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BIODEGRADATION (OECD 301E)
TEST SUBSTANCE_______________________________________________
Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206CE. (1Octanesulfonic acid) (CAS # 2795-39-3).
Remarks: The 3M production lot number was 502. The test sample is FC206CE. Current information indicates it is a mixture of 0.92% PFOS, 15% diethylene glycol butyl ether, 76.09% water, 4% urea, 1.28% Sultone fbamer, 1.55% sodium octyl sulfate, 1.05% polyoxyethylene monooctylphenyl ether, 0.06% sodium lauryl sulfate, and 0.05% tolytriazole.
The following summary applies to a mixture with incompletely characterized concentrations o f impurities. Data may not accurately reflect the biodegradability o f the fluorochemical component of the test sample.
M E T H O D ________________________________________________________
Method: Modified OECD Screening Test, OECD 301E, with DOC Analysis Test type: Ready Biodegradability GLP: No Year Completed: 1989 Analytical monitoring: Dissolved organic carbon (DOC), pH, D.O., and temperature. Statistical methods: Results were determined by calculation of the % DOC removed as compared to the blank control. Test organism source: Activated sludge mixed liquor collected from the Metro Wastewater Treatment Plant, St. Paul, MN (Preconditioned for 7 days and restored to original volume prior to use as inoculum).
Test condition: Dilution water: Millipore Milli-QTM water Mineral Nutrient Medium: Nutrient medium per OECD 301E method. Initial pH 7.0. Stock and test solution preparation: A stock solution was prepared by adding 10 mL of the test substance to one liter of mineral nutrient medium (equivalent to 1300 mg TOC/L). Initial pH 7.3. In order to obtain a final test concentration of 40 mg DOC/L, 18.46 mL of the stock solution was used per 600 mL test volume. Test vessels: 1000 mL Erlenmeyers containing 600 mL test solution and capped with foam plugs. Incubator Conditions: Gallenkamp Constant temperature orbital shaker incubator (constant dark conditions) Temperature: 22 2 C Agitation: Shaken continuously at 100 rpm
001701
Num ber o f concentrations: 1 plus sodium benzoate standard (reference standard) and blank, all in duplicate. Inoculum condition on te s t initiation: TSS 2227 mg/L (TSS in test flask 1.114 mg/L) and initial pH 5.4. Elem ent Basis: Decrease in dissolved organic carbon compared to the blanks. Test substance flask conditions:
pH: Day 0 -7 .3 (both duplicates), Day 2 8 -5 .5 (both duplicates) D.O.: Day 0-8.1 (both duplicates), Day 28-8.8 (both duplicates)
RESULTS________________________________________________________
Nom inal concentrations: Blank control, sodium benzoate at ~20 mg DOC/L and test substance at ~ 40 mg DOC/L.
Elem ent values: 28 Day Degradation - 90% duplicate 1 and 91% duplicate 2. Mean value 91%.
Rem arks: Testing was conducted on a mixture as described in the Test Substance Remarks field. The values reported apply to that mixture and not the fluorochemical proportion alone.
CONCLUSIONS____________________________________________ _ _ _
The FC-206CE % biodegradation based on mean DOC removal was 91% after 28 days.
The reference substance obtained 98% degradation, therefore the inoculum used was viable. .
Subm itter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133
DATA QUALITY___________________________________________________
Reliability: Klimisch ranking 2. Testing meets all criteria for quality testing. However, sample purity was not properly characterized and the study lacks analytical confirmation of the amount of fluorochemical proportion in the solution.
REFERENCES____________________________________________________
The study was conducted by the 3M Environmental Laboratory, St. Paul, MN7 Lab Request number G1358-2,1989.
OTHER________________________ _________________________________
Last changed: 6/26/00
001702
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READY BIODEGRADABILITY
LR S-KVVDate
Analyst
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Test Substance__E C - & Q f o Q t __ ........................................ ....
Test Concentration * j Q
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Inoculum Source M e ra UteSA* TreoL+yvigm- V U n \ AilXeJL
C ^ Pa o Ij M A J
Concentration of suspended solids in inoculum
fresh (in mineral medium)_______________
pre-conditioned (restored to original volute) 5L.
