CTU NO. 4 HOS NO. 5 HOS NO. 6 HDS FCC FEED PREP TANK FARM NO. 7 HOS 9.87 7.64 4.16 3.93 1.36 0.88 26.09 2.28 TOTAL GRAND TOTAL CLBS/YR) 56.21 112420 COMPOSITION LOSS (TAR. ) BNZ TOL ETB XYL CYHX CUN PCUH NAPH BO BO BO BO BO BD BO 3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.30 0.23 0.12 0.12 0.04 0.03 0.78 0.07 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 1.69 3372. PROCESS VOC LOSS COMPOSITION (T/YR.) BNZ COMPOSITION LOSS (TAR. ) TOL ETB XTL CYHX CUM PCUH NAPH CRUDE UET GAS 0.2 BD BO BD BO BD BO BO NO. 3 CTU VAC NO. 2 CTU NO. 4 HDS 9.87 7.64 4.16 0.02 0.02 0.01 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 TOTAL GRAND TOTAL (LBSAR) 21.67 43340 0.04 86.68 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 PROCESS VOC LOSS COMPOSITION (TAR.) BNZ COMPOSITION LOSS (TAR. ) TOL ETB XYL CYHX CUM PCUH NAPH COKER GASOLINE 0.1 4 BD 6.5 1 1 3 BD NO. 1 COKER NO. 2 COKER GAS RECOVERY PLANT 18.02 9.08 5.04 0.02 0.01 0.01 0.72 0.36 0.20 0.00 0.00 0.00 1.17 0.59 0.33 0.18 0.09 0.05 0.16 0.09 0.05 0.54 0.27 0.15 0.00 0.00 0.00 TOTAL GRAND TOTAL (LBS/YR) 32.14 64280 0.03 64.28 1.29 2571. 0.00 0 2.09 4178. 0.32 642.8 0.32 642.8 0.96 1928. 0.00 0 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR..) BNZ TOL ETB XYL CYHX CUM PCUH NAPH SAL 000004289 THERMAL GASOLINE GAS RECOVERY PLANT THERMAL CRACKER 5.04 5.8 TOTAL GRAND TOTAL (LBS/YR) 10.84 21680 14 0.05 0.06 0.20 0.Z3 0.11 216.8 0.43 867.2 BO 6.5 1 1 3 0.00 0.00 0.33 0.38 0.05 0.06 0.05 0.06 0.15 0.17 0.00 0 0.70 1409. 0.11 216.8 0.11 216.8 0.33 650.4 BD 0.00 0.00 0.00 0 PROCESS VOC LOSS COMPOSITION (T/YR.) SABINE HAD L-SHAD L-VHAD 5.3 TOTAL GRAND TOTAL (LBS/YR) 5.30 10600 COMPOSITION LOSS (TAR. ) BNZ TOL ETB XYL CYHX CUM PCUM NAPH STY 35 15 4 BO BD BO BD 6 10 1.86 0.79 0.21 0.00 0.00 0.00 0.00 0.32 0.53 1.86 3710 0.79 1590 0.21 424 0.00 0 0.00 0 0.00 0 0.00 0 0.32 636 0.53 1060 PROCESS VOC LOSS COMPOSITION (TAR.) BN2 COMPOSITION LOSS; (T/YR..) TOL ETB XYL CYHX CUM PCUM NAPH CASINGHEAD 1.9 6.7 BD 3.7 3.7 BO BD 1 CASINGHEAD UNIT 7.55 0.14 0.51 0.00 0.28 0.28 0.00 0.00 0.08 TOTAL GRAND TOTAL (LBS/YR) 7.55 15100 0.14 286.9 0.51 1011. 0.00 0 0.28 558.7 0.28 558.7 0.00 0 0.00 0 0.08 151 PROCESS VOC LOSS COMPOSITION (T/YR.) HTBE UNIT MTBE 0.44 TOTAL GRAND TOTAL (LBS/YR) 0.44 880 METH COMPOSITION LOSS (T/YR.) MTBE 10 90 0.04 0.40 0.04 86 0.40 792 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR. ) BNZ TOL ETB XYL CYHX CUM PCUM NAPH SLOP OIL 1.6 4.9 1.4 6.5 BO 2.15 1 BD FCC FEED PREP 0.88 0.01 0.04 0.01 0.06 0.00 0.02 0.01 0.00 TOTAL GRAND TOTAL (LBS/YR) 0.88 1760 0.01 28.16 0.04 86.24 0.01 24.64 0.06 114.4 0.00 0 0.02 37.84 0.01 17.6 0.00 0 SAL 000004290 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSSi (T/YR.) ETHY. PROPY 1,3 BUT. COKER WET GAS 1 7 0.1 NO. 1 COKER NO. 2 COKER GAS RECOVERY PUNT THERMAL CRACKER 18.02 9.08 5.04 5.8 0.18 0.09 0.05 0.06 1.26 0.64 0.35 0.41 0.02 0.01 0.01 0.01 TOTAL GRAND TOTAL (LBS/YR) 37.94 75880 0.379 758.8 2.655 5311. 0.037 75.88 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR.) ETHY. PROPY 1,3 BUT. SUS GAS 9 25 0.1 ACID PLANT 2.34 0.21 0.59 0.00 TOTAL GRAND TOTAL (LBS/YR) 2.34 4880 0.210 421.2 0.585 1170 0.002 4.68 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR.) ETHY. PROPY 1,3 BUT. FUEL GAS 3.6 5 0.3 BOILERS MTBE HEATERS TANK FARM 6.7 0.44 26.62 26.09 0.24 0.02 0.96 0.94 0.34 0.02 1.33 1.30 0.02 0.00 0.08 0.08 TOTAL GRAND TOTAL (LBS/YR) 59.85 119700 2.154 4309. 2.992 5985 0.179 359,1 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR.) ETHY. PROPY 1,3 BUT. B*B ALKYLATION CASINGHEAD IUNIT HTBE GAS RECOVERY PLANT FCC 8.77 7.55 0.44 5.04 19.57 BO 5 0.3 0.00 0.00 0.00 0.00 0.00 0.44 0.38 0.02 0.25 0.98 0.03 0.02 0.00 0.02 0.06 TOTAL GRAND TOTAL (LBS/YR) 41.37 82740 0 2.068 0.124 0 4137 248.2 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR.) ETHY. PROPY 1,3 BUT. P-P BO 66 0.3 SAL 000004291 ALKYLATION CASINGHEAD UNIT CAT POLY FCC GAS RECOVERY PLANT 8.77 7.55 12.09 19.57 5.04 0.00 0.00 0.00 0.00 0.00 5.96 5.13 8.22 13.31 3.43 0.03 0.02 0.04 0.06 0.02 TOTAL GRAND TOTAL (LBS/YR) 53.02 106040 0 36.05 0.159 0 72107 318.1 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR.) ETKY. PROPY 1,3 BUT. FCC TAIL 16 12 0.2 FCC 19.57 3.13 2.35 0.04 TOTAL GRAND TOTAL (LBS/YR) 19.57 39140 3.131 6262. 2.348 4696. 0.039 78.28 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR.] ETHY. PROPY 1,3 BUT. P-B BO 33 0.2 CRYO GAS PLANT GAS RECOVERY PLANT TOTAL GRAND TOTAL (LBS/YR) 8.33 5.04 13.37 26740 0.00 0.00 2.75 1.66 0.02 0.01 0 4.412 0.026 0 8824. 53.48 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (T/YR. ETHY. PROPY 1,3 BUT CRYO FEEO BO 8 0.3 CRYO GAS PLANT 8.33 0.00 0.67 0.02 TOTAL GRAND TOTAL (LBS/YR) 8.33 16660 0 0.666 0.024 0 1332. 49.98 PROCESS VOC LOSS COMPOSITION (T/YR.) CRYO TAIL GAS COMPOSITION LOSS (T/YR. ETHY. PROPY 1,3 BUT 15 7 BO CRYO GAS PLANT 8.33 1.25 0.58 0.00 TOTAL GRAND TOTAL (LBS/YR) 8.33 16660 1.249 2499 0.583 1166. 0 0 SAL 000004292 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (TAR. ) BN2 TOL ETB XYL CYHX CUM PCUM NAPH STY 0.32 0.77 0.19 1.2 0.56 0.12 0.12 0.15 0.15 COOLING TOUER 19.57 0.06 0.15 0.04 0.23 0.11 0.02 0.02 0.03 0.00 TOTAL GRAND TOTAL (LBS/YR) 19.57 39140 0.06 125.2 0.15 301.3 0.04 74.36 0.23 469.6 0.11 219.1 0.02 46.96 0.02 46.96 0.03 58.71 0.00 0.187 PROCESS VOC LOSS COMPOSITION (T/YR.) COMPOSITION LOSS (TAR. > BNZ TOL ETB XYL CYHX CUM PCUH NAPH STY 0.32 0.77 0.19 1.2 0.56 0.12 0.12 0.15 0.15 PROCESS DRAINS 546.60 0.79 0.56 0.05 0.25 1.42 0.01 0.01 0.00 0.02 TOTAL GRAND TOTAL (LBS/YR) 546.60 1.093,200 0.79 1,574 0.56 1,114 0.05 92 0.25 502 1.42 2,845 0.01 27 0.01 14 0.00 2 0.02 48 SAL 0000^2<?3 LAKE CHARLES PROCESS EQUIPMENT FUGITIVES 1. NO. 3 CTU & VAC EMISSION SOURCE NUMBER SOURCES DAYS ON STREAM 340 VOC NON(LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 1.88 9.31 0.30 FLANGES 1.42 PUMP SEALS: L. LIQUID H. LIQUID 0.77 0.63 COMP. SEALS 0.20 TOTAL 14.51 VOC (TPY/STREAM) = 9.87 # OF SARA STREAMS = 6 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) = 0.00 0.00 0.00 0.00 0.00 2. NO. 2 CTU DAYS ON STREAM * 354 EMISSION SOURCE NUMBER SOURCES VOC NON- (LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 1.75 6.24 0.26 FLANGES 1.12 PUMP SEALS: L. LIQUID H. LIQUID COMP. SEALS TOTAL 0.70 0.52 0.20 10.79 VOC (TPY/STREAM) * 7.64 * OF SARA STREAMS 6 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) * 0.00 0.00 0.00 0.00 0.00 3. NO. 4 HDS EMISSION SOURCE NUMBER SOURCES VALVES: GAS L. LIQUID DAYS ON STREAM = 336 VOC NON (LB/HR) OR LEAKERS 2.16 1.09 # OF SARA STREAMS = 5 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 SAL 00000429** 0 0.00 H. LIQUID FLANGES PUMP SEALS: L. LIQUID H. LIQUID COMP. SEALS TOTAL VOC (TPY/STREAM) = 0.09 0.75 0.25 0.23 0.59 5.16 4.16 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) = 0.00 0.00 0.00 0.00 0.00 4. NO 5 HOS EMISSION SOURCE NUMBER SOURCES DAYS ON STREAM = 338 VOC NON(LB/HR) OR LEAKERS VALVES: GAS L. LIQUID K. LIQUID 0.80 0.51 0.07 FLANGES 0.29 PUMP SEALS: L. LIOUIO H. LIQUID 0.00 0.14 COMP. SEALS 1990 MODIFICATIONS ADD 0.00 0.1256 (0.55 T/YR) TOTAL 1.94 VOC (TPY/STREAM) = 3.93 # OF SARA STREAMS = 2 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 VOC (TPY/STREAM) = 0.00 0.00 5. NO 3 CRU & HOS EMISSION SOURCE NUMBER SOURCES VALVES: GAS L. LIQUID H. LIQUID FLANGES PUMP SEALS: L. LIQUID H. LIQUID COMP. SEALS TOTAL DAYS ON STREAM = 345 VOC NON(LB/HR) OR LEAKERS 2.97 5.78 0.33 1.45 0.91 0.67 0.00 12.11 # OF SARA STREAMS = 5 LEAKERS TOTAL SOURCES VOC (LB/NR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0.00 SAL 000004295 VOC (TPY/STREAM) 10.03 VOC (TPY/STREAH) = 0.00 6. NO. 1 COKER EMISSION SOURCE NUMBER SOURCES DAYS ON STREAM e 329 VOC MON(LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 3.87 3.21 0.05 FLANGES 1.37 PUMP SEALS: L. LIQUID K. LIQUID 0.54 0.09 COMP. SEALS 0.00 TOTAL 9.13 VOC (TPY/STREAH) * 18.02 # OF SARA STREAMS * 2 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) = 0.00 0.00 0.00 0.00 0.00 7. NO. 2 COKER DAYS ON STREAM = 347 EMISSION SOURCE NUMBER SOURCES VOC NON- (LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 1.91 0.97 0.16 FLANGES 0.68 PUMP SEALS: L. LIQUID H. LIQUID COMP. SEALS 1990 MOOIFICATINS ADO 0.28 0.32 0.00 0.03881 (0.17 T/YR) TOTAL 4.36 VOC (TPY/STREAM) = 9.08 * OF SARA STREAMS = 2 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 VOC (TPY/STREAM) = 0.00 0.00 ;. GAS RECOVERY PLANT EMISSION SOURCE NUMBER SOURCES VALVES: DAYS ON STREAM = 345 VOC (LB/HR) OR NONLEAKERS * OF SARA STREAMS > 8 LEAKERS TOTAL SOURCES VOC (LB/HR) SAL 0000042 GAS L. LIQUID H. LIQUID FLANGES PUMP SEALS: L. LIQUID H. LIQUID COMP. SEALS TOTAL VOC (TPY/STREAM) = 1.25 5.96 0.22 0.95 0.91 0.44 0.00 9.73 5.04 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) * 0.00 0.00 0.00 0.00 0.00 9. NO. 6 HDS DAYS ON STREAM = 333 EMISSION SOURCE NUMBER SOURCES VOC NON* (LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 0.58 0.00 0.04 FLANGES 0.18 PUMP SEALS: L. LIQUIO H. LIQUID 0.14 0.08 COMP. SEALS 0.00 TOTAL 1.02 VOC (TPY/STREAM) 1.36 # OF SARA STREAMS 3 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) * 0.00 0.00 0.00 0.00 0.00 10. NO. 7 HDS EMISSION SOURCE NUMBER SOURCES VALVES: GAS L. LIQUID K. LIQUID FLANGES PUMP SEALS: L. LIQUID H. LIQUID COMP. SEALS DAYS ON STREAM * 328 VOC NON- (L8/KR) OR LEAKERS 0.86 0.00 0.03 0.21 0.00 0.06 0.00 # OF SARA STREAMS 2 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 SAL 000004297 TOTAL VOC (TPY/STREAM) = 1.16 2.28 VOC (TPY/STREAM) = 0.00 0.00 11. FCC FEED PREP. EMISSION SOURCE NUMBER SOURCES DAYS ON STREAM = 326 VOC NON(LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 0.21 0.13 0.01 FLANGES 0.08 PUMP SEALS: L. LIQUID H. LIQUID 0.00 0.02 COMP. SEALS 0.00 TOTAL 0.45 VOC (TPY/STREAM) = 0.88 # OF SARA STREAMS - 2 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) = 0.00 0.00 0.00 0.00 0.00 12. FCC DAYS ON STREAM 317 # OF SARA STREAMS = 4 EMISSION SOURCE NUMBER SOURCES VOC (LB/HR) OR NONLEAKERS LEAKERS TOTAL SOURCES VOC (LB/HR) VALVES: GAS L. LIQUID H. LIQUID 2.32 13.32 0.45 0 0.00 0 0.00 0 0.00 FLANGES 1.96 0 0.00 PUMP SEALS: L. LIQUID H. LIQUID 1.25 0.91 0 0.00 0 0.00 COMP. SEALS 1990 FCC MOOS 0.20 ADD 0.1712 (0.75 T/YR) 0 0.00 TOTAL 20.58 VOC (TPY/STREAM) - 19.57 I85388SSCI VOC (TPY/STREAM) = B888BS8888SS 0.00 0.00 13. CRYO GAS PLANT EMISSION SOURCE NUMBER SOURCES DAYS ON STREAM * 341 VOC (LB/HR) OR NON' LEAKERS # OF SARA STREAMS = 3 LEAKERS TOTAL SOURCES VOC (LB/HR) SAL 000004298 VALVES: GAS L. LIQUID H. LIQUID FLANGES PUMP SEALS: L. LIQUID K. LIQUID COMP. SEALS TOTAL VOC (TPY/STREAM) = 2.53 1.65 0.11 0.95 0.39 0.28 0.20 6.11 8.33 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) = 0.00 0.00 0.00 0.00 0.00 14. CAT POLY DAYS ON STREAM = 342 EMISSION SOURCE NUMBER SOURCES VOC NON(LB/KR) OR LEAKERS VALVES: GAS L. LIQUID K. LIQUID 0.89 8.05 0.23 FLANGES 1.03 PUMP SEALS: L. LIQUID H. LIQUID 1.11 0.47 COMP. SEALS 0.00 TOTAL 11.78 VOC (TPY/STREAM) * 12.09 # OF SARA STREAMS * 4 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) * 0.00 0.00 0.00 0.00 0.00 15. NO. 2 CRU & HOS EMISSION SOURCE NUMBER SOURCES VALVES: GAS L. LIQUID H. LIQUID FLANGES PUKP SEALS L. LIQUID K. LIQUID DAYS ON STREAM - 310 VOC (LB/HR) OR NONLEAKERS 2.40 4.49 0.27 1.16 0.56 0.54 # OF SARA STREAMS = 5 LEAKERS TOTAL SOURCES VOC (LB/NR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 SAL 000004 COMP. SEALS TOTAL 0.20 9.62 0 0.00 0.00 VOC (TPY/STREAM) = 7.16 VOC (TPY/STREAM) = 0.00 (SCS88S1S3SSS8SSSS55S55KISSS8SS 16. NO. 1 HOS EMISSION SOURCE NUMBER SOURCES DAYS ON STREAM = 0 VOC NON(LB/HR) OR LEAKERS # OF SARA STREAMS = 0 LEAKERS TOTAL SOURCES VOC (LB/HR) VALVES: GAS L. LIQUID K. LIQUID 0.00 0.00 0.00 0 0.00 0 0.00 0 0.00 FLANGES PUMP SEALS: L. LIQUID H. LIQUID 0.00 0.00 0.00 0 0.00 0 0.00 0 0.00 COMP. SEALS 0.00 0 0.00 TOTAL 0.00 0.00 VOC (TPY/STREAM) * ERR VOC (TPY/STREAM) * ERR SSSSSSSSS88SS8S8SZ838S88888SSS8S: 17. THERMAL CRACKER PAYS ON STREAM = 318 OF SARA STREAMS = 2 EMISSION SOURCE NUMBER SOURCES VOC NON(LB/HR) OR LEAKERS LEAKERS TOTAL SOURCES VOC (LB/HR) VALVES: GAS L. LIQUID H. LIQUID FLANGES PUMP SEALS: L. LIQUID H. LIQUID COMP. SEALS 1990 MODIFICATIONS 0.77 1.42 0.09 0.37 0.21 0.17 0.00 0.009 (0.04 T/YR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0.00 TOTAL 3.04 0.00 VOC (TPY/STREAM) = 5.80 VOC (TPY/STREAM) = 0.00 18. CASINGHEAD UNIT EMISSION NUMBER DAYS ON STREAM 348 VOC NON- # OF SARA STREAMS * 10 TOTAL VOC SAL OOOOO SOURCE SOURCES (LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 1.25 12.45 0.36 FLANGES 1.55 PUMP SEALS: L. LIQUID H. LIQUID 1.74 0.72 COMP. SEALS 0.00 TOTAL 18.07 VOC (TPY/STREAM) = 7.55 LEAKERS SOURCES (L8/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) = 0.00 0.00 0.00 0.00 0.00 19. ALKYLATION UNIT DAYS ON STREAM = 329 EMISSION SOURCE NUMBER SOURCES VOC NON- (LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 1.12 8.79 0.27 FLANGES 1.16 PUMP SEALS: L. LIQUID H. LIQUID 1.25 0.54 COMP. SEALS 0.20 TOTAL 13.33 VOC (TPY/STREAM) = 8.77 # OF SARA STREAMS * 6 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) = 0.00 0.00 0.00 0.00 0.00 20. TANK FARM EMISSION SOURCE NUMBER SOURCES VALVES: GAS L. LIQUID H. LIQUID FLANGES PUMP SEALS: L. LIQUID DAYS ON STREAM = 365 VOC NON- (LB/HR) OR LEAKERS 1.96 37.07 0.99 4.16 6.96 # OF SARA STREAMS * 9 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 SAL 000004301 H. LIQUID COMP. SEALS 1990 MODIFICATIONS 2.12 0.00 0.349 0.53 T/YR) TOTAL 53.61 VOC (TPY/STREAM) = 26.09 0 0.00 0 0.00 VOC (TPY/STREAM) s 0.00 0.00 21. ACID PLANT OAYS ON STREAM = 330 EMISSION SOURCE NUMBER SOURCES VOC NON- (LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 0.78 0.00 0.05 FLANGES 0.24 PUMP SEALS: L. LIQUID H. LIQUID 0.00 0.11 COMP. SEALS 0.00 TOTAL 1.18 VOC (TPY/STREAM) * 2.34 # OF SARA STREAMS 2 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) = 0.00 0.00 0.00 0.00 0.00 22. MOLEX OAYS ON STREAM a 274 EMISSION SOURCE NUMBER SOURCES VOC NON- (LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 0.30 0.41 0.03 FLANGES 0.13 PUMP SEALS: L. LIQUID H. LIQUID 0.00 0.06 COMP. SEALS 0.00 TOTAL 0.93 VOC (TPY/STREAM) * 1.02 # OF SARA STREAMS * 3 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) c 0.00 0.00 0.00 0.00 0.00 23. L-SHAD DAYS ON STREAM * 365 # OF SARA STREAMS * 1 SAL 000004302 EMISSION SOURCE NUH8ER SOURCES VOC NON(L8/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 0.00 0.85 0.00 FLANGES 0.14 PUMP SEALS: L. LIQUID H. LIQUID 0.00 0.00 COMP. SEALS 1990 MODIFICATIONS 0.00 0.018 iC.08 T/YR) TOTAL 1.01 VOC (TPY/STREAM) * 4.42 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 VOC (TPY/STREAM) * 0.00 0.00 24. l-VHAD DAYS ON STREAM = 365 EMISSION SOURCE NUMBER SOURCES VOC NON- (IB/HR) OR LEAKERS VALVES: GAS L. LIQUIO H. LIQUID 0.00 0.17 0.00 FLANGES 0.03 PUMP SEALS: L. LIQUID H. LIQUID 0.00 0.00 COMP. SEALS 0.00 TOTAL 0.20 VOC (TPY/STREAM) = 0.88 # OF SARA STREAMS = 1 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 O 0.00 0 0.00 0 0 0 VOC (TPY/STREAM) = 0.00 0.00 0.00 0.00 0.00 25. BOILERS EMISSION SOURCE VALVES: GAS L. LIQUID H. LIQUID FLANGES NUMBER SOURCES DAYS ON STREAM * 365 VOC NON- (LB/HR) OR LEAKERS 1.00 0.00 0.07 0.31 # OF SARA STREAMS = 1 LEAKERS TOTAL SOURCES VOC (LB/HR) 0 0.00 0 0.00 0 0.00 0 0.00 SAL 000004303 PUMP SEALS: L. LIQUID H. LIQUID COMP. SEALS TOTAL VOC (TPY/STREAK) = 0.00 0.15 0.00 1.53 6.70 0 0 0 VOC (TPY/STREAK) * 0.00 0.00 0.00 0.00 0.00 26. HEATERS DAYS ON STREAM = 365 EMISSION SOURCE NUMBER SOURCES VOC NON- (LB/HR) OR LEAKERS VALVES: GAS L. LIQUID H. LIQUID 0.00 0.00 0.00 131B 0 0 FLANGES 0.00 4854 PUMP SEALS: L. LIQUID H. LIQUID 0.00 0.00 0 0 COMP. SEALS 1990 MODIFICATIONS 0.00 0 TOTAL 0.00 VOC (TPY/STREAH) - 0.00 # OF SARA STREAKS 1 LEAKERS TOTAL SOURCES VOC (LB/HR) 32 1350 4.62 0 0 0.00 0 0 0.00 6 4860 1.13 0 0 0.00 0 0 0.00 0 0 0.00 0.331 6.08 VOC (TPY/STREAH) * 26.62 27. HTBE EMISSION SOURCE VALVES: GAS L. LIQUID H. LIQUID FLANGES PUMP SEALS: L. LIQUID H. LIQUID COMP. SEALS NUMBER SOURCES DAYS ON STREAK = 140 VOC NON(LB/HR) OR LEAKERS 0.00 0.00 0.00 0.00 68 187 0 918 0.00 0.00 0.00 0 0 2 # OF SARA STREAKS = 5 LEAKERS TOTAL SOURCES VOC (LB/HR) 0.07 0.71 0.00 0.12 0.00 0.00 0.40 TOTAL VOC (TPY/STREAK) 0.00 0.00 1.30 VOC (TPY/STREAK) * 0.44 SAL 000004304 PROCESS DRAIN EMISSIONS AP-42 FACTOR = .07 LB/HR PER DRAIN DRAIN COUNT FRACTION COVERED VOC (LB/HR) 852 0.0529 58.06 VOC (TONS/YEAR) = 254.31 ESTIMATED JUNCTION BOX EMISSION = .47 LB/HR PER BOX J.B. COUNT FRACTION COVERED VOC (LB/HR) 142 0 66.74 VOC (TONS/YEAR) = 292.32 TOTAL DRAINS EMISSION = 546.6 Emission factor estimated by R.D. Truelove end S. Cuthbertson COOLING TOWER EMISSIONS AP-42 FACTOR = .7 L8 VOC/MM GAL. WATER WATER FLOW GAL/MIN VOC (TONS/YEAR) 35500 6.53 SAL 000004305 FORSITE CORPORATION 1600 Pacific Avenue Suite 2620 Dallas, Texas 75201 (214) 740-0040 May 3. 1990 P-89229 Mr. Bruce M. Schroer Chemical Engineer PED Environmental 220-11 South Tower 1000 S. Pine Ponca City. Oklahoma 74603 Subject: Transmittal of fugitive equipment leak VOC emission data Lake Charles Refinery Dear Bruce: The enclosed Tables 1 and 2 provide a summary of the data that were used to estimate VOC emissions from sources of fugitive equipment leaks at the Lake Charles Refinery. The summary is based on the refinery-wide equipment count data tables that were submitted to the LDEQ in the March 22. 1990 Permit Correction - Equipment Leak VOC Emissions. We have now merged the new (1989) project specific equipment count with the 1988 process unit total equipment count provided by the Refinery. Please note that since the Refinery's monitoring contractor did not tag equipment in heavy liquid service during 1988. no actual unit specific counts for this equipment exist. For our summary, the total heavy liquid component counts are based on the refinery wide counts included in the 1986 Consolidated Permit (Permit No. 0520-00005-02). Please note that we allocated the heavy liquid equipment count to all process units based on the ratio of the unit's total light liquid component count to the total refinery equipment count. This is a conservative assumption that should not adversely affect the unit specific emissions since the emissions from this equipment accounts for less than 5 percent of the total fugitive VOC emissions. Any discrepancies in this allocation will be corrected later during 1990 as the heavy liquid components are tagged for each unit. 1 understand that you will use this data and calculation methodology in preparing the 1989 SARA 313 emission estimates for the refinery. Please call if you have any questions. t *1 v ,n v . ... .,1 II V I M Project Manager Attachments: 00000430& SAL rnocessiMT P UNfT3 PI Caktaa PCCfP* Ca* n C*m P2 Crude n hm n ftahima n due* PI Itata-ma P2MW f* HD* Add Wait Ahy A/ntaa Cal PWy f DC OaaRaeevanr Plan! Metal P9C PSA Poaar Meuaa snu rcu Tar* Pern cem Marin* 0*4 Tetai SIP Vital (0|) Valve* U*M Liquid 74 SO *ai *M 734 m m 7*4 201 ta* tas 2*2 an 224 0 214 79 21* *20 290 12* 1M 4*2 0 20 7478 0 1012 74 474 212 122 ee* 43* 2* 0 0 ee* *3* 12 S3 151 II *4* 2*0 0 0 10* at r 0 M* 10990 Valve* Heavy Liquid I TABLE; 1909 ESTIMATED EQUIPMENT LEAK VOC 8C I b > PROCESS UHfT CONOCO LAKE CHARLES REFINERY fun? 8*Me U*M Liquid eOUIPMtWT LEA VOC Bounces | Pump * Heavy Liquid Carrpweeer IMl (Hydreeerben) Preatura Renal Velvet (CooveltedXb) PreMur* ReHat VMvae (Itaeew tren#d)(b) ftwipe* !** t a Valve*) Cpertended amptln* Drain* Oraln* Line* Cenneeden* |Uneentr*HdXc| (Cemrellad)le) Juncdon Beia* Total 40 0 I 0 0 0 412 0 0 2 0 0 229 2*2 1* 19 10 0 Ml* 0 0 M 0 IS 1121* 20* 7 0 2 0 210* e 0 42 0 7 4014 90* 10 11 0 0 St 07 0 0 M 0 10 MIS 290 10 4 0 2Stt e 3* 0 12(7 274 i * 1 0 27** 0 0 20 0 $ 12*4 Ml it 12 4 0 SSM 0 0 M 0 10 720* *U 12 122 9 14 0 10 0 Ml* 0 S7 0 10 *MI 0 0 tin 0 0 11 0 2 1727 M2 20 0 0 112 0 0 0 0 0 1041 10* 0 1 9 0 0 10*4 0 0 0 0 0 1117 820 I* It 14 0 82*1 0 e 0 0 **07 MS 14 IS 0 12 0 74* 0 0 M 0 1 (TOO 4*0 1* 10 9 0 0 4*46 0 0 2* 0 4 017 2t 0 0 0 0 2M 0 0 0 0 0 177 42* 12 9 9 0 0 42M * 0 57 0 10 557* M0 0 MS 0 0 10 0 2 77* H M IS 0 12 0 7*4* 0 0 47 a IIS 12 4 11 t 0 0 *237 0 a 0 4 01$ 141 0 0 0 0 140* 0 0 30 0 s IMS .M * 2 0 17 0 0 M e is 114* It* 1 0 0 1*97 0 0 a i s 2217 1*4* 100 42 0 0 IMl* 0 0 i IS 1* 24414 11* S 0 I 42* 0 0 8 0 1 SM 9M 0 0 0 0 2234 0 0 0 0 0 42** 9919 299 290 r 72 1 100012 9 0 808 49 142 129338 SAL 000004307 SHAD VCM VHAO USSHAP UNITS Total llSHAp MSP* UNIT* No. 1 Ctaar LVT-200 12-C* Pi-VAC P4-HCS P7NOS PS-H0S cnvo mo rnr Tetai HOPS TOTAL LESHAP/NSPS *0 * ~n Ml M 1*0 17* SSI 221 11* 4* 94 29#* 9092 171 129 34 131 41 It* 0 a 221 0 331 7% 1370 1704 00 00 0s 0 0 5 8" 0 M IS 104 0 40 0 44 0 17J 7 4* 0 2* 21* It 1* 0 0 7*7 St ~24~ 797 99 24 0 I i 4 0 0 9 9 9 1 9 4 0 0 41* 4 0 e 0 0 7*7 0 0 7M 0 0 0 0 0 1022 0 122 0 0 4 0 0 IS* o 0 1817 o- 0 0 r~ 0 mi 0 248 0 0 IS 8 097 1 0 1019 0 0 9 1 1 1121 t 0 790 9 0 0 0 0 1012 I 0 SS7 0 0 0 0 * 1117 14 0 2408 0 0 0 11 4 4122 0 0 972 0 0 0 18 I 1251 0 0 811 0 4 4 4 1 M2 1 0 4309 0 0 0 11 2 1331 0 0 IS2 9 0 0 8 1 4*0 20 0 18484 0 i 5" "iS" & 2)471 M 9 20029 8 0 m 22 23*97 (a) Equipment count* bated on : 1) ARI data on total equipmont by unR a! the end of 1988 (eieept equipment In Navy liquid Service) and 2) FORSITE prefect tpedtle equipment count* for 1089 profoct*. AD equipment count* ar* ummarfted In the Mareti 22, 1M0 aubmtnat to IN LDEQ 'flequet for Remit Correction - Equipment Leak VOC EmrnNalon*", (b) Preaaure relief valve* that ar* listed a* 'controlled" vent to flare* with a 98% deatructlon efficiency. (e)Drafftt that re lifted "uncontrolled* are eitatlnq drains (Pr* IMS) and were not Installed with a >1*9* end a water*#*! pap. All drain* (poet 1999) hav* been Installed with a >1*0* and a wateraeal trap regardless if the unit It a SIP or LESHAP/NSP9 unit. MM 1:83 PM *04*23* T*H* 1*2 Equip bf LM PROCESSUMT Vafva* (Oaa) Emlttton FMi (SIP) 0.0ttM EmMon Factor AE9HAP/NSFS1 OOOM1 HP UNITS ft Cafctw FCC < CM n cot* n Own liKM WPafamar R0tOniA fSHDS MHOS Md Plant f Arnha CatPeh EDO Gaa Paeuvay Plant Mein PBC --------- ----------PSA Pevar Haiti SAU TCU Ta* Farm COP Marinate* 02* Ml l.tl in AM i.aa 1.11 1*7 080 05* 0.7* ME 1c2m7 0 00 115 030 ------ IJ9 iso ICO 095 0.77 i.aa 0.00 012 Taut SIP 2SL7S Vafvaa Light liquid 00131* 000**5 000 13.12 0*7 *24 2.7* 1.70 20 (.7* 051 000 OOO ITS 140 05 0.70 8.M 0.4t 1245 102 000 ooo 1.42 17.07 000 *.1* iie.7i TABLE 2 1 Ml ESTIMATED EQUIPMENT LEAK VOC EMISSION, at PROCESS UNIT w*(AH amlaalan iMn IWtir| CONOCO LAKE CHARLES REFINERY Valuta Heavy Liquid 000051 000051 002 0.45 0.1* 02* 0.11 0.14 02* 021 007 004 OH 027 024 021 001 022 0.01 02* 021 0.07 0.04 00* o.n 00* 0.10 40 Punp **! Light Liquid 0 0*9*3 00*364 OOO 129 02* 0.70 042 0.14 0.77 0*1 000 0.14 OOO 129 0*7 Ut OOO 0*1 0.00 1.74 020 0.00 0.00 021 O.M 000 000 IMS COUPMCWT LEAK VOC OOUNCE EUMISSIONS (a) Pump 8aata Heavy Liquid Caiyxtaacr S*t (Hydretartan) Prttaura Panel Vafvaa (CenaaOadHb) Prat aura Pallal VMvaa (Uneerttrollad)(b) Flangat (29* O,>n-*ndad Sampling Oialnt Dralna a Vafvaa) Unaa Cannaedona (UneontrelladKcl (Contralladl(e) Junction Aeaaa 0.04720 004720 01*710 0.1*710 0.1(213 _____ ftW> 0.1*213 o.oieao 0.00022 oooeo 0 003 TO 0 00170 00)310 003310 0.07000 0 03500 0.47000 0 07000 Teial 004 0*1 022 022 02* 02f 027 0.47 0.14 0.00 0.11 024 0*1 047 OM 0.44 0.0* 0.72 0*1 0.1 DO* 0.17 111 0.42 042 toss OOO 020 0.00 020 0.00 020 020 0.00 000 0.00 ooo 020 ooo ooo ooo ooo ooo 0.00 020 OS oos ooo ooo ooo o.eo US el ol 0| 0 0i 0i 0i A* 0 e. 9 0. > 0. 0. 0. 0. a> 0. ) 01 0. > 0) 0. > A1 0. 1 a1 09 <o ooo 0.00 0.00 ooo 000 0.00 0.00 0.00 ooo 0.00 ooo 0.00 0.00 ooo 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.19 ooo 0.11 V>.0.00 .H4 IM ** 1.12 />.7^ si0 90 (.fth on h 1.22 l).1l 1.49 ,0.." e * 0.19 r.o1_ am I.'fl 1.1* IJ.tt 1.49 '*145 1.09 `IX 0.0* .9 AM *1.7) All .11 I.SS ivol 1*7 10.4 All 1 &> All ,1G A17 J.*5 419 rp.it, 0 0* ,1) ATI /s i) ooo 000 A00 0.00 000 OOO A00 0.00 0.00 0.00 0.00 0.00 ooo oeo 0.00 oeo 0.00 0.00 oeo 0.00 0.00 AOQ A00 AOO 000 22.00 0.00 000 000 AOO OOO 000 000 000 0.00 AOO AOO AOO AOO 000 000 AOO AOO AOO AOO 0.00 0.00 AOO AOO AOO 000 AOO 0.00 0.14 23 3.01 40* 292 110 411 IN 0.77 0.00 ooo ooo 111 1*3 0.00 IM 070 13* 1.94 in AM 101 4.27 AH 0.00 8142 000 0.00 oeo ooo oeo 0.00 oeo ooo ooo 0.00 ooo ooo 0.00 ooo ooo ooo 0.00 1.79 ooo 0.00 0.00 1.79 1129 OOO Age---------- -s. 000 700 1.2* 4.70 212 215 470 470 OM OOO 000 oeo IS IN AOO 470 O.M 1.79 I.W 282 7.08 118 7.53 A47 0.00 / 18.79 / 80.74 ' I 34 It 20 to 22 21 4 1 1 11 t* IS 1 I* 1 27 14 7 14 * 77 2 11 381.14 SHAD VCM VHAD UrWAP UNITS Taw LESHA* IMPS UNO* No. I CcAar LVT-200 ItCd M-VAC A4-HDS *7HDS M-HO* CAVD PEEDPPEP TcM HOPS ooo 0*9 AM 0*4 ooo 0.17 AM 1*S 117 321 AS 021 A70 000 A70 0.11 11* 1.0* AM ooo A48 ooo 181 1.89 Alt 0.13 11 73 1.71 0.00 000 _0_.00_ 0.00 002 0.09 002 0.01 0.0* 0.03 0 01 0.11 001 "oi*~ 0.00 0.00 0.00 0.00 0*4 023 000 0.00 029 0.00 0.00 02* 0.00 ~140 000 000 ooo 020 ooo 020 - -- t-- 0.00 020 . /V J /J 0 000 A14 000 ow 000 ow OM (0 000 AM If 0.00 AW AW 000 1 04 00 0.00 AM AOO AW AW 0*0 OW 020 --- Ae ooo O.M AOO AW AW ow OW 155 AM 000 0 19 ooo 1.17 Till AOO OM OW 121 OM 11 SO 020 000 ( 19 0.00 AS 11/1 AOO AW AW 031 007 241 009 AOO 10 ooo 0.17 ,*f| AOO OW AW 000 OW 109 oea 000 30 ooo 0.20 i -'*1 000 AW OW ooo OW 1 n 021 020 M 000 ati r ft OOO OW OW It* 042 112 00* 000 00 ooo 021 l./w AOO AW AW 091 021 1 to 001 ooo 00 ooo 0.11 .if OOO OW OW 02* 007 at* 02* 020 1 30 ooo OM fc.n AW OW OW 01* 014 t 002 000 a 00 ooo AM .HJ AW o.w AW 02* 007 oto 172 0.7S is- occ 4.07 AW O.M O.W 441 Tm 35 a TOTAL LESHAPTNSPS no* 143 OSA 1.40 1.13 t.ss IN ooo 441 O.OQ 0.A3 AOO 440 1.54 17.81 (A)EmmlMlofi laciort lor SIP and LESHAP/NSPS unKa war* developed apPcMcany lor the Ltk* Chartaa Refinery baaad on tha taak/no-laak monitoring raaulta avallaMa from tha ongoing laak dalactIon and rapoJr program. The Lit* of lh**e source apaelfle emission lactora hat bean approved by the LOGO. Tha basis lor (ha factors Is described m tha Refinery* March 22, 1090 submittal to tha LDGQ 'Raquaat for Permit Correction Equipment Laak VOC Emleeloftt*. e/a*o aei pm *04*22* Taw* iat Equip by lh SAL 000004308 MlSeaiANEOLQ SMAL1 PflOECTS fR&JSCl Rt (IOC r I etttedl alyt 1 Aelne Clean vp AnttFoaa ld far tte Primary *ja1n Syilea f C Ha 1 n Irat/Prefrac Oebnl l 1 flK(ln l/eergficy fc I OK lo FCC Prglrac Repute* ICO Interstage lex I wl /CC Intlriaimt Air Syrtea Rod 11 'Cat ant FCC Imi'vmnl Air Systen Kadlflcallani ICC Prefrac/Hiln Irie Foir RMI FI c< 11 an* H i furnace Srpat* fEC ICC Hydraulic Actuator* FCC Hegenenter Catalyst D'ilrlth;ir Hc** Ryne AFC > Oatlied th Helm t*0 MM Pinout Ouench Mad* H(0 fleae in |.C0 Pteiaoen FCC Regecerated Catilyil Stripping Modi IIHH til lo Rain F r c l I<hu\er Altrugen lo JupHe-e OpqraiJr l*ti Custody irn*Ier Helen lafxo.fX Resld Preheat Mtaturc Caker HO Syilca OFFgit to Flare ) Reran Tank Fim P\* trail Upgrade 1 Coker Steaanut Blacl Tal.e* Healer 3C9t/Pa*i 4 Flov Contra! reive do. ? Coker Ant I road 01 I umt I (hiemh Oil Syitro FXt L Mg, f (atit FratUtNldf Rater gain i. t CIU KT nt HodlllCitlm m. i Aovar^ro Coruroit rroyetl J Ho. & HUS to lx r me Pit Service Cateade flew Canlrol Ho. 4 H5S Slrtppgr /' P#C Hodl fleet 1 ena J I PBC Walt Amine Cgataclsr Jhevtilam '^CtRlact Foel (at Allnd thru*. 0-1/ * Plant Ride Stead EPuMrig lolil Plane SO r> tOteirrasar* }/DI and 3/0? lube Oil Drain* Rebuild Phenolic Caustic rank* 0*1 Handing Mads: Net Outrne Ctrl lone b O t^O O 0 0 0 Reatie Oleiil Silt Filter Relief Project iapreie Recovered Oil Proce4lng Project llexl ftaripe loading Project CIJ Snort Decoke line epteee KU Soaking Drw tel laf Systed Si Rod* FVir it or) la i Srlle* S/0 Hod* Hxse III (Itdlnate Hot Oil Slovdoun Ot vert Sabine Haler Clarifier Sol Ida Cllfilnate IIC Vaport at CPI Irapi OCSIIR Or. If SIP DR WPS t*S 11 PORTS PVAPS 01 HER oc HI RY II HI CCHP FlAHMS l/TR t/tir 1/rcrM 4/P8/&.1 8F18/R9 IJffF/M l/l?/S0 \ lit 111 /RD ?/rm ?// ?/!/ r/fb/sn i/nisn l/IIPRO 4/f/RD g/tR/io i/fSrRO SA/9* |/tf/*( ?/?3F ?/?*/ 3/1 FRO up iy/aa j/l?m 1/t1/19 RllflM ?/n/o 2/14/90 4///TO 4/I1/1D s/ m S/7/19 l/J/* 3/U/J8 J/tS/W I0/3FW ?/l/RD i;il/M 10 `1S/I4 J/P/7D 10'?I/8S M//0/91 AmI ne Am) nt rtc FCC nr. ftc KC m 1 it FCC. 1 cc ia 1 cc. 1 cc ICC FCC /A niA a. t Colrr Vo. T Coker tg. t Coker a. E Coker . ? Coker Ro. t CeAtr Ho. ! toRer Ho. { Cafter Ho 2 Crude no, t uu He. s nos Aa 4 HQS PBC PM PM Pourer Plant PL* 5*P lank 1m lnl f arm rirm u/toefti fhemo 5 l>cnwl * rlout 1irlini Va r1 Out iattmrater Itilekilrr SEP SIP SJP SIP SIP SIP SIP SIP SIP 3IISIP MV SIP SIP SIP SIP 1 1 II 10 7 l L2 3 SIP II SEP 1 SEP IS SEP 2 SIP i SIP : SIP 4 SIP SIP UP SIP r'lAb o . 5"5""' 2* SIP SIP SIP SIP 3 1 6 Mt 0.0 o An Of SEP SIP 3 ii SIP SIP IS SIP 14 SIP 1 SIP IS Mta.n, C5* <45 o S4 SIP 1 SIP SIP SIP SIP 23 F? I3 (4 a ' R3 `Wt a yrx> f o. ) IS! L S4 SIP SIP 6 27 H 2? 72/ 1231 to hydrocarbon eriltdoni addto o hydrocarbon eolation* aided Clber: fteerueei ID gat elite* and II Ilangr* Aa hydfftCtrbon enisilnni adied. iml to Tte; Aa hydrocarbon ealtslmt itfOM Ho hydrocarbon emltilont added Only Install* antler plalet hydrocarbon e*l*lom iddeo Re hydrocarbon ealuloni addrO Other; Renevet I gag taler Re hydrocarbon million* added do hydrocarbon gklulgni added Either: Reaoeet l HI >a1*e ind l riangei 1 Ml rllre end < Mihfti #. PS O.M .4l 0./2 0 ft O.M 0. s* 9.9* Q 01 0.17 0.0ft 0.00 DOS 0 0 *? OSS O.M O.il 0.05 0.01 0.4A O.M 0.21 0.00 0 13 ) <1e* In iwe eater lerrice a hydrocarbon million* added do hydrocarbon (million* added Ho hyOroearbon emlitlon* added Otter: brent 10 LI egtrai ItM orlatnal (ir.l Otheri Rn 1 It ile (I"iiiiei P9i Hodi) Ha hydteCirben ea'iilgn* eddea Hate r1 a 1 <10 el I VUC Alia iddi 4 turp lemltilgn* - Jonctierr Mi) Other: 100 HBIl/trth dleial barge laading Other: Remoyei IS Hi. | RV. and SI Flange* Sent lo Fan* French Other: Vctan.ei 5 hi. 1 ii. SO flanjr* do hytruegrton edlitlom added 9 St S SI s*ja 1 l**ii a? Pla uiSCFtl Sh*i ***Cki * W'?' a 3 t e Cte <3 1 3 art SC c ic a e S- 5a sS9*t 2? ; JS 5i I 5Z SAL 000004310 rotfrf VIS TOO. i i* * * 06/04/91 12:59 02147400125 UOJECIi Jraject . ; CHM1 Deicrlptleni Preparation) Duccrit> 4*217 cwoto. Ilk! Charlds fttflnerr CALCULATION SHLI1 PtISCEllAIKOUS SHALL ItOJEClS 1W AND THRDK11 6/11/90 <(d-04) Prepared Bp: . iattn. MNS1IE //! Chacked Or: T. Arnold Oatei )/*/ To MMMrlre fuoi tin TOC aalislens due to tqulfeent Itib fraa rarlau* "ulacelleneewi seal 1 prejacte during IHI ond part Of 11*0. UNITS! Table I pretenta a susesrp of Lhe refinery's lonrce-speclflc eel mo* factor* and eqmpeent eewits tar SIP oanltored equipment and presents the eethod used to cslcnlste the fugitive VOC tolsslens free qulpesnt aonltorrd under SIP. ...... ................. ...... -- :ru* " ..... ..... a*.; .TTC-C7T77T2T F0R$IT > CALCULATIONS. Hill t suieuiT ar ecu IPPtERT LEAK VOC SOUNCtS IN ME SI* HOnlTOKK pioiiun CONOCO LAKE CNAPLES tfflNEPf [E -BO) Eguifnent Hon1 tored Under SIP Proprae Only Project t >rral1 Oat* Tairas ICast Valve* (light Liquid) Salves (Mur Liquid] Puep Seals (U gut Liquids) Puep Sella (Item Liquids) {Depresses Seals tWrdroceebon) Pros sure talliT Ttlvtl (Be*) Open-andto Siapllng flange* (a) Li nei Connection Drains Jamctlan Inti 0.003*1 SIP Progra* Kelts Ion Faeters for Equipment Lesha of VOC id/7/011 (b) tc> (iVhr/tavrti) 0.013)1 0.000*1 0.00*1) 0.04720 0.1*719 o.imi 0.00022 0.00)70 0.03)10 0.47000 0.47404 TOTAL LQVmUt COUKT FOt SIP SOBICES CEP-80) TIM SubelUed J/tt/10 to LOCO it port oT IMP fugitive OC la Its lent Pare It Correction FCC Fractionation PPodlffoat lens Project Eqislpeont In VOC Service Deleted Nee cifulpAonL in VOC Service Awied 0 V Light LVT Railcar Loading Equfpaent in VOC Service Deleted He* Equipment In VOC Service Added 0 (1 Miscellaneous Snail Projects L9B9/1990 Equipment In VOC Servlet Deleted New Equlpnent in VOC Service Added 11 94 mr 0*1) B6 0* i) 00 02 2D 23 IS 227 UPDATED ECUimnt COHN! fOS SIP S0NCES (CP-40) 7267 9993 10113 TOTAL writ [OH. ftns SIP SDUtCES Mb/hr) TOTAL EHHSTCMS TltOH SIP SOUNCtS (T/rrj pa.