Document JNME1gvp6m3pgYpGngx3Y9qEX
AR226-2471
DtiPoftJ VifeshiirionWorks P.0. 3dx 121? Perksrsouig. Wy 2802-217
February 17, 2000
Mr. James C. Cox Lubeck Public Service District P.O.BOX 7 0 0 W ashington, W V 26181
. .
RE: LPSD W ater Sam ple Analytical Results
D ear Mr, Cox:
Attached is a copy of the analytical results on w ater samples taken on January 1 9 ,2 0 0 0 from three LPSD wells.
If you have any questions or need additional information, please contact me at 304-863-4271.
Sincerely,
R. L. Ritchey Sr. Environmental Control Consultant W ashington W orks
R L R /g w :d sw A ttachm ents cc: W illiam J. Gibbs
Lubeck Public Service District P.O . Box 700 W ashington, W V 26181
RP001067
L L su Por 38 Nemoursand tmftfty
Printed on terytteri
EID083368
02/17 '00 09**12
ID DUPONT BTP 27
FfiX:
POSE 3
LancasterLaboratories Where quality is a science.
I jL I Sample No. WW 3310240
C o lle c te d : 01/19/00 a t 08:20 by RLB
S ubm itted: 01/20/00 Reported; 02/07/00 D isca rd : 03/09/00 WWK-LPWD-WELL-A Water Sample
Account do: u/u32
........
CRG-E.I.DuPont de Nemours & Co B a rle y m il P laza. B ldg. 27
Routes 141 & 48 W ilm ington 01 19B05
P .0 . LBIQ-63894
Ri. U362
LTAR.T LANDFILL IQOO
CAT NO. ANALYSIS NAME
AS RECEIVED METHOD
RESULTS DETECTION LIM IT UNITS
2324
FC-143
0-80
0 .1 4
uugg//11
The MS/MSD recovery is o u ts id e the QC lim its due to the d ilu tio n reqluu ire d
fo r a n a ly s is . The ICS reco ve ry 1s w ith in th e QC lim its .
The PFDOA and 11H-PFUA surro g a te re co ve rie s are o u tsid e th e QC lim its . The sta te d QC lim its are a d viso ry o n ly u n til s u ffic ie n t data p o in ts can be o btained to c a lc u la te s ta tis tic a l lim its .
QUALITY CONTROL REPORT
SAMPLE HDL
SAMPLE UNITS
BLANK
DUP RPD
MS MSD
MS LC$ LOS
RPD ixs DUP RPD
2324 FC*143 0 .1 4
ug/1
B atch: 000240017A 0.093 J ug/1
(6 ) (6) (2)
48
(2 )
The background resu T t was more th a n fo u r tin e s the Spike added. Matrix Interferences within the sample has caused th e Recovery Percent
of
the
.. MS and/or
uMtSrD. to
. exceed
ln HKQQQ*.
LOS LIMITS LOW HIGH
55
SURROGATE SUf
SURROGATE LIMITS
2324 FC-143
on.TM- w .
TRIAL ID
e.s .si,m .re . 3 .
SURROGATE PFNA
11H-PFUA
PFDDA
RECOVERY X 21 a 9
a. .* -5*.*-" -*.***-1
LOW 1
13 50
HIGH
SO B8 ISO
CAT NO ANALISIS NAME
2324 FC-143
2325 P e s tic id e A lte rn a te W ater E x tr
LABORATORY CHRONICLE
METHOD FC-43 by GC/ECD /91 FC-143 10/91
TRIAL 1 1
.U U V F ,e ANALYSIS ID DATE AND TIME
02/01/00 2220 01/27/00 0930
ANALYST
M ich e lle J . K o lo d a ie jski Deborah M, Zimmerman
8 9 0 1 0 0 < f
RECEIVED
1 COPY TO Wootfward Clyde Diamonds
ATTN: Ms. Sara Seastrom
Questions? C ontact your C lie n t S ervices R epre se n ta tive
Nancy Bornholm
a t (717) 656-2300
19:47:15 0 0001 3
135B03 699917
047 0,00 00022500 ASROOO
FEB O 9 2000
.tO ,
cep load Pata_A( (CfO ttm* ;M-
AccuracyCheckby__La^X__ Dale ^ U l& O
Holding Time Cheek
, ate^lL'U/O
M B .M .B g R
M Z IL
R e s p e c tfu lly Subm itted
u.ustQFL.bDr.tori.(
Robert Strocko, J r . , B.S.
