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STL Burlington Colchester, Vermont Sample Data Summary Package SDG: 117522 SEVERN TRENT STL November 30, 2006 Mr. Charlie Young Weston Solutions 1400 Weston Way West Chester, PA 19380 STL Burlington 208 South Park Drive, Suite 1 Colchester, VT 05446 Tel: 802 655 1203 Fax: 802 655 1248 www.stl-inc.com Re: Laboratory Project No. 26000 Case: 26000: SPG: 117522 Dear Mr. Young: Enclosed are the analytical results for the samples that were received by STL Burlington on October 18th, 2006. Laboratory identification numbers were assigned, and designated as follows: Lab ID Client Sample ID Sample Date Sample Matrix Received: 10/18/06 ETR No: 117522 691475 691476 691477 691478 691479 691480 691481 691481 DP 691482 691483 691484 691485 691486 691487 691488 691489 691490 691491 691492 691493 691494 DBCF01IPF0010041021 D B C F 0 1 IP F 0 0 2 0 0 4 1 021 D B C F 0 1 IP F 0 0 3 0 0 4 1 021 D B C F0 1IP W 0010041021 DBCF01IPW0020041021 DBCF01IPW0030041021 DOUF01IPF0010041021 DOUF01IPF0010REP D O U F 0 1 IP F 0 0 2 0 0 4 1 021 DOUF01IPF0030041021 D O U F 0 1 IP F 0 0 4 0 0 4 1 021 DOLIF01IPF0050041021 DOUF01IPW0010041021 DOUF01IPW0020041021 DL2F01MSW0010041021 D L 2 F 0 1 M S W 0 0 2 0 0 4 1 021 D L 2 F 0 1 M S W 0 0 3 0 0 4 1 021 D L 2 F 0 1 M S W 0 0 4 0 0 4 1 021 D L 2 F 0 1 M S W 0 0 5 0 0 4 1 021 DBCF01MSW0010041104 DBCF01MSW 0020041104 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/22/04 10/22/04 10/22/04 10/22/04 10/22/04 10/22/04 10/22/04 10/22/04 11/04/04 11/04/04 TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE Documentation of the condition of the samples at the time of their receipt and any exception to the laboratory's Sample Acceptance Policy is documented in the Sample Handling section of this submittal. Leaders in Environmental Testing 1.1 Severn Trent Laboratories, Inc. STL November 30, 2006 Mr. Charlie Young Page 2 of 2 In order to accommodate field length limitations in processing the data summary forms, the laboratory did, in certain instances, abbreviate the sample identifiers. Dashes have been removed from the client identifiers in this delivery group. The electronically formatted data provides the full sample identifier. Lipids: There were no exceptions to the method quality control criteria during the analyses of these samples. The analytical results associated with the samples presented in this test report were generated under a quality system that adheres to requirements specified in the NELAC standard. Release of the data in this test report and any associated electronic deliverables is authorized by the Laboratory Director's designee as verified by the following signature. If there are any questions regarding this submittal, please contact me at 802 655-1203. C i n / ' r t "/- 11 / Ron Pentkowski Project Manager Enclosure 1.2 sog * A JJxaX.-- CHAIN OF CUSTODY / ANALYSIS REQUEST FORM EXYGEN RESEARCH SAMPLE RECEIVING T: 814-231-8032 F: 814-231-1580 3117 Research Drive State College, PA 16801 PAGE PROJECT INFORMATION Client: Weston Solutions, Inc. 1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401 Project Manager: Jai Kesari email: .kesarl@westonsolutions.com Project Name: Reference No: Decatur, Alabama 02181-129-081-0001 SES REQ Sampler: Charles Young P.O. #: Quotation #: SAMPLE ANALYSIS ExyLIMS # Client Sample Identification DL3 F01 IPF002 0 041021 DL3 F01 IPF003 041021 DBC F01 IPF001 041021 DBC F01 IPF002 041021 DBC F01 IPF003 041021 DBC F01 IPW001 041021 DBC F01 IPW002 041021 DBC F01 IPW003 041021 DOU F01 IPF001 041021 DOU F01 IPF002 041021 Collection Date 21-Oct-04 21 -Oct-04 21-Oct-04 21-Oct-04 21 -Oct-04 21 -Oct-04 21-Oct-04 21-Oct-04 21-Oct-04 21-Oct-04 Collection Time 23:00 23:10 