Document JN09g5j3zpzGXN2ZN9aMxwnDZ
GENERATOR'S WASTE MATERIAL PROFILE SHEET
PUMtt HWir M MK OHTVF (MBs. 12-***).
SUBMITTED TO WASTE TECH SERVICES
DATE:
April, 1990
WTS JCL
A. GENERAL INFORMATION 1. Generator Name: _PPGIndustri.es, Inc.2. Generator USEPA ID: ^ 008086506
,,
3. Facility Address: J - : Box IQd0
4. Generator State ID:
___________________
Lake Charles. LA
(Columbia Southern Road) 5 jp
70602
6. Technical r^ntarr William H._Cocoer
7 ntu- Assoc.Research Chamst a. Phrmm-(^
B. MAIL WASTE TECH SERVICES
INVOICES TO 1. ED Generating Facility (A, above), or
2. Company Name: _________________________________________3. Phone: (
)
4. Address:_________________ ____________________________________________________________ ,,_____
-------- ------------ -------- --------------------------------------------------------------------------------- 5. Zip Code:
C. 1. NAME OF WASTE WIU Surge Pfcnd Sludge
.. .......................................................
2. PROCESS GENERATING WAS*11* Production of Chlorinated Hydrocarbons
3. Is this waste a Dioxin listed waste as defined in 40 CFR 261.31 (e.g., F020, F021, F022, F023. F026, F027. or F028)? Yes No Ifyes. DO NOT COMPLETE thisform.
D. PHYSICAL CHARACTERISTICS OF WASTE
1. Color.
2. Does the waste have a 3. Physical Stale @70*F:
Black
strong incidental odor?
Solid El Semi-Solid
No 3 Yes If known. Liquid G Powder
desenha: ....
Other
4. Layers:
Multilayered
G Bi-iayered
Single Phased
5. Specific Gravity:
""15. 1.4
6. Free Liquids:
Q Yes G No
Volume:
<10
7. pH: G<2 > 2-4 4-7 7 7-10 10- <12.5 12.5 G Range
N
3. Liquid Flash Point < 73*F Q 73-99*F 100-139*F 140-199*F > 200*F None C3 Closed Cup DOpenCu
E. CHEMICAL COMPOSmON
RANGE
F. METALS Indicate if this waste-contains any <
1. Chlorinated Hydrocarbons
'vater Ash
10 ' 15 -
3D' '25"
% % % %
the following:
i. Geptox/tclp or 2. Q Total
METAL
LESS THAN or ACTUAL
Arsenic
(Parts Per Million) < 5 < 500 0.8B
% Barium
< 100
-24.51
% Cadmium
< 1 < 100 -<QJL
% Chromium % Lead
< 5
-5125
< 5 < 500 --4^7
% Mercury
< 0.2 < 20
u.c
% Selenium
< 1 < 100
<n.n
% Silver
< 5
% Chromium-Hex < 5 < 500
<i.e UNK
Please note: The chemical composition total in the maximum
Copper
< 5
__
column must be greater than or equal to 100%.
TOTAL ICO** % Nickel
< 5 < 134
24.7
2. indicate if this waste contains any of the following:
Thallium
< 5 < 130
UNK
PCB's Cyanides
NONE or LES& THAN or ACTUAL G -.Q < 50 ppm _ 26 ppm _ Q < 50 opm nNT ppm
Zinc ,,
<
- Antimony Q<
n<
5
__ <5.0
Phenolics L_!
< 50 ppm INC ppm
n<
Sulfides
< 50 ppm
ppnv"
SL 046388
GENERATOR'S WASTE MATERIAL PROFILE SHEET (C ntinued)
WES-003
Q. OTHER HAZARDOUS CHARACTERISTICS
1. Is this waste a listed solvent waste as defined by 40 CFfl 261.31 (F001. F002. F003. F004, or FOOS)?
2. Does this waste contain greater than 1000 ppm total haiogenated organic compounds?
3. Indicate if this waste is any of the following:
RCRA Reactive
G Radioactive
G Water Reactive^
G Etiological
G Explosive
G Pesticide Manufacturing Waste
G Shock Sensitive G othr
G Pyrophoric
G None of the above
w Q Yes SI No Q Yes' No
AS' f.t
n--1
H. COMPLETE ONLY FOR WASTES INTENDED FOR FUELS or INCINERATION
Seryllium Potassium Sodium Total Bromine Total Chlonne Total Fluorine Total Sulfur
LESS THAN
G< 5000 ppm G< 5000 ppm
< 5000 ppm
< 2%
< 35%
< 1%
or ACTUAL
-
-UK___ppm J500-- ppm
JM.__%
_LLfi5_%
JM__ %
_LM___%
I. OPTIONAL -- RECLAMATION, FUELS, OR INCINERATION'
PARAMETERS Provide if information is available^-
Range
1. Heat Value (BTU/lb): 500 - 1000__
2.
