Document JJnDRpMadK503wYdR6m0BGvv2
AR226-2659
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RES EARC H
Precise Research. Proven Results.
AR226-2659
Analytical Report
Air Sampling Fluorochemical Report DuPont Washington Works - Air Sampling Program Round 2
Exygen Research Report No. L0001308
///(^_^
Testing Laboratory
Exygen Research , 3058 Research Drive State College, PA 16801
Requester
Michael D Aucoin URS Corporation Barley Mill Plaza Building 27 Room 1260 Lancaster Pike and Rt 141
Wilmineton, DE ,19805
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 1 of 7
3058 Research Drive State College, PA 16801, USA
T: 800.281.3219 F: 814.272.1019
jummary
.
'/'. : ;
,
Seven solid media samples were received by Centre Analytical Laboratories, Inc.(dba Exygen
Research) (Exygen) from DuPont Corporation. The media represent samples of air collected on
OVS tubes. Please see Table 1 for a completed listing of samples received and field air volumes
collected.
,
:
The samples were analyzed for Perfluorooctanoic Acid (C8 Acid) using liquid chromatography / mass, spectrometry (LCMS). The method employed is entitled "Method of Analysis for the Determination of Perfluorooctanoic Acid (PFOA) in OVS Airtubes by LCMS" (James Miller,
Exygen Research, February 17, 2003).
;
The OVS tubes were separated into three fractions for specific fluorochemical analysis. Fraction A consisted of the filter, backing material and plastic ring. Fraction B contained the
first bed of XAD resin and the PUP backing. Fraction C contained the second bed of XAD
resin and PUF backing. Fractions A and B were extracted with 1 mL of methanol. Fraction C was not analyzed but saved for possible future analysis. Perfluorodecanoic Acid (C 10 Acid)
was added as a surrogate spike to each fraction prior to extraction.
'.'' .,',' I \ ' .
'
instrument operating
',; .; '
'
. .
conditions can be found
"..," - . . ''
at the beginning of each
.
analytical run.
.:
Raw
instrument data is given in Appendix A. Chain-of-custody information can be found in
Appendix B.
ALL DATA-CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Page 2 of 7
Results Summary
Request#
WWK-A-AMS1-E2A WWK-A-AMS1-E2B WWK-A-AMS1-E2C WWK-A-AMS1-E2 (Total)
Air Volume Sampled (L)
' ' ; 1475
: ,
1475 :. .
1475
; .
,
\ .
.
C8 Acid .
(mg/m3)
< 0.00007 ; < 0.00007
NA < 0.00014
WWK-A-AMS2-E2 A <; WWK-A-AMS2-E2 B
WWK-A-AMS2-E2 C WWK-A-AMS2-E2 (Total)
1468 1468 1468
0.0009 < 0.00007
NA
0.00.09
WWK-A-AMS3-E2 A WWK-A-AMS3-E2 B WWK-A-EMS3-E2 C WWK-A-EMS3-E2 (Total)
:
WWK-A-AMS4-E2 A
WWK-A-AMS4-E2B WWK-A-AMS4-E2 C
WWK-A-AMS4-E2 (Total)
1462 1462 1462
'
1437
^
^
1437
1437
0.0009 < 0.00007
NA 0.0009
- < 0.00007 < 0.00007 NA < 0.00014
WWK-A-AMS5-E2 A WWK-A-AMS5-E2 B WWK-A-AMS5-E2 C
WWK-A-AMS5-E2 (Total)
1456 1456 1456
.< 0.00007 < 0.00007
.
NA
< 0.00014
WWK-A-AMS6-E2 A WWK-A-AMS6-E2 B .WWK-A-AMS6-E2 C WWK-A AMS6-E2 (Total)
1422 1422 1422
< 0.00007 < 0.00007
NA
< 0.00014
NA - Not Analyzed. B fraction was below the quantitation limit, therefore the backup fraction does not require analysis. 1. "<" is defined as not detected at or above the reported level.
2. Sample results have not been corrected for blank results or control spike recoveries.
3. Please note the following descriptions of the OVS sample tube fractions:
Fraction : A B C
Fraction Description Frit Extract 1st set beads extract 2nd set beads extract
(not analyzed)
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 3 of 7
PC Data
.... .,,,:'. ..-... L-C/\^S\j
,
.