23:25 22:30 23:30 22:35 22:35 22:40 23:00 23:20 eac> oO. 3oc zo Sample Matrix Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue CHAIN OF CUSTODY R elingujsljedBii Date 10/22/04 C ooler ID No.: f Cooler Temp. (C): Time Received By: Date Tim e 12:00 Fed Ex __ _ L- 10/22/04 12:00 rV'/ i lA*r J X l ______ IQ`h ^b b rt7 S 0 Comments PROJECT REQUIREMENTS <5-0 Results Deadline: Laboratory Report Options: Sample Resulls Only Add Case Narrative Add Quality Control Sum m a^ Add Calibration Summary Add Raw Data Other: CHAIN OF CUSTODY / ANALYSIS REQUEST FORM EXYGEN RESEARCH SAMPLE RECEIVING T: B14-231-8032 F: 814-231-1580 3117 Research Drive State College, PA 16801 PAGE _4_ o f _4 PROJECT INFORMATION Client: W eston S olutions, Inc. 1400 W eston Way, B ldg. 5-2 W est Chester, PA 19380 T: 610-701-3761 F: 610-701-7401 Project Manage r: Jai Kesarl em;ail: i.kesari@ w eston solu tion s.com Project Name: Reference No: Decatur, Alabama 02181-129-081-0001 ANALYSES REQUESTED Sampler: Charles Young P.O. #: Quotation #: Grab Sample Composite No. of Containers PFOA SAMPLE ANALYSIS ExyLIMS # Collection C lient Sam|pie Id e n tific a tio n | | Date DOU F01 IPF003 0 041021 21-Oct-04 DOU F01 IPF004 0 041021 21-Oct-04 DOU F01 IPF005 0 041021 22-Oct-04 DOU F01 IPW01 0 041021 22-Oct-04 DOU F01 IPW002 0 041021 22-Oct-04 DL2 f o i; MSW001 0 041021 22-Oct-04 DL2 F01 MSW002 0 041021 22-Oct-04 DL2 F01 MSW003 0 041021 22-Oct-04 DL2 F01 MSW004 0 041021 22-Oct-04 DL2 F01 MSW004 0 041021 22-Oct-04 Collection Time 23:35 23:45 0:00 0:05 0:10 0:20 0:25 0:25 0:30 0:35 X X X X X X X X X X Sample Matrix 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue CHAIN OF CUSTODY R e lin q y js l)0$B yr'' Date 10/22/04 y C ooler ID No.: T im e 12:00 Received By: Fed Ex C ooler Temp. (C): Date Time 10/22/04 12:00 ---- ,'e/j{A*.* ioAv/c 0^30 C om m en ts X X X X X X X X X X PROJECT REQUIREMENTS .O Results Deadline: Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data Other: 'I CHAIN OF CUSTODY / ANALYSIS REQUEST FORM EXYGEN RESEARCH SAMPLE RECEIVING T: 814-231-8032 F: 814-231-1580 3048 Research Drive State College, PA 16801 PAGE _ J _ of _6 PROJECT INFORMATION Client: Weston Solutions, Inc. 1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401 Project Manager: Jai Kesari email: i.kesari@westonsolutions.com Project Name: Reference No: Decatur, Alabama 02181-129-081-0001 ANALYSES REQUESTED Sampler: Charles Young P.O. #: Quotation #: SAMPLE ANALYSIS ExyLIMS # Collection Client Sample Identification ate DBC F01 MS WO01 041104 4-Nov-04 Collection Time 19:15 aa ZO 1 Sample Matrix Tissue Comments DBC F01 MSW002 041104 4-Nov-04 19:20 Tissue DBC F01 MSW003 041104 4-NOV-04 19:23 Tissue DBC F01 MSW004 041104 4-Nov-04 19:25 Tissue DBC F01 MSW005 041104 4-Nov-04 19:27 Tissue DBC F01 MSF001 041104 4-NOV-04 19:40 Tissue DBC F01 MSF002 DBC F01 IPF004 041104 4-Nov-04 041104 4-Nov-04 19:45 20:00 Tissue Tissue DBC F01 IPF005 0 041104 4-NOV-04 DBC F01 IPW004 0 041104 4-Nov-04 20:05 20:00 X X 1 Tissue 1 Tissue XX XX CHAIN OF CUSTODY Cooler ID No.: /t^ .4 ^-"Rellnqulshed/By: Date Time Received By: Cooler Temp. (C): Date Time 0*0 PROJECT REQUIREMENTS Results Deadline: Laboratory Report Options: // y it /r /O f ----------- --------------------------- (H O o FedEx / ---------------------------------- ///fc/ry //oo Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary * Subsample o f macerated tissue to be sent to STL for Percent Lipid analyses________ Add Raw Data Other: I 3058 Research Drive State College, PA 16801 RESEARCH Phone: 814-272-1039 Fax: 814-231-1580 Loain Login Group: L0003679 Login #: Project: Company Name: Submitted By: Login Type: Started: Date Start: Due Date: Login Initiated*: 3789 P0000760 Weston