J4i5New Holland Pike
Group Leader, M etals A n a lysis
CO BOX 124}$ Lancaster. PA t?60S-2475
Uncaster w #pf3torle B a sutnirHery o f Thermo TenaTech Inc., a Therm* Election Company,
717-656-23O0 Fax; 717-656.1681 tee rtvCrSi ;>ae for explanation Of ymhols rid abbreviations.
2116 Rev, 3/13,5
EXD083369
ries
t , h X S a m p le N o , W H 3 3 1 0 2 4 1 C o lle c te d : 01/19/00 a t DB:10 b y RU
S ubm itted: 01.70/00 Reported: 02/07/00 D isca rd : 03/09/00 WWK-LPVTO-MELL-6 Water Sample
tftG -E . I.D uPont de Nemsurs & Co B a rle y M ill P laza. B ldg. 27 Routes 141 a 48 U41nrllifttftrt flP 199G5
p .i). LBIQ-63894 R e l. LE862
LETART LANDFILL* 1000
r ,T NO. ANALYSIS IIAME
AS RECEIVED
,,
METHOD
RESULTS DETECTION LIMIT UNITS
2324
0.440
0.029
ug/1
Thel M5/MSD recovery is o u ts id e th e QC U n its d u e 'to th e d i l u t e required
fo r a n a ly s is . The LCS reco ve ry 1s w ith in th e QC lim its .
The PFDDA and 11H-PFUA su rro g a te re co ve rie s a re o u tsid e th e jlO lim its . The s ta te d QC lim its are a d viso ry o n ly u n til s u ffic ie n t data p o in ts can be obtained to c a lc u la te s ta tis tic a l lim its .
QUALITY CONTROL REPORT
SAMPLE MDL
SAMPLE W ITS
..... BLANK
RPD MS USD
2324 FC0-1.04235 ug/1
8 a t0h.0A93jP ^J40u0g/n1A
16) (6) <2)
(2> The background re s u lt was feore th a n fo u r tin>es th e spiko added,
, . Mt;
<8> M a trix in te rfe re n c e s w ith in th e sample Has caused th e R e o w y Percent o f the
9>ca.3.4j
m
RPD
48 Mi.h
LCS LCS LCS LIMITS LCS OUP RPD LOW HIGH
9 10 nno*
ss
SURROGATE S04WRT
SURROGATE LIMITS
2324 FC-143
TRIAL ID SURROGATE
RECOVERY i
PENA
10
11H-PWA
f
PFDDA
3
LOW
1 13 50
HIGH
1S0
,, ,, ,,,,
,,.,,. .^ .= .1 .--
.................laboratory cw onicle
,,T 5 J' v ~ft; uamc K L , R-Wl I i 1S NWE
MFTHOIJ FC-M3 by GC/ECD
. |1 &
A lte rn a te W ater E x tr fI I M / I T
10/91
TRIAL 1
1
ANALYSIS
,,.