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Carbon Determinations
Carbon Analyzer Dohrmann Xertex
Inoculun Used: Fresh/Pre-oonditioned
.Medium Flask Analyses
Time
(mg/L)
Blank Mean
11
*2 A, mean
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ENVIRONMENTAL LABORATORY
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MODIFIED OECD SCREENING TEST 301E
BEADY BIODEGRADABILITY
LR & lif*}O
Date
Analyst _J e
Test Substance S o c \ v 0 rK &g HZrxa-te. ReeCex\Oz.
Test Concentration
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fresh (in mineral median) _______________ pre-oonditianed (restored to original volune) JL ,2 ,7 ,1
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Carbon Determinations
Carbon Analyzer = DohnnannR Xertex
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Medium
Flask Analyses
Time of incubation (days)-
(mg/L)
0 1 , 3 , 7 14. ZL... 27
28
Blank Mean
1 A,
'a
A, mean
2 B1 *2
B, mean
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D, mean
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50,50
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Evaluation of raw data
Flask
No.
f1 D, 1
(C,mean - bk) ~\
(co,mean - flJJ
x
loof
Percent Degradation after t days
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001712
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1798 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 05/23/1989 DESC: FC-203 CE AND FC-206 CE BIODEG.
DAY 0
CONTRACT LAB(S): EXP COMP DATE: 05/31/1989 DATE COMPLETED: 06/02/1989 PROJECT LEAD: JM STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Please run in duplicate.
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 05/23/89 FC-203 I
...........
DOC DISSOLVED ORGANIC CARBON
2 05/23/89 FC-203 II
...........
DOC DISSOLVED ORGANIC CARBON
3 05/23/89 FC-206 I
...........
DOC DISSOLVED ORGANIC CARBON
4 05/23/89 FC-206 II
...........
DOC DISSOLVED ORGANIC CARBON
40 MG/L 41 MG/L 37 MG/L 36 MG/L
001713
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1797 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 05/23/1989 DESC: LANDFILL STAB FOAM BIODEG.
DAY O
CONTRACT LAB(S): EXP COMP DATE: 05/31/1989 DATE COMPLETED: 06/02/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Please run all samples in duplicate.
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C. I.)
1 05/23/89 MQ
MQ BLANK
DOC DISSOLVED ORGANIC CARBON
2 05/23/89 MEDIUM
NUTRIENT
DOC DISSOLVED ORGANIC CARBON
3 05/23/89 1ST RINSE
FOAM SOLIDS
DOC DISSOLVED ORGANIC CARBON
4 05/23/89 2ND RINSE
FOAM SOLIDS
DOC DISSOLVED ORGANIC CARBON
5 05/23/89 3RD RINSE
FOAM SOLIDS
DOC DISSOLVED ORGANIC CARBON
6 05/23/89 4TH RINSE FOAM SOLIDS
DOC DISSOLVED ORGANIC CARBON
7 05/23/89 BLANK 1
CONTROL
DOC DISSOLVED ORGANIC CARBON
8 05/23/89 BLANK II
CONTROL
DOC DISSOLVED ORGANIC CARBON
9 05/23/89 LEACHATE I ..........
DOC DISSOLVED ORGANIC CARBON
10 05/23/89 LEACHATE II ..........
DOC DISSOLVED ORGANIC CARBON
11 05/23/89 PRE W-SOLIDS ..........
DOC DISSOLVED ORGANIC CARBON
<0.5 MG/L 0.8 MG/L 2000 MG/L 540 MG/L 150 MG/L 52 MG/L <0.5 MG/L <0.5 MG/L 42 MG/L 41 MG/L 1.3 MG/L
001714
06/23/2000
ENVIRONMENTAL LABUH/m u h t ARCHIVED FINAL REPORT
LAB REQUEST NO. G1802 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 05/24/1989 DESC: FC-203CE AND FC-206CE BIODEG.
DAY 1
CONTRACT LAB(S): EXP COMP DATE: 06/02/1989 DATE COMPLETED: 06/02/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Test shares controls & ref. substance with LR G1800, See LR G1801 for day 1 analysis.
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2 DOC
3 DOC
4 DOC
FC-203 I
...........