Solutions, Inc. Jaisimha Kesari, P.E., DEE Immediate Receipt of Samples True 10/25/2004 10/23/2004 Conform COC Sample: Conform COC: Conform Sample: Conform Request: False True True True * Dates entered into "Login Initiated" field prior to 1/5/06 reflect dates of receipt. The field was formerly called "Received Date" Received By: Ammerman, Mark Spread Sample: Label: Exygen SD/PI: Flaherty, John Project Title/Type: Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program / ROUTINE Login Notes: Conform Notes: Identification on the chain (DL2-F01-MSW004-0-041021) does not match the identification on the container (DL2-F01-MSW005-0041021). As per Charles Young, use the identification on the container (DL2-F01-MSW005-0-041021). MSA 10/25/04 Packaae PK0004480 Carton Packages / Containers Date / Condition ShiDoer/ ID Received Date: 10/25/04 10:45 Package & Contents Uncompromised FEDEX 8479 6714 4761 TemD. Control/Terrm. Dry Ice 0.0 Direction / Handled Bv RECEIVED Ammerman, Mark Container# C0048126 C0048127 C0048128 C0048129 C0048130 C0048131 C0048132 C0048133 C0048134 C0048135 C0048136 C0048137 C0048138 C0048139 C0048140 C0048141 C0048142 C0048143 Gross Weiaht 177.60 g 153.40 g 244.60 g 197.10 g 691.20 g 614.50 g 44.40 g 23.30 g 582.30 g 288.40 g 415.00 g 283.80 g 525.00 g 824.30 g 111.60g 150.50 g 87.70 g 174.60 g fi Container Tvoe 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag Preservative NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE Mfa. Lot Mfa. ID 10/17/2006 I rnin rnt Report Version: Oct 12 2006 9:14AM Instance: R0291646 journm Login Login Group: L0003679 Login #: Project: Company Name: Submitted By: Login Type: Started: Date Start: Due Date: Login Initiated*: 3789 P0000760 Weston Solutions, Inc. Jaisimha Kesari, P.E., DEE Immediate Receipt of Samples True 10/25/2004 10/23/2004 Conform COC Sample: Conform COC: Conform Sample: Conform Request: False True True True * Dates entered into "Login Initiated" field prior to 1/5/06 reflect dates of receipt. The field was formerly called "Received Date" Received By: Ammerman, Mark Spread Sample: Label: Exygen SD/PI: Flaherty, John Project Title/Type: Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program / ROUTINE Login Notes: Conform Notes: Identification on the chain (DL2-F01-MSW004-0-041021) does not match the identification on the container (DL2-F01-MSW005-0- 041021). As per Charles Young, use the identification on the container (DL2-F01-MSW005-0-041021). MSA 10/25/04 Packaae PK0004480 Carton Packages / Containers Date / Condition ShiDDer/ ID Received Date: 10/25/04 10:45 Package & Contents Uncompromised FEDEX 8479 6714 4761 TemD. Control/TemD. Dry Ice 0.0 Direction / Handled Bv RECEIVED Ammerman, Mark Container# C0048144 C0048145 C0048146 C0048147 C0048148 C0048149 C0048150 C0048151 C0048152 C0048153 C0048154 C0048155 C0048156 C0048157 C0048158 C0048159 C0048160 C0048161 C0048162 C0048163 C0048164 C0048165 Gross Weiaht 257.40 g 203.50 g 221.40 g 380.30 g 228.70 g 198.30 g 140.10 g 613.40 g 429.60 g 417.10 g 372.90 g 263.60 g 301.40 g 263.30 g 177.80 g 730.50 g 1,256.60 g 113.40 g 105.20 g 55.30 g 53.70 g 52.70 g dH Container TvDe 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag Preservative NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE Mfa. Lot Mfa. ID 10/17/2006 Lnninrnt Report Version: Oct 12 2006 9:14AM Poaq Or\f R Instance: R0291646 .............. 