28.6
3. Viscosity (cps): 4000-20000 q (3 72____ F 1(XrF Q 150.
4. Ash: __2J%
5. Settleable soiids:-_____ _________
6. Vapor Pressure @ STP (mm/Hg): ---------------------------:----------------
7. Is this waste a pumpabie liquid?
(2 Yes . G No
Type of pump? -------------------------- !------------------------------------------
8. Can this waste be heated to improve flow? G Yes (2 No
9. Is this waste soluble in water?
GYes Q No
10. Particle size: Will the solid portion of this waste pass through
a 1/8 inch screen?
(3Yes O.N
J. TRANSPORTATION INFORMATION
1. Is this a OOT Hazardous Material? {3 Yes G No
2. Anticipated Annual Volume/Units:
3. Proper Shipping Name: ^faste Flanmable Liquid, n.o.s. OM-E __________
______
4. Hazard Clk FlaniwhlP Liquid
5.1.D. #: NA9189
6. Additional Description: ( TXP1/E02A____________
7. Method of Shipment E Bulk Liquid G Bulk Solid G Drum (Type/Size):.
-L
8. CERCLA Reportable Quantity (RQ):
1
1500 .Other-. lb
10. USEPA Hazardous Waste? E Yes Q No 12. State Hazardous Waste? G Yes Q No
11. USEPA Hazardous Waste Numbers): 13. State Hazardous Waste Number(s):
DOOl/KEfc
tL
K. SPECIAL HANDLING INFORMATION
G Additional Pagels) Attacr
L. GENERATOR CERTIFICATION I hereby certify that all information submitted in this and ail attached documentacantains tru ; accurate descriptions of this waste matenai, and all relevant information regarding known or suspected hazards in the posaessiot the generator has been disclosed.
Assoc.Res.ChanistJ:
Signature
William H. Cooper 3.
Name (Type or Print)
*
Title
April 9, 1990 4.
Date
SL 46389
31-701
WASTE ANALYSIS REPOST
._
Environmental LaboratoryPPG Industries, Inc., Lake Charles, LA
. W
-
Sample
~ YlTi) S\)r^c*Poy\d Siodje. CDerAwr)*Vs}
Location of Sample - Around pcn-me^ of Pcrr>dy /*
frem b^ky I*
Sample Collector
- Ui.tlCecfier) lo.P, //tier)
sample Method/Device -
Date of Samplings - yftjSI
^rJ,s
. 4cxo~
llrt'y o
Date All Analyses Completed -7/W//
Report Submitted by: /Z/jnn&tfji-r belle
Test Parameters
Standard
Iinitabilitv < Corrosivity ( ) - R/A Reactivity
C ) - N/A
) - HAA pH inch/vr
14flUF min
2 - 12J _ . -3*2. 0.230 max
|
EP Toxicity (mg/L)
( ) ' N/A
As 3.0 max
Be 100.0 max
Cd 1.0 mtt
Cr JJ.fc m*x ...
ft j,e_nw
Hi _ _ _
0 ,lK
s _ 1.0 Rtt1
A*_ _ .
_ 3j0
Lab Lob Snia Identification tfurabar
*7^2 siv
: -
1
i3.sr _ :: 7 3-- i
Other Parameters (if needed)
( > - N/A
________________ OffOtTHATg) HTOTttaaOWrJef ^
Chlnroeshaom-
. _ C9CT
Chloroethmie
. (UCT .
Dlchloraeithene
(thC12>
1.1-Oichlornetbsne _ iTO)
1.1-DlchlncoettMne
(DCET
1.2-Dlohlaroethmse
(cie/trmna)
Trichlorousthane
. (C8C13)
;,2-pichLoriethene
(OCT
1.1.1-IrlchJnroethana CMC)
(CdOTetracfcloreaethane _
Trlcblotmethaoe
(Trlehlor)
l.l.E-Tridbtaroethana (TOO
1.1.1.2-Tetraahlproathans' (awe^
1.1.2.2-tefc*echlweth*li<F (arm)
Tetrachloroetbene
(Perchlor)
PetUaUenethaM
(Penta)
KaHsUnroethen* Rarxachlorobutediene
(Here) (BOO)
HD
7Jd HD 6.Z4 %
DrfJ 96
dfblo 96 6*/? 9f o.yf % At 0 8 %
'/a _ /).A3 %
_ Ut^fCArdkJ*^. _ total cue__________WH % J_
_ ....