*2 I26.ce 1)1.SI sri.od S.ll wtt. TOO a i 0 D 0 0 252 17.SS 71.85 2)0 1 0 0 0 0 4 233 II. aa.i; 0 0 0 0 D 0 0 B ISA .n >1 ;< 7204 0 4 Ml 141 0 50 0 1 u 240 0 L 0 00 o- 0 7D 0 1 191 0 0 0 1260 0 0 7J 9M7B 0 0 D .40 17) 21.07 *4.M 0.00 0.00 4.00 4.04 [ 1.ratio Total For 514 Hon 1 Cored Cqulpivent For Total Refinery 1 00 10 00 00 0 0 e2 *0.1? IU.M 0 142 04.74 212.JJ >344.6B <IbVhr )1509.70 (T/yr SAL 000004311 @002 ) Ih! Jiuiber of r>*ns4* Per equip**1*1 U tttlaalrd ta be 3.C in* tUl rwebar f valve* based an in* rictinlnt tntgatry aver*)* of 3.1 flang*i/va>v*. <b) St* tainton lectors ore based on ltM Lake Charles laflverr laek/no-leas weltering till. Saercog subject to the tie weltering regelreeents r* genttered 1Ipht liquid service, ehlih are MAlterid annually. oacapl for n <C1 fatal SIP Seurtt nils loo* art atwmlned by eumplylnp the totol equipment count by Uie cerrespmdinq Million factor and tenvertlng the lb/fir rtlue to 1/jr iiualm g;d4 Mfjr ina 2 EP-90 (t) 40227 B*60 MSCEU. SMALL POJ 06/04/91 12:59 02147400125 Project / Feral 1 Dale TAIIC ? coioco itrmtRrSUWUtT OF IQVinenr lLA* C SOURCES Id IHE USURP ft/ bSPS MMITOIIltt FIKMTS (ED-90) lake chailis Eqwlpamt Nenltared IIMir IISWaD gr q$PS trg*re* folr Vllves (Set) velvet aim liquid) Velvet (hear/ liquid) Pt0 Seals 4iiqnt Liquids) PuPp Seen (Heavy Liquids) Coapeesaar Seals (Hydrocarbon) Pressure tetlsf Valves (ts> 9.B0391 II4U4I -4 m*t (19/hr/source] 0.0C4H 0.Q9051 9.11SM 9.04770 9.19710 0,09040 Open-ended SaoplInq FI4no*t < el lines Cannedlan > MAD a * Drolnt Junction hut D.09077 0.09370 0.03310 0.01509 0.47 IOIAI EQUIPHERf COUMt fM 1097 i;m 171} 11 3i t IB EISA* a 1 P5 t tESHAP SOURCES (EP-90) ftC Frgctlanatlan Hod1ftcitlant Project Equipment in VK Service Deleted 0 0 00 New Equipment la VOC Service Added e a0 light ill la Hear leedln* iqjlpeent In VOC Service Deleted en Equipment In VOC terete* Added 0 e 00 d 0a NDcelliMMi Small Project* 1M9/1UQ Equipment In VOC Strwtct Otleted 0 B Heir Equipment lei VOC Servlet Added 11 90 0 0 0 9 0 9 0 0 9 09 9 B9 B9 Ba na 0 0 0 0 a 9 ECUlfMni CCUII FDI ItSHAP/(BPS lOUR:IS (LP-09) lift) l/n )2It it J( 9 X 71479 a 1 94 13 0D 0a 0 0 99 99 Id 13 fotAi aiistiHK rime aSDl / LESMAP SMKCS (IbSItr) (e> IE.13 ioiai missions rent ISPS l 1ESHAP SOUKES (l/yr) (*) 43.14 9.47 e.7 IF. ID 1.73 l.0 1.70 (.13 7.44 1.99 4.37 B.9I 0.7* 4.77 9.BO 39 .M 0. OB 9.03 0.14 3. It a.9i 14.77 3.99 FORSITE lebla 7 Intel Far ICSHAP t* HSPS Monitored Equipment 14.44 149.91 Ob/kr) 4l/yr) Table 1 toUl fur All S[P nonlloved Equipment 344 .M 1509.70 (Ib/br) U/vO SAL 000004312 IOIAI For all SIP. LCSMAP. and ASPS Nemureo Equipment 179.17 1HI.U (Ib/hr) (T/yr> 40 We nuaber ot flenqei Tar equipment I* eikltaled ko be 3.1 Mi tetal iMber tf valves bated i the reengnUid Industry inrift of 3.1 HtA|tlirvalve.. 4b> lUHAP/RSPS Million fscters are Milk art 1)90 lki Charles Itflngrjr leiVno-lsik agflllarlna Oala. Sources subject t th USHAP/1ISP4 egnllerlng reqvtresenls art aonlloeed ewslhlj. 40 fetal lJX*P/ISPS source etltskani ere deleralnH by mltfplrlht the tla1 equipment count by the cervetpeeidlrn nlulei factor end eorntrlli** the 19/nr value l I/yr imhIii 97(0 h/> EF-80 (b) 99077 EPOOMSCEU SM*' PFtOJ 003 JUN 6 91 17:32 FROn CONOCO STATIONARY PAGE.002 ME--05 UNIT 3 10 14 24 82 25 38 39 56 96 79 81 75 74 84 90 89 85 86 2 35 83 41 68 50 62 63 15 42 43 23 91 22 5 6 7 8 1990 FINAL UNIT YIELD REPORT - LCR FOR PAUL RADY DESCRIPTION DAYS ON STREAM #3 CTU & VAC /340.00 #4 HDS ^336.29 #5 HDS -Z337.85 MTBE 140.45 #3 CRU & HDS (REFORMER) ^ 34487 LVT - 200 r274.07} /v #1 HDS SHUTDOWN AND MOST EQUIPMENT REGULAR COKER 30.79 PREMIUM COKER 298.36 SUBTOTAL v'329.15 #! fX CALCINER 121.24 #2 CALCINER 306.82 /2 COKER 314.59 #2 COKER - ANODE 32.73 SUBTOTAL ^ 347.32 f\ GRP (GAS RECOVERY PLANT) ^'345.46 /6 HDS S 332.62 #8 HDS 342.35 #7 HDS ^ 328.17 HYDROGEN SYSTEM 350.47 FCC FEED PREP ^ 326.37 CDR UNIT 195.00 i2 CRUDE UNIT (CTU) /353.87 FCC UNIT 316.93 CRYO GAS PLANT ^ 340.97 CAT POLY UNIT ^ 341.61 NP SPLITTER 343.78 LIGHT GASO SPLIT 351,76 #2 CRU 8 HDS (REFORMER) ^ 310.22 REFORMATE SPLITTER 274.60 THERMAL CRACKER 317', 92 CASINGHEAD UNIT (PBC) ^ 348,26 ALKYLATION UNIT ^ 328.64 ACID PLANT ^ 329.91 SULFUR PLANT (SRU) 343.38 NASH PLANT 291.29 REGULAR BLENDING 7,00 UNLEADED BLENDING 303.00 SUPER UNLEAD BLENDING 155.00 MID GRADE UNL BLEND 70.00 COKER COKER - 200 THE MOLEX UNIT IS A PART OF VISTA. WE CHARGE CDR & LVT - 200 WITH MOLEX RAFFINATE & i12 CRU WITH IOLEX GASOLINE. WE ALSO BLEND MOLEX RAFFINATE INTO JET FUELS, BUT WE DON'T HAVE A MOLEX UNIT ON OUR PROPERTY. LV-HAD & LS-HAD ARE RECEIVED FROM VISTA AND DUPONT-ORANGE RESPECTIVELY AND CHARGED TO THE #3 CTU. THERE ARE NO PROCESS SAL 000004313 i -nr F hijc . 00c Source FUGITIVE HYDROCARBON EMISSIONS CONOCO LAKE CHARLES REFINERY (5/6/91) MONITORING QUANTITY INTERVAL EMISSION FACTOR (Ib/hr) YEARLY EMISSIONS (T/yr) 36a Fugitive Leafcs o See EP-80, recalculated using EPA 10/88 leak/ no-leak emission factors a6b Cooling Water System Cooling Water 55.924 N/A (IO6 gat/yr) 36c Wastewater. System Wastewater 683.260 N/A UO3 gal /yr) 36d .Barge-loading o See EP-83. recalculated to correct Inventory omissions 36e Rail Car and Sea Container Loadlno o See EP-84. for recalculated railcar and sea container loading emission fates 0.700 (1) Subtotal 0.200 (1) Subtotal 19.5 68.3 19.5 68.3 Total 87.8 Emissions 2, These emission factors are from AP-42. SM- 00000431^ 'MAY 21 91 7 :5 0 18 5 DAVISON CHEMICAL DIVISION CONOCO-LCHAHLES CONTINENTAL OIL 00- LAKK CHARLES LA 3 NOVA-D . 08-15-00 CURRENT Equilibrium Fluid Catalyst Analyses P.O. Box 2117 Baltimore, Maryfond 21203-2117 Telephone (301) 659-9049 70602 CATALYST INVENTORY: 80 TONS NOMINAL UNIT CAPACITY: 32.000 UNIT TYPE: ORTHO F DATE: 05-07-91 CURRENT CATALYST: S NOVA-D FROM CONOCO TSC SAL 000004315 PAGE.0 0 3 PAGE 12 Send samples to: W.R. Grace & Co.-Conn., Analytical Service Center, 5601 Chemical Road, Baltimore, Maryland 21226-1698; Telephone (301) 355-4900 931 Major" Streams 1. No. 3 CTU & Vac. - Sour Crude, Stab. OH, LSR, Naphtha, Kerosene, and Diesel. 2. No. 2 CTU - Sweet Crude, Stab. OH, LSR, Naphtha, Kerosene, and Diesel. 3. No. 4 HDS - Stripper OH, Kerosene, Diesel, Naphtha, and LSR. 4. No. 5 HDS - Diesel and Overhead Liquid. 5. No. 3 CRU & HDS - Naphtha, Reformate, #3 Strip. OH, Strip/Stab. Offgas, and #3 Deprop. OH. 6. No. 1 Coker - Coker Wet Gas and Coker Gasoline. 7. No. 2 Coker - Coker Wet Gas and Coker Gasoline. 8. Gas Recovery Plant - Misc. Lt Ends, Coker TCU Gas, Cryo P-B, Thermal Gasoline, Coker Gasoline, Abs. Tail Gas, P-P, and B-B. 9. No. 6 HDS - Stripper OH., HDS Gasoline(LSR), and Distillate. 10. No. 7 HDS - #6 HDS Stripper Reflux and Strip. Ovhd Gas. 11. FCC Feed Prep. - Diesel and Slop Oil. 12. FCC - Abs. Tail Gas, P-P, B-B, and FCC Gasoline. 13. Cryo Gas Plant - Cryo Feed Gas, Cryo Gas to Fuel, and P-B. 14. Cat. Poly - P-P, Poly Gasoline, Propane, and Butane. 15. No. 2 CRU & HDS - Naphtha, Molex Gasoline, Stab. Gas, Stab. Liquid, and Reformate. 16. No. 1 HDS - Kerosene and Stab. OH Liquid. 17. Thermal Cracker - Thermal Gasoline and Fract. Gas OH. 18. Casinghead Unit - Field PBC, Ref. PBC Liquid, Misc. Lt. Ends, P-P, Deeth Tail Gas, B-B, Casinghead Gasoline, Propane, Butane, and Iso-butane. 19. Alkylation Unit - B-B, i-Butane, FCC P-P, Propane, Butane, and Alkylate. 20. Tank Farm - Regular, Unleaded, Super Unleaded, Diesel, Kerosene, Naphtha, Crude, Normal Parraffin Feedstock and Fuel Gas. 21. Acid Plant - Amine Acid Gas and SWS Gas. 22. Molex - Kerosene, Molex Gasoline (LSR), and Heavy Raffinate. 23. L-SHAD - Sabine Aromatic Dist. 24. L-VHAD - HAD 25. Boilers - Fuel Gas. 26. Heaters - Fuel Gas. All other units contain no SARA chemicals. Sources: - See 1989 Lake Charles Bluebook chapter and 1988 and 1989 Documentation. SAL 000004316 APPENDIX J PRODUCT LOADING RELEASE DATA AND CALCULATIONS SARA TITLE III, SECTION 313 1990 TOXIC CHEMICAL RELEASE INVENTORY LAKE CHARLES REFINERY 000004317 SAL Product Loading Release Product Loading releases are calculated using AP-42(*) correlations. These correlations were put into spreadsheet format. The required data needed and the source of that data is as follows: 1. Product Thruput(bbls) - Product loading records attached provided by Reid Trekell, Lake Charles Refinery. 2. VRU Efficiency - VRU efficiency according to Clyde Rhodes, LC Transportation. 3. Vapor Molecular Weight - See Emission Factors chapter. 4. Saturation Factor - Splash loading with vapor recovery. (1988 documentation) 5. Vapor Pressure - See Emission Factors chapter. 6. Temperature - See Emission Factors chapter. 7. Compositional Data - See Process Stream chapter. Note: * . AP-42 Chapter 4.4, Transportation and Marketing of Petroleum Liquids. SAL 000004318 LAKE CHARLES LOADING RACK EMISSION COMPOSITION = REG. GASO. THRUPUT(BBLS) VRU EFF (X) = VAPOR MU = SAT. FACTOR = VAPOR PRESS. = TEMPERATURE = 46313 87.5 62 1 8.3 70 VOC LOSS (LBS./YR.) COMPOSITION LOSS (LBS./YR.) BNZ TOL ETB XTL CYHX CUM PCUM NAPK STY 1.8 9.1 2.2 10.6 BD 4.3 2 BD BD 2941.536 9.763 14.38 1.138 4.759 0 1.049 0.498 0 ERR COMPOSITION = UL GASOLINE THRUPUT(BBLS) = VRU EFF (X) = VAPOR MU = SAT. FACTOR = VAPOR PRESS. = TEMPERATURE = 1820488 87.5 62 1 8.3 70 VOC LOSS (LBS ./YR.) 115626.9 BNZ ............. 2.5 COMPOSITION LOSS (LBS./YR.) TOL ETB XYL CYHX ............. ............. ................................ 6.1 1.6 7.7 BD CUM ............. 4.3 PCUM ............. 2 NAPH ............. BD STY ............. BO 533.0 379.1 32.53 135.8 0 41.24 19.59 0 ERR COMPOSITION - SUL GASOLINE THRUPUT(BBLS) = VRU EFF (X) = VAPOR MU = SAT. FACTOR = VAPOR PRESS. = TEMPERATURE = 545301 87.5 62 1 8.3 70 VOC LOSS (LBS./YR.) 34634.39 BNZ ............. 2.8 COMPOSITION LOSS (LBS./YR.) TOL ............. ETB ............. XYL CYHX ................................ 9.8 2.5 12 BD CUM PCUM ................................ 4.3 2 NAPK ............. BD STY ............. BD 178.8 182.4 15.22 63.43 0 12.35 5.869 0 ERR COMPOSITION = DIESEL THRUPUT(BBLS) = VRU EFF (X) = VAPOR MU = SAT. FACTOR = VAPOR PRESS. = TEMPERATURE = 1410483 87.5 130 1 0.009 70 VOC LOSS (LBS./YR.) 203.6831 BNZ ............. BD COMPOSITION LOSS (LBS./YR.) TOL ETB XYL CYHX ............. ............. ................................ BD BD BD BD CUM ............. BD PCUM NAPH ................................. BD 3 STY ............. BD 0 0 0 0 0 0 0 2.220 ERR SAL 000004319 COMPOSITION = JET FUEL (KEROSENE) THRUPUT(BBLS) * 115830 VRU EFF (X) = 87.5 o - II II VAPOR MW SAT. FACTOR VAPOR PRESS. = 0.011 TEMPERATURE = 70 VOC LOSS (LBS./YR.) 20.44365 BNZ ............. BO COMPOSITION LOSS (LBS./YR.) TOL ETS XYL CYHX ............. ............. ............. ............. BD BO BD BO CUM ............. BO PCUM ............. BD NAPH ............. 3 STY ........... BO 0 0 0 0 0 0 0 0.182 ERR SAL 000004320 FROM: Trefcell, W. Reid "O: RADY PAUL SOFTSWITCH/FCENGPE2 CC: Trekell, W, Reid SUBJECT: SARA 313 DATA PRIORITY: 1 ATTACHMENTS: DATE: 06-11-91 TIME: 18:11 PAUL, I HOPE THAT THE FOLLOWING IS THE DATA YOU REQUIRE FOR THE REPORT. IF YOU HAVE ANY QUESTIONS, PLEASE LEAVE A MESSAGE ON MY AXJDIX AND I'LL GET BACK TO YOU ON THURSDAY. I AM ATTENDING A REQUIRED SAFETY SCHOOL THRU WEDNESDAY. REGULAR LEADED 46,313 y y MIDGRADE UNL. 263,019 -- LVT OIL 12,709 ISOBUTANE 610,491 XF14W/C-140 64,166 UNLEADED #2 FUEL LVT-200 N-BUTANE ETHANOL 1,557,469 S, SUPER UNL 1,410,483 y JET/KEROS 27,334 780,959 EP MIX B-B MIX 452 545,301*7 115,830 y 198,390 30,590 THE UNITS ARE BARRELS. THIS DATA WAS SUPPLIED BY CLYDE RHODES, ETN 6574013, BASED ON LOADING RACK THRU-PUT. I WASN'T SURE IF YOU REQUIRED ALL THIS DATA, BUT AT THIS POINT WOULD RATHER GIVE YOU TOO MUCH THAN TOO LITTLE. GARY SMITH WITH FORSITE WILL GIVE YOU A CALL WITH THE MTBE VALVE COUNT. THE THRU-PUT FOR THE UNIT WAS 141,800 BARRELS OR 37.6 MM LBS. GOOD LUCK, EID SAL 000004321 Form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES . PUBLICLY OWNED TREATMENT WORKS (POTWs) .1 pOTU name NA treat Address :ity j County | 1.2 POTW name NA 1 Street Address l j City Page 2 of 5 Cyclohexane Csnooo Lake diaries Refi | County State 1 Zip 1 1 State 1 1 Zip 1 2. OTHER OFF-SITE LOCATIONS <DO NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name EFT | 2.2 Off-site location name CHMI EPA Identification Member (RCRA ID No.) NA | EPA Identification Nuifcer (RCRA ID No.) IAD000777201 Street Address cities Service Hwy 3>10 1 Street Address Rt 2, John Brannon Rd City Sulfur | County 1 Calcasieu | City ] Carlyss | County | Calcasieu State TA I 2ip j 70664 ] State 1 IA | 7(663 lr atioo under control of reporting facility or parent CO. . .Vf? t 1 Yes t M No | Is location under control of reporting facility or parent | company? t 1 Yes tX] No 2.3 Off-site location name NA 1 2.4 Off-site Location name 1 NA EPA Identification Number (RCRA ID No.) Street Address 1, EPA Identification Number (RCRA 10 No.) 11 1 Street Address City | County 1 State 1 Zip 1 Is location under control of reporting facility or parent company? t 1 Yes [ 1 No 2.5 Off-site Location name NA EPA Identification Nuitoer (RCRA ID No.) Street Address 1 City 1 | State | County 1 | Zip { Is location under control of reporting facility or parent j company? I 3 Yes [ J No sssssssasisitsuiiBs 1 2.6 Off-site Location name j NA | EPA Identification Number (RCRA ID No. ) 1 | Street Address City re [ County i 1 Zip 1 1 City l j State | County 1 I Zip 1 Is location under control of reporting facility or parent company? [ ) Yes [ ] No J Is location under control of reporting facility or parent j company? C 1 Yes [ ] No ( } Check if additional pages of Part ll are attached. How many? t 1 EPA Form 9350*1 (1-90) Revised Do not use previous versions 313 ADVISOR SAL 000004322 Page 3 of 5 EPA FORM R PART Ml. CHEMICAL-SPECIFIC INFORMATION Cyclchhexane Lake diaries Ref 1. CHEMICAL IDENTITY (Oo not complete this section if you complete Section 2. 1.11 [Reserved] 1.2 11 CAS Nunber (Enter the nuifeer exactly as it appears on the 313 list. Enter NA if reporting chemical category.) 000110-82-7 11.3 Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 list.) j Cyclohexane 1.4 j Generic Chemical Name (Complete only if Pert I, Section 1.1 is checked "Yes.*' Generic name must be structurally descriptive.) 2. | MIXTURE COMPONENT IDENTITY (Do not complete this section if you conplete Section 1.) | Generic Chemical Name Provided by Supplier (Limit the name to a maximua of 70 characters (e.g., numbers, letters, spaces, I punctuation).) 3. | ACTIVITIES ANO USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) Manufacture the 3.1 chemical: a. ( ] Produce b. l ] Inport | If produce or 1 | import: c. [ e. [ ] For on-site use/processing ] As a byproduct d. [ f. I ] For sale/ distribution ] As an impurity Process the 3.2 chemical: a. [X] As a reactant d. [ 1 Repackaging only b. [ ] As a formulation component c. ( As an article 3.3 j Otherwise use a. [ ] As a chemical b. ( ] As a manufacturing aid | the chemical: processing aid ^8S888SS88SSSS88S583SS85888SSSSS&ftSSSSmSSSSS8SIBBSIIIIIIISBSSSIIIS8MIIIIIl 4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR c. [ ] Ancillary or other use [07] (enter eode) 2S8SS5S8SS1SBIISIIIIISII; 5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases (l bs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.2 5.3.3 iai ti t] j 5.1a C ] [ 1 c 3 1 1 5.2a 1| | 5.3.1a | S.3.2a [ 5.3.3a | I3 [] C] [1 l] ] 1 ] [3 [] c] [] 12000 5.1b [0 ] 2900| 5.2b [0 ] 17 NA NA 5.3.1b [0 ] 5.3.2b I ] 5.3.3b [ ] C. X From Stormwater 5.3.1c NA 5.3.2c 5.3.3c 5.4 Underground Injection 5.4a| t ] ] [1 NA 5.4b [ ] 5.5 Releases to land 5.5.1 On-site landfill 5.5.2 Land treatment/application farming 5.5.3 Surface impoundment 5.5.4 Other disposal I 5.5.1a I 5.5.2a 5.5.3a 1 5.5.4a 1 [] [] t] CI I] [1 [] CI t] [] [] (] NA 5.5.1b C 1 NA 5.5.2b C ] NA 5.5.3b [ ] NA 5.5.4b ( ] [ ] (Check if additional information is provided on Part IV - Supplemental Information) EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR SAL 000004323 A FORM R PART III. CHEMICAL-SPECIFIC INFORMATION (continued) Cyclohexane Conoco Lake Charles Refi 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS A. Total Transfers (Ibs/yr) You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate S. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) 6.1.1 Discharge to POTW (enter location number from Part II, Section 1.) 6.2.1 Other Off-Site Location (enter location ncnber from Part II, Section 2.) 6.2.2 Other Off-Site Location (enter location rxmber from Part II, Section 2.) Other Off-Site Location 6.2.3 (enter location nunber from Part II, Section 2.) 1.C 3 [3 C 3 (3 2. [2 3 13 (3 C 3 2.d 3 2.[3 [3 C3 E 3 1 | [1 j [3 C3 NA 6.1.1b ( 3 50 6.2.1b [O 3 6.2.1c M72 62 6.2.2b tO 3 6.2.2c M72 NA 6.2.3b [ 3 6.2.3c C 3 (Check if additional information is provided on Part IV - Si^plemental Information) sggisCTssssytMwnggyg<Pgf*gyggMMM,MMMggM,,MMMg,aaigMgMMM*B"aaagAasssggsagggaggagggggaBSggsgggg8ssaag,M,Mgggg"??? 7. WASTE TREATMENT METHOOS AND EFFICIENCY ( 3 Not Applicable (NA) - Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. A .teral .astestream (enter code) B. Treatment Method (enter code) 1 C. Range of Influent Concentration j (enter code) D. Sequential Treatment? (Check if applicable) | E. Treatment Efficiency Estimate F. Based on Operating Data? Yes No 7.1a 7.2a 7.3a fW] [A 3 c3 7.1b 7.2b 7.3b e Bii: [A073 [NA 3 | | | 7.1c 7.2c 7.3c [43 [2] [3 7.Id 7.2d 7.3d [ 3 J 7. le [ 3 | 7.2e t 3 | 7.3e 95.00 X |7.If 88.00 X |7.2f X 7.3f [3 [X3 [3 [X3 [3 C3 7.4a 7.5a 7.6a 7.7a 7.8a 7.9a 7.10a C3 [3 t3 c3 I3 c3 [] ; 7.4b | 7.5b | 7.6b | 7.7b | 7.8b [ 7.9b | 7.10b [NA ] [NA 3 [NA 3 [NA 3 [NA 3 [NA 3 [NA ] | | | | | | j 7.4c 7.5c 7.6c 7.7c 7.8c 7.9c 7.10 t3 [1 C3 [3 [3 [3 [3 7.4d 7.5d 7.6d 7.7d 7.8d 7.9d 7.10d t3 [3 C3 C3 [3 [3 [3 | 7.4e ( 7.5e | 7.6e | 7.7e | 7.8e | 7.9e | 7.10e X 7.4f t 3 X |7.5f [ 3 X |7.6f t 3 X |7.7f [ 3 X |7.8f [ 3 X |7.9f [ 3 X |7.10f [ 3 [3 C3 [3 [3 C3 [3 [3 [ ] (Check if additional information is provided on Part IV - Supplemental Information) 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) | 8. Quantity of the Chemical in Wastes Prior to Treatment or Disposal I | C. Index [ | D. Reason for Action (enter code) | Current Prior Or Percent reporting year (Ibs/yr) year (Ibs/yr) Change t ] H [ C 3- EPA Form 9350-1 (1-90) Revised - Do not use previous versions. % Rt ] 313 ADVISOR EPA FOAM R PART IV. SUPPLEMENTAL INFORMATION Use this section if you need additions! space for answers to questions in Part ill. Murker the lines used sequentially from lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) Page 5 of 5 Cyclchexane Ccntooco lake Charles Kef ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part III, Section-5.3) You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases <lbs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies (Enter letter code from Psrt 1 Section 3.10 for stresmfs) in the box 5.3.1 5.3. C 5.3.1 3 3 t 3 5.3.1 la C 3 5.3. { 3s t 1 5.3.1 3a 3 l3 J 3 C3 (3 3 3 I provided.) mt************ ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IH WASTE TO OFF-SITE LOCATIONS (Part in. Section 6) 15.3.1 |5.3.t I5.3.C 3b t 3b 3b C. X From Stormwater j 5.3.1 le 3 5.3.1 3c 3 5.3.C 3c isanwMuaanmm You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) 8. Basis of Estimate (enter code) A.1 i Reporting Ranges j 0 1-499 500-999 { A.2 Enter Estimate JC. Type of Treatment/ | Disposal { (enter code) 1.1 Discharge to PCTW 3 (enter location nunber from Pert 11, Section 1.) 1.1 13 3 6.1.1 3b C 3 6.2.1 Other off-site location ] (enter location nunber from Psrt II, Section 2.) 2. C 3 t3 6.2.1 3b t 116.2. 3c 6.2.1 Other off-stte location 3 (enter location nunber from Part II, Section 2.) 2.1 3 6.2.[ lb t 1 6.2.i 3c Other off-site location 6.2.1 3 (enter location nunber 2.C 13 13 1 3 j j6.2.I 3b I ]|6.2.t 1C from Part II, Section 2.) ssssssssssssssssssssssssssiassssssMsssssssssssssestssautrsssssattsss: :ss*8:sa:sssssss:sss:sss3asss:stsss::sMtc8$s3xCEss:s8s: ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part 111, Section 7) ;ses A. General Vastest ream (enter code) | 6. Treatment | Method i j (enter code) C. Range of Influent Concentration (enter code) | 0. Sequential | Treatment? j (Check if | applicable) 7. la C 3 ! 7. 3b t 3 { 7.1 3C I 1 i 7.1 3d t 3 7. 3a ?. 3a 7.1 3a 7. t la 7. [ la C ] | 7. lb t 1 1 7.E 3b 3 I M lb E C 3 ! M 3b C c 3 1 7.f 3b C 3 J 7. 3 | 7.1 1 'I 7.C 3 I 7.C 3 | 7. 3c 3c 3c 3c 3c 3 C3 3 3 3 1 7-t 3d 3 1 7. 3d 3 1 7. Id t 3 i 7.1 3d 3 1 7.C 3d 3 .[ 3a 1 i 7.1 3b l 3 { 7.1 3c C 3 1 7. t 3d 3 7-t 3 a 7.1 la E 1 1 7.[ 3b [ 3 1 7.1 3b C 3 1 7 [ 3c 3 1 7.1 Id 3 3 1 7 [ 3c 3 I 7.1 Id t 3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions | E. Treatment j Efficiency j Estimate | 7. E 1 7.C ! 7. 1 7. I 7. 1 7. [ 1 7.1 I 7. i 7. le le 3e le le le 3e 3e 3e f. 8ased on Operating Data? Yes X |7.[ 3 f 3 X J7.C X |7.[ 3f If 1 3 X (7. If 1 X |7. If 3 X f7.C 3 f 3 x i?.c 3 f 3 X |7.t )f 3 X (7. If 3 313 ADVISOR No 3 3 3 3 3 3 C1 3 00004*325 SAL 0 EPA U.S. Environmental Protection Agency OXIC CHEMICAL RELEASE INVENTORY REPORTING FORM -ticn 313 of the Emergency Planning and Connvrity Right-to-Know Act of 1986, iO knowi as Title III of the Superfind Amendments and Reauthorization Act. Page 1 of 5 Ethylbenzene Conoco Lake Charles Refi EPA FORM R PART I. FACILITY IDENTIFICATION SECTION 1.1 Are you claiming the chemical identity on page 3 trade secret? [ ] Yes (Answer question 1.2; [Xj No (Do not answer 1.2; Attach substantiation forms.) Go to question 1.3.) 1.2 If `Yes'* in 1.1, is this copy: C 1 Sanitized ( ] Unsanitized 1.3 Reporting Year 2. CERTIFICATION (Read and sign after completing all sections.) I hereby certify that I have reviewed the attached docunents and that, to the best of my knowledge and belief, the siiaiitted information is true and complete and that the amounts and values in this report are accurate based on reasonable estimates using data available to the preparers of this report. Name and official title of owner/operator or senior management official Don R. Unruh Refinery Manager signature | Date signed |06-20-90 3. Facility Identification Facility or Establishment Name Conoco Lake Charles Refinery Street Address 1 old Spanish Trail 3.1 1 City | Westlake 1 State ! ia j County j Calcasieu 1 Zip Code |70669 WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.0. BOX 23799 WASHINGTON, DC 20026*3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Number 70669 CNCLK OLDSP 3.2 This report contains information for (Check one): 3.3 Technical Contact Brandt Butler a. [X ] An entire facility | Telephone Nunber |(318) 491-5599 b. [ ] Part of a facility. 3.4 Piblic Contact Don R. Unruh Telephone Nuitoer (318) 491-5222 3.5 SIC Code (4 digit) I a. 2911 I b. NA | c. NA d. NA [ e. NA f. NA Latitude 3.6 Degrees 030 Minutes 14 Seconds 36 Oegrees 093 longitude Minutes 16 Seconds 20 3.7 Dun & Bradstreet Nurber(s) a. 00-842-7692 j b. NA 3.8 EPA Identification Nurber(s) (RCRA I.D. No.) a. IAD990683716 | b. NA 3.9 NPOES Permit Nunber(s) a. LA0003026 | b. NA 3.10 Receiving Streams or Water Bodies (enter one name per box)I a. Bayou Verdine | b. NA c. NA d. NA e. NA f. NA Underground Injection well Code (UIC) Identification Nunber(s) a. NA I b. NA 4. PARENT COMPANY INFORMATION 4.1 Name of Parent Company E. I. Du Pont De Nemours 4.2 | Parent Company's Dun & 8radstreet Numtfer I 00-131-5704 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVicno cai 000004326 :PA form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED 1H WASTES 1. PUBLICLY OWNED TREATMENT WORKS (POTWs) 1.1 POTW name NA Street Address 1.2 POTW NA Street Address Page 2 of 5 Ethylbenzene Ocnoco Lake Charles Ref City County City County State 2* OTHER OFF-SITE LOCATIONS Zip State I (00 NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY I K FOR RECYCLING OR REUSE)* Zip 2.1 Off-site location name BFI 2.2 Off-site location name 0#E EPA Identification Number (RCRA ID No.) NA I EPA Identification Ninber (RCRA ID Ho.) \ LAD000777201 Street Address Cities Service Hwy 1-10 I Street Address j Rt 2, John Brannon Rd City Sulfur | County Calcasieu City Carlvss | County | Calcasieu State LA I Zip I 70664 I State I LA Is location under control of reporting facility or parent ccnpany? t ) Yes [ Xl No | Is location inder control of reporting facility or parent j company? [ ] Yes [X1 SI8Nktt885SSSSS888358SXSS8885Stt885SSSS88S8888S4l888SSS88S8SSS8S&SS3BSnmStCf52SSSZUti4SSSSSSCSS3SsSSS3S8SStSBtfeSMntSS*tU^ 2.3 Off-site location name NA I 2.4 Off-site location name I NA EPA Identification Number (RCRA ID No.) Street Address | EPA Identification Nunber (RCRA ID No.) 1 | Street Address City State j County 1 | Zip Is location under control of reporting facility or parent company? ( ] Yes ( ] No 2.5 Off-site location name NA EPA Identification Nunber (RCRA ID No.) 1 City 1 | State | County 1 | Zip | Is location under control of reporting facility or parent ) company? ( ] Yes ( ] No I 2.6 Off-site location name j NA EPA Identification Nunber (RCRA ID No.) Street Address I Street Address City | County 1 1 City 1 | County 1 State 1 Zip 1 | State 1 Zip 1 Is location under control of reporting facility or parent company? I ] Yes [ 1 No | Is location under control of reporting facility or parent | company? C ] Yes C 1 No [ ] Check if additional pages of Part II are attached. How many? [ 3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR rvnO004327 Page 3 of 5 , FORM R PART III. CHEMICAL-SPECIFIC INFORMATION Ethylbenzene Conoco Lake Charles Pefi 1. CHEMICAL IDENTITY (Do not coaplete this section if you complete Section 2. 1.1 || [Reserved] ,,,| CAS Number (Enter the msiber exactly as it appears on the 313 list. Enter KA if reporting chemical category.) | 000100-41-4 1.3 || Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 Hat.) 1] Ethylbenzene 1.4 11 Generic Chemical Name (Complete only if Pert I, Section 1.1 is checked "Yes." Generic name must be structurally descriptive.) 2. MIXTURE COMPONENT IDENTITY <Do not complete this section if you complete Section 1.) Generic Chemical Name Provided by Supplier (Unit the name to a maxima of 70 characters (e.g., mmfeers, letters, spaces, punctuation).) 3. | ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) I Manufacture the 3.1 j chemical: a. (X) Produce b. I 3 Import ] If produce or import: I c. (Xl For on-site use/processing e. [ 1 At a byproduct d. ( ] For sale/ distribution f. I X As an impurity | Process the 3.2 chemical: a. [X] As a reactant d. C 1 Repackaging only b. [ X As a formulation component c. [ ] As an article component | Otherwise use | the chemical: a. C ] As a chemical processing aid b. [ ] As a manufacturing aid c. ] Ancillary or other use 4. JUMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR [07] (enter code) 5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases (Ibs/yr) B. Basis of Estimate (enter code) A.1 1 Reporting Ranges | 0 1-499 500-999 | A.2 Enter Estimate 5.1 Fugitive or non-point air emissions 5.1a t3 5.2 Stack or point sir emissions 5.2a t3 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.} 5.3.1 5.3.2 5.3.3 [a] (] [3 5.3.1a 5.3.2a 5.3.3a E3 (] I) 5.4 Underground Injection 5.4a 1 3 5.5 Releases to land 5.5.1 On-site landfill 5.5.2 Land treatment/application farming 5.5.3 Surface impoundnent 5.5.4 Other disposal 5.5.1a 5.5.2a 5.5.3a 5.5.4a ] ] I C1 [ [ C [ [ C3 [] c3 cI L1 (3 1 [3 [3 [3 l3 ! j | C3 l] [3 t3 [3 7300 5.1b (0 1 640 5.2b [0 3 17 NA NA 5.3.1b [0 5.3.2b [ 5.3.3b [ 3 3 3 C. X From Stormwater 5.3.1c NA 5.3.2c 5.3.3c NA NA NA NA NA | 5.4b C 5.5.1b [ 5.5.2b [ 5.5.3b C 5.5.4b [ 31 | 31 11 3 ] 1 (Check if additional information is provided on Part IV - Supplemental Information) EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR SAL 000004328 5* -ORM R PART III. CHEMICAL-SPECIFIC INFORMATION (continued) 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS Pag* 4 of 5 Ethylbenzene Ccnoco lake Charles Ref You may report transfers of less than 1,000 lbs by checking ranges under A. 1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) A.1 | A.2 Reporting Ranges I Enter 0 1-499 500-999 j Estimate 8. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) 6.1.1 Discharge to P0TW (enter location ramber from Part It, Section 1.) 1 -1 1 (3 (3 t 3 NA 6.1.1b ( 3 6.2.1 Other Off-Site Location (enter location ruber from Part II, Section 2.) 2.(2 3 (3 ( 1 (3 96 | 6.2.1b (O ] 6.2.1c 1 M72 Other Off-Site Location 6.2.2 (enter location ramber from Part 11, Section 2.) 2.(1 ] 13 (3 [3 110 6.2.2b (O 3 6.2.2c H72 Other Off-Site Location 6.2.3 (enter location ramber from Part II, Section 2.) 2.