DISSOLVED ORGANIC CARBON 42 MG/L
FC-203 II
...........
DISSOLVED ORGANIC CARBON 44 MG/L
FC-206 I
...........
DISSOLVED ORGANIC CARBON 35 MG/L
FC-206 II
...........
DISSOLVED ORGANIC CARBON 36 MG/L
*s
001/
06/23/2000
ENVIRONMENIAL LABUHAiu n ARCHIVED FINAL REPORT
LAB REQUEST NO. G1801 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 05/24/1989 DESC: LANDFILL STAB FOAM BIODEG.
DAY 1
CONTRACT LAB(S): EXP COMP DATE: 06/02/1989 DATE COMPLETED: 06/02/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Please run all samples in duplicate.
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2
DOC 3
DOC 4
DOC 5
DOC 6
DOC 7
DOC 8
DOC 9
DOC 10
DOC
BLANK I
CONTROL
DISSOLVED ORGANIC CARBON 1.9 MG/L
BLANK II
CONTROL
DISSOLVED ORGANIC CARBON <0.5 MG/L
LEACHATE I ...........
DISSOLVED ORGANIC CARBON 40 MG/L
LEACHATE II ...........
DISSOLVED ORGANIC CARBON 39 MG/L
SOLIDS I
WASHED
DISSOLVED ORGANIC CARBON 0.7 MG/L
SOLIDS II WASHED
DISSOLVED ORGANIC CARBON 1.2 MG/L
LEACH &
SOLIDS I
DISSOLVED ORGANIC CARBON 42 MG/L
LEACH &
SOLIDS II
DISSOLVED ORGANIC CARBON 41 MG/L
REF SUB I SODIUM BENZ.
DISSOLVED ORGANIC CARBON 20 MG/L
REF SUB II SODIUM BENZ.
DISSOLVED ORGANIC CARBON 21 MG/L
001716
06/23/2000
tN V lh U N n tN I ML L /W u rv M u n i
ARCHIVED FINAL REPORT
LAB REQUEST NO. G1820 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 05/26/1989 DESC: FC-203CE AND FC-206CE BIODEG.
DAY 3
CONTRACT LAB(S): EXP COMP DATE: 06/05/1989 DATE COMPLETED: 06/02/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Test shares controls & ref. sub with LR G1800; See LR G1819 for day 3 analyses
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2
DOC 3
DOC 4
DOC
FC 203 I
...........
DISSOLVED ORGANIC CARBON 41 MG/L
FC 203 II
...........
DISSOLVED ORGANIC CARBON 40 MG/L
FC 206 I
...........
DISSOLVED ORGANIC CARBON 32 MG/L
FC 206 II
...........
DISSOLVED ORGANIC CARBON 33 MG/L
001717
06/23/2000
ENVIRUNMbNIAL LABUHMium ARCHIVED FINAL REPORT
LAB REQUEST NO. G1819 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 05/26/1989 DESC: LANDFILL STAB. FOAM BIODEG.
DAY 3
CONTRACT LAB(S): EXP COMP DATE: 06/05/1989 DATE COMPLETED: 06/02/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Please analyze in duplicate.
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2 DOC
3 DOC
4 DOC
5 DOC
6 DOC
7 DOC
8 DOC
9 DOC
10 DOC
BLANK I
CONTROL
DISSOLVED ORGANIC CARBON <0.5 MG/L
BLANK II
CONTROL
DISSOLVED ORGANIC CARBON <0.5 MG/L
LEACH I
LEACHATE
DISSOLVED ORGANIC CARBON 31 MG/L
LEACH II
LEACHATE
DISSOLVED ORGANIC CARBON 33 MG/L
SOLIDS I
PRE-WASHED
DISSOLVED ORGANIC CARBON <0.5 MG/L
SOLIDS II PRE-WASHED
DISSOLVED ORGANIC CARBON <0.5 MG/L
LEACH &
SOLIDS I
DISSOLVED ORGANIC CARBON 30 MG/L
LEACH &
SOLIDS II
DISSOLVED ORGANIC CARBON 33 MG/L
REF SUB I SODIUM BENZ.