. ..
vf 'mw mr m-
A L! brine*
*
odav. : f:
tax
_.
/ki..
6L
Ash
hxTT~4 iWHbt d. ri %
's' .A... 0 t n/ifiRO(
TEST PROCEDURE Parameter
Method Used
LL. 71* U 9
Ignitability N/A
Pensky-Martens Closed Cup Tester ASTM Standard D-93-79
Setaflash Closed Other (specify) Cup Tester ASTM Standard D-3278-78
Corrosivity (pH)
N/A
te^SW-846 Method 9040 pH Measurement
Corrosivity (inch/yr) N/A
National Association of Corrosion Engineers Standard TM-01-69
Other (specify) Other (specify)
Reactivity
N/A
(One affirmative answer will classify waste reactive)
1) Normally unstable without detonating? 2) Reacts violently with water? 3) Forms potentially explosive mixture with water? 4) Cyanide or sulfide bearing waste which can generate toxic gases,
vapor or fumes under pH conditions between 2 and 12.5? 5) Capable of detonation or explosive reaction if subjected to strong
initiating source or if heated under confinement?
6) Readily capable of detonation or explosive decomposition or reaction at standard temperature and pressure?
7) Forbidden Class A, or Class fi explosive as defined in 49 CFR 173.51, 173.53, and/or 173.88?
S 846
Parameter
Method Parameter
EP Toxicity SW-846
As Be
7060 7080
Ag C1HC
(Method 1310)
Cd
7131
N/A Cr 7190
Fb 7420
TCLP* Hg 7470
N/A Se 7740
* Toxicity Characteristic Leaching Procedure
SW-Ai>6 Method
7761 -b5030
M thod Parameter V^Used
b/a.j/r
LDA*1*L>
J)sh _ ,
l-DASbt
Mine.
/?A)hir/vib
AGWS+2-D
CUH<L
LDJOflV-A
Sedij/M________ Cit)&4U . into
LABORATORY IDENTIFICATION
Laboratory: //tf
Uda IaA* <&**}&
----Test Parameters Analyzed and Date
Analvst(s): QriZlK*' JSrvbeU4' 1
Ljaker. Ask. itoA-ialve.. (*l (LLHC.:
-- t
=7 r
'l
Sodi'uM
__
7Mil____ /
cc: File Anne Corbello
Jfile. ' '
SL 046391
31-701
WASTE ANALYSIS REPORT
Environmental Laborat ry
PPG Industries, Inc., Lake Charles, LA vOT3-003
------ " ^JTU Syv<je ficmJ Sampl
Location of Sample - J)er(WJi\/eSy blest bank e?fSur^e. P<m d hSear
Sample Collector
-
Sample Method/Device -
<
V\J;)|{4>mS
^raX , S<teof
Date of Sampling
- fa/aq/ffl
Date All Analyses Completed - IjisfSi
Report Submitted by:
;->X" :;<?)
____
/l-nneaparbe!I,
ANALYSIS RESULTS
Test Parameters
(
Corrosivity
( ) - H/A Reactivity
( } - H/A
1 - WK_eS_
inch/vr
EF Toxicity
(ms/D
C ) - H/A
As
Be
cd ce_
Se
Standard
140 F min 2 - 12.5 0.250 max
-W
5,0 100.0 J-S-qg.. 3.0
_L2_
1.0 5.0
jde/`
Other Parameters (if needed)
< ) H/A
(MeC12)
J2SSL
. 2-Dlchloxoetfaana 1,1.l-Trlchioroethana Tatraohloromettaane
1.1.2-Trlchioroethana
^gcai
(MC)
(CQO
(Trlehlor) (TCB)
1.1.2.2-Tetraehloroethana (arm)
Tetrachloroethene
(Perchlor)
Paptachloroethane
(Pepta)
JSSiL g..ohlorobutadlene (HCBD)
jOAXVL,
MxJLSl
J'JJL &iQU.
diu
22s
briaa.*..