[ } (3 13 t NA 6.2.3b ( 3 6.2.3c [ 3 (Check if additional information is provided on Part IV - Supplemental Information) ISSSt8ailMail1888SSSSW8SSg88gS81888S8888S8S81SlSSSS8WWMHWS8SS9ISSS8t8St8SSSSSSftWlll 7. WASTE TREATMENT METKOOS AMO EFFICIENCY t ] Not Applicable (NA) - Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. A. General Wastestream (enter code) 1 B. Treatment | Method | (enter code) 1 C. Range of | Influent Concentration (enter code) 0. Sequential Treatment? (Check if applicable) 1 E. Treatment 1 Efficiency j Estimate | F. Based on | Operating Data? 1 res No 7.1a 7.2a 7.3a iW [A c3 j 7.1b [ 7.2b | 7.3b [Bill [ AQ7] [NA 3 7.1c 7.2c 7.3c [43 [23 {3 7.Id 7.2d 7.3d C3 C3 [3 | 7.1e | 7.2e | 7.3e 95.00 x I7.1f 88.00 X |7.2f X |7.3f [3 [Xl [3 (X3 (3 t3 7.4a i1 J 7.4b [NA 3 7.4c C3 | 7.4d t 3 | 7.4e X J7.4f [ ] (3 7.5a [3 | 7.5b (NA 3 7.5c [3 | 7.5d [ 3 | 7.5e X |7.5f [ 3 l3 7.6a 7.7a 7.8a 7.9a 7.10a c3 I3 t3 t3 cI | 7.6b | 7.7b | 7.8b | 7.9b | 7.10b [NA 3 (NA ] [NA ] [NA 3 [NA 3 7.6c 7.7c 7.8c 7.9c 7.10 [3 [3 [3 [3 [3 | 7.6d | 7.7d | 7.8d ) 7.9d | 7.10d C3 C3 [3 [3 C3 | 7.6e | 7.7e | 7.8e J 7.9e | 7.10e X |7.6f [ 3 X |7.7f l 3 X |7.8f [ 3 X |7.9f [ 3 X |7.1Of ( 3 (3 I] (3 (3 (3 ( 1 (Check if additional information is provided on Pert IV - Supplemental Information) ssss::sss:sisssss::s::::s:s:ssssKissEssssiiisiiiiiiisxsssuixxEiiisiiisi(aisiizixixziBassi(zsisssss::sssss:::sss:siitrz:sxx3SSSS 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) | B. Quantity of the Chemical in Wastes Prior to Treatment or Disposal | { C. Index | | 0. Reason for Action j (enter code) j M[ 3 Current reporting year (Ibs/yr) Prior year (Ibs/yr) jOr Percent j Change 1 1 t 3* [t 3- EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 1 1 1 1 X| [ 1 j 31 R [ 1 313 ADVISOR SAL 000004329 A FORM R PART IV. SUPPLEMENTAL INFORMATION Use this section if you need additional space for answers to questions in Part III. oer the lines used sequentially from lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) Page 5 of 5 Ethylbenzene Ooricoo late Qiafiatg Refi ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part III, Section 5.3) You may report releases of less than 1,000 lbs by checking ranges wider A. 1. (Do not use both A.1 and A.2) A. Total Releases (Ibs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for streanKa) in the box 5.3.( ] 5.3. C 3 5.3. C 3 I 3 5.3.1 3a [ ] 5.3.t 3a [ 3 5.3.( 3a Cl Cl Cl C) (1 C3 C3 C3 [ provided.) SSN3SSSSSS3S8 ADDITIONAL INFORMATION OH TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) X From Stormwater 5.3.1 3bI 3 5.3.t ]c 5.3.1 3b[ 3 5.3. [ ]c 5.3.t 3b[ 3 5.3. E 3c You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) B. Basis of Estimate (enter code) A.1 | Reporting Ranges | 0 1-499 500-999 j A.2 Enter Estimate C. Type of Treatment/ Disposal (enter code) Discharge to POTU .t ] (enter location nuiber from Pert II, Section 1.) 1.1 ] | | C1 j I] (3 | | | 6.1.C 3b I | 3 6.2. ( Other vff-site location ] (enter location nuiber from Part II, Section 2.) 2. C 3 13 CI 1 C3 j 1 |6.2.[ ]b [ 3 6.2.[ ]c Other off-site location 6.2. C 3 (enter location nuiber from Part II, Section 2.) 2.t 3 | | C3 j (3 C3 1 |6.2.[ ]b E 1 3 |6.2.[ 1c 6.2.1 Other off-site location 1 (enter location nunber from Part It, Section 2.) 2. [ 6.2. [ lb ( I 6.2.1 3c ADDITIONAL INFORMATION ON WASTE TREATMENT METHOOS AND EFFICIENCY (Pert III, Section 7) A. General Usstestream (enter code) { B. Treatment j Method j (enter code) | C. Range of j Influent j Concentration ) (enter code) D. Sequential Treatment? (Check if applicable) 7.C 3 a C3 1 7.1 3b ( 1 7. [ 3 c [ 7-1 3d E 3 7. I ] a C3 1 7.1 lb ( 1 7. [ 3c C 7-C 3d l 3 7. [ ] a ( 3 1 7.1 3b C 1 7.1 3c ( 7.C 3d [ 1 7.1 ] a [ 3 1 7.1 3b C 1 7. [ 3c t 7-t 3d ( 3 7. [ 3a C 3 1 7.C lb ( 1 7.C 3c [ 1 7.1 3d t 3 7.E 3 a C 3 I 7-1 3b l 1 7. [ 3c C3 1 7. [ Id C 3 r 3a [ 3 i 7.t ]b [ 3 I 7. [ 3c I3 1 7. [ 3d C 3 .. 3a C3 1 7.1 3b t 3 | 7.[ 3c [3 1 7. ( 3d t 3 7.[ 3 a C ] ! 7. [ ]b E 3 | 7. [ 3c [3 1 7. [ Id t 3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. | E. Treatment 1 Efficiency | Estimate 1 1 7. [ 3e 1 7. C 3 e 1 7. ( 3e 1 7. [ ]e 1 7. [ le 1 7.1 3e 1 7. [ 3e 1 7.1 3 e | 7. [ 3e F. Based on | Operating | Data? 1 Yes X |7.t If t 3 X |7-C 3 f E 1 X |7-[ 3f E 3 X 17- E If E 3 X 17-1 X 17* C 3f C 3 3f C 3 X |7.[ Jf [ 3 X |7.I 3f [ I X |7-t If [ 3 313 ADVISOR, No E3 C3 E3 EJ t3 [3 [] l] t] SAL 000004330 EPA U.S. Enviromental Protection Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM Section 313 of the Emergency Planning and Comnwrity Right-to-Know Act of 1986, also known as Title III of the Superfund Amendments and Reauthorization Act. Page 1 of 5 Ethylene GCTIOOO Taira Charles Ref;' EPA FORM R PART I. FACILITY IDENTIFICATION SECTION 1.1 Are you claiming the chemical identity on page 3 trade secret? [ ] Yes (Answer question 1.2; [X] No (Do not answer 1.2; Attach substantiation forms.) Go to question 1.3.) 1.2 If MYesM in 1.1, is this copy: C ] Sanitized [ ] Unsanitized 1.3 Reporting Year 1989 2. CERTIFICATION (Reed and sign after completing all sections.) 1 hereby certify that I have reviewed the attached docuaents and that, to the best of my knowledge and belief, the sibmitted Information ia true and complata and that the amounts and values in this report are accurate based on reasonable estimates using data available to the preparers of this report. Name and official title of owner/operator or senior management official Don R. Unruh Refinery Manager Signature 3. Facility Identification Facility or Establishment Name Oonoco Lake Charles Refinery Street Address Old Spanish Trail 3.1 City Westlake I County | Calcasieu State IA 1 Zip Code |70669 Date signed I 06-20-90 WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.0. BOX 23799 WASHINGTON, OC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE 1NVEHT0RY 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Number 70669 OTCLK OIDSP 3.2 | This report contains information for (Check one): 3.3 | Technical Contact 1 Brandt Butler 3.4 | Public Contact Don R. Unruh a. X] An entire facility 1 Telephone Number | (318) 491-5599 | Telephone Number |(318) 491-5222 b. t 3 Part of a facility. 3.5 | SIC Code (4 digit) 1 1 a. 2911 | b. NA Latitude Degrees 030 Minutes 14 | c. NA Seconds 36 1 NA 1 d. 1 1 Degrees | 093 | e. NA Longitude Minutes 16 | f. NA Seconds 20 | 3.7 Dun & Bradstreet Number(s) a. 00-842-7692 3.8 EPA Identification Nutber(s) (RCRA I .D. No.) a. IAD990683716 1 1 b. NA | b. NA 3.9 NPDES Permit Nuiber(s) a. IA0003026 1 1 b. NA Receiving Streams or Water Bodies (enter one name per box)l a. Bayou Verdine b. NA c. NA d. NA e. NA f. NA 3.11| Underground Injection Well Code (UIC) Identification Number(s) | a. NA | b. NA 4. PARENT COMPANY INFORMATION 4.1 I Name of Parent Conpany I E. I. Du Pont De Nemours 4.2 I Parent Company's Dun & Bradstreet Nurber I 00-131-5704 EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR A Form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES 1. PUBLICLY OWNED TREATMENT WORKS (POTWs) 1.1 POTW name NA Street Address 1.2 POTW name NA Street Address Page 2 of 5 Ethylene OctToco Lake Charles Refi City County City County State I Zip | State 5g88irggSCTS8CTl--llI118llWSSgt8a<S8gXS8SgS8S8818ggeSSeSllgWggSSgSXSSggMeCTSe-- 2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). Zip 2.1 Off-site location name BFT 2.2 Off-site location name cran EPA Identification Hunter (RCRA ID No.) NA. I EPA Identification Hunter (RCRA ID No.) I IAD000777201 Street Address Cities Service Hwy @ 1-10 Street Address Rt 2, John Brannon Rd City Sulfur County Calcasieu City Carlyss County Calcasieu State IA Zip 70664 State IA Vfi663 nation under control of reporting facility or parent c- ^any? [ 1 Yes E No 2.3 Off-site location name NA EPA Identification Number (RCRA ID No.) Street Address { Is location under control of reporting facility or parent I company? [ ] Yes [X] No ;SSS8SSS825888SSS8S8$88883l84S:5SSS85SSS&3StlKBaBBtatUCSS>tlsni 2.4 Off-site location name 1 NA | EPA Identification Number (RCRA ID No.) I I Street Address City 1 County l State 1 Zip 1 Is location umder control of reporting facility or parent company? t 3 Yes t ) No 2.5 Off-site location name NA EPA Identification Number (RCRA ID No.) 1 City 1 j State | County 1 | Zip | Is location under control of reporting facility or parent company? t 1 Yes C IB8IKSS88SIISIfS3SI28888SS88 2.6 Off-site location name NA ] No EPA Identification Number (RCRA ID No.) Street Address | Street Address City j County 1 1 City 1 | County i -te 1 Zip 1 | State | Zip Is location under control of reporting facility or parent conpeny? C ] Yes E ] No | Is location under control of reporting facility or parent j company? t 3 Yes [ ] No [ ] Check if additional sages of Part II are attached. How many? t 3 * EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR SAL 000004332 *>A FORM R PART III. CHEMICAL-SPECIFIC INFORMATION Ethylene Oonoco Lake Charles Refi 1. CHEMICAL I0ENT1TY (Oo not collate this section if you couplets Section 2. 1.1 11 (Reserved) 1.2 11 CAS Ntinber (Enter the nutter exactly aa it appears on the 313 list. Enter NA if reporting chemical category.) | 000074-85-1 1-3 1| Chemical or Chemical Category Name (Enter the name exactty as it appears on the 313 list.) I1 Ethylene 1.4 I Generic Chemical Name (Complete only if Part I, Section 1.1 is checked **Yes.M Generic name must be structurally descriptive.) 2. MIXTURE COMPONENT IDENTITY (Do not complete this section if you complete Section 1.) Generic Chemical Name Provided by Supplier (Limit the name to e maximise of 70 characters (e.g.r ntmters, letters, spaces, punctuation).) 3. | ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) Manufacture the 3.1 ( chemical: | a. [X] Produce b. [ ] Import |I IIff pprroodduuccee oorr iimmppoorrtt:: i ] c. [X] For on-site use/processing e. ( ] As a byproduct d. J For sale/ distribution f. ( X As an inpurity ( Process the 3.2 j chemical: a. (X) As a reactant d. C ] Repackaging only b. ( ) As a formulation conponent c. [ 1 As an article component 3 3 | Otherwise use a. ( ] As i chemical b. 1 As a manufacturing aid c. (X] Ancillary or other use | the chemical: processing aid .c:sssss<cssissnssnss:sssSMus9iEssn<sURsssn3ss*is3sisssst*utssxcsssitssaisrsiissi(sinssasMst3*aiHn*uuina*t 4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR (06) (enter code) 5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (0o not use both A.1 and A.2) A. Total Releases (Ibs/yr) A.1 Reporting Ranges j Q 1-499 500-999 | A.2 Enter Estimate B. Basis of Estimate (enter code) 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.3 Discharges to receiving streams or water bodies 5.3.1 ( 1 (Enter letter code from 5.3.2 ( 3 Part I Section 3.10 for 5.3.3 ( ] stream(s) in the box provided.) 5.4 Underground Injection 5.1a | C 3 5.2a | ( 3 I 5.3.1a 5.3.2a 5.3.3a (3 C3 C3 (3 (3 3 3 3 t3 1 3 I1 [3 C3 14000 5.1b [0 3 NA 5.2b [ 3 C. X From Stormwater NA 5.3.1b ( 3 5.3.1c NA 5.3.2b ( 1 5.3.2c NA 5.3.3b ( 3 5.3.3c 5.4a C 3 3 l3 NA 5.4b C 3 5.5 Releases to land 5.5.1 On-site landfill 5.5.2 Land treatmeot/application fanning 5.5.3 Surface impoundment 5.5.4 Other disposal 5.5.1a 5.5.2a 5.5.3a 5.5.4a [3 3 (3 3 3 {3 3 l) 3 l3 3 C) NA 5.5.1b [ NA 5.5.2b ( NA 5.5.3b t NA 5.5.4b t i ] (Check if additional information is provided on Part IV - Supplemental Information) 3 3 3 1 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR SAL ooooo^33 A FORM R PART III. CHENICAL-SPECtFIC INFORMATION (continual) Ethylene Conoco Lake Charles Refi 6. TRANSFERS OF THE CHEMICAL IN UASTE TO OFF-SITE LOCATIONS You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate B. Basis of Estimate (enter code) C. Type of Treatment/ Oisposal (enter code) Discharge to POTU 6.1.1 (enter location nurber from Part 11, Section 1.) 6.2.1 Other Off-Site Location (enter location nunber from Part I!r Section 2.) Other Off-Site Location 6.2.2 (enter location nuiber from Part II, Section 2.) 1.C 3 2.1 3 2. [ ] 13 C 3 C 3 t 3 (3 C 3 13 [3 13 NA | 6.1.1b [ 3 1 6.2.1b [ 3 | 6.2.1c NA 1 NA 6.2.2b l 3 6.2.2c Other Off-Site Location 6.2.3 (enter location number from Part 11, Section 2.) 2.( ] | Ij | j ( ] [ ] [ J J NA | 6.2.3b C 3 | 6.2.3c j III [ ] (Check if additional information is provided on Part IV Supplemental Information) 7. UASTE TREATMENT METHODS AKO EFFICIENCY (X 3 Not Applicable (NA) * Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. k .eneral Wastestream (enter code) 6. Treatment Method (enter code; 1 Range of Influent Concentration (enter code) 1 D. Sequential j Treatment? j (Check if ] applicable) 1 E. Treatment j Efficiency Estimate 7.1a [] 7.1b C 11 7.1c [3 | 7.Id I 3 1 7.1e 7.2a [3 7.2b t 31 7.2c [3 | 7.2d C 3 1 7.2e 7.3a C3 7.3b l 31 7.3c C3 | 7.3d [ 3 1 7.3e 7.4a [] j 7.4b [ 31 7.4c (3 1 7.4d ( 3 i 7.4e 7.5a [3 | 7.5b I 31 7.5c C3 | 7.5d t ] 1 7.5e 7.6a c3 | 7.6b l ]1 7.6c [3 | 7.6d [ 3 1 7.6e 7.7a t] 1 7.7b c 11 7.7c t3 | 7.7d t 3 1 7.7e 7.8a l3 | 7.8b [ 3I 7.8c l3 | 7.8d C 3 1 7.8e 7.9a [3 | 7.9b l 3I 7.9c [3 | 7.9d c 3 1 7.9e 7.10a [] | 7.10b [ 31 7.10 I3 | 7.10d ( 3 1 7.10e [ ] (Check if additional information is provided on Part IV - Supplemental Information) CO si F. Based on Operating Data? Yes X |7.1f t 3 X i7.2f [ 3 X |7.3f [ 3 X |7.4f C 3 X |7.5f t 3 X |7.6f l 3 X 17 - 7f [ 3 X C3 X |7.9f [ 3 X 17.10 f ( 3 No C3 t3 (3 (3 l3 [3 l3 [3 C3 C3 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) | B. Quantity of the Chemical in Wastes j Prior to Treatment or Disposal j | C. Index j j | D. Reason for Action (enter code) j | Current j reporting j year (Ibs/yr) Prior year (Ibs/yr) Or Percent Change [ 3+ M [ I 3- EPA Form 9350-1 (1-90) Revised Do not use previous versions. X r ri 313 ADVISOR ERA FORM R PART IV. SUPPLEMENTAL INFORMATION Use this section if you need additional space for answers to questions in Part III. Ninfaer the lines used sequentially frost lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) Page 5 of 5 Ethylene Conoco Lake Quarles Ref ' ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part HI, Section 5.3) You may report releases of less than 1,000 lbs by checking ranges under A.1 (Do not use both A.1 and A.2) A. Total Releases (Ibs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for streanKs) in the box provided.) 5.3.1 5.3.t 5.3. [ 3 [ ] 5.3.1 3a t ] 5.3.( la t J ,,3, la 1 C1 (1 (3 [] t] C3 [3 l1 t1 1 j 1 1 5.3.1 3b I 5.3.1 3b t 5.3.1 3b C |C. X From stormwater 3J 5.3.t le l| 5.3. [ 3c ij 5.3.[ 3c I ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) B. Basis of Estimate (enter code) A.1 | Reporting Ranges j 0 1-499 500-999 | A.2 Enter Estimate C. Type of Treatment/ Oisposal (enter code) Discharge to POTW 1.[ 3 (enter location number from Part II, Section 1.) 1.( 3 [3 Cl 1 [3 j 6.1.t 3b [ 3 Other off-site location 6.2. [ 1 (enter location nunber from Part II, Section 2.) 2-C ] | | j 6.2.[ ]b ( ] 6.2.[ ]c Other off-site location 6.2.[ 3 (enter location nurber from Part II, Section 2.) 2.1 1 | J t1 | C] [] III 6.2.1 3b C ] 6.2.1 3c ill Other off-site location 6.2.( 3 (enter location ncirber from Part II, Section 2.) 2.[ ] | | [] | (3 III [] I 16.2. [ ]b [ 1(6.2.[ ]c ill ADDITIONAL INFORMATION ON WASTE TREATMENT METHOOS AND EFFICIENCY (Part III, Section 7) A. General Uastestream (enter code) B. Treatment Method j (enter code) C. Range of Influent Concentration (enter code) D. Sequential Treatment? (Check if applicable) 7. [ 3 a 7. [ 3a 7.1 3a (3 C3 (3 1 7.1 1 7.1 1 7.1 3b ( 3b l lb C 7. [ 3c 7. t 3c 7.1 3c [ [ [ 7-E 3d 7.1 3d 7.E Id I3 [3 [3 7. [ 3 a [ 3 1 7.1 lb [ 1 7.1 3c [ I 7. t 3d [ 3 7. [ 3 a [ ] 1 7.1 3b t ] 7.1 3c [ 1 7. [ 3d [ 3 7.1 3 a ( 3 1 7.1 lb c 3 7. [ 3c C 3 1 7. [ Id t 3 . [ 3a [ 3 1 7.1 3b [ 3 7.1 3c C 3 1 7. I 3d t 3 7.1 ]a C 1 1 7.1 3b [ 1 7.1 1c [ 3 1 7 A 3d [ 3 7. C 3a [ 3 1 7.1 lb ( 3 7. [ ]C r ] l 7.1 3d C 1 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. E. Treatment Efficiency Estimate 1 1 7. [ 3e 1 7. [ Je 1 7.1 3 e 1 7.1 3e 1 7. [ 3e 1 7. [ ]e 1 7.1 3e 1 7. [ 3e 1 7.1 ]e | F. Based on I Operating Data? l Yes X (7.1 3 f I X |7.[ If [ 1 X |7. [ If ( 3 X 17.1 If C 3 X |7. If [ 3 X |7. [ 3 f [ 3 X |7.[ 3 f t 3 X |7.t If C 3 X |7.C ] f r 3 313 ADVISOR NO (3 [1 l3 I1 C3 (3 C1 t l3 SAL 0000Q4335 irormental Protection Agency L ' ASE INVENTORY REPORTING FORM f Emergency Planning and Commaiity Right-to-Know Act of 1966, ; Title III of the Siperfund Amentaentt and Reauthorization Act. Pege 1 of 5 } HyUTOCXlloriC acid (] Conoco lake Charles R&fij PART l. FACILITY IDENTIFICATION SECTION =****S**S* iming the chemical identity on page 3 trade aecret? rawer question 1.2; [Xl No (Do not answer 1.2; i sifestantiation forms.) Go to question 1.3.> 1.2 If "Yes** in 1.1, is this copy: t 1 Sanitized t 3 Unsanitized 1.3 Report uig Year I * (Read and sign after collating all sections.) I hereby certify that I have reviewed the attached documents and st of my knowledge and belief, the submitted information is true and complete and that the amounts and values in accurate based on reasonable estimates using date available to the preparers of this report. el title of owner/operator or senior manageamnt official Jnruh Refinery Manager f Date signed |06-20-90 identification i or Establishment Name o Lake Charles Refinery Address panish Trail WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.0. BOX 23799 WASHINGTON, DC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY Lake j County I Calcasieu | zip code |70669 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) ac y Identification Number i9 -<CLK OIDSP report contains information for (Checx one): a. (X 3 An entire facility b. t ] Part of a facility. nical Contact ndt Butler I Telephone Nunber | (318) 491-5599 .ic Contact i R. Unruh Code (6 digit) 1 2911 | b. NA | 1 c.NA { Telephone Nunber 1(318) 491-5222 ! NA d. | e. NA | f. NA | Degrees 030 Latitude Minutes 14 Seconds 36 1 1 Degrees 093 Longitude Minutes 16 Seconds 20 jn & Bradstreet Nuiberls) . 00-842-7692 1 b. NA PA Identification Nuiber(s) (RCRA I.D. No.) ,. IAD990683716 | b. NA 4POES Permit Himber(s) a. IA0003026 I 1 b. NA Receiving Streams or Water Bodies (enter one name per box)! a. Bayou Verdine i b. NA C. NA e NA 1 d. NA 1 f. NA i Underground Injection Well Code (UIC) Identification Number(s) | a. NA 1 b. NA ARENT COMPANY INFORMATION | Name of Parent Company E. X. Cu Pont De Nemours r* 1 Parent Company's Dun & Bradstreet Number j 00-131-5704 ssssssssssssssss==ssss5ssss%sssssssasssssss5ss5sss=sssasss3ss3sss=sssss%s=sssssssssssssssss=s=sssss3sssssssa3sssssssszssssss= EPA form 9350-1 (1-90) Revised - Do r>ot use previous versions. 313 ADVISOR SAL 00000*336 jjjof 3 aid te*crPtiv.> Pace*f y use **** S4I Page 4 of 5 A FORM R PART III. CHEMICAL-SPECIFIC INFORMATION (continued) Hydrochloric acid Ccnooo lake Charles Refi >. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS A. Total Transfers (Ibs/yr) You may report transfers of less than 1,000 lbs by checking ranges wider A.1. (Do not use both A.1 and A.2) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate S. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) .1.1 Discharge to POTU (enter location number from Part 11, Section 1.) 1.( ] J | C] | [] C3 NA | 6.1.1b C J Other Off-Site Location 6.2.1 (enter location rxjitoer from Part II, Section 2.) Other Off-Site Location 6.2.2 (enter location nuifeer from Part II, Section 2.) 2.[ 2.[] 1 I {Cl j t3 CJ I | | NA NA I 6.2.1b I I 3 { 6.2.1c i 6.2.2b [ J 6.2.2c Other Off-Site Location 6.2.3 (enter location nurber from Part II, Section 2.3 2, [ ] | t ] (1 C 3 [ HA | 6.2.3b ( ] j 6.2.3c jI ! ( 3 (Check if additional information is provided on Part IV - Supplemental Information) ssssssxnRU<isitssnss$sntusKmci<sciixntnis*isssc*stwmMMsai>nu*tiiistaHSsissm(iuituccinnttinsxniitiis 7. WASTE TREATMENT NETHOOS AND EFFICIENCY t ] Not Applicable (NA) Check if no on-site treatment is applied to any uastestream containing the chemical or chemical category. A. General Wastestream (enter code) ] B. Treatment | Method i (enter code) C. Range of Influent Concentration (enter code) D. Sequential Treatment? (Check if applicable) 1 E. Treatment j Efficiency j Estimate F. Based on Operating Data? Yes No 7.1a l 7.1b tClll 7.1c [ll 7.Id [ 3 | 7.1e 100. 00 X 17.If eXi [1 7.2a [] | 7.2b [NA ] 7.2c C1 7.2d C 1 | 7.2e X |7.2f [ i C1 7.3a l3 | 7.3b [NA ] 7.3c [3 , 7.3d t 3 | 7.3e X |7.3f i ] [3 7.4a l3 | 7.4b [ NA ) 7.4c [3 | 7.4d [ 3 | 7.4e X |7.4f t 3 [3 7.5a 7.6a 7.7a l3 C] [3 | 7.5b | 7.6b | 7.7b [NA 3 [ NA 3 [NA ] 7.5c 7.6c 7.7c [3 [3 C3 | 7.5d | 7.6d j 7.7d t1 [3 [3 | 7.5e | 7.6e 1 7.7e X |7.5f X 17.6f X |7.7f [3 [3 i3 CI [3 t] 7.8a c3 | 7.8b [NA ] 7.8c [3 | 7.8d C 3 | 7.8e X |7.Bf i ] [3 7.9a I1 | 7.9b [NA 3 7.9c r } 7.9d t 3 | 7.9e X |7.9f t 3 (3 7.10a cJ | 7.10b [NA 3 7.10 i | 7.10d [ 3 j 7.10e X 17.10 f [ 3 [3 [ I (Check if additional information is provided on Part IV Supplemental Information) 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) B. Quantity of the Chemical in wastes Prior to Treatment or Disposal 1 C. Index 1 0. Reason for Action 1 (enter code) 1 M[ ] Current reporting year (Ibs/yr) Prior Or Percent 1 l year Change 1 1 (Ibs/yr) 1 [ ] 1 1 C 1* *1 [ ] 1 ' R [ -3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. ADVIS0R SAL 000004339 -:pa form r part IV. supplemental information Use this section if you need additional space for answers to questions in Part III. mitier the lines used sequentially from lines in prior sections (e.g,, 5.3.4, 6.1.2, 7.11) Page 5 of 5 Hydrochloric acid Ccnoco lake Charles Refi ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part III, Section 5.3) You may report releases of less than 1,000 lbs by checking ranges under A.1 (Do not use both A.1 and A.2) A. Total Releases <Ibs/yr) B. Basis of Estimate (enter code) A.1 1 Reporting Ranges 0 1-499 500-999 j A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for streanKs) in the box provided.) 5.3.1 5.3.( 5.3. 3 3 C 3 5.3. 3a 3 5.3. t 3a 3 5.3. ]a [3 3 E3 [] [3 C3 t] t3 E3 5.3.C 3b t 5.3.1 3b C 5.3.1 3b ( C. X From Storwater 3 5.3.t 3c 3 5.3. t 3c 3 5.3. 3c ADDITIONAL INFORMATION OH TRANSFERS OF THE CHEMICAL IH WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibe/yr) |B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate C. Type of Treatment/ Disposal (enter code) Discharge to POTU 3 (enter location nutter from Part II, Section 1.) Other off-site location 6.2.1 3 (enter location nutter from Part II, Section 2.) 1.[ 2. [ 3 j [ 1 Cl ( 3 3 (3 t 3 6.1.1 3b ( 6.2.1 3b [ 316.2.[ 3c Other off-site location 6.2. t 3 (enter location nutter from Part II, Section 2.) 2. [ 3 1 | C3 E3 3 6.2. ]b l 316.2.[ 3c Other off-site location 6.2.t 3 (enter location nutter from Part II, Section 2.) 2.C 3 l 1 3 3 C I 6.2. ]b [ 316.2. Jc [> EFFICIENCY (Part III, Section 7) A. General Wastestream (enter code) 7. [ ] a [3 7. [ 3 a [3 7. [ 3 a 3 7. 3a r3 | B. Treatment j Method | (enter code) 1 7.1 1 7.1 1 7.C 1 7.1 lb [ 3b c ]b c 3b [ | C. Range of 1 Influent [ Concentration | (enter code) 31 | 7. [ 3c 3 :l | 7. [ 3c C3 :1 1 7.1 3c [3 3 | 7. [ ]C I3 | 0. Sequential Treatment? | (Check if j applicable) 1 7.1 3d C 1 1 7.1 Id 3 1 7.1 3d 3 1 7.1 3d 3 | E. Treatment Efficiency 1 Estimate 1 1 7. C 3 e 1 7.1 ] e 1 7. 3 e 1 7.1 3 e | F. Based on Operating j Date? 1 7es X |7.t 3f C 3 X 17.1 3 f 1 X |7. If 3 X |7.E ]f 3 Mo C3 E3 t3 3 7.t 3 a [ 3 1 7.1 3b [ I | 7. [ 3c [3 I 7.[ ]d 3 7.C 3a C 3 1 7.1 ]b C 1 | 7. 3c [3 1 7.t 3d 3 ' t 3a 3 1 7.C 3b [ I 1 7.1 3 C C3 1 7. 3d l 3 /. ]a [ 3 1 7.1 3b C 3 | 7.[ 3c [3 1 7.1 3d 3 7.1 3a t 3 1 7.1 3b t 3 | 7.C 3c C3 1 7. [ 3d ( 3 EPA form 9350*1 (1*90) Revised - Do not use previous versions. 1 7.C 1 7. 1 7.1 | 7.C 1 7.1 3e ]e 3e 3e 3e X |7.[ ]f [ 3 X 1 7* If 3 X 17. [ Jf 3 X |7.[ If t 3 X |7.t 3f E 1 3*3 ADVISOR C3 C3 1 t3 C3 SAL 000004340 EPA U.S. Environmental Protection Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM I Section 313 of the Emergency Planning and Comounity Right-to-Know Act of 1986, I also known as Title 111 of the Superfira Amendnents and Reauthorization Act. Page 1 of 5 Lead CCCpoundS OCCIOCO Lake Charles Ref.4 | EPA FORM R PART 1. FACILITY IDENTIFICATION SECTION sssssss: 1.1 Are you claiming the chemical identity on page 3 trade secret? [ ] Yes (Answer question 1.2; (Xj No (Do not answer 1.2; Attach substantiation forms.) Go to question 1.3.) 1.2 If "Yes*1 in 1.1, is this copy: I 1 Sanitized [ ] unsanitized 1.3 Reporting Year 1989 2. CERTIFICATION (Read and sign after completing all sections.) I hereby certify that I have reviewed the attached documents and that, to the best of my knowledge and belief, the submitted information is true and coaplete and that the amounts and values in this report are accurate based on reasonable estimates using data available to the preparers of this report. Name and official title of owner/operator or senior management official Den R. Unruh Refinery Manager Signature | Date signed 06-20-90 3. Facility Identification 1 Facility or Establishment Name | Conoco lake Charles Refinery 1 street Address i old Spanish Trail WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.O. BOX 23799 WASHINGTON, DC 20026*3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY 1 City j Westlake 1................................................... State | LA | County j Calcasieu 1 Zip Code |70669 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Number | 70669 CNCLK OU3SP 3.2 | This report contains information for (Check one): 3.3 | Technical Contact 11 Brandt Butler 3.4 j1 Public Contact | Don R. Unruh 3.5 1 SIC Code (4 digit) | | a. 2911 | b. NA 1 vr* j C. NA | Latitude | Degrees j 030 Minutes 14 Seconds 36 a. [X J An entire facility 1 Telephone Number |(318) 491-5599 1 Telephone Number |(318) 491-5222 b. [ ] Part of a facility. l NA 1 d. 1 1 Degrees 093 j e. NA Longitude Minutes 16 1 .T* j f. NA Seconds 20 1 j 3.7 I Dun & Bradstreet Number(s) | a. 00-842-7692 3.8 1 EPA Identification Number(s) (RCRA I .D. No.) | a. IAD990683716 | b. NA | b. NA 3.9 1 NPDES Permit Number(s) j a. LA0003026 | b. NA Receiving Streams or Water Bodies (enter one name per box)| a. Bayou Verdine j b. NA c. NA | d. NA e. NA | f. NA 3.11| Underground Injection Well Code (UIC) Identification Nunber(s) a. NA I b. NA 4. PARENT COMPANY INFORMATION 4.1 ] Name of Parent Company | E. I. Du Pont De Nemours I 4.2 Parent Company's Dun & Bradstreet Number j 00-131-5704 EPA Form 9350*1 (1-90) Revised - Do not use previous versions. 313 AOVISOft SAL 000004341 ?A Form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES 1. PUBLICLY OWNED TREATMENT WORKS (POTWs) 1.1 POTW name NA Street Address City | County 1 1.2 POTW name | NA | Street Address | City lead Ocnpcunds Conoco lake diaries Refi | Ccxsity State 1 Zip 1 | State 1 Z*P l 2. OTHER OFF-SITE LOCATIONS (DO HOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name BFI I 2.2 Off-site location name | CWI EPA Identification Number (RCRA ID No.) NA 1 EPA Identification Nutoer (RCRA ID No.) 1 IAD000777201 Street Address Cities Service Hwy 8 1-10 1 Street Address | Rt 2, John Branncn Rd City Sulfur State LA | County 1 Calcasieu 1 Zip | 70664 ocation under control of reporting facility or parent any? t 3 Yes C X Ho 2.3 Off-site location name NA EPA Identification Nunber (RCRA ID No.) Street Address 1 City 1 Carlyss | County j Calcasieu I State 1 IA | 7(663 | Is location under control of reporting facility or parent j conpany? [ 3 Yes [X] No 1 2.4 Off-site location name | NA | EPA Identification Nuitoer (RCRA ID No.) 1 | Street Address City State | County 1 | Zip | City 1 | State | County 1 | Zip Is location under control of reporting facility or parent company? [ 3 Yes t 3 No 2.5 Off-site location name NA EPA Identification Number (RCRA ID No.) | Is location under control of reporting facility or parent j conpany? l 1 Yes [ ] No I 2.6 Off-site location name | NA ] EPA Identification Nunder (RCRA ID No.) Street Address City County Street Address Ci ty | County *ate | Zip | State | Zip Is location under control of reporting facility or parent conpany? [ 1 Yes t ] No | Is location under control of reporting facility or parent | company? C I Yes { 3 No [ ] Check if additional pages of Part II are attached. How many? t 3 EPA Form 9350*1 (1-90) Revised - Do not use previous versions 313 AOVISOR SAL 000004342 EPA FORM R PART 111. CHEMICAL-SPECIFIC INFORMATION Page 3 of 5 T Ocnpounds Oonooo lake diaries Ref 1. CHEMICAL IDENTITY (Do not complete this section if you couplets Section 2. 1.1 1| [Reserved) 1.2 1| CAS Number (Enter the number exactly as it appears on the 313 list. Enter NA if reporting chemical category.) | NA 1.3 j[ Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 list.) 1| Lead Cccpounds 1.4 | Generic Chemical Name (Complete only if Part I, Section 1.1 is checked NYes.M Generic name sust be structurally descriptive.) 2. MIXTURE COMPONENT IDENTITY (Do not cooplete this section if you cooplete Section 1.) Generic Chemical Name Provided by Supplier (Limit the name to a maximus of 70 characters (e.g., limbers, letters, spaces, punctuation).) 3. i ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) Manufacture the 3.1 chemical: a. 3 Produce b. C 1 Inport If produce or import: c. I ) For on-site use/processing e. 3 As a byproduct d. ) For sale/ distribution f. C 3 As an impurity Process the 3.2 chemical: a. 3 As a reactant d. 3 Repackaging only b. X As a formulation component c. 3 As an article component 3.3 | Otherwise use [ the chemical: a. I 3 As e chemical processing aid b. 3 As a manufacturing aid c. ] Ancillary or other use 4, MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR 05] (enter code) 3SBnssss:ssssi9isiss::zs:ssssass8:nsssssss*ssc3iss*sisssssss3XscM>mssssasssMssss3ssxss:sssss83s3s:ss>ssEsisisaasucs3taSKu 5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. | A. Total Releases (Ibs/yr) 1 0. Basis of 1 Estimate 1 (enter code) 1 (Do not use both A.1 and A.2) A.1 I Reporting Ranges ( A.2 Enter 0 1-499 500-999 | Estimate 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.1a 5.2a t3 l3 3 t1 3 3 400 0 5.1b eO J1 5.2b [O 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.2 5.3.3 Id) C3 [3 5.3.1a 5.3.2a 5.3.3a 3 C3 1 C3 3 3 t3 3 1 1C. X From Stormwater 0 5.3.1b cO 1 1 5.3.1c NA NA 5.3.2b t 1 ! 5.3.2c NA 5.3.3b c 3 i 5.3.3c j 1 5.4 Underground Injection 5.4a) [ ] 3 C3 NA , 5.4b [ 31 "1 5.5 Releases to land 1 5.5.1 On-site landfill 1 5.5.1a 1 2 3 NA 1 5.5.1b c 11 5.5.2 Land treatment/application farming : 5.5.2a 3 C3 (3 NA i 5.5.2b Ij 5.5.3 Surface impoundment 1 5.5.3a 3 (3 [3 NA | 5.5.3b 3| 5.5.4 Other disposal ) 5.5.4a| t 3 3 [ 3 ) NA | 5.5.4b ( 31 [ ] (Check if additional information is provided on Part IV - Supplemental Information) EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR SAL 000004343 Page 4 of 5 :PA FORM R PART 111. CHEMICAL-SPECIFIC INFORMATION (continued) fWiyu'MiTHg Ccnoco lake Charles Refi 6. TRANSFERS OF THE CHEMICAL IN UASTE TO OFF-SITE LOCATIONS You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate C. Type of Treatment/ Disposal (anter code) Discharge to POTW 6.1.1 (enter location renter from Part 11, Section 1.) 1.1 ] Cl Cl Cl HA 6.1.1b C 3 6.2.1 Other Off-Site Location (enter location nuiber from Part II, Section 2.) 2.[ ] Cl t 3 1 1 NA 6.2.1b [ 3 6.2.1c Other Off-Site Location 6.2.2 (enter location nunber from Part II, Section 2.) 2.t 3 Cl C 3 t HA 6.2.2b t 3 6.2.2c Other 0ff*Site Location 6.2.3 (enter location nurber from Part It, Section 2.) 