ID DATE AND TIME
02/01/00 2248
mmm
,,, ANALYST M ic h e lle J . K o lo d z ie js k i
-
1 COPY TO Woodward Clyde Diamonds
ATTN: Ms. Sara Seastrora
KP001069
Q uestions? C ontact yo u r C lie n t S ervices R epresentative
Nancy Bornholm
a t (717) 656-2300
19:47:31 0 0001 3
135803 699917
047 0.00 00022500 ASR00O
m em e n
R e s p e c tfu lly Subm itted
isncsstt* Laboratories 3425 Now HoiMnd Pike
Robert S trocko, J r , , B .s . Erpup Leader. M eta ls A n a lysis
PO S o * 12425
lpcn<?ter, PA i?605-2425 717*056*2309 fax: 7l?*65o`26$1
LsnOiltF U b ^ u r n s k ,
jry of T h ifiM "terraTefh bK , A ThfefffiO SertfOO Cofppjby,
revene idc for xpianabort J lymboH rod abbe*/*4tiom#
221$
ftov. 3/22/
EID083370
*I roster Laboratories Where quality is a science.
L L I Sample No. WW 3310242
C o lle cte d : 01/19/00 a t 08:00 b y RIB
Subm itted: 01/20/00 R eported: 02/07/00 D iscard: 03/09/00
WWK-LPWD-WEU.-F W ater Sample
Account No: 0 /032 " " "
"
CRG-E.l.DuPont cte Nemours & Co
B a rle y M ill P laza. B ld g . 27 Routes 141 & 48 W ilm ington BE 19805
P.D. 1810*63894 R e l. 11862
LETART LANDFILL 1Q0O
CAT NO.
ANALYSIS NAME
AS RECEIVED
RESULTS
method
detection limit units
2324 PC.143
0.313
0.029
ug/1
The M5/f$D recovery U o u ts id e th e QC lim its due to th e d ilu tio n re q u ire d
fo r a n a ly s is , th e IC$ recovery 1-s w ith in th a QC lim its *
th e PfDOA and 11H-PFUA su rro g a te re c o v e rie s a re o u ts id e th e q C llm lts . The sta te d qc lim its a re a d v is o ry .o n ly u n til s u ffic ie n t data p o in ts can be obtained to c a lc u la te s ta tis tic a l lim its .
QUALITY CONTROL report
SAMPLE MDL 2324 FC-143 0.029
8!
SAMPLE UNTO
ug/1
BLANK
B atch: 000240D17A 0.093 3 ug/1
WP RPD MS MS0
MS RPD
t6> C6) (2)
48
< . 5 * * * _ ?
LCS LCS LCS LIMITS
LC5 OUP RPD LOW HIGH
3 55
M .W ..
2324 FC-143
CAT NO ANALYSIS NAME 2324 PC-143 2325 P e s tic id e A lte rn a te W ater E x tr
SURROGATE SUMMARY
TRIAL ID
SURROGATE PFNA UH-PFUA
PFDDA
RECOVERY 7 4
3
SURROGATE LIMITS
LOW1
HIGH 50
13 08
50 150
SE.E3a3$fr6!*&t:
LABORATORY CHRONICLE
METHOD FC-143 by GC/ECD 10/91 FC-143 10/91
TRIAL
1 1
ANALYSIS ID DATE AND TIME
02/ 01/ 00' 2315 01/27/00 0930
ANALYST
,.
M ic h e lle J . K o lo d zie jsM
Deborah M. Zimmerman
i COPY TO Woodward Clyde Diamonds
ATTN: Ms. Sara Seastrom
RP001070
Q uestions? C ontact your C lie n t S ervices R epresentative
Nancy Bornholm
a t C717) 656-2300
19:47:45 D 0001 3 .
135803 699917
047 0.00 00022500 A5RO00
member
R e s p e c tfu lly Subm itted
U ntaster laboratories 542$ n?w Holland >k
R obert S trocKo. J r . . 8.S . Group Leader, M etals A n a ly s is
P O Boa tt425
Isnedtter, PA t?$0$'i425 7l7 5?-i3Dq U r. 7' 7-S56` 26Bl
Unc.rjtor u ^tn ^to n e . n a vubiriiurry of T fjw rw TefnaTcth fp f, *Thermo Etedfoa Cornpany. ?M reverse side for explanation of symWds and abbreviations.
H l$
Rev. 3/J3/:
!
EID083371