ML
SL 046392'
TEST PROCEDURE
LL llrt '
Parameter
Method Used
Ignitabllity N/A
Pensky-Martens Closed Cup Tester ASTM Standard D-93-79
0 Setaflash Closed Other (specify) Cup Tester ASTM Standard D-3278-78
Corrosivity
(pH) N/A
<Z^SW-846 Method 9040 pH Measurement
Q Other (specify)
Corrosivity (inch/yr) N/A
National Association of Corrosion Engineers Standard TM-01-69
Other (specify)
Reactivity
N/A
(One affirmative answer will classify waste reactive)
1) Normally unstable without detonating? 2) Reacts violently with water? 3) Forms potentially explosive mixture with water? 4) Cyanide or sulfide bearing waste which can generate toxic gas s,
vapor or fumes under pH conditions between 2 and 12.5? 5) Capable of detonation or explosive reaction if subjected to strong
initiating source or if heated under confinement? 6) Readily capable of detonation or explosive decomposition or
reaction at standard temperature and pressure? 7) Forbidden Class A, or Class B explosive as defined in
49 CFR 173.51, 173.53, and/or 173.88?
SV 846
Parameter
Method Parameter -
EP Toxicity
As
7060
. Ag
Stf-846
Be
7080
C1HC
(Method 1310)
Cd
7131
SednJ r*1
N/A Cr 7190
Fb 7420
TCLP*
Hr _ _ . 7470
N/A Se 7740
* Toxicity Characteristic Leaching Procedure
SV 846 Method
7761 5030
!a>/0
Parameter
_ Ll/ilr if
itethod rna Used
\JJ21S-At
/ r>JLSTAJl D
a
-
TJkBORATORY IDENTIFICATION
Laboratory: ffd
LA OJuDtJeJ.
Test Parameters Analyzed and Date
Analvst(s): <^'/
'TfiJrrynV V/ZSntL.
<*AMLy Lj*Ut, M;
4 * 1,^ <L 1
ihzffX
cc: File Anne Corbello
*
SL 046393
31-701
WASTE ANALYSIS REPORT
Envir nmental Laboratory PPG Industries, Inc., Lake Charles, LA
,
V\}T3 -00^>
sample Location of Sample
- ViTU
p>-nd
- S (j>i)A<axd 4*
*
Sample Collector
- M^Oe/iand ntjinc*rs
Sample Method/Device - (jrane. fended over Pmdf Se.d/^erd' dredger /fbnd grid
Date of Sampling-
- 7/}2f2t 0U3o~ Uz0
Date All Analyses Completed - ff/ajE/yy '
Report Submitted by: /T/^we. OarhiHo
xte-iixr
Test Paranstsss
Ianitability < Corrosivity
( ) - n/a
) - M/A pa lnch/yr
Standard
1A0P min 2 - -12...3 . 0.230 max
77^
Lab Lo* Samola Idantiflcation Huofoar
17+-I&.______
/ 7.3
1
11j
I I
W^STa
As
3.0 max
Lnl
Ba
100.0 max
1*2.
<m*/L)
i VT/i 1--
( ) ' H/A
Md-AJs
od
1.0 max
<o*4~f
cr_ _
3.0 max .
3*1*2.
n 3.0 max
a* _
. 0.2 max
2,14
3a
1.0 max
<0, 03b
As
5.0 ***
<1.12-
Aii'c/tei
fi0j*/>ev
_____AviJs'MagJl*/
J.1,0
LI 'Ll_______
<3.37
Be-yJWlv Z
<0,3h
csaiaxuAm raatcaaoB tmmi+i*
Othar Parnaatara
ChloreatlMMOiloroathaoa Pirhlnrn--thana
(VCX
(EC) (MaC12)
O.oS
(1C naadad)
1.1-Dichloroathana
(VDC)
1. l-Dlchlowathana _ iDOt)
( ) - M/A
1.2-Dichloroathana
(eia/trans)
Trlchlaxemath ana 1.2-Dichloroatbana
(CHC13) (EDCT
1-/3
! iJone.
1.1. 1-Triehloxoatbana (MC)
Tatraehlnronatbana
(CC1A)
Trichloroathana
(Trleblor)
1.1.2-Trichlnroathana (TCE)
1.1.1.2-Tatraotaloroatbana (unaym)
1.1.2.2-Tatraohloroathana (arm)
TatraehliproatJiaua
(Parchlor)
PantaeUoroathana
(Panta)
Haxaehlnroafchana
(Ha*a>
Haxachlarobutadlana (8CBD)
" 0*7
0,23. _ b.s2 _ 0.U _
a.s 7
4*32_ 0,41* 0.H4. I.3Z
U(JK*J0kJ*S
4,20 _
total mac
0J7. (M) . -JL^tPL.
11
1 ,
j
[
1
PA-
J13 /
-----------**-*-/<
j
y)SCnsiU
Jov'oiz?
r/ S'- .