2.1 3 I | l3 | [3 (3 111 | HA | 6.2.3b C 3 ] 6.2.3c 111 [ 3 (Check if additional information is provided on Part IV - Supplemental Information) 7. UASTE TREATMENT METHOOS AND EFFICIENCY (X 3 Not Applicable (NA) - Check if no on-site treatment is applied to any uastestream containing the chemical or chemical category. General Uastestream (enter code) | 8. Treatment j Method S (enter code) C. Range of Influent Concentration (enter code) 0. Sequential Treatment? (Check if applicable) j E. Treatment | Efficiency j Estimate F. Based on Operating Data? Yes NO 7.1a 7.2a 7.3a C1 3 3 | 7.1b | 7.2b | 7.3b t t 3 7.1c 7.2c 7.3c t3 C3 t1 7.Id 7.2d 7.3d C1 l3 t3 | 7.1e | 7.2e | 7.3e * 7.1f X 7.2f X 7.3f [3 l3 C3 C3 c3 l3 7.4a 7.5a 7.6a 1 3 I1 | 7.4b | 7.5b | 7.6b C [ l 3| 1| 3| 7.4c 7.5c 7.6c [1 t3 [3 7.4d | 7.5d | 7.6d [3 t3 [3 | 7.4e 1 7.Sc | 7.6e X |7.4f X |7.5f X |7.6f [3 l3 t1 l3 [1 [3 7.7a 7.8a t1 C3 | 7.7b | 7.8b r t 3| 1| 7.7c 7.8c C3 t3 | 7.7d | 7.8d t1 C1 | 7.7e | 7.Be X |7.7f X |7.8f l1 C3 t3 t3 7.9a 7.10a C3 [1 | 7.9b | 7.10b C i 3| ]| 7.9c 7.10 (3 [] | 7.9d [ 7.10d (3 [1 | 7.9e j 7.lOe X |7.9f l 3 X |7.lOf [ 1 cJ [3 t ] (Check if additional information is provided on Part IV - Supplemental Information) 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON UASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) | B. Quantity of the Chemical in Wastes | Prior to Treatment or Disposal 1 MC 3 | Current j reporting j year <lbs/yr) 1 1 Prior year (Ibs/yr) Or Percent Change [ 3+ C ] EPA form 9350-1 (1-90) Revised - Do not use previous versions. X C. Index [3 | 0. Reason for Action | (enter code) 1 11 j 1 | RC 3 313 ADVISOR SAL 000004344 SPA FORM R PART IV. SUPPLEMENTAL INFORMATION Use this section if you need additional space for answers to questions in Part III. Musher the lines used sequentially from lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) (Part ill, Section 5.3) THE ENVIRONMENT Page 5 of 5 Tftari fl-sn w i inle Gcnooo lake Charles Ref- You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.C 5.3. ( 3 3 ( 3 5.3.1 3a t 3 5.3. [ 3a ( 3 5.3. C 3a A. Total Releases (Ibs/yr) B. Basis of Estimate (enter code) A.1 | Reporting Ranges 0 1-499 500-999 | A.2 Enter Estimate [1 t3 t3 C1 C3 l3 t1 3 C] 5.3.[ ]b [ 5.3.1 lb ( 5.3.1 ]b ( C. X From Storawater 5.3.t 3c 5.3.1 3c 5.3. [ ]c ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) Discharge to POTW '.( ] (enter location number from Part 11, Section 1.) 1.[ ] A. Total Transfers (Ibs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate C. Type of Treatment/ Disposal (enter code) (3 l 3 (3 1 6.1.t 3b [ ] Other off-site location 6.2.( 3 (enter location nuttoer from Part II, Section 2.) 2. [ ] | [3 j (] [3 6.2.[ 3b E 1 3|6.2.[ 3c Other off-site location 6.2. C I (enter location nunher from Part II, Section 2.) 2.1 3 Cl (3 1 tI j 1 |6.2. ]b [ t 3|6.2.( 3c Other off-site location 6.2.1 ] (enter location nuitoer from Part II, Section 2.) 2. [ 1 13 t 3 13 6.2. [ lb ] 6.2.t )c ADDITIONAL INFORMATION ON WASTE TREATMENT METHOOS ANO EFFICIENCY (Part III, Section 7) A. General Uastestream (enter code) 7. [ 3 a [3 6. Treatment Method (enter code) 1 7.[ 3b C C. Range of Influent Concentration (enter code) i 1 7. [ 3c t3 | D. Sequential Treatment? j (Check if j applicable) 1 7.1 3d C 3 | E. Treatment Efficiency j Estimate 1 1 7. [ 3e 7. t ] a C ] 1 7.1 3b C 3 1 7.C 3c C3 1 7.1 3d [ 3 1 7. [ ] e 7. [ ] a c 3 1 7.1 3b [ 3 | 7.C 3c [3 1 7.1 3d 3 i 7.1 3e 7. [ ] a c 3 1 7.1 3b t 3 1 7. [ 3c 3 1 7.1 3d 3 1 7.1 3e 7. [ 3a [ 3 1 7.1 3b t 3 1 7.1 3c [3 1 7. [ Id C ] 1 7. [ ]e 7.1 ] a [ 3 I 7.[ 3b c 3 1 7. [ 3c t3 1 7.1 3d C 1 1 7.C 3e t ]a 7. [ 3 a t3 c3 i 7.1 1 7.[ 3b i 3b c 3 1 7. [ 3 1 7. [ 3c Jc C3 [3 1 7.1 1 7.1 3d 3d 3 3 1 7.1 1 7.1 3e 3e 7. [ 3a E 3 1 7.[ 3b t 3 1 7.1 ]c 3 1 7.1 Id t 3 1 7. [ 3e EPA Form 9350-1 (1-90) Revised Do not use previous versions F. Based on Operating Data? Yes X |7-[ 3 f 3 X |7. ]f E 3 % |7* 3f C 3 X |7-[ If C 3 X |7.t 3f C 3 X |7.[ ]f C 3 X |7- 3f 3 X |7. 3f E 3 X |7.[ 3 f 1 313 ADVISOR Ho ] t3 3 C3 [] ] 1 3 00000*34-5 SAL I EPA U.S. Environmental Protection Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM 'Ction 313 of the Emergency Planning and Coanunity Right-to-*Cnow Act of 1986, i .so known as Title III of the Stperfund Amendaants and Reauthorization Act. Pege 1 of 5 Manganese CCCDOUndS QonOOO Lake Cnarles Rel I EPA FORM R PART I. FACILITY IDENTIFICATION SECTION SIR 1.1 Are you claiming the chemical identity on page 3 trade secret? I 1.2 If MYesM in 1.1, is this copy: [ ] Yes (Answer question 1.2; (Xl No (Do not answer 1.2; [ [ ] Sanitized C ] Unsanitized Attach substantiation forms.) Go to question 1.3.) j 1.3 Reporting Year 1989 2. CERTIFICATION (Read and sign after completing all sections.) I hereby certify that I have reviewed the attached docuaents and that, to the best of my knowledge and belief, the submitted information is true and complete and that the amocnts and values in this report are accurate based on reasonable estimates using data available to the preparers of this report. Marne and official title of owner/operator or senior management official Don R. tJnruh Refinery Manager Signature i Date signed 106-20-90 3. Facility Identification Facility or Establishment Name Conoco lake diaries Refinery Street Address Old Spanish Trail WHERE TO SEMO COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.O. BOX 23799 WASHINGTON, DC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY City Westlake State LA | County 1 Calcasieu 1 Zip Code |70669 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Member 70669 QTCLK OLDSP 3.2 | This report contains information for (Check one): a. [X] An entire facility b. 1 ] Part of a facility. 3.3 | Technical Contact | Brandt Butler 1 Telephone Nuiber |(318) 491-5599 3.4 | Public Contact Don R. Unruh 1 Telephone Nuiber |(318) 491-5222 3.5 | SIC Code (4 digit) 1 1 a. 2911 | b. NA Latitude Degrees 030 Minutes 14 1 | c.NA Seconds 36 1 1 d. NA 1 | Degrees 093 | e. NA Longitude Minutes 16 | f. NA Seconds 20 i 3.7 Dun & Bradstreet NLirtoer(s) a. 00-842-7692 3.8 EPA Identification Ninber(s) (RCRA I.D. No.) a. LAD990683716 1 1 b. NA 1 b- NA 3.9 NPOES Permit Nuiber(s) a. LA0003026 1 b. NA 3.10 Receiving Streams or Water Bodies (enter one name per box)| a. Bayou Verdine 1 b. NA c. NA 1 d- NA e. NA 1 I* NA 1| Underground Injection Well Code <UIC) Identification Nuiber(s) | a. NA | b. NA 4. PARENT COMPANY INFORMATION 4.1 | Name of Parent Company | E. I. Du Pont De Nemours 1 4.2 Parent Company's Dun & Bradstreet Nuiber | 00-131-5704 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR <;AL 000004346 EPA Fora R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES 1. PUBLICLY OWNED TREATMENT WORKS (POTWs) 1.1 POTW name NA Street Address 1 1.2 POTW name 1 NA j Street Address Page 2 of 5 Manganese Conoco lake Charles Kef* City 1 County j City | County State !1 Zip 11 | State 1 1 Zip 1 2. OTHER OFF-SITE LOCATIONS (00 NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name BET 1 2.2 Off-site location name j CVMT EPA Identification Number (RCRA ID No.) NA 1 EPA Identification Number (RCRA ID No.) | IAD000777201 Street Address Cities Service Hwy 1-10 City Sulfur State IA | County 1 Calcasieu l Zip | 70664 I Street Address | Rt 2, John Brannon Rd 1j ciJCarlyss t State 1 IA | County | Calcasieu | 75663 4$ location under control of reporting facility or parent company? t 1 Yes [X No | Is location under control of reporting facility or parent j company? [ ] Yes [X] ssssssssssssssssssssssssssssssssasssssssssssssssssssssasBSKittsscisskMcmccsess&ssssBSSSSSSSssssssszssimsstmmsatsiuaie 2.3 Off-site location name NA | 2.4 Off-site location name I NA EPA Identification Number (RCRA 10 No.) Street Address l EPA Identification Number (RCRA ID No.) 1 | Street Address City State | County 1 | Zip Is location under control of reporting facility or parent conpany? [ ] Yes t ] No 2.5 Off-site location name NA EPA Identification Number (RCRA ID No.) 1 City 1 | State | County 1 | Zip | Is location under control of reporting facility or parent | company? l ] Yes C ] No 1 2.6 Off-site location name l NA | EPA Identification Number (RCRA ID No.) Street Address | Street Address City j County 1 1 City County State ! Zip 1 j State Zip Is location under control of reporting facility or parent conpany? t 1 Yes t ] No | Is location under control of reporting facility or parent | company? t 1 Yes l ] No [ ] Check if additional sages of Part It are attached. How many? C ] . EPA Form 9350-1 (1*90) Revised - Do not use previous versions 313 ADVISOR SAL 000004347 EPA FORM R PART HI. CHEMICAL-SPECIFIC INFORMATION Manganese ccraxunds Conoco lake aiarles Refi 1. CHEMICAL IDENTITY (Do not complete this section if you complete Section 2. K1 | Reserved] 1.2 l CAS Nkfltoer (Enter the number exactly as it appears on the 313 list. Enter HA if reporting chemical category.) NA 1.3 | Chemical or Chemical Category Mama (Enter the name exactly as it appears on the 313 list.) { Manganese Qanpounas 1.4 Generic Chemical Name (Cooplete only if Part I, Section 1.1 is checked "Yes." Generic name must be structurally descriptive.) ttitisseiiti .2 | MIXTURE COMPONENT IDENTITY (Do not complete this section if you cooplete Section 1.) | Generic Chemical Name Provided by Supplier (Limit the name to a maxisue of 70 characters (e.g., ntnbers, letters, spaces, | punctuation).) sxsssssssnnuasisMnm*mwtisisHssss<*iicwtiEMtutti(uasss*Rsisccs3siHci3ssssa*atnnBs<3ins 3. | ACTIVITIES ANO USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) ( Manufacture the 3.1 1 chemical: | | Process the 3.2 ] chemical: ] a. C 3 Produce 3 Import b. 1 j If produce or import: | e. I 3 For on-site use/processing e. 1 1 As a byproduct d. t 1 For sale/ distribution f. C I As an impurity a. t ] As a reactant d. I 3 Repackaging only b. C X As a formulation component c. ( 1 As an article component ' 3 | otherwise use a. [ 1 As a chemical b. C 3 As a manufacturing aid c. I ) Ancillary or other use | the chemical: processing aid s:ssssesia*H8S8asssscssass3Sisscss5StssssszsssMSScrss33ss*s3nssssssasses8ssx3SSsssBS8asxssss>ss:MiSM*Mssn*Mss 4. ..AXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR t05l (enter code) 3gS3SSSS3S33S3K3SS33S3333S3338333BS333S3X33S333S33333>S3CS3333S3C33333t38e313S313C3S333XBISSC33SB3S:B333S3:333333tI3S333tS3: 3SSSB3BB 5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 ibs by checking ranges under A.1. (Do not use both A.1 and A,2) 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.2 5.3.3 taj ti ti 5.4 Underground Injection 5.1a 5.2e 5.3.1a 5.3.2a 5.3.3a A. Total Releases (Ibs/yr) A.1 1 Reporting Ranges | A.2 Enter 0 1-499 500-999 j Estimate B. Basis of Estimate (enter code) J | j I 1 1 E] [1 t3 I 250 5.1b tO ] j ci l3 c3 1 0 5.2b tO ) j C1 C3 [1 i J (3 | ) I3 ) 1 c3 i 1 C. X From Stormwater 0 5.3.1b f 0 3 j 5.3.1c NA NA 5.3.2b l 3 ' 5.3.2c NA 5.3.3b [ 3 i 5.3.3c | 5.4a 1 3 ] [ 1 1 NA | 5.4b E 3 5.5 Releases to land 1 5.5.1 On-site landfill | 5.5.1a 5.5.2 Land treatment/application farming 1 5.5.2a 5.5.3 Surface impoundnent | 5.5.3a 5.5.4 utner disposal | 5.5.4a 1 ] 3 [1 E3 C1 C] [1 1 t3 | c3 1 c3 j E1 NA NA NA NA 5.5.1b C 5.5.2b ( 5.5.3b l 5.5.4b t 3 J 3 3 (Check if additional information is provided on Part IV Supplemental Information) EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR SAL 000004348 EPA FORM R PART III. CHEMICAL-SPECIFIC INFORMATION (continued) Page 4 of 5 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers <Ibs/yr) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate B. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) Discharge to POTW 6.1.1 (enter location number ' from Part II, Section 1.) Other Off-Site Location 6.2.1 (enter location nunber from Part II, Section 2.) Other Off-Site Location 6.2.2 (enter location nuiber from Part II, Section 2.) Other Off-Site Location 6.2.3 (enter location nunber from Part II, Section 2.) 1.[ ] 2.1 3 2.[ 3 2.1 ] t3 I3 CI I | [3 j C3 Cl t3 [) C1 | 1 NA 6.1.1b [ ] C3 6.2.1b C 3 | 6.2.1c NA 1 C1 | 1 NA 6.2.2b [ 3 6.2.2c (] III | NA j 6.2.3b C 3 j 6.2.3c III ( 1 (Check if additional information is provided on Part IV - Supplemental Information) 7. WASTE TREATMENT METHODS AND EFFICIENCY [X ] Not Applicable (NA) * Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. A. General Wastestream (enter code) 6. Treatment Method (enter code) C. Range of influent Concentration (enter code) D. Sequential Treatment? (Check if applicable) E. Treatment Efficiency Estimate 7.1a C3 | 7.1b t 31 7.1c [3 1 7.Id I 3 1 7.1e 7.2a C3 | 7.2b [ 31 7.2c [3 1 7.2d C 3 1 7.2e 7.3a 7.4a C3 [3 | 7.3b | 7.4b C c 31 31 7.3c 7.4c [3 C3 1 7.3d 1 7.4d t3 [3 1 7.3e 1 7.4e 7.5a t] | 7.5b [ 31 7.5c [3 1 7.5d L 3 1 7.5e 7.6a t3 | 7.6b C 31 7.6c C3 1 7.6d C 3 1 7.6e 7.7a 7.8a C3 C3 | 7.7b | 7.8b [ I 31 31 7.7c 7.8c C3 C3 1 7.7d 1 7.8d C] I3 1 7.7e 1 7.8e 7.9a l3 | 7.9b C 31 7.9c C3 1 7.9d C 3 1 7.9e 7.10a [3 | 7.10b [ 11 7.10 f3 1 7. lOd [ 3 1 7.10e [ ] (Check if additional information is provided on Part IV - Supplemental Information) F. Based on Operating Data? Yes X |7.If t 3 X |7.2f 3 X |7.3f 3 X |7.4f 3 X |7.5f 3 X |7.6f C 3 X |7.7f [ 1 X |7.Sf [ 3 X |7.9f t ] X 17.10f t 3 No C] C3 t3 [3 [3 E3 C1 c3 [3 c3 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) | B. Quantity of the Chemical in Wastes j Prior to Treatment or Disposal 1 C. Index 1 1 M( 3 | Current j reporting j year (tbs/yr) Prior year (Ibs/yr) |Or Percent j Change 1 1 1+ |C 3 1 j *1 C 3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 1 D. Reason for Action 1 (enter code) 1 1 1 1 1 1 RC 3 313 ADVISOR Page 5 of 5 FORM R PART XV. SUPPLEMENTAL INFORMATION Use this section if you need additional space for answers to questions in Part III. ,Aber the lines used sequentially frost lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) Manganese Gtmounds Conoco Lake Charles Fefi ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part III, Section 5.3) You may report releases of less than 1,000 lbs by checking ranges inder A.1. (Oo not use both A.1 and A.2) A. Total Releases (tbs/yr) B. Basis of Estimate (enter code) A.1 | Reporting Ranges 0 1-499 500-999 | A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies 5.3. [ 1 t ] 5.3.1 la C 3 Cl [1 5.3.t lb [ ] (Enter letter code from 5.3.C 1C] 5.3.t la [1 [ 1 Cl 5.3.C lb C 1 Part I Section 3.10 for 5.3.1 3 t 1 5.3.[ la Cl Cl 11 5.3.C lb [ ] streem(s) in the box provided.) :SESssssasss9sssEscnnissiin:ssssitsi8:sssimt<sss*iisst>sssissnii8cinnsssiaisxi! ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) X Fran Stonmater 5.3. C lc 5.3.[ ]c 5.3.1 1c You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) B. Basis of Estimate (enter code) A.1 | Reporting Ranges 0 1-499 500-999 j A. 2 Enter Estimate C. Type of Treatment/ Disposal (enter code) Discharge to POTW 6 1 (enter location nurber from Part II, Section 1.) 1.1 ] Cl Cl l C1 | 6.1.[ lb [ ] 6.2. C Other off-site location ] (enter location nurber from Part II, Section 2.) 2. [ 1 1 1 3 t1 C1 i |6.2.I lb [ 1 ]|6.2.[ lc 6.2. C Other off-site location ] (enter location nuiber from Part 11, Section 2.) 2.C 1 1 1 3 I1 [1 1 |6.2.C lb [ 1 ]J6.2.[ lc Other off-site location 6.2. C 1 (enter location nurber from Part II, Section 2.) 2.[ I 6.2.t lb ( ]16.2.C ADDITIONAL INFORMATION ON WASTE TREATMENT METHOOS AND EFFICIENCY (Part III, Section 7) A. General Wastestream (enter code) j B. Treatment | Method j (enter code) C. Range of Influent Concentration (enter code) D. Sequential Treatment? (Check if applicable) | E. Treatment Efficiency Estimate 7.C 3a [ 1 1 7.1 ]b [ 3 1 7.1 lc [3 1 7.1 Id 1 1 7.1 le 7. [ 1 a [ ] 1 7.t lb I 3 1 7.C lc [3 1 7. [ Id 1 1 7.1 3 e 7. la 3 1 7.1 lb C 3 1 7. [ lc I3 1 7. [ 3d t 1 1 7.C le 7.C 1 a 7. 1 1 a I] t] 1 7. [ 1 7. [ lb C lb [ 3"l 7. t 1 1 7. [ lc lc C1 C1 l 7.1 1 7.[ Id Id t1 C3 i 7.C 1 7.1 le 3e - r la I 3 1 7.1 lb [ 3 1 7.1 lc (3 l 7. [ 3d [ 3 1 7. [ le ] a [ 1 1 7.1 ]b C 3 1 7.1 lc [1 1 7.1 Id t 1 1 7.C ]e /. c 1 a C ] 1 7. 1 lb ( 3 l 7.1 3c c] 1 7.1 3 d [ ] 1 7.C ] e 7.1 la t 1 1 7-1 lb [ 3 1 7. [ ] c C1 1 7.1 Id C 1 1 7. C 3 e EPA Form 9350-1 (1-90) Revised - Do not use previous versions Based on Operating Data? Yes No X |7.[ If ] [3 X 17. 3f 1 l1 X 17. [ ]f ] [1 X 17. t ]f 1 [1 X |7.[ 3 f 3 (] X 17* t If t 3 C1 X |7*t If C 1 C1 X |7-C If c 1 c] X |7.I If l 3 [1 313 ADVISOR SAL 000004350 EPA U.S. Envircnmentai Protection Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM Section 313 of the Emergency Planning end Ccanunlty Right-to-Know Act of 1986, also known as Title III of the Svperfund Amencfcientt and Reauthorlxatlon Act. Page 1 of 5 Methanol Gcnooo lake Charles Refi EPA FORM R PART I. FACILITY IDENTIFICATION SECTION 1.1 Are you claiming the chemical identity on page 3 trade secret? ( ] Yes (Answer question 1.2; IX] No (Do not answer 1.2; Attach substantiation forma.> Go to question 1.3.} 1.2 If MYesN in 1.1, is this copy: t ) Sanitized I 3 Unsanitized 1.3 Reporting Year 1989 2. CERTIFICATION (Read and sign after completing all sections.) I hereby certify that I have reviewed the attached documents and that, to the best of my knowledge and belief, the submitted information is true and complete and that the amounts and values in this report are accurate besed on reasonable estimates using data available to the preparers of this report. Name end official title of owner/operator or senior management official Don R. Unruh Refinery Manager Signature I Date signed |06-20-90 3. Facility Identification | Facility or Establishment Name I Conooo lake Charles Refinery Street Address Old Spanish Trail 3.1 City Westlake 1 County |Calcasieu State LA 1 Zip Code |70669 WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.0. BOX 23799 WASHINGTON, DC 20026*3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Nurber | 70669 CNCLK 0LE6P 3.2 | This report contains information for (Check one): a. CX 3 An entire facility b. ( ) Part of a facility. 3.3 | Technical Contact 1 Brandt Butler 3.4 j Public Contact Eton R. Unruh 1 Telephone Nunber j(316) 491-5599 I Telephone Nuiber 1(316) 491-5222 3.5 | SIC Code (4 digit) 1 1 a. 2911 | b. NA I c. NA 1 1 d* NA j e. NA | f. NA | 1 3.6 | | Degrees 030 Latitude Minutes 14 Seconds 36 1 1 | Degrees 093 Longitude Minutes 16 Seconds 20 3.7 j Dun & Bradstreet Nunber(s) a. 00-842-7692 1 1 b. NA 3.B | EPA Identification Nunber(s) (RCRA I.D. No.) 1 a. IAD990683716 | b. NA 3.9 | NPOES Permit Nunber(s) 1i a. IA0003026 i 1 b. NA j| Receiving Streams or Water Bodies (enter one name per box)| 11 a. Bayou Verdine b. NA I c. NA | e. NA 1 d. NA 1 f. NA i.11| Underground Injection Well Code (UIC) Identification Nunber(s) a. NA I b. NA 4. PARENT COMPANY INFORMATION 4.1 | Name of Parent Company E. I. Da Pont De Nemours | 4.2 I Parent Company's Oun A Bradstreet Nunber | I 00-131-5704 EPA Form 9350*1 (1*90) Revised - Do not use previous versions 313 ADVISOR SAL 000004351 >A Form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES 1. PUBLICLY OWNED TREATMENT WORKS (POTVS) 1.1 POTW name NA Street Address City | County 1 1.2 POTW name | NA | Street Address 1 | City Page 2 of S Methanol Oonooo lake Charles Rei j County State 1 Zip 1 | State i 1 Zip 1 Z. OTHER OFF-SITE LOCATIONS <00 NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name BFI 1 2.2 Off-site location name 1 OUI EPA Identification Nunber (RCRA ID No.} NA | EPA Identification Nuiber (RCRA ID No.) | LAD000777201 Street Address Cities Service Hwy 1-10 1 Street Address 1 Rt 2, John Brannon Rd City Sulfur | County 1 Calcasieu 11 c>Cjcyarlyss | County 1 Calcasieu state IA 1 Zip j 70664 1 State 1 IA | 7*5663 ication under control of reporting facility or parent Cv<^any? E 3 Yea C X No f Is location under control of reporting facility or parent | company? E 3 Yes EX] No 8S828SSISSISSISIIBSSS8 ^8S888S888a888SSS88SS88SS8S8aV8a8S8S8S88SS88IS88SX88S8888SS88S88888888S 2.3 Off-site location name NA 1 2.4 Off-site location name 1 NA EPA Identification Nunber (RCRA ID No.) Street Address | EPA Identification Nunber (RCRA 10 No.) i J Street Address City State | County 1 | Zip Is location under control of reporting facility or parent company? E 1 Yes E 3 No 2.5 Off-site location name NA EPA Identification Nunber (RCRA 10 No.) 1 City 1 | State | County 1 | Zip | Is location under control of reporting facility or parent | company? t 3 Yes E 3 No 1 2.6 Off-site location name j NA EPA Identification Number (RCRA ID No.) Street Address Street Address City | County | City j County 'te I Zip I State I Zip Is location under control of reporting facility or parent company? I I Yes [ ] No | Is location under control of reporting facility or parent | company? C 1 Yes t 1 No [ ] Check if additional pages of Part II are attached. How many? [ ] ' EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 A0V1S0R SAL 000004352 EPA FORM R PART III. CHEMICAL-SPECIFIC INFORMATION Methanol Conoco lake Charles Ref 1. CHEMICAL IDENTITY (Do not coaplete this section if you canplete Section 2. 1.1 | (Reserved] 1.2 I CAS Number (Enter the renter exactly as it appears on the 313 list. Enter NA if reporting chemical category.) I 000067--56--1 1.3 I Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 list.) I Methanol 1.4 | Generic Chemical Name (Conplete only if Part I, Section 1.1 is checked "Yes." Generic name aust be structurally descriptive.) 2. | MIXTURE COMPONENT IDENTITY (Do not complete this section if you cooplete Section 1.) | Generic Chemical Name Provided by Supplier (Limit the name to a maximum of 70 characters (e.g., renters, letters, spaces, | punctuation).) 3. } ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) | Manufacture the 3.1 I chemical: a. t 3 Produce b. [ ] Import j If produce or import: | c. I ] For on-site use/processing e. C 3 As i byproduct d. [ ] For sale/ distribution f. C 3 As an impurity Process the 3.2 chemical: a. [ ] As a reactant d. ( ) Repackaging only b. [ 3$ As i formulation component c. t 3 As an article cofl*wnent 3.3 | Otherwise use I the chemical: a. [ ] As a chemical processing aid b. I 3 As a manufacturing aid SSSSSSSSSSnSStfSStCStSEBSSXSSSSXBI 4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR c. tX] Ancillary or other use [06] (enter code) Sssssssssssssssssssss&sssssfssssitistssissssssssssssssi 5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases (l bs/yr) 8. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A. 2 Enter Estimate 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part l Section 3.10 for stream(s) in the box provided.} 5.3.1 5.3.2 5.3.3 [ a] [] [] | 5.1a 5.2a 1 5.3.1a 5.3.2a 5.3.3a E3 t3 C3 [3 (3 [3 [3 3 3 3 [3 l1 l3 [3 l3 1500 5.1b [0 3 1200 5.2b 10 3 C. X From Stormwater 0 5.3.1b [0 3 5.3.1c NA NA 5.3.2b C 3 5.3.2c NA 5.3.3b [ 3 5.3.3c 5.4 Underground Injection 5.4a| [ ] 3 l3 NA 5.4b [ 3 5.5 Releases to land 5.5.1 On-site landfill 5.5.2 Land treatment/application farming 5.5.3 Surface impoundnent 5.5.4 Other disposal 5.5.1a 5.5.2a 5.5.3a 5.5.4a 3 I3 t3 3 [3 [] 3 l3 C1 3 [3 [ 3 NA 5.5.1b [ 3 NA 5.5.2b [ ] NA 5.5.3b l 3 NA 5.5.4b t )1 ] (Check if additional information is provided on Part IV - Supplemental Information) EPA Form 9350-1 (1-90) Revised - Oo not use previous versions. 313 ADVISOR SAL 000004353 A FORM R PART III. CHEMICAL-SPECIFIC INFORMATION (continued) Pag* 4 of 5 Methanol Conoco lake Charles Ref1 u TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) A.1 I A.2 Reporting Ranges Enter 0 1-499 500-999 j Estimate B. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) Discharge to POTU 5.1.1 (enter location nuMser from Part 11, Section 1.) 1.C 3 El El [ 3 NA 6.1.1b C 3 Other Off-Site Location 6.2.1 (enter location nurtser from Part II, Section 2.) Other Off-Site Location 6.2.2 (enter location nustoer from Part II, Section 2.) Other Off-Site Location 6.2.3 (enter location nurber from Part 11, Section 2.) 2. E ] 2.1 ] 2.1 ] 1 | t] j E3 111 ) | NA | 6.2.1b [ ] | 6.2.1c III 13 C 3 Cl NA J 6.2.2b C 3 6.2.2c ] j [3 j [] 1 3 j j NA 6.2.3b 1 6.2.3c [ 3 (Check if additional information is provided on Part IV - Supplemental Information) 7. WASTE TREATMENT HETHOOS AND EFFICIENCY C ] Not Applicable <NA) - Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. A. -neral Wastestream (enter code) | B. Treatment j Method | (enter code) | C. Range of | Influent 1 Concentration j (enter code) | D. Sequential j Treatment? | (Check if j applicable) E. Treatment Efficiency Estimate F. Based on Operating Data? Yes 7.1a Ml | 7.1b Bll] | 7.1c [4] | 7.id l1 7.1e 100. 00 X 7.1f c ] 7.2a 7.3a t3 t3 | 7.2b | 7.3b t NA 3 [NA ] | | 7.2c 7.3c [3 [3 | 7.2d | 7.3d [3 [3 7.2e 7.3e X |7.2f X )7.3f [3 E3 No [X] t3 C3 7.4a CJ | 7.4b [NA 3 J 7.4c [3 | 7.4d [ 3 1 7.4e 7.5a 7.6a 7.7a 7.8a 7.9a 7.10a C3 E3 3 r3 c3 E3 | 7.5b j 7.6b | 7.7b | 7.8b [ 7.9b 1 7.10b [NA ] [ NA 1 [NA ] [NA ] [ NA ] [ NA ] | | | | | | 7.5c 7.6c 7.7c 7.8c 7.9c 7.10 [1 [3 [1 [3 [1 [3 | 7.5d | 7.6d | 7.7d | 7.8d | 7.9d | 7.10d [1 [3 E3 [3 [3 E3 | 7.5e | 7.6e | 7.7e j 7.Be \ 7.9e | 7.10e [ ] (Check if additional information is provided on Part IV - Supplemental Information) It |7.4f t 3 X |7.5f [ 3 X |7.6f E ] X 17*7f [ ] X )7.8f c 3 X |7.9f [ 3 X 17.10 f 1 t3 E3 [3 c1 E) C3 E3 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) 8. Quantity of the Chemical in Wastes Prior to Treatment or Disposal C. Index | D. Reason for Action | (enter code) 1 M[ ] | Current j reporting | year (Ibs/yr) l | Prior year (Ibs/yr) [Or Percent [Change j U ! [tl- %[3 R[ 3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR SAL 000004354- Page 5 of 5 EPA FORM R PART IV. SUPPLEMENTAL INFORMATION Use this section if you need additional space for answers to questions in Part III. Nunber the tines used sequentially from tines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) Methanol Oonoco Lake Charles Ref ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part III, Sections.3) You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases <lbs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.3 Discharges to receiving streanm or water bodies (Enter letter code from Part 1 Section 3.10 for stream(s) in the box provided.) 5.3.t ] 5.3.1 3 5.3.1 1 | C ]15-3.C I ] (5.3.1 [ ] 5.3.1 j | ]a )a ]a l) C] C] 11 l3 13 13 13 I] X From Stormater 5.3.C lb I 3 5.3.t ]c 5.3.t Jb C 1 5.3.1 3c 5.3. C ]b C ] 5.3.1 ] c ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) 1 A. Total Transfers (Ibs/yr) |B. Basis of | Estimate ) (enter code) A.1 | Reporting Ranges 1 0 1-499 500-999 | 1 A.2 j Enter Estimate C. Type of Treatment/ Disposal (enter code) Discharge to P0TU .1.1 3 (enter location nurtoer from Part II, Section 1.) Other off-site location 6.2.1 I (enter location nuiber from Part II, Section 2.) 1.[ ] 2.[ ] ti :3 j C) | I [] j (3 [] l [6.1.1 3b C 1 3 (6.2.[ )b ( I J 6.2.t }c I Other off-site location 6.2. [ ] (enter location nunber from Part II, Section 2.) 2.( ] | ] | [] [] |6.2.I ]b [ I 3 16.2.C 3c I Other off-site location 6.2.1 3 (enter location nunber from Part II, Section 2.) 2.[ [6.2.[ ]b l I 116.2.[ Jc I ADDITIONAL INFORMATION ON WASTE TREATMENT METHOOS AND EFFICIENCY (Part lit. Section 7) A. General uastestream (enter code) | B. Treatment | Method j (enter code) | C. Range of Influent | Concentration j (enter code) | D. Sequential Treatment? j (Check if j applicable) 7. C 3a C ] 1 7.1 3b C 31 | 7. [ )c t3 1 7- [ 3d [ 3 7. [ ]a 7. [ 3 a [3 t3 1 7.C 1 7.1 3b [ ]b [ 1 | 7.1 1 | 7.1 ]C 3c [] l3 l 7. E 1 7-t 3d 3d C3 (3 7.1 3a t J 1 7-1 ]b [ J | 7.1 Jc [3 1 7.1 3d I 3 7.1 3a t 3 1 7.1 3b C 1 1 7.[ 3c t3 1 7. C 3d C 1 7. [ 3 a [ 3 1 7.1 3b l 3 | 7.1 3c (3 1 7. [ 3d [ 1 7.: 3a 7. C 3 a 3 [3 1 7.1 1 7.1 3b [ 3b C 3 | 7.[ 3 | 7.E ]c 3c (] l3 1 7-t 3d [ 3 1 7.1 3d C 3 7.1 la [ 3 1 7. E 3b t 3 1 7.1 3c [3 1 7.1 EPA Form 9350-1 (1*90) Revised - Do not use previous versions. 3d C3 | E. Treatment Efficiency | Estimate 1 1 7.1 3e 1 7.C 1 7. C ]e ]e ! 7.1 3 e 1 7.1 3 e 1 7.1 ]e 1 7-t 3e 1 7. [ 3e 1 7-t 3e | F. Based on Operating Data? | Yes X 17-1 3 f l 3 X |7.[ If [ 3 X |7.t 3 f [ 3 X |7.[ If I 3 X |7-1 If l 3 X |7-t X 17-1 X |7.t 3f 3 3f [ 3 3f [ 3 X 17. C 3f [ 3 313 ADVISOR No [3 t3 [3 t3 3 [3 3 l3 SAL OOOOO4355 EPA U.S. Environmental Protection Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM Section 313 of the Emergency Planning and Community Right-to-know Act of 1986, also known as Title III of the St^serfiaid Amendments and Reauthorization Act. 1 of S Molybdenum OCDOCO TaVn QlSUTlOS Rsfl I EPA FORM R S5V PART I. FACILITY IDENTIFICATION SECTION 1.1 Are you claiming the chemical identity on page 3 trade secret? | 1.2 If HYesM in 1.1, is this copy: [ ] Yes (Answer question 1.2; [Xl No (Do not answer 1.2; l C 1 Sanitized l 1 Unsanitized Attach substantiation forms.) Go to question 1.3.) j 1.3 Reporting Year 1989 2. CERTIFICATION (Read and sign after completing all sections.) I hereby certify that I have reviewed the attached documents and that, to the best of my knowledge and belief, the submitted information is true and complete and that the mounts arvi values in this report are accurate based on reasonable estimates using data available to the preparers of this report. Name and official title of owner/operator or senior management official Den R. Unruh Refinery Manager Signature I Date signed I 06-20-90 3. Facility Identification Facility or Establishment Name Conoco Lake Charles Refinery Street Address Old Spanish Trail WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.0. BOX 23799 WASHINGTON, DC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY City Westlake State LA 1 County | Calcasieu I Zip Code |70669 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Nunber 70669 CNCXK OLESP 3.2 | This report contains information for (Check one): 3.3 | Technical Contact j Brandt Butler a. [Xl An entire facility I Telephone Nurber |(318) 491-5599 b. [ ] Part of a facility. 