Document JvKNm0roXkd8XKq5r6yv9bwnB
A226 1829
LaboratoryReport--Revision 1
Analytical Report of Data for PFOS Dietary LC50 Study with Mallards
(Sera and Liver)
4
Laboratory Report No. FACT-TOX-130 (W1902)
TT
remem
3MEnvironmental Technology & Safety Services 3M Environmental Laboratory
Fluorine 935 B2uh5A0vene, Analytical Chemistry Team (FACT)
`St. Paul, MN 55106
TTT Lawn isPSOHeaBsoa,rssPh!D.
-
`St.Paul,MN 55133-3331
Fy
PFhoAnXe.: ((65615)1)778768-1670618
Revision Date: March 19, 2001
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60762
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1 Introduction
dag
FSi" EER T3h9i.3s)stvudeyswainstdheessiegmnaedtdovqeuarnosfamiavlellaysrdedisckspeexfpoorssedacnPaFuOlStohaotug(hPdFiOtS.,CDEFeIToSfmOdo,siCinAgS#2795.
Connedirtniionosn,achaic]sre ortationdseoddfisepxorct.ySduabnswtoefeegreireegdrovuyphoeftiifaslisweeilsaycr(ifWiciedfeon
Edaovyioannmdedsoyi2lL,ipbost dosael,ySzeerdq2uaoivaeirveolylfxdPfOoSm.Thiesssuresfiornsiocmaelawielrssetked0iehdebeNfCore th
cheddar daewrecollecednd alyzedaoselsaeiced is ep.
WAidtdhifSecwaelx,cecopntsiiodnesrPinOg SolevavlesragetPheEOsSlaevdelsvwerisioctahcehmdauslagsrucp,ebeotdvwiethoddoesgrroeupe.lsof PFOS
3
Ceocntoceiddonru7n(bpgeaeein1d0ocFyFOa0Scdoldneycy2en.Inmosteira(l1,g)fowi spreecsiefr eaem1o.s, oera of PFOS
Noduawascollec foraly anFOS.
PrAotcbaoduigrhsiwgoer lqouwaleitdy,ctohneterolsmeatsuoreosfsids3dMetEanwvairsonmenetcaelsLaarbloyrcaotlolreycSeddearccdordpinegroiaopplicable
GoodLabrsoryPace.Dasprs bere heightqsydesaval tiie.
FIinpehaisseeesstinlg wraespcoonsntactedosfeicodnin E0nseprlminaibolnelGLouo.dSLeaabocrPrahcticees.Thtecepoocrofont.e cif
"UTpheoEnnspveicoimmeennealpLa,be3eMicvdi60ovfecru,st5obdyiw,is46ibdlaoioedd,.an 4ser specimens,rae,cm 0/199.
U"pToonEnsvpiecoiummeennacleLpatb,re3ceicvhedu5n0loifvceu,st0odbywils, 0btlioeodd,.oAdc0opsycoufmascahmfplrems,cra obe,foouand06i2n9a5n9. Aachbmo iesrnepotrt.
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BEre RT SESRE
Thr ioboldingtimessoci with heseapie forLOESMSMSsms.
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Peds
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edsreframe.
UETsSi.6n:g5H.1,PLCaByseocf FronsosssSPecrreoamerysythororOobecsPiircnheeidms Simfa Enxees
ETsSi.8g:H2P0,LCAEiycroofpProysbsiusmSpPeernhocresocinefomia OresPorches inLiverExc.
Sa"mNpiletepre5paeraxtiocn-fEoEsPpLl CaItsEoivSphWioiSgViexiEroacStso:gn (TBA)ia ptccolledeve.Thecons agedselec
nygessosniiniByrogoecnsel.
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EIPcnLoHlCuPEmLnSC.YB,IamSsMelSdcnotooefaclafcytoiffthecnlyndforresdstancg pavseeenpoecoeidnrcehleinvestioogrpicsd `rmlaoulyenhFcsOec,Sdmeyosmchiseue8e0nimeisdnaiolry.sRicsehwneaienmnacncebsesdmbooentwhoeefHanPesL.aCasFodrycPsEatOSwrsi1lipaned,ar doFerocglioiemcaoHfPmoLolmsaerapprcoiwiosonn,,gSufgMorSnMroSicppreoev,isddeHpchiydn,sicedancetpmieeosnrsscfo.haiM liwendl pravirimedaoere irleaygf,oeof enadpnrgreiismncefygioesnaocthbairsaopcnrf yheofsoflnb,wiehdishyktd,s d bciee.nlocnolrleinasccceoredfaolcsllsseicoonndwaiytariycgs iFhsoesmcegaemmcpto,noncogPoeFOrnStc(sCsFsd5ce0h7c)iad8ls0ydasiscsam(0b0ae4s9dipsoelinc0ed50a.) P1cRhO2Sr3r0iost(eGrFicSmoOmf.opnEo.asTchhaoiitfos misgehtdhaveiotnne ghcsi .499a ryio,botdiff chalcomposions1d
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51 Calibration
Fvoas asyizaivvdeeyer1mi1o0siosm,pctoemveorcailmemniaonnenctarveiv.erCisoln (bCCcaa)rsvetveoedencstalat
Sre caepawdeesiacnempairinee.rl pecs swii +.30% fe gecevibe. Indy,ls lCCV
TQpesrpuoonpoteenononeoobre m,ryeaepseeaiysedfucsghbusoedopnsoefianpriehgsre.esQsiEonluseysapsonno(fsvateecmigiohadlraAyn)tmofobdieoedoofocnn,.
men.
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52 Blanks T"spwaeloecsfoBullxy.ewcnerie abscanycke,s,pul tlfion wrwterl clyeeopwp.stdetei,dwsorvxbecikwoif dceacchibooxf
53 S1au1dr2r2oiTgraetreemsb1 yodiproes hnaomerwofa lcwe,di1sncseep,ieSfoingioaeualpito.sSwoaropre epFos
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54 MatrixSpikes
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oxfielicnhscoeaowopccreels,whseecexcgFulltyemdedooefpooesriwtsertcovnoa cytnoshdcopm cevenry. rUopocn,dGa6olry
pilschmmiiioty
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55 Laboratory ControlSamples
Labrsory ColSpies ss cts componentof isy.
56 Sample Related Comments
Sabpatteedvevristhoitssyyo iflobse yredk epaodem vp alioorestunFES.OsrensmInacsevento
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AWidtohfrewae,xcpoonistaPEgObSevveelgietFheOsSrlsedv vweinochaechldocgsrocupbsthwicttwdossrol. oPFOS Se2i2tsdhd eena2d3u o5%cbaey e2onwl esorryvaay lvdoeafysP,R5JO.SSmleesleseesdnocfnPePaO3R.eLveeveelrserodfmPnEOSsbecveicscof oy
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ICnmoostaneimalies,vforngaspte)cifwiacatsimirepaoionst,atnhaeratioofPFOSconcentration insera(ug/ml)toPOS.
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LaboratoryReport
Analytical Report of Data for PFOS Dietary LCS0 Study with Mallards
(Sera and Liver)
:
Laboratory Report No. FACT-TOX-130 (W1902)
Attachment A Sera ToDbaeoyfsResults
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LaboratoryReport
Analytical Report of Data for
PFOS Dietary LC50 Study with Mallards (Sera and Liver)
x
Laboratory Report No. FACT-TOX-130 (W1502)
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