He* -j- }/a
/ ^ 7a/ f/
Ok lari tn r. _ n , < *7 % -
loafz.y
3Q. r? *4,
_ J\sh
3 / /jt-i
<ri:
_ =t4,/ A %
1
|
1
I
I
- mtiqi
TEST PROCEDURE
LL7T5 `
Parameter
Method Used
Ignitability N/A
B^Pensky-Martens Closed Cup Tester ASTM Standard D-93-79
Setaflash Closed Other (specify) Cup Tester ASTM Standard D-3278-78
Corrosivity (pH)
N/A
0^SV-846 Method 9040 pH Measurement
Other (specify)- - --
Corrosivity (inch/yr) N/A
National Association of Corrosion Engineers Standard TM-01-69
Other (specify)
Reactivity
''N/A
(One affirmative answer will classify waste reactive)
1) Normally unstable without detonating? 2) Reacts violently with water? 3) Forms potentially explosive mixture with water? 4) Cyanide or sulfide bearing waste which can generate toxic gases,
vapor or fumes under pH conditions bertween 2 and 12.5? 5) Capable of detonation or explosive reaction if subjected to str ng
initiating source or if heated under confinement? 6) Readily capable of detonation or explosive decomposition r
reaction at standard temperature and pressure? 7) Forbidden Class A, or Class B explosive as defined in
49 CFR 173.51, 173.53, and/or 173.88?
| SW 846
Parameter ! Method Parameter
EP Toxicity
As
706J
Ag _
SW-846 (Method 1310)
Ba Cd
_
boID- _
C1HC MeA-A IJ
GTN/A
Cr foAJ ft pfeU rfler/jA Fb 7420
tclp*
Hg _
7470
O'N/A
Se
774/
* Toxicity Characteristic Leaching Procedure
SW 846 r
Method
Parameter
____ Z?6___ 5030
sesv
Jsh
lotc
JfeaA VaIuh.
nL.
ALLMC,
MMethod Used
LD-Z57J LD1SU. '
8 LJ)25L2.I>
jhcjrtnrfa'*'
LABORATORY IDENTIFICATION
Laboratory: Ga/iT lab Pore. LaU
Test Parameters Analyzed-and Date
Analvst(s): 5Mcrrrls; TLtp. y 'Vjj.ervau _ .
A/UAab fltiltt
Vhcrns/-/.y
i/miTs h
' ' ^ ' r----------
______________ F A-nne.
--------- Bfck
___ tM/a___________________________________
cc: File Anne Corb llo
Ljorr-J Corner
/
0A6395
31-701 Sample
WASTE ANALYSIS REPORT
Environmental Laboratory PPG Industries, Inc., Lake Charles, LA
Wts-*>5
"VJT'O SuY^e.'Po'n.< Soulty Wes'}- ^ ve.Jvay'4'
Location of Sample -u)
4 SAmfO^ pc mi5 3,4,1,$*
Sample collector
-
Sample Method/Device - (^-<xne
JLyijweers
_______
9ier P^dy^diyn^ni clre.Jje.Y J/eortd
Date of Sampling-
- 7/fSjtS &k3o-f}3
*
Date All Analyses Completed - %Report Submitted by: f~, A^h^ndoriedc
Test Parameters
Tenitabilitv t
Corrosivity ( 1 - N/A Reactivity
C (/r - N/A
) - N/A
pH inch/vr
Standard
140P min 2 ' 12*3 . 0.230 max
- 774- _
SU-
_
Lab Lox Samola Identification Nunfeer
.
Zie 774
--> . , -
i
1
As
3.0 max
o.&\-
(a*/D
( ) - N/A
~TdAL A\e.Ms
Be
100.0 max
37,1
Cd
1.0 max
<o*s4-
Cr
3-0
4D3
Pb
S.O max
UDl
B* . - -
Se
0.2 max 1.0 max
it* 2<o.sm
A* ............ 3.0 max
<1,91*
AHc.ke. i
AL.b
i>flpe? _
____4wi-#)nA->\/ _
f&rith'uiA rrmtKt*dtmvnxc$naa~tm)ijt4/e
_____
~
i
1
i '
i i
Other Parameters (if needed)
( ) - N/A
Chlnroathamm-
_ (TOT: _
I Chloroethane
(SC) . _ 6,QT
ntehlnrd--rhene
1.1-Dlet^Inroethene
(ttaC12) (TOC)
1.1-Dlchloroethene
1.2-Diehloroethene
(Off) (cie/trena)
_ (2,2,7
Trichioromethane 1.2-Dichloroethane
(CHC13) (BO
<0*73 7./4
l.l.l-Triehloroethene - (ME)
Tetre^hlflrooatbane
(00.4)
_ (2,4/
Trichloroethene
(Trichlor)
1.1.2-T*iehln*oethe (TOE) _
_ i*n
1.1.1.2-Tatrachloroethane (unarm)
0.4-2*
1.1.2.2-TefcrecMmroettane (eym) _
1*30 _
T.tr.rhlnroethene -
(Perchlor)
7.74
p*r.t.r.hloxoethene
(Pente)
3-ir1 ppA Ytecas '4\/ J/^Sh 5'47575 r< as
JJ^aT~ foliJA. .... v e*
4/4,5- i?7 /
--------- : -r--
A)at-e\ 4s*94 %
--
JDejnSt 4v/ f,OJ7.