3.4 | Public Contact Don R. Unruh 3.5 | SIC Code (4 digit) | 1 a. 2911 j b. NA | j c.NA 1 J.O Degrees 030 Latitude Minutes 14 Seconds 36 3.7 | Dun & Bradstreet Nunber(s) 1 a. 00-842-7692 3.8 EPA Identification Nunber(s) (RCRA I.D. No.) a. IAD990683716 1 Telephone Nuifeer |(316) 491-5222 1 1 d. NA | e. NA 1 Longitude | Degrees 093 Minutes 16 1 1 b- NA 1 b. NA 1j f. sNTMA Seconds 20 11 3.9 NPDES Permit NuTper(s) a. IA0003026 f 1 b- NA 3.10 Receiving Streams or Water Bodies (enter one name per box) 1 a. Bayou Verdine 1 b. c. NA 1 d. NA NA e. NA i f. NA 11 Underground Injection Well Code (UIC) Identification Nuiber(s) a. NA 1 b. NA 4. PARENT COMPANY INFORMATION 4.1 I Name of Parent Company | E. I. Du Pont De Nemours | 4.2 I Parent Company's Dun & Bradstreet Niinber j | 00-131-5704 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR SAL 000004356 EPA Form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES 1. PUBLICLY OWNED TREATMENT WORKS (POTWs) 1.1 POTW name NA Street Address City 1[ County I 1.2 POTW name I NA j Street Address 1 | City Page 2 c Molybdenum tricocide Ocnooo Ieke Cbarlps | County State ;1 Zip | State 1 2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 1 Zip }_________________ 2.1 Off-site location name BFI 1 2.2 Off-site location name 1 CWMX EPA Identificat ion Nurber (RCRA ID No.) NA ( EPA Identification Nurber (RCRA ID No.) j IAD000777201 Street Address Cities Service Hwy 1-10 | Street Address | Rt 2, John Brannon Rd City Sulfur | County | Calcasieu 1 j CCityarlyss | County j CalcasieL State IA 1 Zip | 70664 Is Location under control of reporting facility or parent company? t 3 Yes [ S Ho 2.3 Off-site location name NA 1 State 1 IA | 7(5663 Is Location under control of reporting facility or pare company? t 1 Yes $:isssissss3S3ansaissssss<8$issMfMCtniMinn' 2.4 Off-site location name NA EPA Identification Nurber (RCRA ID No.) | EPA Identification Nurber (RCRA ID No.) 1 Street Address | Street Address City State | County 1 | Zip Is location under control of reporting facility or parent company? [ 3 Yes C 1 No 2.5 Off-site location name NA EPA Identification Nurber <RCRA ID No.) I City i | State | County 1 | Z'P | Is location under control of reporting facility or par | conpany? [ 3 Yes I 2.6 Off-site location name NA EPA Identification Nurber (RCRA ID No.) Street Address City County Street Address City County State I Zip I State I Zip Is location under control of reporting facility or parent company? [ I Yes l ] No | Is location under control of reporting facility j company? I3 J [ 3 Check if additional pages of Part II are attached. How many? [ 1 EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR SAL 000004357 est^ooooo tvs 80SIA0V l `suoiSJaA snoiA^Jd asn aou oq - pasiAay (06-0 t-0S6 uuoj vd3 (uoiieuMOjuj ]ejusu*3}ddns - AI usd uo papiAOjd si uoiaenuo^ui isooiaippe >i ^oayD) i t HVS'S I l ) q*s`s ! 1 ] q2`5*S \ t ) qi*s*5 j VN VN W W t) C) [) t] 1 t3 t [ ( t3 t3 l t3 i ers's 1 e`S*S | 2'S*S i BCS'S 1 issodsip jamo ?*S'S auauouoodwi assiJDS 'S*5 Sutwjs# uoiaeonqae/Auaiuaeaai puei z'S"S m*pu3 aiis-uo rs*s puei oa sassaiay 5*5 ! c 3 qvs 3`-S 32*rs PC*S aaasmuoas >uoJi % *3 t C l ) qrrs ) qz'*s ) qcrs VN 1 t ) t t 1 a^'S VN VN VN L] t1 [] [ l1 [3 t3 CI l3 e'*S Z'*S eV*'S uotaoafui punojsjapun y*s (-papiAOJd xoq am ui (s)uieajas t 3 ** Jo# 01 * uoiaoas 1 aasd t 3 2``S apoa uaaaai jaau3) C 1 i/*S satpoq jaasn jo suisajas BuiAiaoaj oa saejeqosio `$ it ) i............... 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(jA/sqi) sassa^ad )evn -y 311S-H0 AN3WNOBIAN3 3H1 01 1O1H3H0 3H1 iO S3SV313K '5 SSSCSCEXSCCSSSSSXSS:SSSSS3SS3:SS3SXSSS3S3SSSSSa3SEZSSassI3SBasS>3SKKXSUs::SS:SSS83SSSS3SSSSSSSS3SSXSSSSSSSSSSftSt3SSSSSS:CS (apoo Jaaua) cgo3 V3A JJVaH3*ry3 3H1 SN1W10 3WJA AW IV 3JJS-H0 IVOIWJO 3Hi JO iNDOMV HOWIX aaMnMm>SnnS3SSS*SSSS3SSSSE>SSUSSSSSSCSEaSMBSSSSeiSSSS&SSSSSS3SaasSMSSS3$SS*SSSSSSCSSXK3S8XS8<3SSSSS*SSt pis fiuissaoojd :ieoiuip am ) asn jai|AO 40 Ajs^iouv [ j *3 pis 6uijnaos*nueu s sy [ j *q isotwaqo a sy i)) ** asn asmjamo | ** * auauoduoo apijj# us sy i i *o auauoduioo uoiisinuuoj e sy [ ] *q A)uo SuiBsyoeday t ) -p ausaoeaj e sy [ ] *e AatJnduu us sy [ ) > uoianqijasip /a)is joj [ j *p aonpojdAq t sy t Buissaoojd/asn sais-uo joi c ] *a j *o :uodun jo aonpoad >i uo(*in c ) *q aonpoud [ J *s t^eoiuwip | Z'Z am ssapoud | :}90t(U9<13 | l* MJ ajnaosjrausH \ CA^dds asm ))t yaaMO) AiniDVi 3Hi IV TOIH3H3 3Hi 30 S3S0 <WV S3UIAU3V 1 * C(uopsnaand 'saoods 'toaaas) 'sjaqunu **8*a) suaaovjeip QZ *o natx a oa aweu am ajn) japddns Aq papiAOJd awey asoiwaip opauag Cl uoiaoas aaaidwoo rwA *t uopoas siqa aaaidwoo aou oo) A1UH3Q1 IH3HCMH03 attfUXlW | *2 :s3883scssxasc>s>Mss3sssnsssamssnH33US8<ss3aMMntsMcassttss3mwRMS33s(s3ss*asssms {'SAiadijasap Apsjnaoruas aq asnu ausu ouauas h*s*Ak payoaip } i*l uoiaoas T ajed Ajuo aaajdwoo) assy pojwaio oijauao | *t`i appcotJT amsfpc^xcw I <*asn l am uo sjssdd* ai ss Apoaxa awsu am jaaua) away Ajo6aa*9 jsoiuaio jo leouuaip j *; S-42-ETET00 , <*Ajoft3o >B?twauo BuiaJodaj p yy jama *a*n l m uo sasadde at ss Apovxa jaqunu am Jju3) jacpny SVD ) Z`) tpaAjasay] j c: 3WI OOOUQO 9ppODpa mnuapqAxcM S A 5 aftad *2 uoiaaas saaicteoa noA >i uoiaoas siqa aasi^soo aou oq) A1JAH3Q1 1V31H3H3 '< iscsussssssssssmsms'- NOliVKUOdHI DI3I33dSO]H3HO * HI l*d H HHQi o >f!ni-ineaww; Page 4 of 5 ERA FORM R PART III. CHEMICAL-SPECIFIC INFORMATION (continued) Molybdenum triood.de Ccnooo lake Charles Ref 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.T end A.2) A. Total Transfers (Ibs/yr) 8. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate C. Type of Treatment/ Disposal (enter code) Discharge to POTW .1.1 (enter location nuober from Part II, Section 1.) 6.2.1 Other Off-Site Location (enter location cumber from Part 11, Section 2.) 1.(] 1 | t] j (] t3 2.t I (3 C3 [. NA | 6.1.1b [ 1 ] NA 6.2.1b ( 3 6.2.1c Other Off-Site Location 6.2.2 (enter location nurber from Part II, Section 2.) 2.1 ] [3 C3 l3 NA 6.2.2b ( 3 6.2.2c Other Off-Site Location 6.2.3 (enter location mmber from Part 11, Section 2.) 2.C ] C1 t3 [ ] NA 6.2.3b ( ] ! 6.2.3c 1 t 3 (Check if additional information is provided on Part IV - Supplemental Information) ::sss:sssssssssuut$stsssxsss:sssi:ssssss:rs3:ssssEsss:sKcsxSEt*ttCatcnsssacsiiusxuiinsssss3xxiiiiiitisfiiiKitiMn 7. WASTE TREATMENT METKOOS AND EFFICIENCY [X 1 Mot Applicable (NA) Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. A. General Wastestream (enter code) B. Treatment Method (enter code) C. Range of Influent Concentration (enter code) D. Sequential Treatment? (Check if applicable) E. Treatment Efficiency Estimate F. Based on Operating Oata? Yes No 7.1a 7.2a 7.3a 7.4a 7.5a 7.6a C3 l3 [3 [3 c3 l3 7.1b 7.2b 7.3b | 7.4b | 7.5b | 7.6b l l [ I [ [ 3 3 3 3| 3| 3| 7.1c 7.2c 7.3c 7.4c 7.5c 7.6c [3 [3 t3 [] [3 C3 7. Id 7.2d 7.3d | 7.4d | 7.5d | 7.6d l] (3 [3 (3 l3 t3 7-1* 7.2e | 7.3e | 7.4e | 7.5e | 7.6e * 7.1f X 7.2f X 7.3f X 7.4f X 7.5f X |7.6f (3 t3 [3 C3 t3 l3 l3 [3 C3 C3 t 3 [3 7.7a c3 | 7.7b l 3| 7.7c t3 | 7.7d C 3 | 7.7e X 17 - 7f c 3 [3 -4 CD 7.8a 7.9a 7.10a t3 [1 c3 | 7.8b | 7.9b | 7.10b l l ( 3| 3| 3| 7.8c 7.9c 7.10 c3 [3 c3 | 7.8d | 7.9d | 7.10d l3 [3 C3 | 7.8e | 7.9e | 7.10e X [3 X |7.9f c 3 X |7.1Of [ 3 (3 [3 C3 [ ] (Check if additional information is provided on Part IV - Supplemental Information) 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) 8. Quantity of the Chemical in Wastes Prior to Treatment or Disposal C. index | D. Reason for Action (enter code) Current reporting year (Ibs/yr) Prior year (Ibs/yr) Or Percent Change C 3+ C 3- tPA Form 9350-1 (1-90) Revised - Do not use previous versions. X R t- ] 313 ADVISOR SAL 000004359 Page 5 of 5 EPA FORM R PART IV. SUPPLEMENTAL INFORMATION Use this section if you need Additional space for answers to questions in Part III. j*ber the lines used sequentially from lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) Molybdenum trioocLcte Oanoco lake Charles Refi ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part III, Section 5.3) You may report releases of less than 1,000 lbs by checking ranges tnder A.1 (Do not use both A.1 and A.2) A. Total Releases <lbs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for streanKs) in the box provided.) 5.3.C 5.3.1 5.3.1 ] I ] C 3 5.3.1 3a I 3 5.3.t ]a E 3 5.3. C 3a [3 c3 c3 C3 l3 [3 (3 C3 3 5.3. C )b C 5.3. C )b C 5.3.1 ]b C ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) B. Basis of Estimate (enter code) A.1 l Reporting Ranges 0 1-499 S00-999 | A.2 Enter Estimate C. X From Stormwater 1 S.3. [ 1c 3 5.3.C lc 3 5.3.f 3c C. Type of Treatment/ Disposal (enter code) Discharge to POTW l.[ ) (enter location number from Part II, Section 1.) 1.( 3 3 3 1 3 | 6.1. 3b [ 3 Other off-site location 6.2.1 ] (enter location nuiber from Part II, Section 2.) 2.1 3 3 3 3 6.2.[ ]b [ 1 J j6.2.t ]c Other off-site location 6.2.[ ] (enter location nunber from Part II, Section 2.) 2.1 ) | 3 | E3 1 [3 j j 6.2.[ 3b 3 6.2.[ ]c Other off-site location 6.2. [ 3 (enter location nunber from Part II, Section 2.) 2.E 3 3 [] 1 E3 j 1 |6.2.1 ]b [ 1 ] |6.2.[ 3c ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Pert III, Section 7) A. General Uastestream (enter code) | B. Treatment | Method j (enter code) C. Range of Influent Concentration (enter code) D. Sequential Treatment? (Check if applicable) | E. Treatment Efficiency | Estimate 1 7. [ la 3 1 7.[ 3b C 3 7.[ 3c [ 7.E 3d 1 1 7.[ 3e 7. [ 3 a [ 3 1 7. [ 3b 3 7- E 3c [ 7.E Id E 3 1 7.1 3e 7.1 3a l 3 1 7.C 3b t 3 7.E 3c E 7-t 3d C 3 1 7- C ]e 7.C 3 a [ 3 1 7.1 3b C 3 1 7.[ ]e t 7.r Id 1 1 7. [ 3e 7 t ]a [ 3 1 7.1 3b C 3 1 7.1 3c C1 1 7.1 3d t 3 1 7.1 ]e 7. [ 3a [ 3 1 7.[ 3b ( 3 1 7.[ 3c E3 1 7.C 3d [ 3 1 7.C le 7 C 3a E 3 1 7.1 3b C 1 1 7.1 3c [3 1 7.[ 3d t 3 1 7.1 ]e . ( 3a C 3 1 7. t 3b C 3 | 7.1 3c E3 1 7.1 3d E 3 1 7-1 3 e 7. [ 3 a [ 3 1 7.1 ]b 3 1 7.[ 3c ] 1 7.[ 3d ( 3 1 7.C 3 e EPA Form 9350-1 (1-90) Revised - Oo not use previous versions F. Based on Operating Data? | Yes X |7.[ 3 f ( X 17- E If X |7-[ 3 f t 3 X (7. X |7. 3f E 1 3f 3 X 17. 3 f C 3 X |7.t 3f 3 X |7-t If [ 3 X |7.[ If [ 3 315 ADVISOR No E3 3 3 E3 3 3 [3 C3 3 SAL 000004360 EPA U.S. Environmental Protaction Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM Section 313 of the Emergency Planning and Canmity Right-to-Know Act of 1986, I also knom aa Title III of the S^terfund Aunhenti and Reauthorization Act. Page 1 of 5 Naphthalene CcnOOO Talca Paries Ref EPA FORM R PART I. FACILITY IDENTIFICATION SECTION 1.1 Are you claiming the chemical identity on page 3 trade secret? J 1.2 If MYesM in 1.1, is this copy: C 3 Yes (Answer question 1.2; (Xi No (Do not answer 1.2; 1 E 3 Sanitized ( 3 Unsanitized Attach siAactantiation forma.) Co to question 1.3.) | 1.3 Reporting Year 1989 2. CERTIFICATION (Read and sign after eespleting all sections.) I hereby certify that I have reviewed the attached doeueents and that, to the best of my knowledge and belief, the admitted information is true and complete and that the amounts and values in this report are accurate based on reaeormble estimates using data available to the preparers of this report. Name and official title of ouner/operator or senior manageamnt official Don R. Unruh Refinery Manager Signature 3. Facility Identification Facility or Establishment Neste Conoco Lake Charles Refinery Street Address Old Spanish Trail Date signed I06-20-90 WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.O. BOX 23799 WASHINGTON, DC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY City Westlake State LA 1 County j Calcasieu | Zip Code |70669 2. APPROPRIATE STATE OFFICE (See instruction in Appendix G) TRI Facility Identification Umber 70669 CNCLK OIDSP 3.2 | This report contairs information for (Check one): a. (Xl An entire facility b. t ) Part of a facility. 3.3 j Technical Contact | Brandt Butler | Telephone Nurber |(318) 491-5599 3.4 | Public Contact Don R. Unruh 1 Telephone Nurber 1(318) 491-5222 3.5 | SIC Code (4 digit) 1 1 a. 2911 | b. NA Latitude 1 | c.NA 1 NA 1 d. | e. NA Longitude | f. NA ! Degrees 030 Minutes 14 Seconds 36 | Degrees 093 Minutes 16 Seconds 20 3.7 | Dun & Bradstreet Nuitoer(s) 1 a. 00-842-7692 1 1 b. NA 3,| EPA Identification Number(s) (RCRA I.D. No.) a. IAD990683716 3.9 NPOES Permit Nurtoer(s) a. LA0003026 1 1 b- NA 1 1 b. NA Receiving Streams or Water Bodres (enter one name per box)| a. Bayou Verdine 1 b. NA c. NA t d. NA e. NA I f- NA .,.11 Underground Injection Weil Code <UIC) Identification Niarber(s) a. NA 1 b. NA 4. PARENT COMPANY INFORMATION 4.1 I Name of Parent Company | E. I. Du Pent De Nemours I 4.2 I Parent Company's Dun & Bradstreet Nmtoer j | 00-131-5704 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR SAL 000004361 \ Form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES 1. PUBLICLY OWNED TREATMENT WORKS <POTUs) 1.1 POTV name NA Street Address City J County 1 1.2 P07W name | NA J Street Address | City Page 2 of 5 Naphthalene Ocnooo lake Charles Refi | Couity State 1 Zip 1 j State j Zip 2. OTHER OFF-SITE LOCATIONS (DO HOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name BFI 1 2.2 Off-site location name I am EPA Identification Hunter (RCRA ID No.) NA | EPA Identification Hunter (RCRA ID No.) 1 IAD000777201 Street Address Cities Service Hwy @ 1-10 city Sulfur |j County Calcasieu 1 Street Address j Rt 2, John Brannon Pd 1| Car.lyss | Couity j Calcasieu State LA j Zip | 70664 nation under control of reporting facility or parent c- --any? t I Yes C X No 2.3 Off-site location name NA EPA Identification Nuiter (RCRA ID No.) I State 1 IA | 7^663 | Is location under control of reporting facility or parent | conpany? ( ] Yes [X] No ssssssssssnsscssHCsnsx 1 2.4 Off-site location name 1 NA | EPA Identification Nuiter (RCRA ID No.) Street Address City State | County 1 | Zip | Street Address 1 City 1 | State | County 1 | Zip Is location under control of reporting facility or parent company? C ] Yes t ] No 2.5 Off-site location name NA EPA Identification Nuiter (RCRA ID No.) | Is location under control of reporting facility or parent | conpany? C ] Yes t J No BSSSSSS8SSSS8SS88SSSS8BtSSSSSCSSISSSSS 2.6 Off-site Location name NA EPA Identification Nuiter (RCRA ID No.) Street Address Street Address City | County City County Tte Zip State Zip Is location under control of reporting facility or parent company? I 1 Yes l I No Is location under control of reporting facility or parent company? C 3 Yes f ( ] Check if additional pages of Part II are attached. How many? Cl ' EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR SAL 000004362 No Page 3 of 5 CPA FORM R PART 111. CHEMICAL-SPECIFIC INFORMATION Naphthalene Oonoco Lake Charles Ref? 1. CHEMICAL IDENTITY (Do not complete this section if you complete Section 2. 1.11 (Reserved] 1.2 [ CAS Nimfaer (Enter the nuafaer exactly aa it appears on the 313 list. Enter NA if reporting chemical category.) [ 000091-20-3 1.3 11 Chemical or Chemical Category Name (Enter the name exactly aa it appears on the 313 list.) | Naphthalene 1.4 | Generic ebonies! Nano (Complete only if Part I, Section 1.1 is checked "Yes." Generic none nust be structurally descriptive.) 2. MIXTURE COMPONENT IDENTITY (Oo not complete this section if you cooplete Section 1.) Generic Chemical None Provided by Supplier (Unit the name to e maximise of 70 characters (e.g., nudaers, letters, spaces, punctuation).) uintnitumtituiiuiuiinaia 3. | ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) Manufacture the 3.1 chemical: a. C ] Produce b. ( 1 Inport If produce or import: c. ( ] For on-site use/processing e. [ ) As a byproduct d. ( ] For sale/ distribution f. C 3 As an impurity Process the 3.2 chemical: a. [X] As a reactant d. ( 3 Repackaging only b. [ ] As a formulation cowponent c. [ ] As an article cooponent 3.3 | Otherwise use I the chemical: a. C ] As a chemical processing aid b. [ ] As a manufacturing aid !8tXSSeCtSCtXSllftCtCCCBHmSSSSSl MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR c. [X] Ancillary or other use [07] (enter code) ssssstsssfisssiusssnsisnniSRSfsiusmtsntfstsiutssMtustiltsttttitiiMttittgttmssiRCSSiiiisiissssssncgMsstiistvtaittaBta S. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases (l bs/yr) 8. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.2 5.3.3 [a] C] [] 5.4 Underground Injection 5.1a 5.2a t1 t1 (] 1 (3 (3 5.3.1a 5.3.2a 5.3.3a C] [1 [] ] t] ] () ] l3 5.4a| t ] ] (] 7300 5.1b (0 3 3200| 5.2b [0 ] 34 NA NA 5.3.1b [M ] 5.3.2b ( ] 5.3.3b c ] C. X From Stormwater 5.3.1c NA 5.3.2c 5.3.3c NA | 5.4b [ 1 5.5 Releases to land 5.5.1 On-site landfill 5.5.2 Land treatment/application farming 5.5.3 Surface impoundnent 5.5.4 Other disposal 5.5.1a 5.5.2a 5.5.3a 5.5.4a ] (1 [] ] [] ( ] ] [] [ 1 ] [1 t1 1 NA 5.5.1b ( ] NA 1 5.5.2b l 3 NA j 5.5.3b [ 1 NA i 5.5.4b c J ] (Check if additional information is provided on Part IV - Supplemental Information) EPA Form 9350-1 (1-90) Revised - Oo not use previous versions. 313 ADVISOR SAL 000004363 Page 4 of 5 EPA FORM R PART III. CHEMICAL-SPECIFIC INFORMATION (continued) Naphthalene Qcnoco lake Charles Refi 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS A. Total Transfers (Ibs/yr) You may report transfers of less than 1,000 lbs by checking ranges tsider A.1. (Do not use both A.1 and A.2) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate B. Basis of Estimate (enter cede) C. Type of Treatment/ Disposal (enter code) 6.1.1 Discharge to P0TW (enter location ranber from Part II, Section 1.) 1.1 3 1 [ [] | [3 (3 NA 6.1.1b [ 3 6.2.1 Other Off-Site Location (enter location number from Part II, Section 2.) 2.(2 3 (3 (3 (3 980 6.2.1b [O 3 6.2.1c K72 Other Off-Site Location 6.2.2 (enter location nunber from Part II, Section 2.) 2.(1 3 ( 3 (3 (3 1200 6.2.2b (0 3 6.2.2c M72 Other Off-Site Location 6.2.3 (enter location nurber from Part 11, Section 2.) 2.[ 3 (3 (3 (3 6.2.3b E ] | 6.2.3c NA 1 [ ] (Check if additional information is provided on Part IV - Supplemental Information) 7. WASTE TREATMENT METHOOS AND EFFICIENCY ( ] Not Applicable (NA) - Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. eneral Wastestream (enter code) B. Treatment Method (enter code) C. Range of Influent Concentration (enter code) D. Sequential Treatment? (Check if applicable) E. Treatment Efficiency Estimate F. Based on Operating Data? Yes NO 7.1a 7.2a fWl [A] 7.1b 7.2b [Bill [ A07) 7.1c 7.2c (43 [23 7.Id 7.2d E3 E3 7-1* 7.2e 95.00X 7.1f 88.00 X |7.2f E3 [X] E X] [3 7.3a 7.4a 7.5a 7.6a [3 E3 [3 [3 7.3b ! 7.4b | 7.5b | 7.6b [NA ] [NA 3 [NA 3 [NA 3 j | | 7.3c 7.4c 7.5c 7.6c C3 [3 E3 E3 | 7.3d j 7.4d | 7.5d | 7.6d E3 E3 t3 E3 7.3e | 7.4e | 7.5e | 7.6e X 7.3f X |7.4f X |7.5f X |7.6f [3 [3 t3 [3 C3 E3 E] {3 7.7a 7.8a 7.9a 7.10a (3 t3 [3 E1 | 7.7b | 7.8b 1 7.9b I 7.10b [NA 3 [NA ] [NA i [NA ] 1 | | 1 7.7c 7.8c 7.9c 7.10 E3 E3 E3 I3 | 7.7d | 7.8d 1 7.9d 1 7.10d E1 (3 E3 C3 | 7.7e | 7.Be | 7.9e I 7.10e X |7.7f [ 3 X |7.8f [ 3 X |7.9f [ 3 X |7.10f [ 3 E3 [1 t3 [] [ 3 (Check if additional information is provided on Part IV - Supplemental Information) 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) | B. Quantity of the Chemical in Wastes j Prior to Treatment or Disposal | | C. Index I D. Reason for Action (enter code) M[ ] Current reporting year (Ibs/yr) Prior year (Ibs/yr) Or Percent Change [ ) [ 3- EPA Form 9350-1 (1-90) Revised - Do not use previous versions. X [ 1 I 3| R ( '3 313 ADVISOR SAL 000004364 Page 5 of 5 <-PA FOAM R PART IV. SUPPLEMENTAL INFORMATION Use this section if yog need additional spece for answers to questions in Part 111 timber the lines used sequentially fro* lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) Naphthalene Ocnoco lake Claries Refj ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part III, Section 5.3) You may report releases of less than 1,000 lbs by checking ranges under A.1. (0o not use both A.1 and A.2) A. Total Releases (Ibs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies (Enter letter code from Pert 1 Section 3.10 for strean(s) in the box provided.) 5.3.1 5.3. [ 5.3.1 3 ) 3 S.3.C 3 5.3.C C ) 5.3.1 CI 3 3 t1 3 3 3 3 1 5.3.C 3b t 5.3. 3b ( 5.3. 3b [ ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part in, Section 6) You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate C. X From Stormwater 5.3.1 Jc 5.3.1 )c 5.3.1 3c iriimxuxitnuuti C. Type of Treatment/ Disposal (enter code) Discharge to POTW '.[ 3 (enter location nuitoer from Part 11, Section 1.) 1. 3 | [3 | C3 3 6.1. [ 3b t 3 Other off-site location 6.2. [ 3 (enter location nuiber from Part II, Section 2.) 6.2.1 Other off-site location ] (enter location number from Part II, Section 2.) 2. ( 3 2. [ 3 ti 1 11 3 [3 | 11 1 11 3 `1 1 6.2.[ 3b [ 6.2.1 3b [ 1 3|6.2.[ 1 3c 1 3|6.2.[ 3c Other off-site location 6.2. C 3 (enter location mutter from Part II, Section 2.) 2.C ) 3 I 3 |6.2. ]b t ADDITIONAL INFORMATION ON WASTE TREATMENT METH00S AND EFFICIENCY (Part III, Section 7) 6.2.C 1C issssmsss A. General Uastestream (enter code) { 8. Treatment 1 Method ) j Center code) C. Range of Influent Concentration (enter code) D. Sequential Treatment? (Check if applicable) 7. t la 7. [ 3 a 7. [ 3a 7.[ 3a 7.1 la C3 C3 3 3 C3 I 7.C 3b l | 7. [ 3b 1 7-t 3b 1 7.1 3b 1 7. 3b C 3 1 7. 3 1 7. [ 3 1 7. [ 3-1 7. [ 3 1 7.C 3c lc ]c 3c lc r3 t3 [3 c3 c3 1 7.1 3d I 3 1 7. 3d C 1 1 7-C Id t 3 | 7. 3d 3 1 7. Id 3 7. 3a C 3 | 7,1 3b 3 1 7.1 3c [J 1 7.1 3d 3 . t la 7.C 3 a 7. 3 a 3 C1 t3 1 7.[ 1 7.[ ! 7.1 3b [ 3b [ 3b 3 1 7. [ 3 l 7. 3 1 7. [ 3c lc 3c t3 [3 [1 | 7. [ Id 3 1 7.1 Id t 3 1 7- 3d [ 3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. | E. Treatment Efficiency | Estimate 1 1 7.1 ]e 1 7.1 3e l 7- 3e 1 7.t le f 7.C 3e i 7- 1 7-1 1 7-C 1 7.C ] 3e Je ]e ' ] F. Based on 1 Operating j Data? j Yes X |7. X |7. X |7.[ X |7.t If [ 3 If 3 3f [ 3 3f 3 X |7-C U [ 3 X |7.C If t 1 X |7.[ 3 f 3 X 17- X 17-1 3f [ 3 If 3 313 ADVISOR NO t3 1 3 C3 J t3 3 3 [3 S`*t 0004365 EPA U.S. Environment*t Protection A9ency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM 'ction 313 of the Emergency Planning end Cemmity Right-to-Know Act of 1986, so known as Title III of the Superfml Amendments and Reauthorization Act. Page 1 of 5 Phosphoric QCRTOOO lake Charles Refj. EPA FORM R PART I. FACILITY IDENTIFICATION SECTION 1.1 Are you claiming the chemical identity on page 3 trade secret? 1.2 If HYesM in 1.1, is this copy: [ ] Yes (Answer question 1.2; iXl No (Do not answer 1.2; I J Sanitized ] unsanitized Attach sibetantiation forms.) Go to question 1.3.) 1.3 Reporting Year 1989 2. CERTIFICATION (Read and sign after completing all sections.) I hereby certify that 1 have reviewed the attached docuaents and that, to the best of my knowledge and belief, the siiasitted information is true and cooplete and that the anoints and values in this report are accurate based on reasonable estimates using data available to the preparers of this report. lime and official title of owner/operator or senior management official Don R. Unruh Refinery Manager Signature I Date signed I 06-20-90 3. Facility Identification Facility or Establishment Name Conoco lake diaries Refinery Street Address Old Spanish Trail WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.0. BOX 23799 WASHINGTON, DC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY City Westlake State IA 1 County i Calcasieu 1 Zip Code |70669 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Number 70669 CHC1X OLDSP 3-2 1 This report contains information for (Check one): 3-3 | Technical Contact l Brandt Butler 3.4 | Public Contact Don R. Unruh a. An entire facility b. [ ] Part of a facility. 1 Telephone Ninber |(318) 491-5599 1 Telephone Member j(318) 491-5222 3.5 | SIC Code (4 digit) ] 1 a. 2911 | b. NA Latitude Degrees 030 Minutes 14 | | c.NA Seconds 36 1 1 d. NA i | Degrees 093 { e. NA Longitude Minutes 16 | f. NA Seconds 20 | 3.7 Dun & Bradstreet Kirber(s) a. 00-842-7692 3.a EPA Identification Nunber(s) (RCRA I.D. No.) a. IAD990683716 1 1 b. NA | b. NA 3.9 NPDES permit Nunt>er(s) a. IA0003026 b. NA Receiving Streams or Water Bodies (enter one name per box)1 a. Bayou Verdine b. NA c. NA 1 d. NA e. NA f. NA ' | Underground Injection Well Code (U1C) Identification Ncmber(s) a. NA | b. NA 4. PARENT COMPANY INFORMATION 4.1 | Name of Parent Company | E. I. Du Pont De Nemours J 4.2 Parent Company's Dun & Bradstreet Nunber l 00-131-5704 EPA Form 9350-1 (1*90) Revised - Do not use previous versions. 313 ADVISOR SAL 000004366 'PA fore R Part 11. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES gw--*l 1. PUBLICLY OWNED TREATMENT WORKS (POTWs) 1.1 POTW name NA Street Address City County I 1.2 POTW name I NA | Street Address I City Page 2 of 5 Phosphoric acid Conoco lake Charles Re.' Cocnty State | Zip | State J Zip sitBiniiiwwgwttMimtiiHltMiftmMWtiMiMmMWiiMiiMMiumiwwigmgiiifitiMWgiiiMtgtwmii 2. OTHER OFF-SITE LOCATIONS (DO HOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name BET 2.2 Off-site location name CMH EPA Identification Huiber (RCRA ID No.) NA I EPA Identification Nunber (RCRA ID No.) I LAD000777201 Street Address Cities Service Hwy @ 1-10 street Address Rt 2, John Brannon Rd City Sulfur | County Calcasieu j City j Carlyss County Calcasieu State IA Zip 70664 State IA 7663 s location under control of reporting facility or parent company? ( ] Tes l X) No Is location under control of reporting facility or parent company? ( ] Yes (X7 2.3 Off-site location name NA 2.4 Off-site location name NA EPA Identification Number (RCRA ID No.) Street Address | EPA Identification Humber (RCRA ID No.) 1 | Street Address City State | County 1 | Zip 1 City 1 | State | County 1 | Zip is location under control of reporting facility or parent company? [ ] Yes [ ] No 2.5 Off-site location name NA EPA Identification Nurber (RCRA ID No.) Street Address | Is location under control of reporting facility or parent | company? [ I Yes [ ] No 2.6 Off-site location name 1 NA | EPA Identification Nuitoer (RCRA ID No.) 1 | Street Address City | County 1 1 City 1 | county State 1 Zip 1 Is location under control of reporting facility or parent company? ( ] Yes C 1 No | State | Zip 1 Is location under control of reporting facility or parent company? [ ] Yes ( ] No C ] Check if additional pages of Part II are attached. How many? [ ) EPA Form 9350-1 (1-90) Revised - Oo not use previous versions 313 ADVISOR SAL 000004367 Page 3 of 5 SPA FORM R PART III. CHEMICAL-SPECIFIC IHFORMATION Ihosphoric acid Conoco lake Oiarles Refi 1. CHEMICAL IDENTITY (Do not complete this section if you eci^lete Section 2. 1.1 | [Reserved] 1.2 I CAS Nintoer (Enter the nufeer exactly as It appears on the 313 list. Enter NA if reporting cheaical category.) 007664-38-2 1.3 | Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 list.) j Phosphoric acid 1.4 | Generic Chemical Name (Complete only if Part I, Section 1.1 is checked "Yes." Generic name must be structurally descriptive.) .2 | MIXTURE COMPONENT IDENTITY (Do not complete this section if you complete Section 1.) j Generic Chemical Name Provided by Supplier (Limit the name to a meximui of 70 characters (e.fl., nuitoers, letters, spaces, | punctuation).) 3. I ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) | Manufacture the 3.1 j chemical: a. [ ] Produce b. [ ] Import | If produce or inport: | c. ( 3 For on-site use/processing e. C 1 As a byproduct d. [ ] For sale/ distribution f. [ 3 As an impurity | Process the 3.2 j chemical: a. [ 3 As a reactant d. [ ] Repackaging only b. [ ] As a formulation conponent c. [ ] As an article conponent T.3 | Otherwise use j the chemical: a. (X) As a chemical processing aid b. [ ] As a manufacturing aid c. C ] Ancillary or other use V MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR [04] (enter code) S. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) | A. Total Releases (Ibs/yr) I IB. Basis of I Estimate (enter code) j................... --........ -- --1 A.1 j A.2 I Reporting Ranges j Enter j | 0 1-499 500-999 j Estimate j 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.2 5.3.3 t ai c] [] 5.1a 5.2a [3 t3 [3 l3 [J t1 5.3.1a 5.3.2a 5.3.3a [3 t3 [3 [3 [3 [3 [3 C3 [3 NA 5.1b [ 3 NA 5.2b l 3 C. X From Stormwater 0 5.3.1b [M 1 5.3.1c NA NA 5.3.2b l 3 5.3.2c NA 5.3.3b [ 3 5.3.3c 5.4 Underground Injection 5.5 Releases to land 5.5.1 On-site landfill 5.5.2 Land treatment/application farming S.5.3 Surface impounefenent 5.5.4 Other disposal 5.4a 3 l 5.5.1a 1 5.5.2a 1 5.5.3a i 5.5.4a | c3 13 [3 [3 (3 C] C] [) [3 t3 [3 C3 [3 (3 j NA NA NA NA 5.4b C 3 5.5.1b t 5.5.2b t 5.5.3b [ 5.5.4b [ ] 3 3 3 (Check if additional information is provided on Part IV - Supplemental Informatior EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR SAL 000004368 Page 4 of 5 EPA FORM R PART III. CHEMICAL-SPECIFIC INFORMATION (continued) Phosphoric acid Ccnooo lake Charles Ref' 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) Discharge to POTU 6.1.1 (enter location Timber from Part It, Section 1.) l.t 3 A. Total Transfers (Ibs/yr) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 1 | C3 j Cl 1 [1 | | NA 8. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) 6.1.1b C ] 6.2.1 Other Off-Site Location (enter location number from Part II, Section 2.) 2.(2 3 (1 (3 ( 3 0 6.2.1b E 0 3 6.2.1c M72 Other Off-Site Location 6.2.2 (enter location number from Part II, Section 2.) 2.(1 3 (3 (3 (3 6.2.2b (0 3 | 6.2.2c 0 1 Other Off-Site Location 6.2.3 (enter location nunfeer from Part II, Section 2.) 2.1 3 I3 (3 [3 | 1 NA | 6.2.3b [ 1 ] | 6.2.3c 1 ( ] (Check if additional information is provided on Part IV - Supplemental Information) H72 7. WASTE TREATMENT METHOOS AND EFFICIENCY I 3 Not Applicable (NA) - Check if no on-site treatment is applied to any uastestream containing the chemical or chemical category. A. General Uastestream (enter code) 1 a. Treatment | Method ] (enter code) 1 C. Range of 1 Influent j Concentration j (enter code) I 0. Sequential } Treatment? 1 (Check if | applicable) I E. Treatment | Efficiency | Estimate F. Based on Operating Data? Yes NO 7.1a 7.2a 7.3a 7.4a 7.5a 7.6a 7.7a 7.8a 7.9a 7.10a (W tS [3 (] C3 [3 [3 l3 c3 [] | 7.1b [ Cll] | 7.2b [C113 | 7.3b c NA 3 | 7.4b [NA 3 | 7.5b [ NA 3 | 7.6b [NA ] | 7.7b (NA 3 | 7.8b | 7.9b [NA ] [NA ] | 7.10b [NA 3 | | | | 1 | | 1 | | 7.1c 7.2c 7.3c 7.4c 7.5c 7.6c 7.7c 7.8c 7.9c 7.10 [13 [13 [3 [J [3 t3 (3 [3 [3 l] | 7.Id | 7.2d | 7.3d | 7.4d | 7.5d | 7.6d | 7.7d | 7.8d | 7.9d | 7.10d [3 C3 [3 [3 [3 [3 l3 C3 [3 l3 | 7.1e 100,00 X |7.If [X] | 7.2e 100,00 X |7.2f [ j | 7.3e X |7.3f [ 3 | 7.4e X J7.4f r 3 | 7.5e X |7.5f [ 3 | 7.6e X |7.6f c 3 | 7.7e X |7.7f i 3 j 7.8e X |7.8f c 3 | 7.9e X 17.9f [ 3 | 7.lOe X |7.1Of c 3 [3 tX3 t3 [3 [3 [3 [3 [1 t3 C3 [ 3 (Check if additional information is provided on Part IV * Supplemental Information) 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) M[ ] | B. Quantity of the Chemical in Wastes j Prior to Treatment or Disposal | C. index 1 1 | Current j reporting | year (Ibs/yr) Prior year (Ibs/yr) |0r Percent |Change I It 1* It l 1 1 1 xj [ ] | D. Reason for Action j (enter code) I 1 1 j R [ 3 EPA Form 9350-1 (1-90) Revised * Do not use previous versions. 313 ADVISOR SAL 000004369 Page 5 of 5 EPA FORM R PART IV. SUPPLEMENTAL INFORMATION Use this section if you need additional space for answers to questions in Pert III. oer the lines used sequentially from lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) stssssssMSsasvswsnsi ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT {Part III, Section 5.3) jfooapharic acid Conoco Lake Charles Refi You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases (Ibs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1*499 500-999 A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.C 3 5.3.1 ] 5.3.1 3 | l 315.3. [ C 1 [5.3. C t 3 5.3.C | [ ]a la }a t3 (1 C3 13 Cl I1 13 I1 r3 5.3. 5.3.C 5.3.t lb l lb ( lb C C. X From Stormwater ] 5.3.C 1c ] 5.3.C Jc 3 5.3.1 1c ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part 111, Section 6) You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) A.1 | A.2 ]B. Basis of | Estimate { (enter code) | Reporting Ranges 1 0 1-499 500-999 { Enter 1 Estimate j C. Type of Treatment/ Disposal (enter code) Discharge to POTU l.t ) (enter location number from Part II, Section 1.) 