1111111...111111.... Login Sample ID L0003679-0001 Container C0048126 Matrix SOLID L0003679-0002 C0048127 SOLID L0003679-0003 C0048128 SOLID L0003679-0004 C0048129 SOLID L0003679-0005 C0048130 SOLID L0003679-0006 C0048131 SOLID L0003679-0007 C0048132 SOLID L0003679-0008 C0048133 SOLID L0003679-0009 C0048134 SOLID L0003679-0010 C0048135 SOLID L0003679-0011 SOLID C0048136 OOS Investigation #: OOS-04-071 L0003679-0012 C0048137 SOLID L0003679-0013 C0048138 SOLID L0003679-0014 C0048139 SOLID L0003679-0015 C0048140 SOLID L0O03679-0Q16 C0048141 SOLID Fraction Fish S a m p le s Sample DL3-F01-IPF001-0-041021 Fish DL3-F01-IPF002-0-041021 Fish DMC-F01-IPF001-0-041021 Fish DMC-F01-IPF002-0-041021 Fish DMC-F01-IPW001-0-041021 Fish DMC-F01-IPW002-0-041021 Fish DMC-F01-MSW001 -0-041021 Fish DMC-F01-MSW002-0-041021 Fish DL2-F01-IPF001-0-041021 Fish DL2-F01-IPF002-0-041021 Fish DL2-F01-IPF003-0-041021 Fish DL2-F01-IPF004-0-041021 Fish DL2-F01-IPF005-0-041021 Fish DL2-F01-IPW001-0-41021 Fish DL2-F01-MSF001-0-041021 Fish DL2-F01-MSF002-0-041021 :$ t rTCtr * tm _jQ ^ ,0 in o| * fflL (TJJ oq Date SamDled 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/22/2004 10/22/2004 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/21/2004 Date Due 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/17/2006 Login.rpt Report Version: Oct 12 2006 9:14AM ___________ Page 3 of 5___________ Instance: R0291646 I L0003679-0017 C0048142 SOLID L0003679-0018 C0048143 SOLID L0003679-0019 C0048144 SOLID L0003679-0020 C0048145 SOLID L0003679-0021 C0048146 SOLID L0003679-0022 C0048147 SOLID L0003679-0023 C0048148 SOLID L0003679-0024 C0048149 SOLID L0003679-0025 C0048150 SOLID L0003679-0026 C0048151 SOLID L0003679-0027 C0048152 SOLID L0003679-0028 C0048153 SOLID L0003679-0029 C0048154 SOLID L0003679-0030 C0048155 SOLID L0003679-0031 C0048156 SOLID L0003679-0032 C0048157 SOLID L0003679-0033 C0048158 SOLID L0003679-0034 10/17/2006 Login.rpt SOLID Login Fish DL2-F01-MSF003-0-041021 10/21/2004 10/25/2004 Fish DL2-F01-MSF004-0-041021 10/21/2004 10/25/2004 Fish DL1-F01-IPF001 -0-041021 10/21/2004 10/25/2004 Fish DL3-F01-IPF003-0-041021 10/21/2004 10/25/2004 Fish DL3-F01-IPF004-0-041021 N f. Fish DL3-F01-IPF005-0-041021 t. H i 't* | S' fi Fish DBC-F01-IPF001-0-041021 "X \\ A * Fish DBC-F01-IPF002-0-041021 Et Fish DBC-F01-IPF003-0-041021 Fish DBC-F01-IPW001-0-041021 Fish DBC-F01-IPW002-0-041021 S i" yO s^ s r >^ S^ o- 5 88 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/21/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 Fish DBC-F01-IPW003-0-041021 10/21/2004 10/25/2004 Fish DOU-F01-IPF001-0-041021 10/21/2004 10/25/2004 Fish DOU-F01-IPF002-0-041021 10/21/2004 10/25/2004 Fish DOU-F01-IPF003-0-041021 10/21/2004 10/25/2004 Fish DOU-F01-IPF004-0-041021 10/21/2004 10/25/2004 Fish DOU-F01-IPF005-0-041021 10/22/2004 10/25/2004 Fish DOU-F01-IPW001-0-041021 10/22/2004 10/25/2004 Report Version: Oct 12 2006 9:14AM Instance: R0291646 ___________ Page 4 of 5...................................................................... ...................... ......I.. C0048159 L0003679-0035 C0048160 SOLID L0003679-0036 C0048161 SOLID L0003679-0037 C0048162 SOLID L0003679-0038 C0048163 SOLID L0003679-0039 C0048164 SOLID L0003679-0040 C0048165 SOLID Login Fish DOU-F01-1PW002-0-041021 Fish DL2-F01-MSW001-0-041021 Fish DL2-F01-MSW002-0-041021 Fish DL2-F01-MSW003-0-041021 Fish DL2-F01-MSW004-0-041021 Fish DL2-F01-MSW005-0-041021 10/22/2004 10/22/2004 10/22/2004 10/22/2004 10/22/2004 10/22/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 Login Reviewed By: __________________________________________ Date/Time: 10/17/2006 LoqinJm t _ Report Version: Oct 12 2006 9:14AM Pane * nf * Instance: R0291646 .. 