Aish . . 74.*^
ftevaekiesoethene
(Here)
Serachlorobatadiene (HC80)
pdreuDtck hia benzene*
__ _ 0.02*
---
--
-
0/4 Ka/**)A5
- 4 ?4.
/) .rt
total ax
0)h MB /s -.^.7x77-.
-tYertie-
^yl d Za^ l~ot^/3eeM* JT p*4 /
cr. 0463^6
TEST PROCEDURE
LLTV
Parameter
Method Used
Ignitability N/A
n/Pensky-Martens Closed Cup Tester ASTM Standard D-93-79
Seraflash Closed Other (specify) Cup Tester ASTM
Standard D-3278-78
Corrosivity (pH)
N/A
ffl^SW-846 Method 9040 pH Measurement
Other (specify)^ &-/
Corr sivity (inch/yr) N/A
National Association of Corrosion Engineers Standard TM-01-69
Other (specify) ' j11
Reactivity
c/N/A
(One affirmative answer will classify waste reactive)
1) Normally unstable without detonating? 2) Reacts violently with water? 3) Forms potentially explosive mixture with water? 4) Cyanide or sulfide bearing waste which can generate toxic gases,
vapor or fumes under pH conditions between 2 and 12.5? 5) Capable of detonation or explosive reaction if subjected to str ng
initiating source or if heated under confinement? 6) Readily capable of detonation or explosive decomposition or
reaction at standard temperature and pressure? 7) Forbidden Class A, or Class B explosive as defined in
49 CFR 173.51, 173.53, and/or 173.88?
Stf 846
Parameter
Method Parameter
EP Toxicity SW-846
As Ba
706L teb/h
C1HC
(Method 1310)
Cd
N/A
cr n 1*010
/L'as-L
Fb 7420
tclp* N/A
Hg_. _ Se
7470 774 /
1
* T xicity Characteristic Leaching Procedure
SW 846 Method
-- 776O 5030
SOfTO . H>/0
' Parameter
3 ltJa4-trr
Ash
^Method Used
LD JL<S"7I Lf) -4StU UDdHTtol Lf) JSFLJL/B
dLU/L ViScoS^J
ttfUZincJrJ'
LABORATORY IDENTIFICATION Laboratory: PPQ
LaA
Test Parameters Analyzed and Date
Analvst(s):
Marrl! (Iah-a,
3ru/u/f-f-
w lA'ZAsrt^. S?r>ber'-i- /W4v/ 4-
pfS 7 ,v,P
F.Ayt^a- P/rrbe.llO-------------------F---t-e--d-.-,-P--<--L--L--J--j-,-
` 1' ^ _ _____________________________________
cc File Anne Corb llo
0rv\f
SL 04639
31-701
WASTE ANALYSIS REPORT
sample
Environmental Laboratory PPG Industries, Inc., Lake Charles, LA
" WT J Surge-Am d A/d*4k asi 4oaJr*jp
Location of Sample - /V *juaAr*>& 4
^
Sample Collector
- flfe&lla'nd Syijinee-rs
Sample Method/Device - (Sr^e. ex/ent/eJ Mvt Pmd, Seined (bedjefJPoK^tjy/cl
Date of Sampling1
- 7//S>f$& Jfa30- //3
Date All Analyses Completed - iUf/tf
'
Report Submitted by: /7/fwe. (Z>rbeKf)
9<e Gtj
Tast Parmnatars
IanitabiUty ( Corrosivity
c )-
W^$7a
) - K/A D0 meh/vr
Standard O
1*0 F min 2 - 12.3 0.250 max
775"
Lab Los Samela Idantification Ruebar
*.z
7 7^"
1
CP turiftiir (ms/L) ( ) - H/A
! o^a( fy\ci<kls
Otbsr Param*tars (if naadad) ( ' ) ' H/A
/VD <'
JkJ-edtcL
As Ba Cd Cr lb Ht. Sa AS
Afic.ke.1 _