DISSOLVED ORGANIC CARBON <0.5 MG/L
REF SUB II SODIUM BENZ.
DISSOLVED ORGANIC CARBON
<0.5 MG/L
001718
06/23/2000
LAB REQUEST NO. G1797
SAMPLE DATE
CODE
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
CONTINUED
DESCRIPTION RESULT
12 05/23/89 PRE-W
SOLIDS II
DOC DISSOLVED ORGANIC CARBON 1.1 MG/L
13 05/23/89 LEACH &
SOLIDS I
DOC DISSOLVED ORGANIC CARBON 43 MG/L
14 05/23/89 LEACH &
SOLIDS II
DOC DISSOLVED ORGANIC CARBON 43 MG/L
15 05/23/89 LEACHATE
AS-IS
DOC DISSOLVED ORGANIC CARBON 2000 MG/L
16 05/23/89 REF SUB I
SODIUM BENZ.
DOC DISSOLVED ORGANIC CARBON 21 MG/L
17 05/23/89 REF SUB II SODIUM BENZ.
DOC DISSOLVED ORGANIC CARBON 20 MG/L
c MDL or (95% C.I.)
001719
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1834 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 05/30/1989 DESC: FC-203CE AND FC-206CE BIODEG.
DAY 7
CONTRACT LAB(S): EXP COMP DATE: 06/09/1989 DATE COMPLETED: 06/02/1989 PROJECT LEAD: JU STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Test shares controls & ref sub. with LR G1800; see LR G1833 for day 7 analyses
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2 DOC
3 DOC
4 DOC
FC 203 I
...........
DISSOLVED ORGANIC CARBON 33 MG/L
FC 203 II
...........
DISSOLVED ORGANIC CARBON 35 MG/L
FC 206 I
...........
DISSOLVED ORGANIC CARBON 30 MG/L
FC 206 II
...........
DISSOLVED ORGANIC CARBON 30 MG/L
001720
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1833 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 05/30/1989 DESC: LANDFILL STAB. FOAM BIODEG.
DAY 7
CONTRACT LAB(S): EXP COMP DATE: 06/09/1989 DATE COMPLETED: 06/02/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Please run in duplicate.
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2 DOC
3 DOC
4 DOC
5 DOC
6 DOC
7 DOC
8 DOC
9 DOC
10 DOC
BLANK I
CONTROL
DISSOLVED ORGANIC CARBON <0.5 MG/L
BLANK II
...........
DISSOLVED ORGANIC CARBON <0.5 MG/L
LEACH I
...........
DISSOLVED ORGANIC CARBON 29 MG/L
LEACH II
...........
DISSOLVED ORGANIC CARBON 29 MG/L
SOLIDS I
...........
DISSOLVED ORGANIC CARBON <0.5 MG/L
SOLIDS II
...........
DISSOLVED ORGANIC CARBON <0.5 MG/L
LEACH +
SOLID I
DISSOLVED ORGANIC CARBON 32 MG/L
LEACH +
SOLID II
DISSOLVED ORGANIC CARBON 27 MG/L
REF I
SODIUM BENZ.
DISSOLVED ORGANIC CARBON 0.5 MG/L
REF II
SODIUM BENZ.
DISSOLVED ORGANIC CARBON
0.6 MG/L
001721
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1874 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0222 PROJECT NO: 9970013000 DATE RECEIVED: 06/06/1989 DESC: FC-203CE & FC-206CE BIODEG DAY 14
CONTRACT LAB(S): EXP COMP DATE: 06/16/1989 DATE COMPLETED: 06/12/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Test shares controls and ref. substance with LR G1800; See LR G1873 for day 14 analyses.
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2
DOC 3
DOC 4
DOC
FC 203 I
...........
DISSOLVED ORGANIC CARBON 5.0 MG/L
FC 203 II
...........
DISSOLVED ORGANIC CARBON 4.3 MG/L
FC 206 I
...........
DISSOLVED ORGANIC CARBON 4.2 MG/L
FC 206 II
...........
DISSOLVED ORGANIC CARBON 2.9 MG/L
001722
6/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1873 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0222 PROJECT NO: 9970013000 DATE RECEIVED: 06/06/1989 DESC: LANDFILL STAB. FOAM BIODEG.