1.1 3 | C1 ] tJ | Cl j j 6.1.C 3b { | 3 6.2. f Other off-site location 3 (enter location number from Part 11, Section 2.) 6.2. C Other off-site location 3 (enter location number from Part II, Section 2.) 2.C 1 2.1 3 Cl [] 1 C3 j Cl C3 1 C3 j 6.2.C 3b C 1 J6.2.C lb C 1 116.2. [ lc 1 1 3(6.2.C Jc Other off-site location | 6.2. [ 1 (enter location number 2.1] } r 3 I] I) from Part II, Section 2.) \ =SSSSSSSS8SSStS8tSSS%SSA3SSSRSaCS3B8SS8SS88St&S*8S8fe5SCS8SSBSS8StSS&3SSS3S&NSSSSSfS ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part III, Section 7) 6.2. C 3b C ] )6.2.C )c 1 :s(siEsisctsccs3fsstBsxsMsassKs*:sassasiss A. General Wastestreem (enter code) | B. Treatment j Method 1 f (enter code) ( C. Range of ) Influent | Concentration | (enter code) D. Sequential Treatment? (Check if epplicable) | E. Treatment j Efficiency j Estimate 1 F. Based on Operating Oata? 1 Yes MO 7. t ] a C 1 1 7.C ]b C 1 7. C lc t 7.1 Id C 3 1 7.1 le X |7.C If C 1 C3 7.1 la [ 1 ! 7.1 lb C 1 | 7.C ]c C 7. t Id C 1 1 7.E 3e X |7.C If C t3 7, t la C J 1 7.1 Jb C J | 7.1 3c C 7.1 3d C 1 1 7.[ ] e X 17 > t If C 1 l3 7. [ 1 a C 3 1 7. C lb c 1 | 7.1 lc C 1 7.1 Id C 1 i 7.C ]e X 17. C 3f t 3 C3 7. [ 1 a C 3 1 7.1 lb c 1 | 7. [ lc C1 \ 7-C 3d C 1 1 7.1 le X |7.[ If t 1 C3 7.1 la C J I 7.1 b c 3 1 7.1 lc ri 1 7.1 Id C 3 \ 7.1 3e X |7- t If C 1 C3 r 1a C 1 1 7.1 lb l 1 l 7.C lc ci i 7.C Id l J | 7.1 le X |7.I If E 3 [1 . ,, la C 3 1 7.1 lb c 1 | 7.1 lc ti 1 7.1 Id [ 1 1 7. [ le X |7.t If t 3 C1 7. t 1 a i 3 1 7.1 lb r 1 J 7.[ lc ti 1 7.1 3d C 1 | 7.1 le X 17.[ If [ 1 C3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 31> AOVISOR. SAL 000004370 EPA U.S. Environmental Protaction Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM Section 313 of the Emergency Planning and Community Right-to-Know Act of 1986, elao known at Title III of the Superfwd Amendments and Reauthorization Act. Page 1 of 5 ftxpylene (Ptcpene) GcnOOO lake Charles Ref4 I EPA FORM R PART I. FACILITY IDENTIFICATION SECTION 1.1 Are you claiming the chemical identity on page 3 trade secret? [ ] Yes (Answer question 1.2; [X] No (Do not answer 1.2; Attach substantiation forms.) Go to question 1.3.) 1.2 If MYesN in 1.1, is this copy: C ] Sanitized C ] Unsanitized 1.3 Reporting Year 2. CERTIFICATION (Reed and sign after completing all sections.) I hereby certify that 1 have reviewed the attached doeuaants and that, to the best of my knowledge and belief, the submitted information is true and complete and that the amounts and values in this report are accurate based on reasonable estiaates using data available to the preparers of this report. Name and official title of owner/operator or senior management official Den R. Unruh Refinery Manager Signature I Date signed |06-20-90 3. Facility Identification Facility or Establishment Name Conoco lake Charles Refinery Street Address old Spanish Trail 3.1 City Westlake 1 County |Calcasieu State IA | Zip Code |70669 WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.0. BOX 23799 WASHINGTON, DC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Nuiber 70669 CUCLK OIDSP 3.2 ; This report contains information for (Check one): 3.3 1 Technical Contact 1 Brandt Butler 3.4 | Public Contact 1 Don R. unruh 3.5 | SIC Code <4 digit) 1 i a. 2911 | b. NA 1 j c.NA 1 Latitude | 1 Degrees Minutes Seconds 030 14 36 a. OC a An entire facility b. 1 ) Part of a facility. 1 Telephone Nunder |(316) 491-5599 1 Telephone Nunder | (318) 491-5222 1 1 d. NA 1 | Degrees 093 | e. NA Longitude Minutes 16 | f. NA Seconds 20 | 3.7 | Dun & Bradstreet Nuiber(s) a. 00-842-7692 3.8 EPA Identification Nmber(s) (RCRA l.D. No.) a. IAD990683716 1 1 b. NA | b. NA 3.9 NPDES Permit Nmber(s) a. IA0003026 b. NA 3.10 Receiving Streams or Water Bodies (enter one name per box)| a. Bayou Verdine b. C. NA 1 d. NA NA e. NA f. NA ..11 Underground Injection Well Code (UIC) Identification Humberts) a. NA 1 b. NA 4. PARENT COMPANY INFORMATION 4.1 Name of Parent Company : E. I. Du Pont De Nemours 4.2 1 Parent Company's Oun & Bradstreet Nurfeer 00-131-5704 EPA Form 9350*1 (1-90) Revised Do not use previous versions. 313 AOVISOR SAL 000004371 >A Fora ft Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IH WASTES susssasssssnattassn: 1. PUBLICLY OWNED TREATMENT WORKS (POTWs) 1.1 POTW name NA Street Address 1.2 POTW name NA Street Address Page 2 of 5 Propylene (Propene) Ocnoco Lake diaries Refi City County City | County State Zip State I zip 2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name BFI 2.2 Off-site location name craa EPA Identification Nuntoer (RCRA ID No.) NA EPA identification Nuifcer (RCRA ID No.) IAD000777201 Street Address Cities Service Hwy 1-10 Street Address Rt 2, John Brannon Rd City Sulfur County Calcasieu City Carlyss | County ( Calcasieu state IA 1 Zip | 70664 State LA 78663 ocation under control of reporting facility or parent .. -xiny? [ 3 Yes [Xl No 2.3 Off-site location name NA Is location under control of reporting facility or parent company? ( 1 Yes [X] No !8S8tlSStfSSSSS88SSS:388SCS8S5S5SSB8S838S8S888S&858l3Sd88atS8SStBl3888X 2.4 Off-site location name NA EPA Identification Number (RCRA 10 No.) | EPA Identification Number (RCRA ID No.) 1 Street Address | Street Address City [ County State ! Zip I Is location under control of reporting facility or parent company? [ ] Yes [ 1 No 2.5 Off-site location name NA EPA Identification Number (RCRA ID No.) 1 City 1 | State | County 1 | Zip Is location under control of reporting facility or parent company? 1 Yes C ] No B838S88S3C8S3S83888S8S8S8888S838SSS8388&SS38S8SSS8SS8S888888S888: 2.6 Off-site location name NA | EPA Identification Number (RCRA ID No.) Street Address j Street Address City ate | County l ! Zip | City 1 | State | County 1 1 Zip Is location under control of reporting facility or parent company? C ] Yes [ ) No | 1$ location under control of reporting facility or parent | company? ( ] Yes C 1 No t ] Check if additional pages of Part II are attached. Hou many? [ ] '- EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR SAL OOOOO4372 Page 3 of 5 EPA FORM R PART III. CHEMICAL-SPECtFIC INFORMATION Propylene (Eropene) Conoco Lake Quarles Ref; 1. CHEMICAL IDENTITY (Do not complete this section if you conplete Section 2. 1.11| (Reserved) 1.2 1 CAS Nwber (Enter the nuiber exactly as it appears on the 313 list. Enter HA if reporting chemical category.) | 000115-07-1 1.3 1| Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 list.) j Propylene (Propene) 1.4 | Generic Chemical Name (Conplete only if Part I, Section 1.1 is checked NYes.M Generic name must be structurally descriptive.) ass 2. MIXTURE COMPONENT IDENTITY (Do not conplete this section if you complete Section 1.) Generic Chemical Name Provided by Supplier (Limit the name to a maxima of 70 characters (e.g., lumbers, letters, spaces, punctuation).) itHiniiiitinntiimisnNMiiiitinnmmwtMiiiiinmiimiiitinMui ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) | Manufacture the 1 chemical: Process the 3.2 chemical: a. (X) Produce b. [ ] Inport | If produce or import: I ) e. (X] For on-site use/processing e. I ] As a byproduct d. [ ) For sale/ distribution f. ( X As an inpurity a. [X] As a reactant d. C ) Repackaging only b. [ ) As a formulation component c. C 3 As an article component 3 3 | Otherwise use | the chemical: a. ( 3 As a chemical processing aid b. [ 3 As a manufacturing aid MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR c. (X) Ancillary or other use tscsiessscsisaua (083 (enter code) xiunuti(ntsts!i:ssssssassssssss:$ssssESErsnBisss:isssssznni(nsci) RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases (Ibs/yr) A.1 1 Reporting Ranges j 0 1-499 500-999 | A.2 Enter Estimate B. Basis of Estimate (enter code) 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.2 5.3.3 [3 [3 C3 5.1a | { 1 5.2a | | 5.3.1a 5.3.2a 5.3.3a C3 c3 (3 I3 (3 (3 (3 C1 [1 (] (] (3 t3 C3 1100001 5.1b (O 1 NA 5.2b [ 3 C. X From Stormwater NA 5.3.1b [ 3 5.3.1c NA 5.3.2b ( 3 5.3.2c NA 5.3.3b ( 3 5.3.3c 5.4 Underground Injection 5.4a [ 3 C 3 I 3 NA 5.4b ( 5.5 Releases to land 5.5.1 On-site landfill 5.5.1a c 3 c 3 ( 3 5.5.2 Land treatment/application fanning 5.5.2a c 3 c 3 t ] 5.5.3 Surface inpomdnent 5.5.4 Other disposaL 5.5.3a c 3 ( 1 c 3 5.5.4a ( 3 [ 3 t 3 NA 5.5.1b I NA 5.5.2b [ NA 5.5.3b ( NA 5.5.4b ( ) (Check if additional information is provided on Part IV - Supplemental Information) 31 3| ] ] ]| EPA Form 9350*1 (1*90) Revised Do not use previous versions. 313 ADVISOR SAL 00004373 Page 4 of 5 PA FORM R PART III. CHEMICAL-SPEC!F1C INFORMATION (continued) Propylene (Propene) Oonoco Lake Charles Ref1 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Oo not use both A.1 and A.2) A. Total Transfers (Ibs/yr) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate B. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) .1.1 Discharge to POTW (enter location nuaber from Part II, Section 1.) 1.C 1 l] I] l NA 6.1.1b C ] 6.2.1 Other Off-Site Location (enter location mnber from Part II, Section 2.) 2.1 ] t 3 C 3 11 NA 6.2.1b [ 1 6.2.1c Other Off-Site Location 6.2.2 (enter location nuiber from Part II, Section 2.) Other Off-Site Location 6.2.3 (enter location nuiber from Part II, Section 2.) 2.C 3 2.1 3 C3 1 j C3 j [3 13 t3 | NA 6.2.2b t 1 | 6.2.2c 11 [] 111 | NA | 6.2.3b C ] j 6.2.3c III [ ] (Check if additional information is provided on Part IV - Supplemental Information) 7. WASTE TREATMENT HETHOOS AND EFFICIENCY [X 3 Not Applicable (NA) - Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. a. general Wastestream (enter code) | B. Treatment j Method j (enter code) | C. Range of j Influent j Concentration - j (enter code) 0. Sequential Treatment? (Check if applicable) E. Treatment Efficiency Estimate 7.1a C] | 7.1b [ 3| 7.1c t3 7.Id t3 7.1e 7.2a t3 | 7.2b C 3| 7.2c t3 7.2d l3 7.2e 7.3a C] | 7.3b ( 1| 7.3c [3 7.3d [3 7.3e 7.4a t3 | 7.4b [ 3| 7.4c [3 7.4d I3 7.4e 7.5a c3 | 7.5b [ 3| 7.5c t] 7.5d l1 7.5e 7.6a [] | 7.6b [ 1| 7.6c t3 | 7.6d I3 7.6e 7.7a (3 | 7.7b [ ]| 7.7c l3 | 7.7d [3 7.7e 7.8a c3 | 7.8b [ 3| 7.8c [3 | 7.8d l1 7.8e 7.9a [] | 7.9b t 3| 7.9c C] | 7.9d I3 7.9e 7.10a cJ | 7.10b t 3| 7.10 (3 | 7.10d C3 7. lOe [ 3 (Check if additional information is provided on Part IV - Supplemental Information) F. Based on Operating Oata? Yes X |7.1f t 3 X |7-2f [ 3 X 17*3f C 3 X |7.4f l 3 X 17 - 5 f t 3 X [ 7.6f C 3 X |7.7f ( 1 X |7.8f l 1 X | 7.9f [ 3 X 17.1 Of C 3 No C3 1i 13 [1 [1 (3 C3 [] (3 [3 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) 6. Quantity of the Chemical in Wastes Prior to Treatment or Disposal j C. Index 1 0. Reason for Action 1 (enter code) 1 Mt ] Current reporting year (Ibs/yr) Prior year (Ibs/yr) |Or Percent (Change 1 l 3+ | [ 3- 1 1 1 1 X\ [ 3 l 1 1 1 1 Rt 1 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. Cx, - 313 ADVISOR bAL OOOO04374. Page 5 of 5 EPA FORM R PART IV. SUPPLEMENTAL. INFORMATION Use this section if you need additional space for answers to questions in Part III. Nimber the lines used sequentially fram lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) Propylene (Propene) Ccnoco lake Charles Refj ADOITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part III, Section 5.3) You nay report releases of less than 1,000 lbs by checking ranges under A.1 (Do not use both A.1 and A.2) A. Total Releases (tbs/yr) B. Basis of Estimate (enter code) A.1 I Reporting Ranges 0 1-499 500-999 j A.2 Enter Estimate 5.3 Discharges to receiving 1l streams or water bodies 5.3.[ ] E ] I5.3.E 3a E 1 E 3 E 3 (Enter letter code from 5.3.1 [ 1 15.3.1 3 a | ] E ] E 3 [ Pert 1 Section 3.10 for 5.3.1 [ J 5.3. E u\ t ] r ] E 3 | streenKs) in the box provided.) i1 1 SHIRXMIttC>(S88*MSSSllS*nsutMSIKStlXSSS8S:snS*rtS*CCCnt<IS<>MSt8)!S! ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) 5.3.E 5.3. E 5.3. E 3b E 3b E 3b E You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) A.1 | A.2 |B. Basis of Estimate | (enter code) | Reporting Ranges 0 1-499 500-999 | Enter 1 Estimate j C. X From Stormwater 3 5.3. E 3c 3 5.3. E 3c 3 5.3. E 3c C. Type of Treatment/ Disposal (enter code) Discharge to POTW 1.E 3 (enter location number from Part II, Section 1.) Other off-site location 6.2. E 3 (enter location nmber from Part II, Section 2.) 1.E 3 2.[ 3 [3 C3 1 E3 | 1 |6.1.[ ]b [ ] | 1(3 j [3 E3 III 6.2. E ]b [ ]|6.2.E 3c [| j Other off-site location 6.2. E 3 (enter location lumber from Part II, Section 2.) 2.E 3 [3 E 3 E 3 1 6.2.E lb [ 1 1 ](6.2.C 3 C 1 Other off-site location 6.2.[ 1 (enter location nimber 2.1 3 t 3 C 3 (3 from Part II, Section 2.) 3SSSSSS8S88tS8S8SS5SSSSSIII8SBSSSSSSSSS8S2SSSSSSIBtSSSSSS88&SCSS88SSlBIfiS8S8S8S888S ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part III, Section 7) 1 6.2. E 1 3b t 1 316.2. E 3c 1 A. General Uastestream (enter code) | B. Treatment j Method 1 | (enter code) | C. Range of 1 Influent ] Concentration | (enter code) | D. Sequential Treatment? | (Check if j applicable) E. Treatment f ficieney Estimate F. Based on Operating Data? Yes 7.1 ] a 7. C }a 7. [ ]a 7. [ ]a [3 [3 C3 C] 1 7.1 1 7.1 1 7. [ 1 7-1 lb C 3b c 3b E )b C 1 7.1 1 7. E 1 | 7.[ 3c 3c 3c H 7.E 3 c t] E3 [1 (3 1 7. E 1 7. ( 1 7. [ 1 7.1 ]d 3d Id 3d I1 E3 [3 tJ 7.E le 7.E 3 e 7- E 3e 1 7.1 ]e X 7.E X 7.E X 7.[ X |7-E 3f C 3 If [ 3 3f t 3 3f : 3 7. [ 3 a E 3 1 7. E ]b [ ] | 7.1 3c I3 1 7. t 7. C ]a C ] 1 7.E ] b ( 3 | 7.[ ]c C) 1 7.1 \E 1 a ( 3 1 7. E ]b c 3 | 7.[ 3c 3 1 7. [ 7. [ 3a E 3 1 7.E 3b E 3 | 7.[ 3c t1 1 7.1 7. I 3a [ 3 1 7.C 3b t 3 | 7.[ 3c [3 1 7.1 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 3d 3d 3d 3d 3d t3 I3 [1 (3 [3 1 7. E 1 7. I 1 7. [ 1 7.1 1 7.1 ]e 3e ]e 3e 3e % |7. [ If [ 3 X |7.[ 3 f C 3 X |7.[ ]f [ 1 X 17- C 3 f E 3 X |7.[ 3f E 3 313 ADVISOR No C] [3 [3 I3 c3 () [3 E* E3 SAL 000004375 I EPA U.S. Environmental Protection Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM 'ection 313 of the Emergency Planning and Community Right-to-fcnow Act of 1986, i .Iso known as Titte ill of the Superftmd Amendments and Reauthorization Act. a EPA FORM R PART I. FACILITY IDENTIFICATION SECTION page 1 of 5 Styrene OcnOQO Lake Charles Refi 1.1 Are you claiming the chemical identity on page 3 trade secret? | 1.2 If "Yes'* in 1.1, is this copy: C 3 Yes (Answer question 1.2; cXl No (Do not answer 1.2; | I ] Sanitized C ] Unsanitized Attach siAistantiation fonrns.) Go to question 1.3.) | 1.3 Reporting Yeer 1989 2. CERTIFICATION (Read and sign after completing all sections.) 1 hereby certify that 1 have reviewed the attached documents and that, to the best of my knowledge and belief, the submitted information is true and cosplete and that the amocnts and values in this report are accurate based on reasonable estimates using data available to the preparers of this report. Name and official title of owner/operator or senior management official Don R. Unruh Refinery Manager Signature I Date signed |06-20-90 3. Facility Identification Facility or Establishment Name Conoco Lake Charles Refinery Street Address old Spanish Trail WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.0. BOM 23799 WASHINGTON, DC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY City Westlake State LA | County |Calcasieu | Zip Code |70669 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Nunber 70669 CNCXX OIDSP 3.2 | This report contains information for (Check one): a. (X] An entire facility b. C 3 Part of a facility. 3.3 | Technical Contact I Brandt Butler 1 Telephone Number | (318) 491-5599 3.4 1 Public Contact 1 Don R. Unruh 1 Telephone Nuitoer 1 (318) 491-5222 3.5 1 SIC Code (4 digit) | | a. 2911 | b. NA | Latitude I Degrees j 030 Minutes 14 | c. NA Seconds 36 1 1 d. NA 1 | Degrees 093 | e. NA longitude Minutes 16 | f. NA Seconds 20 | 3.7 1 Dun & Bradstreet NunberCS) | a. 00-842-7692 | b. NA 3.8 1 EPA Identification Nurrber(s) (RCRA I .D. No.) | a. LAD990683716 | b. NA 3.9 1 NPDES Permit Nuirber(s) | a. IA0003026 j b. NA Receiving Streams or Water Bodies (enter one name per box)! a. Bayou Verdine 1 b. NA c. NA | d. NA e. NA | f. NA 1 Underground Injection Well Code (UIC) Identification Nuiber(s) a. NA | b. NA 4. PARENT COMPANY INFORMATION 4.1 Name of Parent Conpany 1 E. I. Du Pont De Nemcurs 1 4.2 I Parent Con^any's Dun & Bradstreet Nunber 00-131-5704 EPA Form 9350-1 (1-90) Revised Do not use previous versions 313 ADVISOR SAL 000004-J7X ERA Form R Part II. OFF-SITE LOCATIONS TO MUCH TOXIC CHEMICALS ARE TRANSFERRED IN HASTES 1. PUBLICLY OWNED TREATMENT WORKS (POTUs) 1.1 POTW name NA Street Address 1.2 POTW name NA Street Address Page 2 of 5 Styrene Oonoco lake Charles Ref City County City Coimty State Zip State I Zip ii i anroiitsgaiaswwfwtswiwwwwMismtimintiMroiiiMnumMMMMMtuiMiMammMmmwww 2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name BFI 2.2 Off-site location name CWMI EPA Identification Ninber (RCRA ID No.) NA I EPA Identification Ninber (RCRA ID Ho.) | LAD000777201 Street Address Cities Service Hwy @ 1-10 I Street Address I Rt 2, John Brarmcn Rd City Sulfur State LA County Calcasieu Zip 70664 I City S Carlyss I State LA Coiaity Calcasieu Z7i^663 s location under control of reporting facility or parent conpany? [ } Yes [ X No SSS8SSSS9SSSSSSSISISSBCSISSSSISSSSBirSS8S88SaS5S8SaSSSSS8SS 2.3 Off-site location name NA EPA Identification Ninber (RCRA ID No.) Street Address | Is location under control of reporting facility or parent j company? [ ] Yes (X) !SSSSSSSIIISItESSSSSSKXZIISSIlnilSZIEZXIlSSSEEISSSSSU8SBISSStS. 2.4 Off-site location name 1 NA | EPA Identification Nurber (RCRA ID No.) 1 | Street Address Ci ty State | County 1 | Zip Is location under control of reporting facility or parent company? ( ] Yes C ] No 2.5 Off-site location name NA EPA Identification Ninber (RCRA ID No.) Street Address I City 1 j State | County 1 | Zip | Is location under control of reporting facility or parent I conpany? ( ] Yes ( 3 No I 2.6 Off-site location name NA | EPA Identification Ninber (RCRA ID No.) 1 J Street Address City State | County 1 | Z'P | City | State | County 1 | Zip Is location under control of reporting facility or parent conpany? t ] Yes [ 3 No | Is location under control of reporting facility or parent j conpany? ( 3 Yes ( 3 No [ 3 Check if additional pages of Part II are attached. How many? ( ] EPA Form 9350-1 <1-90) Revised - Do not use previous versions 313 ADVISOR SAl 0000043 77 EPA FORM R PART UI. CHEMICAL-SPECIFIC INFORMATION Styrene Qcnoco lake Charles Refi 1. CHEMICAL IDENTITY (Do not ceaplete this section if you complete Section 2. 1.1 1| [Reserved] 1.2 |1 CAS Muitoer (Enter the nimber exactly as it appears on the 313 list. Enter NA if reporting chemical category.) | 000100-42-5 1.3 | Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 list.) 1 Styrene 1.4 I Generic Chemical Name (Complete only if Part Ir Section 1.1 is checked HYes.M Generic name must be structurally descriptive.) 2. j MIXTURE COMPONENT IDENTITY (Do not complete this section if you complete Section 1.) ] Generic Chemical Name Provided by Supplier (Limit the name to e maximin of 70 characters (e.g., rentiers, letters, spaces, | punctuation).) KisfsxasiattssitS3uniiiiuiiissiiiKiiHsiMMSitimiiiciiniinniiic(ii*xs3<iiii*SHifiszss3StmcttMitssSKn(mxs! 3. I ACTIVITIES AHO USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) Manufacture the 3.1 chemical: a. [ ] Produce b. [ ] Import | If produce or import: j c. E ) For on-site use/processing e. { 3 As a byproduct d. I ] For sale/ distribution f. [ ] As an impurity | Process the 3.2 chemical: a. tX] As a reactant d. [ ] Repackaging only b. [ 3 As a formulation component c. [ 3 As an article component ,3 | Otherwise use l the chemical: a. [ I As a chemical processing aid b. [ 3 As a manufacturing aid c. [ ] Ancillary or other use SS8SI88388S88SSeSS8S888SaStftB8SBICtSt8S83888888CStS88S38SSSSfSttl8IISBSS88S88SSSI33S88S5888SSSSSS581CS88SIIStSSSSCtSSt3 . MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR [05] (enter code) 3. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases (Ibs/yr) B. Basis of Estimate (enter code) A.1 | Reporting Ranges | 0 1-499 500-999 | A.2 Enter Estimate 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 S.3.2 5.3.3 [ 9] [3 [3 5.4 Underground Injection | 5.1a 1 c 1 | S.2a 1 1 15.3.1a j 5.3.2a 5.3.3a I ] ] 1 [] C3 ] 3 3 [] j [3 1 [] t3 [3 ! I | 5.4a| [ 3 3 [3 | 1100 | 5.1b [O 3 o 5.2b CO 3 17 NA NA 5.3.1b [O 3 5.3.2b t 3 5.3.3b C 3 C. X From Stormwater 5.3.1c NA 5.3.2c 5.3.3c NA j 5.4b [ 1 5.5 Releases to land 1 1 5.5.1 On-site landfill 5.5.1a t ] 1 t3 | NA 5.5.1b [ 5.5.2 Land treatment/application farming 5.5.2a 1 l 1 3 3 NA | 5.5.2b C 5.5.3 Surface impounament 5.5.3a [ 1 [ 3 3 1 NA | 5.5.3b t 5.5.4 Other disposal 5.5.4a i < ] [ ] 3 NA | 5.5.4b ; ] (Check if additional information is provided on Part IV - Supplemental Information) 3 3 3 3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR EPA FORM R PART 111. CHEMICAL-SPECIFIC INFORMATION (continued) Page 4 of 5 Styrene Ocnooo lake Charles Ref 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (lb6/yr) A.1 I Reporting Rsnges | 0 1-499 500-999 j A.2 Enter Estimate B. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) Discharge to POTW 6.1.1 (enter location nuifeer from Part II, Section 1.) Other Off-Site Location 6.2.1 (enter location nuaber from Part II, Section 2.) Other Off-Site Location 6.2.2 (enter location nuaber frca Part II, Section 2.) l.t ] 2.(2 ] 2.[1 } [3 t3 [1 [3 t3 1 t t3 [ 1 NA 1 6.1.1b [ ] 1 0 6.2.1b E 0 ] 6.2.1c El E 3 E 0 6.2.2b (0 1 6.2.2c M72 M72 Other Off-Site Location 6.2.3 (enter location nuitoer from Part II, Section 2.) 2.[ ] t I [ 1 I I | NA | 6.2.3b [ 3 | 6.2.3c 11 1 t 1 (Check if additional information is provided on Part IV - Supplemental Information) :ssssss:stssctsntisitsHninni*istt:sss:s:sst:siss:sssss::sssH(s:zsssscesznis:sss:ssss:sss:nM:sss:sscissHssimBsiw 7. WASTE TREATMENT METHOOS ANO EFFICIENCY ( ] Not Applicable (NA) - Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. A. General Wastestream (enter code) 7.1a iWl 7.2a C] 7.3a [] 7.4a tI 7.5a c3 7.6a cI 7.7a (] 7.8a EI 7.9a (] 7.10a (I | 8. Treatment | Method | (enter code) ] 7.1b I Bill | 7.2b [NA 3 | 7.3b [ NA ) | 7.4b [NA i | 7.5b [NA ] | 7.6b [NA l | 7.7b [NA ] ) 7.8b | 7.9b [NA ] [NA ] | 7.10b [ NA ] C. Range of Influent Concentration (enter code) 7.1c [4] 7.2c [] 7.3c [] 7.4c [3 7.5c t3 | 7.6c t1 | 7.7c [3 | 7.8c t3 | 7.9c [3 | 7.10 [3 0. Sequential Treatment? (Check if applicable) 7.Id l3 7.2d t3 7.3d l3 7.4d E3 7.5d C3 7.6d [3 | 7.76 [3 | 7.8d [3 | 7.9d c3 | 7.lOd [3 1 E. Treatment J Efficiency Estimate ; F. Based on | Operating Oata? | Yes | 7.1e | 7.2e | 7.3e | 7.4e | 7.5e 90. 00 X 17-If X |7.2f X 17-3ff X [7.4f X |7.5f [3 [] [3 [3 [] | 7.6e X ]7.6f l 3 | 7.7e | 7.8e X |7.7f X |7.8f [3 C3 | 7.9e | 7.lOe X |7.9f C 1 X |7.lOf [ 3 No EX) E3 (j E3 C3 r3 e3 t3 [3 [3 [ ] (Check if additional information is provided on Part IV - Supplemental Information) 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) 8. Quantity of the Chemical in Wastes Prior to Treatment or Disposal C. Index | D. Reason for Action I (enter code) Current Prior Or Percent reporting year Change year (Ibs/yr) Clbs/yr) t 3+ I M( t I- %! RC 1 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. ^13 ADVISOR SAL 000004379 EPA FORM R PART IV. SUPPLEMENTAL INFORMATION Use this section if you need additional space for answers to questions in Pert III. .nber the lines used sequentially from lines in prior sections (e.g., 5.3.A, 6.1.2, 7.11) Page 5 of 5 _______ Styrene .... OLmsjjj Lake Charles Rel ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE EHVIRONMENT (Pert III. Section 5.3) You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases (Ibs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part 1 Section 3.10 for 5.3.1 5.3.t 5.3. 3 3 3 1 [ 3 I5.3.C 3a C 3 |5.3.C ]e E 3 ,,3, 3a ] t3 (3 C3 C1 (] C3 [3 [3 5.3. 3b E 5.3.C lb 5.3.E lb C streanKs) in the box provided.) 1 ___________ 5SlSSS88S83IEBItl8tSSSS28aSSBIIIIIIBIinSIBtSSI3888SCS8m8tSSmSS8S8SSSBSSBBBC: mtsss ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) You may report transfers of less than 1,000 lbs by cheeking ranges under A.1. (Do not use both A.1 and A.2) | A. Total Transfers (Ibs/yr) I j }B. Basis of Estimate I (enter code) J------- --------- --------- --------------------------------------- j j A.1 | A.2 | Reporting Ranges Enter I 0 1-499 500-999 | Estimate j C. X From Stormwater 3 5.3.1 lc 3 5.3.1 lc 3 5.3.1 lc _________________ {C. Type of Treatment/ Disposal j (enter code) I | | Discharge to POTU i.[ ] (enter location nurber from Part II, Section 1.) 1.C ] | j [3 | I] | l1 | I 6.1.[ ]b C | 3 Other off-site location 6.2. C 3 (enter location nunber from Part It, Section 2.) Z.( ] | 1(3 | 13 C1 ill I 16.2. [ 3b 3 6.2. [ ]c ill Other off-site location 6.2. [ 3 (enter location nunber from Part II, Section 2.) 2.C 6.2.( 3b t I 3 16.2. ( )c Other off-site location 6.2.1 3 (enter location nuiber from Part II, Section 2.) 2.C I 16.2.[ )b ( I 3 6.2. 3c ADDITIONAL INFORMATION ON WASTE TREATMENT METHOOS AND EFFICIENCY (Part III, Section 7) A. General Uastestream (enter code) 7.1 3 a 7. [ 3 a [3 3 7. ( 3a l3 7. C 3a 3 1 8. Treatment Mthod 1 (enter code) 11 7.1 3b \ 7.1 1 7.[ 3b t 3b [ 1 7A 3b | C. Range of | Influent j Concentration | (enter code) ] ! 7. c ] | 7.[ 3 1 7.C 3 | 7.1 3c 3c lc ]c [3 3 3 3 | D. Sequential j Treatment? | (Check if j applicable) 1 7.C 1 7.t 1 7.1 1 7.C 3d 3d 3d 3d [3 [3 13 ] | E. Treatment Efficiency | Estimate 1 1 7. C 3 e i 7. t le i 7.C 3 e 1 7.1 3e | F. 8ased on Operating j Data? | Yes X |7.[ 3f 3 X |7- X |7.C 3f 3 If C 3 X 17-1 3f 3 No 3 [] 3 [3 7. 3a 7.1 3a ' r 3a ..l ]a C3 C3 [3 3 1 7. lb ( 1 7-[ 3b t i 7.1 ]b [ 1 7.1 3b 3 | 7.[ 3 | 7. [ 3 1 7. [ 1 ! 7.C 3c 3c 3c ]c 3 3 [3 C3 1 7.1 3d [ 3 1 7. 3d ] 1 7.C 3d C 3 1 7.1 3d 3 1 7.C 1 7.1 1 7.1 \ 7.1 ]e 3e ]e le X |7.t 3f 3 X |7.[ 3f ( 3 X 17- 3f E 3 X |7.C 3 f 3 ] 3 J 3 7. [ 3 a 3 1 7.1 3b C 3 | 7.1 3c l1 i 7. [ 3d [ 3 ! 7.1 3e X |7* C If 3 3 EPA Form 9350-1 (1*90) Revised Do not use previous versions. 313 ADVISOR SAL 000004380 EPA U.S. Environmental Protection Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM Section 313 of the Emergency Planning and Community Right-to-Knov Act of 1986, also known as Title III of the Si^erfund Amendment* and Reauthorization Act. Page 1 of 5 Sulfuric acid Hnfyvno Lake Charles Ref EPA FORM R PART I. FACILITY IDENTIFICATION SECTION KSttfiSSSSSSSSSSSI 1.1 Are you claiming the chemical identity on page 3 trade secret? C ] Yes (Answer question 1.2; (Xj No (Oo not answer 1.2; Attach substantiation forms.) Go to question 1.3.) 1.2 If "Yes** in 1.1, is this copy: t I Sanitized I 1 Un*aniti2ed 1.3 RejDortmg Year 2. CERTIFICATION (Read and sign after consisting all sections.) I hereby certify that I have reviewed the attached docueents and that, to the beet of my knowledge end belief, the submitted information is true and consists end that the amooits and values in this report are accurate based on reasonable estimates using data available to the preparers of this report. Name and official title of owner/operator or senior management official Dot R. Unruh Refinery Manager Signature | Date signed 106-20-90 3. Facility Identification Facility or Establishment Name Conoco Lake diaries Refinery Street Address Old Spanish Trail WHERE TO SENO COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.O. BOX 23799 WASHINGTON, OC 20026*3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY City Westlake State LA 1 County j Calcasieu 1 Zip Code |70669 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Nuttoer 70669 CNCLK OIDSP 3.2 | This report contains information for (Check one): a. K 1 An entire facility b. ( ] Part of a facility. 3.3 | Technical Contact j Brandt Butler | Telephone Nunber | (318) 491-5599 3.4 1 Public Contact | Eton R. Unruh 1 Telephone Noitoer |(318) 491-5222 3.5 1 SIC Code (4 digit) j | a. 2911 | b. NA | c. NA 1 NA 1 d. | e. NA ( f. NA | j Latitude r | Degrees | 030 Minutes 14 Seconds 36 1 | Oegrees 093 Longitude Minutes 16 Seconds 20 3.7 1 Dun & Bradstreet Nonber(s) | a. 00-842-7692 | b. NA 3.8 I EPA Identification Nurber(s) (RCRA I .0. No.) | a. IAD990683716 | b. NA 3.9 1 NPOES Permit Noitoer(s) j a. IA0003026 ] b. NA I Receiving Streams or Water Bodies (enter one name per box)I I a. Bayou Verdine I b. 3.10............. ...... | c. NA 1 d. J e. NA 1 f- NA NA NA ..11| Underground Injection Well Code (UiC) Identification Nimber(s) | a. NA 1 b. NA 4. PARENT COMPANY INFORMATION 4.1 | Name of Parent Company E. I. Du Pont De Nemours 4.2 I Parent Coopany's Dun & Bradstreet Harper I 00-131-5704 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR SAL 000004381 >k Form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES 1. PUBLICLY OWNED TREATMENT WORKS (POTWs) 1.1 POTW name NA Street Address 1.2 POTW name NA Street Address Page 2 of 5 Sulfuric acid Gcnoco Lake Charles Refi City I County I City I County State | Zip I I State I | Zip I 2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE>. 