(Laa/ier
____ ATM:y*\D'n 1 flcri/lliUM'
3.0 max 100.0 max _ 1.0 max _ 3.0 max 3.0_ma* 0.2 max 1.0 max 5.0 max
CblonsttHM
ne
Cblorostiunw
_ (fO_
Diehlorowathana
<M*C12>
1.1-Diehlormathao* . (PBC)
1. l-Dichloroathan* (09)
1.2-Dlehloroathana
(eis/trails)
Tri ehlnrcmathana
(CBC13)
1.2-Diehloroatbana . (IDC>
1.1.1-Irichloroathsna (MCI
Tatracfajoraa* thus
(GCLA)
Triehloroathan*
(Trichlor)
1.1.2'Trichlorosthsns (TC8)
1.1.1.2-T*t***talo*q**bam*' (warm) 1.1.2.2-Tatxachloro*ebn*-<*ym>
Tatraehloroathana
(Parchlor)
Pantsrhloroathana
(Pants)
Raxaehlnroathsna
(Hajca)
Haxsehlorebotadisna (BOD)
UfJ Ky\o.vJ)lS
!*>4 A.5& <-OA7
3 4 SO ID*Ut <a*e>2&> 4/,_ 7ZJtAJA
<-Ta/S" ^ L ___-.
--_0.3
N>
A.SZ_ _ MS'
_ J?-1S _
A 571
3 .fir 0*31 >,3g )*/L -
V 4/3<?
;1
1 i
-----------------------(
J
11
1
1 i
WKa M /4
/
y. '
ijsco* /// dr.Atft 1- 63^1/7 <*4>S
1 1
1
AW pahte.
S~7T.L
7^7A" A
"
Tf
fit!byIn e, S3*if-ft
,_______
UJoJ-t \
/A. /JU %
j)&Y\ Sr' Ali / Z*(rt7
<23, ? '
-
--
|
1
j
4#-- 1
----
1 1
total clbc__________ kLhjam^L
- SL 0^639
erer) C t~
TEST PROCEDURE
LL3l-
Parameter
Method Used
Ignitability N/A
Oransky-Martens Closed Cup Tester ASTM Standard D-93-79
Setaflash Closed Other (specify) Cup Tester ASTM Standard D-3278-78
Corrosivity (pH)
N/A
G3/SW 846 Method 9040 pH Measurement
Other (specify)
Corrosivity (inch/yr) N/A
National Association of Corrosion
Engineers Standard TM-01-69
Other (specify)
Reactivity
Ef N/A
(One affirmative answer will classify waste reactive)
1) Normally unstable without detonating? 2) Reacts violently with water? 3) Forms potentially explosive mixture with water? 4) Cyanide or sulfide bearing waste which can generate toxic gases,
vapor or fumes under pH conditions between 2 and 12.5? 5) Capable of detonation or explosive reaction if subjected to str ng
initiating source or if haated under confinement? 6) Readily capable of detonation or explosive decomposition or
reaction at standard temperature and pressure? 7) Forbidden Class A, or Class B explosive as defined in
49 CFR 173.51, 173.53, and/or 173.88?
! Stf 846
Parameter
Method Parameter
EP Toxicity
As
706/
As
SW-846
Ba Ubth
C1HC
(Me-hod 1310)
Cd
b>a( 6 -
Mp4afs
a n/a
Cr IfOtb
Pb 7420
TCLP* Ha 7470
a N/A Se 774./
* Toxicity Characteristic Leaching Procedure
SW 846 Method 7760
5030
JolO
Parameter
LJb-4-e.r Ask w
dk h-cinp. dL/JP,
VfcSfoa.'.Ay.
^^Metnod Used
li)~Z5-L>L
Lrx2<rA3.
LDzsia.A jI/SSP}nt.ex
LABORATORY IDENTIFICATION Laboratory :/?/V? Sa/iI, Lah ih Once. Lah
Test Parameters Analyzed and Dace
Analvst(s):
Morris derrt~ Me-Uls S/n/fX
V/Sros/ly ' TfagJSS
rohed fieri*/1-
44m/ j/d/de d.
P6Af_ -7]/Ml f ...........
'
Ann 2ex.Ircito----------------
...