DAY 14
CONTRACT LAB(S): EXP COMP DATE: 06/16/1989 DATE COMPLETED: 06/12/1989 PROJECT LEAD: JM STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2
DOC 3
DOC 4
DOC 5
DOC 6
DOC 7
DOC 8
DOC 9
DOC 10
DOC
BALNK I
CONTROL
DISSOLVED ORGANIC CARBON <0.5 MG/L
BLANK II
CONTROL
DISSOLVED ORGANIC CARBON <0.5 MG/L
LEACH I
..........
DISSOLVED ORGANIC CARBON 1.9 MG/L
LEACH II
..........
DISSOLVED ORGANIC CARBON 3.2 MG/L
SOLIDS I
..........
DISSOLVED ORGANIC CARBON <0.5 MG/L
SOLIDS II
..........
DISSOLVED ORGANIC CARBON <0.5 MG/L
LEACH +
SOLIDS I
DISSOLVED ORGANIC CARBON 3.8 MG/L
LEACH +
SOLIDS II
DISSOLVED ORGANIC CARBON 3.1 MG/L
REF SUB I
SODIUM BENZ
DISSOLVED ORGANIC CARBON 0.8 MG/L
REF SUB II SODIUM BENZ
DISSOLVED ORGANIC CARBON <0.5 MG/L
001723
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1907 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 06/13/1989 DESC: FC-203CE AND FC-206CE BIODEG.
DAY 21
CONTRACT LAB(S): EXP COMP DATE: 06/20/1989 DATE COMPLETED: 06/16/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Test shares controls & ref. substance with LR G1800, see LR G1906 for day 21 analyses.
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2 DOC
3 DOC
4 DOC
FC 203 I
...........
DISSOLVED ORGANIC CARBON 4.7 MG/L
FC 203 II
...........
DISSOLVED ORGANIC CARBON 4.7 MG/L
FC 206 I
...........
DISSOLVED ORGANIC CARBON 3.1 MG/L
FC 206 II
...........
DISSOLVED ORGANIC CARBON 2.0 MG/L
001724
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1906 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 06/13/1989 DESC: LANDFILL STAB FOAM BIODEG.
DAY 21
CONTRACT LAB(S): EXP COMP DATE: 06/20/1989 DATE COMPLETED: 06/16/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2
DOC 3
DOC 4
DOC 5
DOC 6
DOC 7
DOC 8
DOC 9
DOC 10
DOC
BLANK I
CONTROL
DISSOLVED ORGANIC CARBON <0.5 MG/L
BLANK II
CONTROL
DISSOLVED ORGANIC CARBON <0.5 MG/L
LEACH I
LEACHATE
DISSOLVED ORGANIC CARBON 2.3 MG/L
LEACH II
LEACHATE
DISSOLVED ORGANIC CARBON 3.1 MG/L
SOLIDS I
...........
DISSOLVED ORGANIC CARBON <0.5 MG/L
SOLIDS II
...........
DISSOLVED ORGANIC CARBON <0.5 MG/L
LEACH +
SOLIDS I
DISSOLVED ORGANIC CARBON 2.4 MG/L
LEACH +
SOLIDS II
DISSOLVED ORGANIC CARBON 1.5 MG/L
REF SUB I SODIUM BENZ.
DISSOLVED ORGANIC CARBON <0.5 MG/L
REF SUB II SODIUM BENZ.
DISSOLVED ORGANIC CARBON <0.5 MG/L
001725
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1936 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 06/19/1989 DESC: FC-203CE & FC-206CE
BIODEG.
DAY 27
CONTRACT LAB(S): EXP COMP DATE: 06/26/1989 DATE COMPLETED: 06/23/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
Test shares controls & ref. substance with LR G1800, see LR G1935 for day 27 analyses.
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2 DOC
3 DOC
4 DOC
FC-203 I
...........
DISSOLVED ORGANIC CARBON 3.0 MG/L
FC-203 II
...........
DISSOLVED ORGANIC CARBON 4.2 MG/L
FC-206 I
...........
DISSOLVED ORGANIC CARBON 3.1 MG/L
FC-206 II
...........