11111....................... SamDle ID L0003772-0001 Container C0049450 Matrix SOLID L0003772-0002 C0049451 SOLID L0003772-0003 C0049452 SOLID L0003772-0004 C0049453 SOLID L0003772-0005 C0049454 SOLID L0003772-0006 C0049455 SOLID L0003772-0007 C0049456 SOLID L0003772-0008 C0049457 SOLID L0003772-0009 C0049458 SOLID L0003772-0010 C0049459 SOLID L0003772-0011 C0049460 SOLID L0003772-0012 C0049461 SOLID L0003772-0013 C0049462 SOLID L0003772-0014 C0049463 SOLID L0003772-0015 C0049464 SOLID L0003772-0016 C0049465 SOLID L0003772-0017 10/17/2006 SOLID Login Fraction Fish Samples SamDle DBC-F01-MSW001 -0-041104 Fish DBC-F01-MSW002-0-041104 Fish DBC-F01-MSW003-0-041104 Fish DBC-F01-MSW004-0-041104 Fish DBC-F01-MSW005-0-041104 Fish DBC-F01-MSF001 -0-041104 Fish DBC-F01-MSF002-0-041104 Fish DBC-F01-IPF004-0-041104 Fish DBC-F01-IPF005-0-041104 Fish DBC-F01-IPW004-0-041104 Fish DBC-F01-IPW005-0-041104 Fish DOU-F01-IPW003-0-041104 Fish DOU-F01-IPW004-0-041104 Fish DOU-F01-IPW005-0-041104 Fish DL2-F01-IPW002-0-041104 Fish DL1-F01-MSW001-0-041104 Fish DL1-F01-MSW002-0-041104 Report Version: Oct 12 2006 9:14AM Pano A r t f 7 Date SamDled 11/04/2004 Date Due 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 11/04/2004 11/08/2004 Instance: R0291811 iiiiiiin SEVERN TRENT Sample Data Summary Package - Geotechnical GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DBCF01IPF0010041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691475 Date Received: 10/18/06 Method LIPIDS Parameter %Liplds Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL 1 0.1 Cone. 5.9 Qual. Printed on: 11/20/06 08:11 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DBCF01IPF0020041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691476 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL Cone. Qual. 1 0.1 4.9 Printed on: 11/20/06 08:11 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DBCF01IPF0030041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691477 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL 1 0.1 Cone. 6.9 Quai. Printed on: 11/20/06 08:11 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DBCF01IPW0010041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691478 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL 1 0.1 Cone. 9.5 Qual. Printed on: 11/20/06 08:11 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DBCF01IPW0020041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691479 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL Cone. Qual. 1 0.1 4.1 Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DBCF01IPW0030041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691480 Date Received : 10/18/06 Method LIPIDS Parameter %Llpids Determination Analytical Analytical Run Date Batch Units DF RL Cone. Qual. 11/17/06 % 1 0.1 3.6 Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DOUF01IPF0010041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691481 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL 1 0.1 Cone. 0.4 Qual. Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Duplicate Sample Report Summary Client Sample No. DOUF01IPF0010REP Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691481 DP Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units Sample Duplicate Result Sample Result Cone. Qual. Cone. Qual. RPD* 0.4 0.4 Control Limit for RPD is + /- 20%, unless otherwise specified. Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DOUF01IPF0020041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691482 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL 1 0.1 Cone. 1.8 Qual. Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DOUF01IPF0030041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691483 Date Received : 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL 1 0.1 Cone. 3.8 Qual. Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DOUF01IPF0040041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691484 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL Cone. Quai. 1 0.1 5.5 Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DOUF01IPF0050041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691485 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL 1 0.1 Cone. 0.3 Qual. Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DOUF01IPW0010041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDG No.: 117522 Lab Sample ID: 691486 Date Received : 10/18/06 Method LIPIDS Parameter VoLlpIds Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL 1 0.1 Cone. 1.9 Qual. Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DOUF01IPW0020041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691487 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL Cone. Qual. 1 0.1 1.0 Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DL2F01MSW0010041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691488 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL Cone. Qual. 1 0.1 1.4 Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DL2F01MSW0020041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691489 Date Received: 10/18/06 Method LIPIDS Parameter YoLipIds Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL 1 0.1 Cone. 1.3 Qual. Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DL2F01MSW0030041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691490 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch Units DF RL Cone. Qual. 11/17/06 % 1 0.1 0.4 Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DL2F01MSW0040041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691491 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL 1 0.1 Cone. 1.3 Quai. Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DL2F01MSW0050041021 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691492 Date Received: 10/18/06 Method LIPIDS Parameter %Lipids Determination Analytical Analytical Run Date Batch Units DF RL Cone. Qual. 11/17/06 % 1 0.1 0.5 Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DBCF01MSW0010041104 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691493 Date Received: 10/18/06 Method LIPIDS Parameter %Llplds Determination Analytical Analytical Run Date Batch 11/17/06 Units % DF RL Cone. Qual. 1 0.1 1.2 Printed on: 11/20/06 08:12 AM GEOTECHNICAL / GENERAL CHEMISTRY Sample Report Summary Client Sample No. DBCF01MSW0020041104 Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids: Contract: Case No.: 26000 Client: WESTN2 SDGNo.: 117522 Lab Sample ID: 691494 Date Received: 10/18/06 Method LIPIDS Parameter %Llpids Determination Analytical Analytical Run Date Batch Units DF RL Cone. Qual. 11/17/06 % 1 0.1 1.3 Printed on: 11/20/06 08:12 AM Percent Lipids Calculations Date: Time: 11/17/2006 2200 Analyst: ETR(s): Client: TPB 117507,117522 W ESTN2 Sample ID M B 111706E 691404 691475 691476 691477 691478 691479 691480 691481 691482 691483 691484 691485 691486 691487 691488 691489 691490 691491 691492 691493 691494 691481DP Sample Weight (g) 10.00 3.00 10.02 10.02 10.00 10.04 10.02 10.03 10.04 10.04 10.01 10.03 10.00 10.01 10.03 10.03 10.01 10.02 10.02 9.97 10.01 10.00 10.01 Dish ( g) 1.0121 1.0083 0.9996 0.9966 0.9765 1.0164 1.0377 1.0373 1.0452 1.0456 1.0187 1.0432 1.0209 1.0010 1.0106 1.0343 1.0435 1.0170 0.9804 0.9957 1.0384 1.0332 1.0447 Dish/Residue (g) 1.0118 1.0160 1.0592 1.0454 1.0454 1.1122 1.0788 1.0737 1.0490 1.0640 1.0569 1.0986 1.0239 1.0204 1.0203 1.0480 1.0567 1.0206 0.9930 1.0007 1.0501 1.0463 1.0492 Extract Final Volume (mLs) 10 3 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Aliquot Used in Determination ( mLs ) 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 % Lipids < 0.1 0.8 5.9 4.9 6.9 9.5 4.1 3.6 0.4 1.8 3.8 5.5 0.3 1.9 1.0 1.4 1.3 0.4 1.3 0.5 1.2 1.3 0.4 #D IV / 0 ! #D IV / 0 ! #D IV / 0 ! STL B urlington 117507117522M B111706E 11/20/2006
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