"
7/l//ff * f.
cc: File Anne Corb llo
Urvj Joiner
46399
31-701
WASTE ANALYSIS REPORT
Environmental Laboratory PPG Industries, Inc., Lake Charles, LA
vv > 003
Sample
- \^T0 Sorje pa*Aj&rdh Wes/ ^uadyaj/xdr
Location of Sample - rfvJ
4 Saznfl)fiomh //,/2,/f)^ *
Sample collector
-
And *j*srs
Sample Metbod/Device - Cya>\^ emended, oyer 1ahJ./Sedl^<^ni dredy**J$rtd
Date of Sampling - 7fIS/U 0b30- 1130
Date All Analyses- Completed - ?/z4/?7
ANALYSIS RESULTS
-
Report Submitted by: f^nne. Ctrr^ellt . . j/47/Si.
Teat Paranetara
Corroaivity ( ) - N/A Reactivity
(wT- N/A
EP Teaieaay-
(ns/U
C ) N/A
Tolat
M*Ws
ineh/yr
Standard
1*0 F win
2 - 12-S
0.230 max
22^
Aa Ba 100.0 Cd
J. "FL wr 5.0 1 JL
hP-^L _LJL
itonk
JUL AJL <6tS'l ab.7. JuJiL. lldL%
j3S&. /4.3 ^5V
222l
Other Paranetara (it naadad)
( ) - N/A
qgiqu^irmgxaiapa;3Me^^ ll S4pqSeBf--- -____Cg-L'___
Plchlar^athama; _ J0&2L Lt:P^MffSWPfa. . .. gpcj
1.1-Plchloroathane (P(XI
1.2-Dlchloroathie
(qla/trana)
iggai
J2jJJL 5f^2
$2
Tatrauhlntnnathanc Trlchloroethane
(CdO
JlEiSSiSSl
jg'-ja. jUdf-,
.l.l.2->Xateaafahaoathana<WWi)
1.1.2.2-Tatraoblniqethane(am)
TatrachJjoroethanc
(Parchlor)
(Paata)
Harachloroatha Haxachlorobutadiana
JlSiL (BCBP)
.gtaz Q.77
fig
M'+ *h
J&342-
exzr\<Lt- Pcmd Jvid L&b Loc^BookJE ptbi
SL 04640
TEST PROCEDURE
u- 77b
Parameter
Method Used
Ignitability O N/A
'"'Pensky-Martens Closed Cup Tester ASTM Standard D-93-79
Setaflash Closed Other (specify) Cup Tester ASTM
Standard D-3278-78
Corrosivity (pH)
N/A
^SW-846 Method 9040 pH Measurement
Other (specify)?
Corrosivity (inch/yr) eTn/A
National Association of Corrosion Engineers Standard TM-01-69
O Other (specify)! JA
**
Reactivity
*<f . rZ*"
1) Normally unstable without detonating?
[/ N/A
2) Reacts violently with water?
.
3) Forms potentially explosive mixture with water?
(One
4) Cyanide or sulfide bearing waste which can generate toxic gases,
affirmative
vapor or fumes under pH conditions between 2 and 12.5?
answer will classify waste reactive)
5) Capable of detonation or explosive reaction if subjected to strong initiating source or if heated under confinement?
6) Readily capable of detonation or. explosive decomposition or reaction at standard temperature and pressure?
7) Forbidden Class A, or Class. B-explosive as defined in
49 CFR 173.51, 173.53, and/or 173.88?
V. 4 i\ ,`
-t-----------------------11
EP Toxicity SW-846
(Method 1310)
Parameter Aa Ba Cd
Stf 846 Method
706?
fpGfO -
Parameter
Aft....... C1HC--
SW 846 Method
7760 5030-
~
if/gMethod
Parameter
Used
JiiApy
LD &5%L LTiotSTLt
CZ'N/A
Cr-
Pb" 7420
TCJ^* Hg 7470
S'N/A Se 774/
* Toxicity Characteristic Leaching Procedure
Inrft
l4hit. CU I/I <ti M t> . CL//^
..i/usrgs//^ -
Lr\D<rb3 Zb L&JtorteX A
LABORATORY IDENTIFICATION
Laboratory: 0A&
Lxh `f-Onry LaJl _ Test Paremeters Analyzed and Date
Analvst(s) : Kebtfj: Afavr/r r;*.e.(/r
A/)* Us. t/jfJn
yistAsiti ty/Aa-tt? , Ash.eU*s.'J-'s. Mail Ifaluy dl.CUUL s>/J 7/jjJBi'...
/izuaJL__________________ daJieJlz---------A----'-u--i-t-- .__
1/ Anne Corbello
^
i-d.rry' Uomwf
1/Rle. v^TS D03 (>)
_
;v
_
sl 0464oi
e V*.
**