DISSOLVED ORGANIC CARBON 2.9 MG/L
001726
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1935 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 06/19/1989 DESC: LANDFILL STAB. FOAM BIODEG.
DAY 27
CONTRACT LAB(S): EXP COMP DATE: 06/26/1989 DATE COMPLETED: 06/23/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2 DOC
3 DOC
4 DOC
5 DOC
6 DOC
7 DOC
8 DOC
9 DOC
10 DOC
BLANK I
CONTROL
DISSOLVED ORGANIC CARBON
BLANK II
CONTROL
DISSOLVED ORGANIC CARBON
LEACH I
LEACHATE
DISSOLVED ORGANIC CARBON
LEACH II
LEACHATE
DISSOLVED ORGANIC CARBON
SOLIDS I
..........
DISSOLVED ORGANIC CARBON
SOLIDS II
..........
DISSOLVED ORGANIC CARBON
LEACH +
SOLIDS I
DISSOLVED ORGANIC CARBON
LEACH +
SOLIDS
DISSOLVED ORGANIC CARBON
REF SUB I SODIUM BENZ
DISSOLVED ORGANIC CARBON
REF SUB II SODIUM BENZ
DISSOLVED ORGANIC CARBON
<0.5 MG/L <0.5 MG/L 1.8 MG/L 2.0 MG/L <0.5 MG/L <0.5 MG/L 2.8 MG/L 1.9 MG/L <0.5 MG/L <0.5 MG/L
001727
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1941 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 06/20/1989 DESC: FC-203CE & FC206CE BIODEG DAY 28
CONTRACT LAB(S): EXP COMP DATE: 06/27/1989 DATE COMPLETED: 06/23/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
TEST SHARES CONTROLS + REF SUBSTANCE W/ LRG1800, SEE LRG1940 FOR DAY 28 ANALYSES.
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C.I.)
1 DOC
2 DOC
3 DOC
4 DOC
FC 203 I
...........
DISSOLVED ORGANIC CARBON 3.0 MG/L
FC 203 II
...........
DISSOLVED ORGANIC CARBON 4.8 MG/L
FC 206 I
...........
DISSOLVED ORGANIC CARBON 3.7 MG/L
FC 206 II
...........
DISSOLVED ORGANIC CARBON 3.3 MG/L
001728
06/23/2000
ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT
1
LAB REQUEST NO. G1940 REQUESTOR NAME: MTE/EAR DEPARTMENT: 0535 PROJECT NO: 9970013000 DATE RECEIVED: 06/20/1989 DESC: LANDFILL STAB FOAM BIODEG DAY 28
CONTRACT LAB(S): EXP COMP DATE: 06/27/1989 DATE COMPLETED: 06/23/1989 PROJECT LEAD: JW STOCK PHONE NO: 651-778-6438 3M FAX NO: 651-778-6176
SAMPLE DATE
CODE
DESCRIPTION RESULT
MDL or (95% C. I.)
1 DOC
2 DOC
3 DOC
4 DOC
5 DOC
6 DOC
7 DOC
8 DOC
9 DOC
10 DOC
BLANK I
CONTROL
DISSOLVED ORGANIC CARBON
BLANK II
CONTROL
DISSOLVED ORGANIC CARBON
LEACH I
LEACHATE
DISSOLVED ORGANIC CARBON
LEACH II
LEACHATE
DISSOLVED ORGANIC CARBON
SOLIDS I
PRE-WASHED
DISSOLVED ORGANIC CARBON
SOLIDS II
PRE-WASHED
DISSOLVED ORGANIC CARBON
LEA.+SOLID I ..........
DISSOLVED ORGANIC CARBON
LEA+SOLID II ..........
DISSOLVED ORGANIC CARBON
REF SUB I Na BENZOATE
DISSOLVED ORGANIC CARBON
REF SUB II Na BENZOATE
DISSOLVED ORGANIC CARBON
<0.5 MG/L <0.5 MG/L 4.1 MG/L 4.4 MG/L <0.5 MG/L <0.5 MG/L 3.7 MG/L 3.9 MG/L <0.5 MG/L <0.5 MG/L
v *
oor