2.1 Off-site location name BFI 1 2.2 Off-site location name j CWMI EPA Identification Number (RCRA 10 No.) NA I EPA Identification Number (RCRA ID No.) | IAD000777201 Street Address Cities Service Hwy 1-10 1 Street Address j Rt 2, John Brannon Rd City Sulfur | County j Calcasieu j Carlyss | County j Calcasieu State LA | Zip j 70664 1 State 1 IA 1 75663 cation under control of reporting facility or parent cu.y#ny? I ] Yes [ Xl No | Is location under control of reporting facility or parent | conpeny? [ ] Yes (Xl No 2.3 Off-site location name NA 1 2.4 Off-site location name 1 NA EPA Identification Number (RCRA ID No.) 1 EPA Identification Number (RCRA ID No.) 1 Street Address J Street Address City State | County 1 | Zip 1 City 1 | State j County | Zip Is location under control of reporting facility or parent company? C 3 Yes [ 3 No 2.5 Off-site location name NA EPA Identification Number (RCRA ID No.) Street Address | Is location under control of reporting facility or parent | company? [ 3 Yes [ 3 No I 2.6 Off-site location name I NA [ EPA Identification Number (RCRA ID No.) I j Street Address City ~te | County I j Zip I I City 1 I State I | County I | Zip I Is location under control of reporting facility or parent cofloany? [ 3 Yes [ ] No j Is location unoer control of reporting facility or parent | company? I 3 Yes [ ] No [ ] Check if additional pages of Part II are attached. How many? t 3 ' EPA Form 9350-1 (1-90) Revised - Oo not use previous versions 313 ADVISOR SAL 0000043Q2 *PA FORM R PART III. CHEMICAL-SPECIFIC INFORMATION Page 3 of 5 Sulfuric acid Oonooo Lake diaries Ref: 1. CHEMICAL IDENTITY (Do not complete this section if you complete Section Z, 1.1 1| [Reserved] 1.2 11 CAS Nutber (Enter the nuifeer exactly as it appears on the 313 list. Enter NA if reporting chemical category.) | 007664-93-9 1.3 1| Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 list.) j Sulfuric acid 1.4 | Generic Chemical Name (Complete only if Part I, Section 1.1 is checked "Yes.1* Generic name must be structurally descriptive.) --tr,*,,,***"**""****,,*******">****"**"*"*"*****-"-"*,*********I,,,"*,******I*>" 2. MIXTURE COMPONENT IDENTITY <Do not complete this section if you complete Section 1.) Generic Chemical Name Provided by Supplier (Limit the name to a maxima of 70 characters (e.g., nmfeers, letters, spaces, punctuation).) misninixiMtniniistniiiitsniiniminiattttinBtttisx 3. | ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) | Manufacture the 3.1 chemical: a. [Xl Produce b. [ ] Import | If produce or import: j c. [Xl For on-site use/processing e. [ 1 As a byproduct d. ( ] For sale/ distribution f. ( X As an impurity | Process the 3.2 I chemical: a. I ] As a reactant d. [ 3 Repackaging only b. [ 1 As a formulation component 3 | Otherwise use j the chemical: a. (X] As a chemical processing aid b. [ ] As a manufacturing aid 4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIKE OURING THE CALENDAR YEAR c. [ 3 As an article component c. [X] Ancillary or other use masaBii t07j (enter code) S8SSSSSSSSSSrSSS85tS588SS3SSnSS388SCSt31t58358SS989SS8S8SS8S8S98KSSS85ftS8SS88588$838S85SS8SS55SfS8885B9CStSISSS3C88SS61&8StSSSBS8 5. RELEASES OF THE CHEMICAL TO THE ENVIRONMEHT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) I A. Total Releases (Ibs/yr) I IB. Basis of j Estimate I Center code) [------------------ ----------- ------------------------------------ j I A.1 I A.2 | Reporting Ranges | Enter | | 0 1-499 500-999 | Estimate j 5.1 Fugitive or non-point air emissions 5.1a [ ] 5.2 Stack or point air emissions 5.2a | ] 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.2 5.3.3 [ ai [] (] 5.3.1a| 5.3.2a 5.3.3a| l) [] (] 5.4 Underground Injection 5.4a| C ] 5.5 Releases to land 5.5.1 On-site landfill 5.5.2 Land treatment/application farming 5.5.3 Surface inpoundment 5.5.4 Other disposal 1 5.5.la| 1 5.5.2a) 1 5.5.3a | 5.S.4a| [] [1 C] ( cX cl [3 i3 [] [3 [] c) t] i] [J 1 [1 [] ] (3 1 i | j [3 t] 1 3 [] 1 | | 1 j 1 5.1b [O 480 | 5.2b [0 1 01 5.3.1b [M NA | 5.3.2b NA | 5.3.3b C 1 C. X From Stormwater 5.3.1c NA 5.3.2c 5.3.3c NA | 5.4b 3 1 NA | 5.5.1b ] NA I 5.5.2b C 3 NA | 5.5.3b ] NA 5.5.4b ( 3 [ ] (Check if additional information is provided on Part IV * Supplemental Information) EPA Form 9350-1 (1-90) Revised Do not use previous versions. 313 ADVISOR SAL 000004383 PA FORM R PART 111. CHEMICAL-SPEC!FIC INFORMATION (continued) Sulfuric acid Conoco lake Charles Refi 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS A. Total Transfers (Ibs/yr) You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate B. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) Discharge to POTW 6.1.1 (enter location number from Part II, Section 1.) Other Off-Site Location 6.2.1 (enter location number from Part II, Section 2.) Other Off-Site Location 6.2.2 (enter location nurber from Part II, Section 2.) 1.C ] t 3 11 t 3 2.[ ] I j [1 j [) [1 2.C ] [1 Cl Cl NA | 6.1.1b C 3 1 6.2.1b ( 3 | 6.2.1c NA 1 NA 6.2.2b C 3 6.2.2c Other Off-Site Location 6.2.3 (enter location number from Part II, Section 2.) 2.[ J 1 j [] j Cl [1 NA 6.2.3b [ 1 6.2.3c C ] (Check if additional information is provided on Part IV * Supplemental Information) ::isss:::ssiKincNSKniftsunsii(M:a(tsss:sssssssssaanKKnisanBsnusszBnsssxnni:ss:iKss:ssutaxaftssssus 7. WASTE TREATMENT METHOOS AND EFFICIENCY [ ] Hot Applicable (HA) - Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. A. ..eneral Wastestream (enter code) 1 8. Treatment | Method | (enter code) 1 C. Range of | Influent | Concentration (enter code) j D. Sequential ( Treatment? (Check if | applicable) 1 E. Treatment 1 Efficiency | Estimate F. Based on Operating Data? Yes No 7.1a CM) | 7.1b tCll) 7.1c [13 | 7.Id [ 1 j 7.1e 100. 00 X J7.1f [Xl [1 7.2a C3 | 7.2b [NA 3 7.2c t | 7.2d [ 3 | 7.2e X 7.2f l ] [1 7.3a I3 | 7.3b [NA l 7.3c C | 7.3d C 3 | 7.3e X 17.3 f r 3 [3 7.4e 3 | 7.4b t NA ] 7.4c C | 7.4d [ 3 | 7.4e X |7.4f C 3 C3 7.5a 3 | 7.5b [ NA ] 7.5c [ | 7.5d [ 3 | 7.5e X |7.5f [ 3 [3 7.6a 1 1 7.6b [NA 3 7.6c [3 | 7.6d [ 3 | 7.6e X 17.6f [ 3 CI 7.7a 3 | 7.7b I NA 3 7.7c C3 | 7.7d [ 3 | 7.7e X |7.7f c 3 [3 7.8a 3 | 7.8b i NA 3 7.8c [3 | 7.8d [ 3 | 7.8e X |7.8f c 3 C3 7.9a 3 | 7.9b [ NA 1 7.9c C3 | 7.9d C 3 | 7.9e X |7.9f i J C3 7.10a c3 | 7.10b [NA 3 7.10 [3 | 7.lOd [ 3 | 7.lOe X |7.10f [ 3 I3 [ ] (Check if additional information is provided on Part IV - Supplemental Information) 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. lype of Modification (enter code) | B. Quantity of the Chemical in Wastes Prior to Treatment or Disposal | M[ 3 Current reporting year (Ibs/yr) Prior year (Ibs/yr) |Or Percent jChange It : It 3 - EPA Form 9350-1 (1-90) Revised - Do not use previous versions. i C. Index 1 1 0. Reason for Action (enter code) | | 1 1 *1 [ 3 * R[ 3 SAL 313 ADVISOR 000004384 EPA FORM R PART IV. SUPPLEMENTAL INFORMATION Use this section If you need additional space for answers to questions in Part III. Nunber the Unas used sequentially froai lines in prior sections (e.g.f 5.3.4, 6.1.2, 7.11) Page 5 of 5 Sulfuric acjcji 00(1000 La)Ce Charles Ref ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part III, Section 5.3) You nay report releases of less than 1,000 lbs by checking ranges inder A.1 (Do not use both A.1 and A.2) A. Total Ralaaaas (Ibs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.3 Discharges to recsiving streams or water bodies (Enter letter code from Part I Section 3.10 for 5.3.C 5.3. [ 5.3. [ ] ] 1 t ] 5.3.1 3a [ ) 5.3. E Is [ 1 5.3. C la t] t1 C] c] t] [] [1 c] c] 1 1 1 1 stream<s) in the box provided.) 1 iaiMiaiitmtmMUta ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) 5.3. t lb t 5.3.1 lb [ 5.3.C lb C You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibe/yr) | B. Basis of Estimste (enter code) A.1 | Reporting Ranges j 0 1-499 500-999 j A.2 Enter Estimate C. X From Storawster 3 S.3. t le 1 5.3.[ 3c 3 5.3. t le C. Type of Treatment/ Disposal (enter code) Discharge to POTW 1.1 ] (enter location nurber from Part 11, Section 1.) 1.1 ] 13 Cl 1 t1 j 6.1.[ lb [ ] Other off-site location 6.2.( ] (enter location nuiber from Part II, Section 2.) 2.1 1 | [3 | I) ill l1 6.2.t lb ( ]|6.2.t )c ill Other off-site location 6.2. [ ] (enter location nunber from Part II, Section 2.) 2.1 J | I t1 j t) III 111 6.2.1 )b C ) 6.2.1 ]c ill Other off-site location 6.2.[ 1 (enter location number from Part II, Section 2.) 2.C ADDITIONAL INFORMATION ON WASTE TREATMENT METHOOS AND EFFICIENCY (Part III, Section 7) 6.2. t lb [ ] 6.2.1 1c isxisssa A. General Uastestream (enter code) B. Treatment Method (enter code) | C. Range of 1 Influent | Concentration j (enter code) | D. Sequential Treatment? j (Check if j applicable) 7.C 3 a [3 7.[ ]b [ 1 7. [ 3c [] 1 7.1 3d C 3 7.1 3a l3 7.C 3b t 1 | 7.1 3c (] 1 7.C 3d l 3 7. [ 3a C3 7.C 3b C 3 | 7. [ 3c (3 l 7-C Id C 3 7. [ 3 a (3 7.[ 3b [ 3 | 7.[ 3c t] 1 7.C 3d 1 ] 7. t 3a [ 3 1 7.r 3b r 3 | 7. [ 3 C [3 1 7.1 3d C 3 7. t 3 a [ 3 1 7.C 3b c 3 | 7. [ 3c C3 1 7-C Id l 3 1 3a [ 3 1 7.C 3b c 3 | 7.[ 3c [3 1 7-C 3d t 3 7. [ 3a [ J 1 7.1 3b i 3 | 7.1 3c [3 1 7.1 3d C 3 7.C 3a l 3 l 7.1 ]b c 3 | 7.1 3c t3 l 7.C Id [ 3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. E. Treatment Efficiency Estimate 7.[ 3e 7.[ 3e 7.[ 3 e 1 7.C 3 e 1 7. [ 3e 1 7. [ 3 e 1 7.C 3 e ! 7. [ 3 e 1 7.C le F. Based on Operating Oata? Yes x 7.C X 7.C X 7-1 X 7- 1 X 7.[ X |7.[ If C J 3f t 3 3f [ 3 3f C 3 If [ 1 3f ( ] X |7.[ If [ 3 X |7.C 3f t 1 X |7.t 3 f 1 3 313 ADVISOR No C1 C1 (1 CI C1 C] C3 ( C3 S4L 000043e5 EPA U.S. Environmental Protection Agency TOXIC CHEMICAL RELEASE 1NVEMTORY REPORTING FORM ction 313 of the Emergency Planning end Ccmnuiity Right-to-Know Act of 1986, so known as Title HI of the Sijjerfund Amendments and Reauthorization Act. Page 1 of 5 Toluene CcnOQO lake Charles Refi EPA FORM R PART 1. FACILITY IDENTIFICATION SECTION 1.1 Are you claiming the chemical identity on page 3 trade secret? I 1.2 If "Yes* in 1.1, is this copy: C 1 Yes (Answer question 1.2; tX) No (Do not answer 1.2; | I ] Sanitized I 3 Unsanitized Attach siiastantiation forms.) Go to question 1.3.) | 1.3 Reporting Year 1989 2. CERTIFICATION (Read and sign after completing all sections.) I hereby certify that 1 have reviewed the attached docunents and that, to the best of my knowledge and belief, the submitted information is true and complete and that the amounts and values in this report are accurate based on reasonable estimates using data available to the preparers of this report. Name and official title of owner/operator or senior management official Den R. Unruh Refinery Manager Signature I Date signed 106-20-90 3. Facility Identification Facility or Establishment Name Conoco lake Charles Refinery Street Address Old Spanish Trail .1 City Westlake | Comty I Calcasieu State LA | Zip Code |70669 WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.0. BOX 23799 WASHINGTON, DC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Nurtoer 70669 OTCIK OIESP 3.2 | This report contains information for (Check one): 3.3 | Technical Contact t Brandt Butler 3.4 | Public Contact 1 Don R. Unruh 3.5 | SIC Code (4 digit) | 1 a. 2911 | b. NA | | e.NA Latitude Degrees 030 Minutes 14 Seconds 36 3.7 Dun & Bradstreet Nuiber(s) a. 00-842-7692 3.8 EPA Identification Nuiber(s) (RCRA l.D. No.) a. LAD990683716 3.9 NPDES Permit Nutber(s) a. LA0003026 a. (X) An entire facility b. [ i Part of a facility. 1 Telephone Number | (318) 491-5599 1 Telephone Nuiber | (318) 491-5222 1 1 d. NA 1 | Degrees 093 | e. NA Longitude Minutes 16 | f. NA Seconds 20 | 1 1 b- NA 1 b. NA 1 1 b. NA Receiving Streams or Water Bodies (enter one name per box)! a. Bayou Verdine | b. NA C. NA 1 d. NA e. NA 1 f- NA Underground Injection well Code (UIC) Identification Nurber(s) | a. NA 1 b. NA 4. PARENT COMPANY INFORMATION 4.1 I Name of Parent Company IE. I. Da Pont De Nemours I 4.2 I Parent Conpeny's Dun & Bradstreet Number | | 00-131-5704 EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR SAL 000004386 'PA Form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS APE TRANSFERRED IN WASTES I. PUBLICLY OWNED TREATMENT WORKS (POTWs) 1.1 POTU name HA Street Address City County 1.2 POTU name HA | Street Address I................................. j City Page 2 of 5 Toluene Ocnoco lake diaries Ref County State I Zip | State Zip 2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name BET 2.2 Off-site location name OfKL EPA Identification Nuitoer (RCRA ID No.) HA EPA Identification Ninber (RCRA ID No.) LAD000777201 Street Address Cities Service Hwy @ 1-10 Street Address Rt 2, John Brannon Pd City Sulfur i County I Calcasieu I ciJ , 1 Carlyss ( County I Calcasieu State IA Zip 70664 State IA 7663 .s location under control of reporting facility or parent company? I I Yes ( Xl No ssstcsssissaiiiciiassssssisssitssssssBsiszsssirasiixssssi 2.3 Off-site location name HA Is location under control of reporting facility or parent company? t ] Yes (X] tCMxstiHssss5S38Sssss8SSSssss$ss::s:sssssscss(Si mt:n; 2.4 Off-site location name HA EPA Identification NuiPer (RCRA ID No.) Street Address | EPA Identification Number (RCRA ID No.) 1 | Street Address City | County 1 State i Zip 1 is location under control of reporting facility or parent company? [ ] Yes [ ] No 2.5 Off-site location name NA EPA Identification Nurber (RCRA ID No.) Street Address | City 1 | State | County 1 | Zip | Is location under control of reporting facility or parent ] company? ( ) Yes [ ] No :KXZSSKiicsssstKBs:iiisssxicsssMsss:":sss:"rfSSSSss3SsssuKii [ 2.6 Off-site location name HA | EPA Identification Nunber (RCRA ID No.) 1 | Street Address City itate | County | Zip | City 1 | state | County 1 | Zip Is location under control of reporting facility or parent company? T ] Yes [ ] No | Is location under control of reporting facility or parent j company? I ] Yes [ ) No [ ] Check if additional pages of Part I] are attached. How many? c ] . EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR SAL 000004387 Page 3 of 5 EPA FORM R PART III. CHEMICAL-SPECIFIC INFORMATION iistnusssi 1. CHEMICAL IDENTITY (Do not conplete this section if you conplete Section 2. Toluene Ccnoco lake Charles Refi 1.1 11 [Reserved) 1.2 1I CAS Nuiber (Enter the nunber exactly as it appears on the 313 list. Enter NA if reporting chemical category.) 1 000108-88-3 1.3 || Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 list.) 1j Toluene 1.4 I Generic Chemical Name (Complete only if Part 1, Section 1.1 is checked "Yes.** Generic name eust be structurally descriptive.) 2. MIXTURE COMPONENT IDENTITY (Do not complete this section if you complete Section 1.) Generic Chemical Name Provided by Supplier (Limit the name to a maxim* of 70 characters <e.g., nuitoer*, letters, spaces, punctuation).) sssstssssssssttsssmssssssstsuiHEssttssxsssmiiaiiHicsstnHistatsimcssissscsxMHncnusssssscnmtHistcnaimicsmttit 3. | ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) | Manufacture the 3.1 chemical: a. (X] Produce b. t ] Import | If produce or import: j j c. [X] For on-site use/processing e. [ I As a byproduct d. [ ] For sale/ distribution f. [ X As an impurity | Process the 3.2 chemical: a. fX] As a reactant d. [ 3 Repackaging only b. T 3 As a formulation component c. I 3 As an article component ',3 | Otherwise use a. t 3 As a chemical b. [ 3 As a manufacturing aid c. [ ] Ancillary or other use l the chemical: processing aid ::s:sss:sisttsssnunnssiEs:iHSiumtisituiiiiiiintt<ns(ictiKcassissnsc(isaiusn(t(i((nM(itii<m(i( . MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR (08l (enter code) 5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.2 5.3.3 C cU (3 l3 5.4 Underground Injection ! 5.1a 5.2a S.3.1a 5.3.2a 5.3.3a A. Total Releases (Ibs/yr) B. Basis of Estimate (enter code) | j j A Reporting Ranges 0 1-499 500- 999 l3 C lI c C3 {1 l3 3 3 [ c [3 (] [3 t3 A.2 Enter Estimate 37000 7000 1 i 5.1b tO ) 5.2b tO 3 34 NA NA 5.3.1b tM ) 5.3.2b t 1 5.3.3b t 3 C. X From Stormwater 5.3.1c NA 5.3.2c 5.3.3c 5.4a| [ 3 [ 3 ( 3 | NA | 5.4b t 3 5.5 Releases to land 5.5.1 On-site landfill 5.5.2 Land treatment/application farming 5.5.3 Surface impoundment 5.5.4 Other disposal 1 5.5.1a 1 5.5.2a 1 5.5.3a 1 5.5.4a 1 t3 l3 t3 EJ t3 c1 [3 l] [3 [3 r3 [3 ! | I 1 | NA NA NA 5.5.1b [ 5.5.2b [ 5.5.3b [ 5.5.4b ( ) 3, 3 ]i 3 (Check if additional information is provided on Part IV - Supplemental Information) EPA Form 9350-1 (1-90) Revised - Do not use previous versions 313 ADVISOR SAL 000004388 EPA FORM R PART Ml. CHEMICAL*SPECIFIC INFORMATION (continued) Page 4 of 5 Toluene Conoco Lake diaries Ref 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS You may report transfers of less than 1,000 lbs by checking ranges wider A.1. (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate B. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) Oischarge to POTU 6.1.1 (enter location nunber from Part 11, Section 1.) 1.( ) C3 t3 I3 NA 6.1.1b [ 3 Other Off-Site Location 6.2.1 (enter location nuiber from Part II, Section 2.) 2.(2 3 1 | C3 j l3 13 170 6.2.1b C O 3 6.2.1c M72 Other Off-Site Location 6.2.2 (enter location nunber from Part 11, Section 2.) 2.[1 ] C 3 (3 t 3 210 6.2.2b (O ] 6.2.2c M72 Other Off-Site Location 6.2.3 (enter location nuiber from Part II, Section 2.) 2.1 1 I | [] j C3 II! [1 j NA | 6.2.3b [ ] j 6.2.3c III [ ] (Check if additional information is provided on Part IV Supplemental Information) sst,icssunnsfnx*ssciscsss<n*>ittisistss*i(ittss*nckstcsisisn*siiniiuMsstsfnHSfsits(S*cistsiftitscinai 7. WASTE TREATMENT METHOOS AND EFFICIENCY C 3 Not Applicable (NA) - Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. A. General Wastestream (enter code) | B. Treatment | Method j (enter code) C. Range of Influent Concentration (enter code) 0. Sequential Treatment? (Check if applicable) E. Treatment Efficiency Estimate F. Based on Operating Data? Yes 7.1a (W | 7.1b [Bill 7.1c [4] 7. Id [3 7.1e 90.00 X |7.1f 3 7.2a (A 1 7.2b [ A07] 7.2c [23 i 7.2d [3 7.2e 88.00 X 17.2f [X] 7.3a t3 j 7.3b [NA 3 | 7.3c [3 | 7.3d C 3 , 7.3e X 17 - 3f t 3 7.4a t3 | 7.4b C NA i ; 7.4c [3 | 7.4d [ 3 | 7.4e X |7.4f [ 3 7.5a [3 | 7.5b [NA 3 | 7.5c [3 | 7.5d ( 3 1 7.5e X |7.5f [ 3 7.6a [3 | 7.6b (NA 3 | 7.6c [3 | 7.6d [ 3 | 7.6e X |7.6f l 3 7.7a C3 [ 7.7b (NA 3 | 7.7c C3 | 7.7d [ 3 | 7.7e X |7.7f c 3 7.8a c3 | 7.8b [NA ] | 7.8c t | 7.8d [ 3 | 7.8e X |7.8f [ 3 7.9a [3 | 7.9b [NA 3 | 7.9c C | 7.9d [ 3 | 7.9e X |7.9f r 3 7.10a c3 | 7.10b [ NA ] | 7.10 [ | 7.10d [ 3 | 7.10e X 17.10 f t 3 t 3 (Check if additional information is provided on Part IV * Supplemental Information) NO tX] [3 [3 (3 C3 [3 I3 c3 [3 (3 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility, items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) B. Ouantity of the Chemical in Wastes Prior to Treatment or Disposal C. index 0. Reason for Action (enter code) M[ 3 Current reporting year (Ibs/yr) Prior year (Ibs/yr) |Or Percent Change 3+ 3 R( 3 EPA Form 9350*1 (1*90) Revised - Do not use previous versions. 313 ADVISOR SAL 0000043HQ EPA FOAM R PART IV. SUPPLEMENTAL INFORMATION Use this section if you need additional space for answers to questions in Part III. .fiber the lines used sequentially froei lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) sssnsssesscsi ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Part III, Section 5.3) Page 5 of 5 Toluene Qonoco lake Charles Rfifi You may report releases of less than 1,000 lbs by checking ranges under A.1 (Do not use both A.1 and A.2) A. Total Releases (lb$/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies 5.3.[ J (Enter letter code from 5.3.[ 3 Part 1 Section 3.10 for 5.3.t ] [ ] 5.3. la l 3 5.3. 3 a | [ ] 5.3.t 3a| [3 ] 3 Cl ) [J [1 ) [) stream(s) in the box provided.) I i::sssniss88SmisMssssssss3<iess ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN UASTE TO OFF-SITE LOCATIONS (Part III, Section 6) 5.3. 3b ( 5.3. 3b 5.3.E 3b C. X From Stormwater ] 5.3. 3c 3 5.3. 3c 3 5.3.1 3c :SSSS8SSSSRS8SSSS888SSlta rou may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) Discharge to POTU '. 3 (enter location nurber from Pert U, Section 1.) 1.E ] | A. Total Transfers (lbs/yr> |B. Basis of Estimate j (enter code) i | A.1 | Reporting Ranges | 0 1-499 500*999 |A.2 Enter Estimate |C. Type of Treatment/ | Disposal j (enter code) 1 1 1 | 3 (3 3 1 16.1. 3b 'I Other off-site location 6.2. 3 (enter location nuiber from Part II, Section 2.) 2. ] | | . ] | t3 3 111 I 16.2. 3b 3 6.2. 3c II Other off-site location 6.2. [ 3 (enter location nunber from Part II, Section 2.) 2.E 6.2.1 ]b ] 16.2.E ]c Other off-site location 6.2. t 3 (enter location nutber from Part II, Section 2.) 2.C 3 | | 3 | 3 III l3 I 16.2.[ 3b C ] 6.2. 3c 111 ADDITIONAL INFORMATION ON UASTE TREATMENT METHOOS AND EFFICIENCY (Part III, Section 7) A, General Wastestream (enter code) | B. Treatment 1 Method J j (enter code) | C. Range of 1 Influent ] Concentration | (enter code) | D. Sequential I Treatment? | (Check if j applicable) 7. 1 3 a 3 1 7- 3b 1 1 7. [ 3c 3 1 7.[ 3d 3 7. [ la 7. 1 3a C1 3 1 7.C I 7.E lb lb 1 1 7.1 1 1 7. [ 1c 3c 3 3 1 7 -1 3d l 3 1 7. Id 3 7. [ 3a [ 1 1 7.1 3b 1 1 7.E 3c ] 1 7.1 3d 3 7.1 la 7. 3a r 3a l1 t3 t3 1 7. t 1 7.t 1 7.1 lb l 3b t 3b C 1 1 7.1 1 1 7. [ 1 1 7. )c 3c 3c t3 3 3 1 7.[ 1 7.1 1 7.1 3d 3d Id 3 3 3 i . L 3a 3 1 7.1 lb 3 1 7. [ 3c 3 1 7. 3d 3 7. [ 3a C 3 | 7.1 3b 3 1 7.1 3c 3 1 7. Id 3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. | E. Treatment l Efficiency ( Estimate 1 1 7.1 3 e 1 7-t le 1 7.1 3 e 1 7. [ 3 e 1 7. 3 e I 7.1 1 7.[ le le 1 7.1 le 1 7.C le | F. Based on [ Operating | Data? | Yes X )7. [ If 3 X |7. X |7.[ If t 1 3f t 1 X 17* 3 f [ 3 X |7. X | 7. [ X |7.[ If 3 3f C 3 ]f t 3 X |7-C X 17- If c 3 3f [ 3 313 ADVISOR No 3 3 3 3 3 3 3 3 C3 SAL 000004390 EPA U.S. Environmental Protaction Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM Section 313 of the Emergency Planning and Conunity Right-to-Know Act of 1986, | also known as Title III of the Superfwd Amendments and Reauthorization Act. Page 1 of 5 1,2,4-Trimethylbenzene CQnOCO Tales friarioa Ref* | EPA FORM R ursis::=:=>xs PART I. FACILITY IDENTIFICATION SECTION ssaicsssssa 1.1 Are you claiming the chemical identity on page 3 trade secret? [ ] Yes (Answer question 1.2; [X] No <0o not answer 1.2; Attach si^stantiation forms.) Go to question 1.3.) 1.2 If MYesM in 1.1, is this copy: ( ] Sanitized C j (Jnsanitized 1.3 R^orting Year 2. CERTIFICATION (Read and sign after completing all sections.) I hereby certify that I have reviewed the attached documents and that, to the best of my knowledge and belief, the submitted information is true and complete and that the amounts and values in this report are accurate based on reasonable estimates using data available to the preparers of this report. Name and official title of owner/operator or senior management official Don R. Unruh Refinery Manager Signature I Date signed j 06--20--90 3. Facility Identification Facility or Establishment Name Conoco Lake Charles Refinery Street Address Old Spanish Trail 3.1 city Westlake 1 County | Calcasieu State LA 1 Zip Code |70669 WHERE TO SEND COMPLETED FORMS: 1. EPCRA REPORTING CENTER P.0. BOX 23799 WASHINGTON, DC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRI Facility Identification Nuifaer 70669 CNCLX OIDSP 3.2 | This report contains information for (Check one): a. Oil An entire facility b. ( 1 Part of a facility. 3.3 | Technical Contact 1 Brandt Butler 3.4 | Public Contact Don R. Unruh 1 Telephone Nuitoer |(318) 491-5599 1 Telephone Nimtoer |(318) 491-5222 3-5 | SIC Code (4 digit) | 1 a. 2911 | b. NA j | c.NA 1 1 d. NA | e. NA | f. NA 3.6 1| Degrees 030 Latitude Minutes 14 Seconds 36 1 | Degrees 093 Longitude Minutes 16 Seconds 20 3.7 | Dun & 8radstreet Nunber(s) 1 a. 00-842-7692 3.8 | EPA Identification Nurfcer(s) (RCRA ].D. No.) 1 a. IAD990683716 3.9 | NPDES Permit Number(s) 1 a. IA0003026 1 1 b- NA 1 b- NA 1 1 b. NA 3.1oj Receiving Streams or Water Bodies (enter one name per box) 1 1a. Bayou Verdine b* NA c. NA 1 1 e. NA l d. NA 1 NA i.llj Underground Injection Well Code <UIC) Identification Nuifcer(s) a. NA 1 b. NA 4. PARENT COMPANY INFORMATION 4.1 | Name of Parent Company 1I E. I. Du Pant De Nemours 1 ! 1 Parent Company's Dun & Bradstreet Nipber 00-131-5704 pA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR c;A| OOOOQ4391 | 'A Form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES :ssss8s::ss:zss8snsas8SSKsss8snns8sns8f(:sxcS8fi 1. PUBLICLY OWNED TREATMENT WORKS (POTWs) 1.1 POTW name NA Street Address City I County 1 1.2 POTW name j NA | Street Address 1 j City Page 2 of 5 1,2,4-Trimethyli3enzene Conoco lake Charles Refi ExxctsEiui>>stx:iixii: j County State 1 Zip j State 1 Zip 1l 1 8SS8W88M8X888888S8Sg8M8SSS8a*g8SSssBasiBiBssstisitaacsssii 2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name BET 1 2.2 Off-site location name | CWMX EPA Identification Winter (RCRA ID No.) NA 1 EPA Identification Number (RCRA ID No.) | IAD000777201 Street Address Cities Service Hwy @ 1-10 1 Street Address | Rt 2, John Brannon Rd City Sulfur | County j Calcasieu | City 1 Carlyss [ County | Calcasieu State LA I 2ip j 70664 1 State 1 iA | 7*5663 oeation under control of reporting facility or parent . pany? [ 3 Yes [55 No 2.3 Off-site location name NA j Is location under control of reporting facility or parent | conpany? [ 3 Yes tXl No 1 2.4 Off-site location name | NA 8S8834BSaasaB888aklBB8388 EPA Identification NiirPer (RCRA ID No.) | EPA Identification Nuiber (RCRA ID No.) ! Street Address j Street Address City 1 County State l Z'P 1 Is location under control of reporting facility or parent company? [ 1 Yes [ ] No 2.5 Off-site location name NA EPA Identification Number (RCRA ID No.) Street Address Ci ty ) County I City l | State j County 1 | Zip [ Is location under control of reporting facility or parent | company? [ ] Yes C 3 No I 2.6 Off-site location name I NA [ EPA Identification Nurber (RCRA ID No.) 1 j Street Address 1 l City j County ate 2 ip State Zip Is location under control of reporting facility or parent company? I 3 Yes [ 3 No | Is location under control of reporting facility or parent j company? [ ] Yes [ ] Ho l ] Check if additional pages of Part II are attached. How many? 13 ' EPA Form 9350-1 <1-90) Revised - Do not use previous versions 313 ADVISOR sal. QOOnrss. EPA FORM R PART 111. CHEMICAL-SPECIFIC INFORMATION Page 3 of 5 1,2,4-TrimethyliDenzerie Ocnoco lake Cnarles Ref* 1. CHEMICAL IDENTITY (Do not complete this section if you complete Section 2. i.i | [Reserved] 1.2 1 CAS Nurber (Enter the ruber exactly as it appears on the 313 list. Enter NA if reporting chemical category.) 000095-63-6 1.3 || Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 list.) lj 1,2,4-Trimethylbenzene 1.4 | Generic Chemical Name (Complete only if Part 1, Section 1.1 is checked "Yes." Generic name must be structurally descriptive.) iisscsscmsctici 2 MIXTURE COMPONENT IDENTITY (Do not conplete this section if you complete Section 1.) astzsxsi Generic Chemical Name Provided by Supplier (Limit the name to a mmxisua of 70 characters (e.g., rmnbers, letters, spaces, punctuation).) 3. | ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check all that apply.) | Manufacture the 3.1 | chemical: 1 Process the 3.2 chemical a. [Xl Produce b. [ ] Import j If produce or import: j | c. (X) For on-site use/processing e. [ ] As a byproduct d. [ ] For sale/ distribution f. t X As an impurity a. [X] As a reactant d. [ ] Repackaging only b. [ ] As a formulation component c. ( 1 As an article component 3.3 Otherwise use the chemical: a. [ ] As a chemical processing aid b. [ ] As a manufacturing aid c. [ 1 Ancillary or other use SS :SC*Sll8SIiaiKIKMSSSStimSSSSSXSStKXIlSZSSnSSSSSSSSSCStSkSSSSSSSSSSSSXSSCSSS:kIBSIIElIE=CSSsrS:tSS8SlSIIISlBB8IBtlBBSI H. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR [07) (enter code) 5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases (Ibs/yr) 6. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions | 5.1a | 5.2a 3 1 [1 [1 3 [) 8000 150 5.1b [O ] 5.2b [0 ] 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.2 5.3.3 [ 3] C] [] 5.3.1a 5.3.2a 5.3.3a ] 1 ) ] t] ] [) ] [i 17 NA NA 5.3.1b [0 ] 5.3.2b [ 3 5.3.3b C 3 C. X From Stormwater 5.3.1c NA 5.3.2c 5.3.3c 5.4 Underground Injection 5.4a t ] ] t) NA 5.4b [ ) 5.5 Releases to land 5.5.1 On-site landfill 5.5.2 Land treatment/application farming 5.5.3 Surface impoundment 5.5.4 Other disposal 1 5.5.laj 5.5.2a| 5.5.3a j 5.5.4a| [] [] [] [) C1 r) c) () t] [) i) [) I NA j 5.5.1b [ 3 NA | 5.5.2b r ) NA j 5.5.3b [ 3 NA j 5.5.4b [ 3 ) (Check if additional information is provided on Part IV - Supplemental Information) EPA Form 9350-1 (1-90) Revised - 0o not use previous versions. 313 ADVISOR SAL 000004393 Page 4 of 5 *PA FORM R PART III. CHEMICAL-SPECIFIC INFORMATION (continued) :niasszsssca S. TRANSFERS OF THE CHEMICAL IN UASTE TO OFF-SITE LOCATIONS 1,2,4-Trimethylbenzene Cdnoao lake Cnarles Pefi You may report transfers of less than 1,000 lbs by checking ranges under A.1 (Do not use both A.1 and A.2) A. Total Transfers (Ibs/yr) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate B. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) 6.1.1 Discharge to POTU (enter location nurter from Part II, Section 1.) 1.E 3 [3 l ] [3 NA 6.1.1b t 3 Other Off-Site Location 6.2.1 (enter location nuiter from Part 11, Section 2.) 2. (2 3 [3 1 [3 50 6.2.1b [O 3 6.2.1c M72 Other Off-Site Location 6.2.2 (enter location muter from Part II, Section 2.) 2.Cl 3 13 1 3 [3 1 62 6.2.2b [O ] 6.2.2c M72 Other Off-Site Location 6.2.3 (enter location nutter from Part II, Section 2.) 2.1 3 13 1 3 [3 NA ; 6.2.3b [ | 6.2.3c 1 11 t [ ) (Check if additional information is provided on Part IV Supplemental Information) 5SIR88Sm$8SS88SSSSSSSSS88888SSISIISSSS58855888S88888559888mC3BS85SmmSSSSS8SS8SSI 7. UASTE TREATMENT METHOOS AND EFFICIENCY C 3 Not Applicable (NA) - Check if no on-site treatment is applied to any wastestream containing the chemical or chemical category. A. ierel wastestream (enter code) 7.1a iWi 7.2a [A 3 7.3a L3 7.4a c3 7.5a l3 7.6a 7.7a [3 C1 7.8a 7.9a [3 [3 7.10a c1 B. Treatment Method (enter code) 7.1b 7.2b [Bill [ A07] 7.3b [NA 3 | 7.4b [ NA 3 | 7.5b t 7.6b | 7.7b | 7.8b | 7.9b | 7.10b [NA ] [NA ] [NA ] [NA ] [NA ] [NA 3 C. Range of Influent Concentration (enter code) 7.1c [4] 7.2c [2] [ 7.3c [ | 7.4c [ | 7.5c [3 [ 7.6c [3 | 7.7c [3 | 7.8c [3 | 7.9c [3 | 7.10 [1 1 D. Sequential j T reatment? (Check if | applicable) | 7.1d | 7.2d [] [3 | 7.3d | 7.4d E3 [3 l 7.5d [3 | 7.6d | 7.7d | 7.8d 1 7.9d | 7.10d [3 [3 [3 [3 [3 E. Treatment Efficiency Estimate j F. Based on | Operating Data? 1 Yes 7.1 7.2e 7.3e 7.4e 95.00 X |7.1f 88.00 X |7.2f X |7.3f X |7.4f [3 L X) [3 l] 7.5e 7.6e 7.7e 7.8e 7.9e 7. lOe X |7.5f [ 3 X |7.6f [ 3 X |7.7f [ 3 X |7.8f l ] X |7.9f t 3 X 17.10f C 3 No [X] (3 C3 [3 [3 [3 t3 [3 C3 [3 [ ] (Check if additional information is provided on Part IV - Supplemental Information) 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON WASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of uhat information to include.) See the instructions for coded A. Type of Modification (enter code) | B. Quantity of the Chemical in Wastes Prior to Treatment or Disposal } C. Index [ | D. Reason for Action (enter code) j M[ ] j Current reporting | year (Ibs/yr) | Prior |0r Percent 1 year (lbs/yr> |Change |[ 3 + j It I' X| [ EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 1 j 3| RI 313 ADVISOR SAL 000004394 Page 5 of 5 EPA FORM R PART IV. SUPPLEMENTAL INFORMATION Use this section if you need additional space for answers to questions in Part III. Nunfeer the lines used sequentially fron lines in prior sections (e.g., 5.3.4, 6.1.2, 7.11) 1,2,4-JItiniethyIbenzer)e Oonoco Lake Cnarles Refi ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT (Pert III, Section 5.3) You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A. Total Releases Clbs/yr) B. Basis of Estimate (enter code) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.1 5.3.1 1 1 [ ) 5.3. 3al t ] 5.3.1 3a| t ] 5.3.1 )a| i1 C3 C3 C3 C3 [3 l3 l3 [3 [3 5.3.1 3b l 5.3.1 3b C 5.3.1 3b ( C. X Froai Stonwater 3 5.3.[ 3c 3 5.3.C 3c 3 5.3.t )c ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6) You may report transfers of less then 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) | A. Total Transfers <Ibs/yr) 1............................... | A.1 | | Reporting Ranges } | 0 1-499 500-999 j A.2 Enter Estimate B. Basis of Estimate (enter code) Type of Treatment/ Disposal (enter code) Discharge to POTW 3 (enter location nuifcer from Part 11, Section 1.) Other off-site location 6.2. [ 3 (enter location number from Part II, Section 2.) 6.2.1 Other off-site location 3 (enter location nunber from Part It, Section 2.) Other off-site location 6.2.t 1 (enter location number from Part II, Section 2.) 1.[ 3 2.C 3 2.C 3 2.[ ] 1 j [3 i j [3 13 C3 C3 1 1 1 1 [3 | 1 1 C^ (3 l3 1 1 1 (1C) 6.1.1 3b ( 3 1 |6.2.C 3b ( 1 |6.2.l 3b [ 1 3|6.2.( 1 3c l 3 |6.2.[ 3c 6.2.[ ]b l ] 6.2.1 ]c ADDITIONAL INFORMATION ON WASTE TREATMENT METHOOS AND EFFICIENCY (Part III, Section 7) A. General Wastestream (enter code) 7.C 3 a C3 | B. Treatment I Method | (enter code) 1 r.t 3b ( | C. Range of t Influent Concentration 1 (enter code) 1 7. [ 3c [3 0. Sequential Treatment? (Check if | applicable) 1 7.C 3d [ ) E. Treatment Efficiency Estimate 1 1 7.[ }e 7. [ 3 a 7.t 3 a l3 [3 1 7.1 1 7.[ 3b [ 3b C 1 7. [ 1 7.1 Jc ]e (3 l3 1 7. [ I 7.1 3d Id [3 [3 1 7.C 1 7.1 3e ]e 7. [ ] a t 3 1 7.C 3b c 3 1 7.[ 3c [3 1 7.1 Id [ 3 1 7.1 3 e 7. [ ]a 7. [ 3 a P 3a 7. [ 3a 7. [ 3 a C3 [3 [3 t3 [1 1 7.1 3b t 1 7.1 3b [ 1 7.1 3b ( 1 7.1 3b [ 1 7.1 3b ( 1 1 7. [ 3 1 7.1 3 7.1 3 7. [ 3 7. ( 3c 3c 3c 3c 1c (3 [3 [3 [3 l3 1 7.1 Id | 7.1 Jd 1 7.1 3d 1 7.[ 3d 1 7.C Id [3 t3 [3 [3 C3 1 7. [ 1 7. [ 1 7.1 1 7.C 1 7. ( 3e ]e 3e 3e 3e EPA Form 9350-1 (1-90) Revised - Do not use previous versions. F. Based on Operating Data? Yes X 7.1 3f C 3 X 7.[ ]f C 3 X 7-1 X |7-E 3f [ 3 3f ( 3 X I7.E ]f [ 3 X 17-1 If C 3 X I7.C if [ 3 X 17. E 3f [ 3 X 17. [ If l 3 313 .ADVISOR No l3 C3 (3 (3 c3 [3 l3 l3 [3 SAL 000004395 EPA U.S. Environmental Protection Agency TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM ction 313 of the Emergency Planning and Community Right-to-Know Act of 1966, i .so known as Title HI of the Superfund Amendaents and Reauthorization Act. Page 1 of 5 | Xylene (mixed IscnSTS) > | CCOOGO * aVo Charles Refi j | EPA FORM R PART I. FACILITY IDENTIFICATION SECTION sm:s:ss:ssssssisiznssssttssmEsiimnszxitstsscxisxaiisnsssst: 1.1 Are you claiming the chemical identity on page 3 trade secret? ( ] Yes (Answer question 1.2; (X) No (Do not answer 1.2; Attach substantiation forms.) Go to question 1.3.) BSSSSSSSSSSS&a 1.2 If "Yes** in 1.1, is this copy: ( ] Sanitized ( ] Unsanitized 1.3 Report mg Year 2. CERTIFICATION (Read and sign after conpleting all sections.) I hereby certify that I have reviewed the attached docunent* and that, to the best of my knowledge and belief, the submitted information is true and complete and that the amowts and values in this report are accurate based on reasonable estimates using data available to the preparers of this report. Name and official title of owner/operator or senior management official Don R. Unruh Refinery Manager Signature I Date signed |06-20-90 3. Facility Identification Facility or Establishment Name Conoco lake Charles Refinery Street Address Old Spanish Trail UHERE TO SEND COMPLETED FORKS: 1. EPCRA REPORTING CENTER P.O. BOX 23799 WASHINGTON, DC 20026-3779 ATTN: TOXIC CHEMICAL RELEASE INVENTORY City Westlake state LA t County [ Calcasieu { Zip Code |70669 2. APPROPRIATE STATE OFFICE (See instructions in Appendix G) TRl Facility Identification Nunber 70669 CNCLK OIDSP 3.2 1 This report contains information for (Check one): 3.3 j Technical Contact Brandt Butler a. (li 3 An entire facility 1 Telephone Hunter |(318) 491-5599 b. [ ] Part of a facility. 3.4 | Public Contact Don R. Unruh 1 Telephone Number | (318) 491-5222 3.5 | SIC Code (4 digit) j 1 a. 2911 | b. NA Latitude 3.6 Degrees Minutes 030 14 | | c.NA Seconds 36 1 1 d. NA | | Degrees 093 1 e. NA Longitude Minutes 16 | f. NA Seconds 20 j 3.7 Dun & Bradstreet NtrPer(s) a. 00-842-7692 3.8 EPA Identification Nunber(s) (RCRA I.D. No.) a. LAD990683716 1 1 b. NA I b. NA 3.9 NPDES Permit NurPer(s) a. IA0003026 1 b. NA Receiving Streams or Water Bodies (enter one name per box) | a. Bayou Verdine i b. NA c. NA 1 d. NA e. NA 1 f. NA Underground 1 njection Weil Code (UtC) Identification Munber(s) | a. NA 1 b. NA 4. PARENT COMPANY INFORMATION 4.1 I Name of Parent Company | E. I. Du Pont De Nemours 1 4.2 I Parent company's Dun & Bradstreet Nuifcer | | 00-131-5704 EPA Form 9350-1 (1-90) Revised - Oo not use previous versions. SAL 000004396 313 ADVISOR ERA Form R Part II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IK WASTES 1. PUBLICLY OWNED TREATMENT WORKS (POTUs) 1.1 POTW name NA Street Address 1.2 POTW name NA Street Address Page 2 of S Xylene (mixed iscmers) Conoco lake Charles Re City County City County State Zip State I Zip 2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHICH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE). 2.1 Off-site location name EFT 2.2 Off-site location name CSMI EPA Identification Number (RCRA ID No.) NA I EPA Identification Nuitoer (RCRA ID No.) I IAD000777201 Street Address Cities Servioe Hwy 1-10 Street Address Rt 2, John Brannon Rd City Sulfur | County l Calcasieu I c'ty , j Carlyss County Calcasieu State LA Zip 70664 State IA 7*5663 j location imder control of reporting facility or parent company? C 1 Yes ( X No 2.3 Off-site location name NA { Is location under control of reporting facility or parent | company? [ ] Yes (X) tBSSSStS&SSSSSSS5S8SSS8SSS9SkSSS888S5S888SsS-48SlllB*StllltttSSI I 2.4 Off-site location name NA EPA Identification tixartoer (RCRA ID HO.) ] EPA Identification Number (RCRA ID No.) 1 Street Address | Street Address Ci ty State | County 1 | Zip 1 City 1 | State | County 1 | Zip Is location under control of reporting facility or parent company? [ ] Yes [ ] No 2.5 Off-site location name NA EPA Identification Number (RCRA ID No.) Street Address | Is location under control of reporting facility or parent | conpany? I ] Yes ( ] No I 2.6 Off-site location name | NA | EPA Identification Number (RCRA ID No.) 1 | Street Address City ate | County 1 | z*p 1 City l | State j County t j Zip Is location under control of reporting facility or parent conpany? [ ] Yes ( ] No | Is location under control of reporting facility or parent j company? [ ] Yes [ J No [ ] Check if additional pages of Part II are attached. How many? [ ] EPA Form 9350-1 (1*90) Revised - Do not use previous versions SAL 000004397 313 ADVISOR FORM R PART III. CHEMICAL-SPECIFIC INFORMATION Xylene (mixed isomers) Ccnoco lake Cftarles Kefi 1. CHEMICAL IDENTITY (Do not complete this section if you complete Section 2. 1.11| [Reserved] 1.2 I1 CAS Nuntoer (Enter the mnPer exactly as it appears on the 313 list. Enter NA if reporting chemical category.) | 001330-20-7 1.3 j| Chemical or Chemical Category Name (Enter the name exactly as it appears on the 313 list.) 1 Xylene (mixed isomers) 1.4 J Generic Chemical Name (Conplete only if Part l. Section 1.1 is checked "Yes.** Generic name mjst be structurally descriptive.) ssaxMlsscststssttnssisslicnnsiMiiinniuutsnssanasixMssKnmMsntssssaMSiasmtnsKZsMWutsznnsustnMtiimiK 2 MIXTURE COMPONENT IDENTITY (Do not complete this section if you complete Section 1.) Generic Chemical Name Provided by Supplier (Limit the name to a maximja of 70 characters (e.g., rxnPera, letters, spaces, pirtctuati on),) gMt:s33333sisaais:S3s3sssnsnssx*<3i3seisxciiins>nc:ix33:x3sasscasx33sssSxmsss:8S>s:SKs:sssssBS3s3ss$3x*sixtsssuasc 3. | ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check ail that apply.) | Manufacture the 3.1 j chemical: a. cXj Produce b. [ ] Import J If produce or import: j | c. [X] For on-site use/processing e. C 3 As a byproduct d. [ ] For sale/ distribution f. [ X As an inpurity j Process the 3.2 j chemical: j a. [X] As a reactant d. C ] Repackaging only b. { I As a formulation conponent c. [ ] As an article component 3 1 Otherwise use the chemical: a, [ 1 As a chemical processing aid b. ( I As a manufacturing aid c. [ ] Ancillary or other use V 33s:S3S3S3SS3333S3StlSt3IX3aI3S<3I3HX3SISa3St3X3ISSE333nS3SSS3ir333SS33SS3SSS33SS3SSS3333B(33S3lS3tS>St3(I>tINim 4. J(IMUN AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR [08] (enter code) 5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE You may report releases of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) j A. Total Releases (Ibs/yr) B. Basis of Estimate (enter code) j j j A.1 l Reporting Ranges [ 0 1-499 500-999 | A.2 Enter Estimate 5.1 Fugitive or non-point air emissions 5.2 Stack or point air emissions 5.3 Discharges to receiving streams or water bodies (Enter letter code from Part I Section 3.10 for stream(s) in the box provided.) 5.3.1 5.3.2 5.3.3 [3] l3 [] | 5.1a ] 5.2a i 1 5.3.1a ) 5.3.2a | 5.3.3a [] r) ri C3 [I C ( ( {] [] [1 1 [) 1 cI [] [3 37000 5.1b tO 3 i 25001 5.2b to ] 17 NA NA 5.3.1b [0 3 5.3.2b t 3 5.3.3b t 3 C. X From Stormwater 5.3.1c NA 5.3.2c 5.3.3c 5.4 Underground Injection | 5.4a ] [] [1 NA | 5.4b t 3 5.5 Releases to land l 5.5.1 On-site landfill 5.5.1a 5.5.2 Land treatment/application farming ( 5.5.2a 5.5.3 Surface impoundment I 5.5.3a .5.4 Other disposal | 5.5.4a ] [] [3 3 l1 [3 J [] c3 J c1 l3 1 NA | 5.5.1b t 3 NA \ 5.5.2b t 3 NA | 5.5.3b t 3 NA | 5.5.4b C 1 (Check if additional information is provided on Part IV - Supplemental Information) - j:s:s:3:s=33:s::s3:::s::::3333:S33333x:s: ======== ======= ===== ===== =====:&ss:ussssss %ss:ssss%sss%sss ============================ EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ACVISOR SAL 000004398 Page 4 of 5 -- FORM R PART III. CHEMICAL-SPECIFIC INFORMATION (continued) ............................................................................................. 6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS A. Total Transfers (Ibs/yr) You may report transfers of less than 1,000 lbs by checking ranges under A.1. (Do not use both A.1 and A.2) A.1 Reporting Ranges 0 1-499 500-999 A.2 Enter Estimate Xylene (mixed i seiners) Ccnooo Lake diaries Pefi B. Basis of Estimate (enter code) C. Type of Treatment/ Disposal (enter code) Discharge to POTW 6.1.1 (enter location nurber from Part 11, Section 1.) 1.1 3 () (3 [) NA 6.1.1b [ ] Other Off-Site Location 6.2.1 (enter location number from Part II, Section 2.) 2.(2 ) | | (] | [) C) 450 6.2.1b C 0 3 6.2.1c Other Off-Site Location 6.2.2 (enter location number from Part 11, Section 2.) 2.(1] I | [) | () [) 6.2.2b [O 3 | 6.2.2c 530 l Other Off-Site Location 6.2.3 (enter location number from Part II, Section 2.) 2.C ) (3 C ) (3 6.2.3b C 3 | 6.2.3c NA 1 I 3 (Check if additional information is provided on Part IV - Supplemental Information) M72 M72 7. UASTE TREATMENT HETHOOS AND EFFICIENCY [ ] Not Applicable (NA) - Check if no on-site treatment is applied to any uastestreem containing the chemical or chemical category. A. ueneral Uastestream (enter code) B. Treatment Method (enter code) C. Range of Influent Concentration (enter code) D. Sequential Treatment? (Check if applicable) 1 E. Treatment j Efficiency Estimate F. Based on Operating Data? Yes 7.1a 7.2a i!W] [A 3 7.1b 7.2b ( Bll] C A07] 7.1c 7.2c [43 (23 7. Id 7.2d [3 [3 | 7.1e | 7.2e 95.00 X |7.If 88.00 X |7.2f C3 [Xl 7.3a 7.4a 7.5a [3 [3 [3 7.3b 7.4b | 7.5b [NA 3 [NA ] (NA 3 7.3c 7.4c 7.5c [3 [3 [3 7.3d 7.4d l 7.5d [3 C3 [3 l 7.3e | 7.4e | 7.5e X 7.3f X 7.4f X |7.5f [3 [3 [3 7.6a 7.7a 7.8a 7.9a t3 I3 c3 (3 | 7.6b | 7.7b | 7.8b | 7.9b [NA ] [ NA ] [NA 3 [ NA ] | | 7.6c 7.7c 7.8c 7.9c [3 [3 [3 t3 | 7.6d [ 7.7d | 7.8d | 7.9d C3 [I [3 [3 ] 7.6e | 7.7e | 7.8e 1 7.9e X |7.6f X |7.7f X |7.8f X |7.9f [3 [J l3 [3 7.10a C3 | 7.10b [NA 3 [ 7.10 [3 | 7.10d [ 3 j 7.lOe X \7.lOf [ 3 [ ] (Check if additional information is provided on Part IV - Supplemental Information) No [X] [3 [3 cJ [3 c3 :3 i3 [3 c3 8. POLLUTION PREVENTION: OPTIONAL INFORMATION ON UASTE MINIMIZATION (Indicate actions taken to reduce the amount of the chemical being released from the facility. items and an explanation of what information to include.) See the instructions for coded A. Type of Modification (enter code) B. Quantity of the Chemical in Uastes Prior to Treatment or Disposal C. Index D. Reason for Action (enter code) HC 3 | Current reporting | year (Ibs/yr) 1 Prior year (Ibs/yr) Or Percent Change t 3+ t 3- X [ 3 - R( 3 EPA Form 9350-1 (1-90) Revised - Do not use previous versions. 313 ADVISOR SAL 000004399 CALCULATIONS SARA TITLE III, SECTION 313 1989 TOXIC CHEMICAL RELEASE INVENTORY LAKE CHARLES REFINERY SAL 000004400 Calculations The attached release inventory gives a unit by unit comparison of emissions in 1988 and 1989. For specifics on the 1988 releases, consult the 1988 SARA 313 documentation. The calculated releases for 1989 are attached or found in the following sections: Storage Tanks - Appendix H Wastewater Treatment - Appendix G API, DAF, IAF Emissions - Appendix G Loading Loss - Appendix J Process Equipment Fugitives - Appendix I Process Drains - Appendix I Cooling Tower - Appendix I Solid Waste Release - Appendix F Spreadsheets are referenced for many of the calculations. These spreadsheets are available from Bruce Schroer, PED, Ponca City. SAL 000004401 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = AMMONIA 1988 RELEASE (LB/YR.) AIR POINT RELEASES NA AIR NON-POINT RELEASES CTU (#2, #3) inhibitor wastewater Trtmt Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-site (BFI) Off-Site (CWMI) Total Off-Site Release 410 1752 2162 2162 3117 NA NA NA 0 1989 RELEASE (LB/YR.) NA 410 1217 1627 1627 2172 NA NA NA 0 ooooo^02 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = BENZENE 1988 RELEASE (LB/YR.) 1989 RELEASE (LB/YR.) AIR POINT RELEASES Storage Tanks AIR NON-POINT RELEASES Loading Loss Process Equipment Fugitives #3 CTU & Vac #2 CTU #4 HDS #3 CRU & HDS #1 Coker #2 Coker Gas Recovery Plant #6 HDS FCC Feed Prep FCC #2 CRU & HDS Thermal Cracker PBC Molex SHAD/VHAD Tank Farm Process Drains Separators API DAF IAF Cooling Water Wastewater Trtmt Landfarm Waste Trtmt Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 16951 1181 876 789 461 1738 114 22 200 190 118 394 987 75 1806 72 2541 5059 276 116 4 2 125 187 351 17684 34635 39 0 NA NA 0 8605 1826 740 720 380 1240 40 20 120 100 40 320 1500 120 300 80 3660 4360 1792 112 4 2 125 163 NA 17764 26369 34 NA 62 50 112 000004A03 SAL SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = 1,3-BUTADIENE 1988 RELEASE (LB/YR.) AIR POINT RELEASES NA AIR NON-POINT RELEASES Fuel Gas Fugitives Process Equipment Fugitives #1 Coker #2 Coker Gas Recovery Plant FCC Cryo Cat Poly Thermal Cracker PBC Alky Acid Plant Tank Farm Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 149 38 7 138 286 90 123 7 230 125 2 147 1342 1342 NA NA NA NA 0 1989 RELEASE (LB/YR.) NA 200 40 20 120 320 100 80 20 40 120 0 160 1220 1220 NA NA NA NA 0 sac 000044 04 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = CHLORINE 1988 RELEASE (LB/YR.) 1989 RELEASE (LB/YR.) AIR POINT RELEASES NA NA AIR NON-POINT RELEASES Cool. Tower, Boil. Injet WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 2000 NA NA NA NA 0 2000 NA NA NA NA 0 000004^05 SM- SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = CUMENE 1988 RELEASE (LB/YR.) AIR POINT RELEASES Storage Tanks AIR NON-POINT RELEASES Loading Loss Process Equipment Fugitives #3 CRU & HDS #1 Coker #2 Coker Gas Recovery Plant FCC Feed Prep FCC #2 CRU & HDS Thermal Cracker Tank Farm Process Drains API Separators Cooling Water Wastewater Trtmt Landfarm Waste Trtmt Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 565 69 1442 380 73 307 168 1826 555 75 6324 4 2 47 296 1053 12621 13186 39 0 NA NA 0 1989 RELEASE (LB/YR.) 655 144 1320 380 180 200 42 2080 1060 120 6687 31 2 47 129 NA 12422 13077 17 NA 62 50 112 SAL 000004406 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = CYCLOHEXANE 1988 RELEASE (LB/YR.) AIR POINT RELEASES Storage Tanks AIR NON-POINT RELEASES Process Equipment Fugitives #3 CTU $ Vac #2 CTU #4 HDS #3 CRU & HDS #1 Coker #2 Coker Gas Recovery Plant #6 HDS FCC #2 CRU & HDS Thermal Cracker PBC Molex Tank Farm Process Drains Separators API DAF IAF Cooling Water Wastewater Trtmt Landfarm Waste Trtmt Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 8476 1184 1048 651 424 380 73 307 246 358 588 75 3191 96 980 516 208 8 4 219 78 1259 11893 20369 39 0 NA NA 0 1989 RELEASE (LB/YR.) 2857 1520 1080 640 380 380 180 200 140 400 1140 120 580 140 1040 3303 208 8 4 219 34 NA 11716 14573 17 NA 62 50 112 000004^07 SAL SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT - ETHYLENE 1988 RELEASE (LB/YR.) AIR POINT RELEASES NA AIR NON-POINT RELEASES Fuel Gas Fugitives Process Equipment Fugitives #1 Coker #2 Coker Gas Recovery Plant FCC Cryo Thermal Cracker Acid Plant Tank Farm Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 1786 380 73 154 5728 2691 75 202 2941 14030 14030 NA NA NA NA 0 1989 RELEASE (LB/YR.) NA 2300 380 180 100 6500 2580 120 420 1860 14440 14440 NA NA NA NA 0 SAL 000004408 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = ETHYLBENZENE 1988 RELEASE (LB/YR.) AIR POINT RELEASES Storage Tanks AIR NON-POINT RELEASES Loading Loss Process Equipment Fugitives #3 CTU & Vac #2 CTU #4 HDS #3 CRU & HDS FCC Feed Prep FCC #2 CRU & HDS PBC SHAD/VHAD Tank Farm Process Drains API Separator Cooling Water Wastewater Trtmt Landfarm Waste Trtmt Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 1613 125 165 146 90 1166 106 1074 449 461 290 4461 20 8 74 187 217 9039 10652 39 0 NA NA 0 1989 RELEASE (LB/YR.) 635 138 220 160 80 1220 20 0 980 0 420 3785 106 8 74 81 NA 7292 7927 17 NA 113 96 209 SAL OGOOO^09 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = HYDROCHLORIC ACID 1988 RELEASE (LB/YR.) AIR POINT RELEASES 16 AIR NON-POINT RELEASES Demin. Resin Regen. TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 614 630 0 NA NA NA 0 1989 RELEASE (LB/YR.) 30 614 644 0 NA NA NA 0 SAL 000004410 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = LEAD COMPOUNDS 1988 RELEASE (LB/YR.) AIR POINT RELEASES 0 AIR NON-POINT RELEASES Leaded Gaso. Addn. TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 403 403 0 NA NA NA 0 1989 RELEASE (LB/YR.) 0 403 403 0 NA NA NA 0 SAL 000004411 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = MANGANESE COMPOUNDS 1988 RELEASE (LB/YR.) AIR POINT RELEASES 0 AIR NON-POINT RELEASES Leaded Gaso. Addn. TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarin) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 250 250 0 NA NA NA 0 1989 RELEASE (LB/YR.) 0 250 250 0 NA NA NA 0 ooooo^2 sM- SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = METHANOL 1988 RELEASE (LB/YR.) AIR POINT RELEASES Storage Tanks AIR NON-POINT RELEASES Process Equipment Fugitives Cryo Refrig Deicing Fuel Oil Blending(A023) Propane Blending Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 760 72 482 964 1518 2278 0 0 NA NA 0 1989 RELEASE (LB/YR.) 1210 72 482 964 1518 2728 0 NA 0 0 0 SAL 000004413 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = MOLYBDENUM TRIOXIDE 1988 RELEASE (LB/YR.) AIR POINT RELEASES NA AIR NON-POINT RELEASES HDS Catalyst Handling WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 120 NA NA 21000 NA 21000 1989 RELEASE (LB/YR.) NA 120 NA NA NA NA 0 SARA 3X3 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = NAPHTHALENE 1988 RELEASE (LB/YR.) AIR POINT RELEASES storage Tanks AIR NON-POINT RELEASES Loading Loss Process Equipment Fugitives #3 CTU & Vac #2 CTU #4 HDS #5 HDS #6 HDS #7 HDS FCC Feed Prep #1 HDS PBC Molex SHAD/VHAD Tank Farm Cooling Water Landfarm Waste Trtmt Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-site (CWMI) Total Off-Site Release 1238 3 987 874 542 117 142 56 118 208 384 55 436 2941 59 269 7191 8429 47 0 NA NA 0 1989 RELEASE (LB/YR.) 3187 9 1280 920 520 220 80 160 60 NA 160 80 620 3120 59 NA 7288 10475 34 NA 1218 980 2198 5AU ooooo^15 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT - PHOSPHORIC ACID 1988 RELEASE (LB/YR.) AIR POINT RELEASES NA AIR NON-POINT RELEASES NA WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 0 NA 0 NA 0 1989 RELEASE (LB/YR.) NA NA 0 NA 0 0 0 SAL 000004416 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = PROPYLENE 1988 RELEASE (LB/YR.) AIR POINT RELEASES NA AIR NON-POINT RELEASES Fuel Gas Fugitives Process Equipment Fugitives #1 Coker #2 Coker Gas Recovery Plant FCC Cryo Cat Poly Thermal Cracker PBC Alky Acid Plant Tank Farm Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 2480 2663 511 17380 30430 8611 27934 528 28061 15198 560 1471 135827 135827 NA NA NA NA 0 1989 RELEASE (LB/YR.) NA 3200 2680 1300 11760 34560 8260 17060 880 10680 13900 1160 2600 108040 108040 NA NA NA NA 0 SAL 000G04A17 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = STYRENE 1988 RELEASE (LB/YR.) AIR POINT RELEASES Storage Tanks AIR NON-POINT RELEASES Process Equipment Fugitives SHAD/VHAD Process Drains Cooling Tower Wastewater Trtmt Landfarm-Waste Trtmt Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 27 726 1 6 90 56 879 906 39 0 NA NA 0 1989 RELEASE (LB/YR.) 0 1040 6 6 39 NA 1091 1091 17 NA 0 0 0 SAL 000004418 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = SULFURIC ACID 1988 RELEASE (LB/YR.) AIR POINT RELEASES 464 AIR NON-POINT RELEASES TOTAL AIR RELEASE <499 <963 WATER RELEASE 0 LAND RELEASE NA 1989 RELEASE (LB/YR.) 478 <499 <977 0 NA SAL 000004429 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = TOLUENE 1988 RELEASE (LB/YR.) 1989 RELEASE (LB/YR.) AIR POINT RELEASES Storage Tanks AIR NON-POINT RELEASES Loading Loss Process Equipment Fugitives #3 CTU & Vac #2 CTU #4 HDS #3 CRU & HDS #1 Coker #2 Coker Gas Recovery Plant #6 HDS FCC Feed Prep FCC #2 CRU & HDS Thermal Cracker PBC Mo lex SHAD/VHAD Tank Farm Process Drains Separators API DAF IAF Cooling Tower Wastewater Trtmt Landfarm Waste Trtmt Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 14194 1006 1233 1092 678 4876 1522 292 1231 142 384 2792 2121 302 4421 55 1089 16618 177 72 3 1 301 90 620 41118 55312 39 0 NA NA 0 004A20 SAL 000 7011 1650 1600 1140 380 3820 1540 740 840 80 100 1100 3540 500 1060 80 1560 15299 1293 72 3 1 301 78 NA 36777 43788 34 NA 207 168 375 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = 1,2,4-TRIMETHYLBENZENE 1988 RELEASE (LB/YR.) AIR POINT RELEASES Storage Tanks AIR NON-POINT RELEASES Loading Loss Process Equipment Fugitives #3 CRU & HDS #1 Coker #2 Coker Gas Recovery Plant FCC Feed Prep FCC #2 CRU & HDS Thermal Cracker Tank Farm Process Drains API Separators Cooling Water Wastewater Trtmt Landfarm Waste Trtmt Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 167 19 360 1141 219 923 78 1110 139 226 2941 3 1 47 296 847 8350 8517 39 0 NA NA 0 1989 RELEASE (LB/YR.) 152 68 320 1160 560 640 20 1260 260 380 3108 16 1 47 129 NA 7969 8121 17 NA 62 50 112 sal 0000442! SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY COMPONENT = XYLENE 1988 RELEASE (LB/YR.) AIR POINT RELEASES Storage Tanks AIR NON-POINT RELEASES Loading Loss Process Equipment Fugitives #3 CTU & Vac #2 CTU #4 HDS #3 CRU & HDS #1 Coker #2 Coker Gas Recovery Plant FCC Feed Prep FCC #2 CRU & HDS Thermal Cracker PBC Tank Farm Process Drains Separators API DAF IAF Cooling Water Wastewater Trtmt Landfarm Waste Trtmt Total Non-point Release TOTAL AIR RELEASE WATER RELEASE LAND RELEASE On-Site (Landfarm) Off-Site (BFI) Off-Site (CWMI) Total Off-Site Release 7708 631 657 757 362 3816 2473 475 2000 510 7052 1469 490 6803 21667 131 53 2 1 470 187 983 50989 58697 39 0 NA NA 0 1989 RELEASE (LB/YR.) 2512 576 840 600 340 4020 2500 1200 1360 120 2040 3240 800 580 17786 583 53 2 1 470 81 NA 37192 39704 17 NA 533 454 987 *AL ooo04422 ease Calculations f\rr\rv\On i<=\ AIR R>.'nf- Release -- /Wl L.C Rort - Re/&C($e. ` ^3 *\s\ /5 / nj ec CT6^ "fe inh.'b'I Corpos-'e^ Rti'"L Release M = (*/ *0.01-7.% - 4(ffifv)*0jOo,i') "> M, (e*<.) x'Z-H '5_x /n r x C CTOs * O.ZoHhA = - \V^S~fe Refe_Ase l <-fvvc/ __ /4-.V' tb jZ i3 yp /J Ree Ap^x & *To*fa f Non-Re l-e^^L. - /^27 /<" ^ /COO \a//)7 6^s S : Engi'toeJ~' '^ CP (c.<J l=S`'o v^. Rele^^e- = ZZCC- 3 (-2.-Z&&) (-5ec G /J-/VA Re ie^e NA- ^i'Y4>-er~ chensi'c ^ Ry N<?Cj ra of Pc/ oe \/o (cW <' 2-P^ & T^ip/e i)-I ^s^cait e r>a 1 "Actr) S) FI. *cy<- / v4a.li/e YSo <esi * *-*7 "fVorv, ^ ^ Ctu \Ic- S^rce co o n r RprX See A?s/)5 C.* Apx A~ $al. 0000^3 ' Cf^-LCULJ]-T10N St* CAL Or-( n ^ L.C. ACR Ini' Release. -- fl/o *>,n^" /^-jgl'H^_ - NA__________ Chlon,'tng_ )s /nj'gci'ejf ~^W cool> /i^ ^>to^ 5~ boifer' vA/^-/er 5^s*^^S "fe pre^^f A^rab^l ~1~0 tv'er* r" ^jp^'Vi'A, 6>o (e_r Jr^j0cifb^<i ~~ H's'/^c'/f Vft/es 2? Rsle*s<L r J^-zC.oi2}'V<2C,oo IS 'J*- c<\c-i\ '. ii >r zV hr x ^.OIS Vyr dllor: <? =/ Xnj,^ (S^Si's - Es iL)^ic\Y'ie WatbR /^ele^se. - /V/?~ ^ ^^ s>luL>*'l.,'{y ian-7^^ & \SoUi,ze$) IRRb Release. - IfA ( C\S> ^.o u S . Ar n f5 preset / rl V'VC' 5, o) s<? AppY-. & Soo/hi e^ Ovo SAL 000004424 kELEAse CA-LC.UCATIONS H~ycjr-ooto [or.'c /Loof L.c AiR Refa ,'r-rf I 2<=t 5<S ~RlR) ~ Se^i- O'OcO.J, L^, . />,? x ~LU ~H'< (JlTZzbrprrfi^----- "Sfe-^ez--Pvefeq^e. d s keef) 0.2,1 p-S`A rM ^^ i--*:--Pl5[2Lj!8Pi_^^ Hcf s>L k\-p^.vp /Release /-fC/ *S uS.c( p><-- e'^Q.irve,r'*5\"f>'o*-s , bo/ I e_r~ ^aPj-- IT ter- pes*'^ pjp`-Pe E*ypn+ Sconces p ^vso^e _I /^~y^ V PP Release = (f4/*' ^ 'k) sL) | p,offL^)?T+)J H(,l(e) + {^(.Ooft}Jjp 2-5 iPi_ v 345 >e> x 0.352 Hcf = /</ P //c/ (^/>) EPs^ -- Pr) Oj '(g ee r' rva^ C^/ Ccj / A~/? ot-i Vv/^re<? /Release --O 8 AS<s 8 ele^se pfR 88 o'T EP/uf^8 ^ 6?-^ ) Cs<?<5 Apf?x Gp O') cP? ^ppx CL -- 1^2" /?/oeLop P ^ 0ls/)5 P CRc f-lc^JLooL oi ChQr~:$-ffy > Pps-'t- pO 55 < /I pox' & p ^-.i . > i o^i F^ <* ^Vi/" * ooooo^25 SAL VOC EMISSION CALCULATIONS FIXED ROOF DATE TIME PERIOD : MONTH,YR START : MONTH.YR END LOCATION POINT SOURCE I.D. # MATERIAL STORED TANK CAPACITY (bbls) THEUPUT {bbls/yr) -- - = - -- - 17-May-90 JAN 89 DEC 89 LAKE CHARLES HCL TANK HCL 238 6334 BREATHING LOSS TANK DIAMETER (ft) TANK HEIGHT (ft) VAPOR SPACE HEIGHT (ft) DAILY TEMP CHANGE (F) MOLECULAR WEIGHT VAPOR PRESSURE (psia) PRESSURE (psia) PRODUCT FACTOR PAINT FACTOR SMALL TANK FACTOR BREATHING LOSS (lbs) D= H= h= dT = Mv = Pv Pa = Kc = Fp = C= Lb - 11 15 7.5 20 30 0.31 14.7 1 1 0.56 22 WORKING LOSS MOLECULAR WEIGHT VAPOR PRESSURE # OF TURNOVERS PER YEAR TANK CAPACITY (gal) TURNOVER FACTOR PRODUCT FACTOR WORKING LOSS (lbs) Mv Pv N-- VKn Kc ~ Lv? - 30 0.31 26.613445378 9998 1 1 59 TOTAL LOSS (Ib/yr) Lt - Lb + Lw 81 sal 00oo^6 KlE7*-se Calculations d orv-npoursds i'.c, (\\R Po'xnir feie^se ' O') ysz.le * / ^ ."T^^k T'^roo^^pcy'f" = \o(j'2iJn iL tel x v /.s^^ Jj. ^ Q.-ZM7- *p\ ( l?kL _ /q/ ... s-'x deAt/i'er ~Hv^ ^see A)n 7fmpir - /."?>& <V*j') / E^- ~fc''A A 3^yco( s^a/ oa T^op j kvg release &lu e Yo -fa.v\ lc >/e^Pv<> , %. &?(ese ^ O f? Pi c yee <=< ,.cJ sA?e'f) s^r Nop-pi-- Rele^s-g Fo3 . EjP~i Wee - TEL- Cl^-d WWW) aolcfFVe Sy'S^e^-n "fc Soupc^5 ~ J- puwvp^ lO 3(# -p/A^es FL5, Release ' I(T.ov-?') -*- lo(.ooo5t) + 36 (.ooi%)l l^-j~ * 2`/ ^ X St,r ^ / I li Pb X ^5?-.Cr< - Ho^> 11 Ph r^eEl release') B^s-'s - E ; t-\ *? <?_ t- < CP f CU Ui'o.*"\ W Ate R /PeJe^se = //) tV&Cy iz> LMh Rele^s^- ^ (V/f CN& l-e<Y C-(eA ?\o < d r\ (0 Cd) Aopx CL se^ *rpf> 1*1 %% ShsebooC P^ys.'cAl Prop.? H ;e5 T^Wf ?") (bppxr p -- 5of/^( WPs'/'p i"spcss a f (Plw') cv> SAL 000004427 Release Alcolat/oA/s CLorrypt^^j^As L.c. fhR Po ,'r\ -f- Re le^se , SY3. ~Tc\^k *Thr'Q(Jcjhpu~t' ~ ^"^3 ^Q 55 ~ ^ /t ^ I g*l IUI fll^TT * HtS~/b * e{'L^\ ,, h I (j=>ee <*H^cAedl spr&KcLskeei) /V<jkv -po .'nt Re( g^se ~ E-5 E^p^A Saorce. - EHy I '^T System ft) ft1"7~ /<k a^ctcled^ Ys> ^So/'O^ >s Scppl-e^e^-/" de-el<'<n^ us^e <=>~Y" Jen <jC'i< YYrTYY^ S<ocjrces " c.sY-^'fe VP^ 0.0A7 -1 p^-^p ^ v 7^oZ2u3 = -PJ<K^e_$ <2x ?. 4) O.OOQ^ psv. Rel^se -[l (>o<ji) ^IoRoogsi) + Zb.oo yj ) LE nm~ X 0.2-RR ^ ^ - ZSO R,- r E|n Cp^ra^rt t^e-hal release,) S*v\ =- e^5 'ne<^.'^ *j CJ c.^ [s"Yvq n L4/V0 se = CD / Very /:///e. w/5 Ye 'Y^j-- Yo ^ef Yo S^sYe^^ /?<s(e-v5e ~ AM ^Ms g^sol.Ve ~h\^k cleanouf RO see n-pp>< CL " il^S B>lu<?bo~P /n C7D PPv^.'c^/ Proper-/-,'<? 5 Y>L/e CiH^cbecJ fE) 5ES i\fpy Q> - Esrv^vaM sclor^ (^l1) S^e fippy ~ Soi-1^ C(^lr>Y>') SAL 000004428 I^ELEA-sEL df)L-C_ULf)TtoNS f\i_ P& ,b~f ReleA$ e Loss Cr^k- ano ' 17-10 L.C. Pjo^ -po.'yit ?e/ eese. Fu3:+:U<, S><DurcGJ? ~ P.rapine. - (j9At /taz^R-ef 0.7 ) bl&^d:^- w ~ assume 2 '"pjec'f'ian Sp^P /o dr-yo Ed.(z ~ t'c (~^y) pr^p^^e. i'njcfon pc/d/f^e) l Aoz? lAjeoP.^ 1 L-l-- pu^p foe/ C\c<e/7Vb) 've/s 3 L) 34S'p ICi ~^F y?~ OSo rt) ^2 ~ /^ J' yr s-e^ /s reJ&\se^( -fc <=uV~ ^ peAv^;^e/ se^P "/& 5eu/Cr OoaH An , rl<zOH os) CJ$WC________ui^rn*i /fP 6>Z.P /&Col^cO) * 7.Vg^{ ^ P-p-^ & 7/7 yr D rel&^se = &AO On & ) -" "7<Z VV Jo'/*( /\4sn - pf Re/^_S^ - /,?/^ 7r MeOA sp> r EPic,-'*^ eer-'n^j ^0 pe*" il^ E/S "see /^/?x H (2S) S&CAij: ^,js.'srt "ftc^r -- /f-pp>><r C?)per 6-, Hapk'W5 H>dC5- 2-^0 -- /f ^0 esP-'Wfe by S'fe/e_^S"o^^s P-c, Pefy 4 (s') ~ f\-ppx C. AZ'' oooo* sM- t^/Are^ /?e/ eo5e &=\S^ -- ft L.C. C) C(&0 /o de^C'c^J ed pej- EA/f Srf-RA- 3 f3 gui'cla<ac<2, o|occ^e^i~f" ^ *'oee rs'*^ EZ-3~K-^vic<f^ j-M) <3/n - S.Ve /^/e*se ' Ci^^Jcfkr^) Q CfOo^/o de-j r^eJft'ifrcV) of- <p\t^y f>1&Otf fa Ofi-S'-te. ftefe^e - /VA *.S'0> E^j-'neerE^-A'*'***^ see CO HA? CMe^d^f- (o k^J fre*ch*ye*if C Sv>p<e-<^teA ~HW MeOH <*t very A*/ del ~ /$}Of?^ A o*^s / <n 1A/<^$faz \/o Ici.'ft L z#d'Xatn (S I^tJ? J& ) SAt oooo0<*430 ReL EA5 CfhULUCAT IONS ur^\ I c~i '<3 *cL ^ L.C V .x' RelgAse A//} Abn ~poReie_a,sg ' IQO J6 c^f- loss (Hb5 c*t tW.^N ^ fVo /:z- v*~ ^ ^ ^ /Slowv/aw.y y = /j0^7 /-A C^i fast x <y HdSun\-k x . to /<56?7 /i MD$f (o,Sy x 0,o?6 ^ a^Oije <:o /o ^2 + O.Y3 * <3,/? /700) os^se II <3 lL/yr- Plo 03 0^0 `%r) &a.Si' E*^\ ^ ^ ce " < Es^. Ae V#7B Release - /V/f- ^ $SScJ*-v^_ v\c> m c,vp co ^ ~i'Kc~f~ '^/// iaa^s-/*? ^ oW -fe overlieP*,v^ presence o~ C0^ fl/t'C? o^.Plys^~ rs <cisoluL>l^*%p no ^fffue^xi- reXe^^e) L/WO ApfO'K ~~ 5obc?( W<*s~/c fR&l<^c<$e dc.1 CuU^'a^^ ^ JEs^'^Rpe Py S~fei/e P.C, ^e-fy O') ,C, KZ)$ ca+ r*nPo p>(p(~ l--loycl PiDC. tb) Hf>s 0*"f~ co^pos<-h' ^ cko^'c* '`n f\ppyr p p) Dej~ P' EP4 9*^4 G G^.O^re Property ol^Tc, IW o *v\ Pt-?'^ CAf SAL 00000443X b) frrrR P~h Release oalgulatioa/s Spiro r/c, Ako ~p~t R e-/gp^se Po/y W<cH > top ci ^ L . C, WAl &({ Release ~O B^:5 = pH /vv* *io r`,#"\ a <s> P" e$7t/e*fP ^Ae+wcc.^ & " (J- -- Vv/oiSPiv^per- iO0Ci*\iz}r)r^ report^ X % LMO Or,- S.'-fe. ^?ele^se - ofc-stfe - Nfi~ a ( Wef Spe^nE CaP po/y O'pa/ysp IS r\eu>fn*l>zet{ pr.br -fa /WR//) Bc\s -- E n 2 *' *^<2 C_T~`VaC, Ez */"> rr^c,'f^_ <0 i-,Ct r^cPy opeM^o^ .6. ). hCersey') SAL 000004432 RBLE/4s CLAL.CUJ L-firTtottS Sol-Rjrc'c. A-cJ-A L^C, m Pc? :n~t Pe le*se ^o.y 6) Ho Sior^^_ Pe(e^c <lvp - m% ^ io~h p$\\) "p7 "fed Pr^Uvc-h'** = 7?ySOO '??% Z/^sy ^5a UI (^(J^) ,v - 23,6^2 fc-s Cftp-^iC) c^) J /hcSol PUnf- 3en,;5fe^ = O.Q~2 & refuse x Z,3,>r 2 tZbhs xO.i? ^soy {o*^\ pratAvced -- P(j>H lt> fiso S^s3 eer,'^ C*lc*>lcli>'bt Hon-pQ:^f- Relapse. - ^ E^p*n'f~ AcM ^^ r A( fcy Coo/.'kv^ Toi-v^p^ (^S^CAlX -fUc-fers olonV -pP /i pc\\/y ihor^cn fi jV<^S ^ r' 3,TQ e>( 'Pc/y^] (fc^Po^-f" ff^SOy 1 P r~ wy pU^P ^Ff 2 pl^^'P -- _2 E:. 37 repo^fe&l' ' Pfc ^ c vw' ^ wprep Release - Q fWs = pH moo^-for,'^ oH1 e-ff/oenf (ief^een 6- <W) U/YO ReleAse V4 0) Pprryi CA 0 k-v i C A / -5 / kiee^s bocjl^ Cz) n%3 Blueiy^k - iee A-pfX- c- 7) PP-yz e-y;;., Yacte.- - %>* g i . , /] (<-(') p.'^.c,T,--SeM - rno^' ^or-^c. re3poc-f/rppy C5"~ SAL 000004431 So- 75.7 hU 73.5 kblt'g 77 7 /is SAL 000004-434