,,
,
,,
;
,
,.
-
,
. .
Please note: One control sample was spiked with each perfluorooctanoic acid to give a final concentration of 500 pp
through the tube at a rate of 1-liter per minute for one hour (60 liters of air). The fractions were separated and analy
acceptable range for control recovery is 75-125%.
Request # Control 1
CSAcid (amount spiked - ppb)
500
CSAcid (amount recovered -
503
ppb)
CBAcid (percent recovery
101
Blanks
Request # WWK-A-AMSFBLK-E2 A WWK-A-AMSFBLK-E2 B
Vol. Of Air (L)
'
'1
/
,0 .
0
'
-
' 1
CSAcid (ug/fraction)
<0.10 . <0.10
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Page 4 of 7
urroeates
A surrogate spike (C10 Acid) was added to all OVS tubes to give a final concentration of 500 ppb in the extract.
Surrogate spike recoveries are given in the following table. There are no set criteria forsurrogate spike
recoveries. Advisory, ranges are 75-125%.
;
-
Sample*
WWK-A-AMSFBLK-E2 A WWK-A-AMSFBLK-E2 B
WWK-A-AMS1-E2A WWK-A-AMS1-E2B WWK-A-AMS2-E2 A WWK-A-AMS2-E2B WWK-A-AMS3-E2 A WWK-A-AMS3-E2 B WWK-A-AMS4-E2 A WWK-A-AMS4-E2 B . WWK-A-AMS5-E2 A WWK-A-AMS5-E2B. WWK-A-AMS6-E2 A WWK-A-AMS6-E2 B
Control Spike A Control Spike B
Amount Spiked
(PPb)
500
500
500
500
500
500
.
500
..
500
500
500
! .500
500
500
, 500 ;
500
500
Amount Recovered (PPb)
644 329 707 392 . 666 :
405
' 666
'
'
'
396
- 697 403
732 437
-.
.
. 763 :
-375 612 392
Percent Recovery (%) 129* 66* 141* 78 133*
81
133* 79 139* 81
146* . 87
153* 75
122 78
Surrogate recovery outside of advisory range
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 5 of 7
Calculations
Request #
WWK-A-AMSFBLK-E2 A WWK-A-AMSFBLK-E2 B
WWK-A-AMS1-E2A WWK-A-AMS1-E2B WWK-A-AMS2-E2 A
'"
WWK-A-AMS2-E2 B WWK-A-AMS3-E2 A WWK-A-AMS3-E2 B WWK-A-AMS4-E2 A WWK-A-AMS4-E2 B WWK-A-AMS5-E2 A WWK-A-AMS5-E2 B WWK-A-AMS6-E2 A WWK-A-AMS6-E2 B
Control Spike A Control Spike B
Vol. Of Air (L)
0
0
1475 1475 1468 1468 1462 1462 1437 1437 1456 1456 1422 1422
0
0
CSAcid
(raw-ppb)
<10 <10 <10 <10
1340
<10
1266
<10 <10 <10
49
<10 <10 <10
454 49 . .
CSAcid (ug/fraction)
<0.10 <0.10 <0.10 <0.10
1.3 .
<0.10
1.3
<0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
0.45
<0.10
C8 Acid (mg/m3)
< 0.00007 < 0.00007
0.0009 < 0.00007 : 0.0009 < 0.00007 < 0.00007 < 0.00007 < 0.00007 < 0.00007 < 0.00007 < 0.00007
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Page 6 of 7
Example Calculation
.
For sample WWK-A-AMS2-E2 A C8 Acid,
[1340 ng/ml ofC8 Acid x (1 ml) x (1 ug7 1000 ng) x (1 mg/ 1000 ug) ] /
1000L)] :
\: : ^ :
[(1468 L) x (1 m3 /
.
0.0009 mg /m3 , :4-.:
' ^
Signatures
Paul Connolly, LCMS Team Leader I'
ajL / ^ ^ L ^ ' ,
yflohn M. Flaherty, Vio6 President
Other Lab Members Contributing to Data James Miller
'
'
'
'
^ .
.
ALL DATA-CONTAINED IN THIS REPORT WAS GENERATED B Y EXYGEN RESEARCH
Page 7 of 7
Table 1. Login Information / Field Data
Sample ID
Exygen . Lab ID
WWK-A-AMSFBLK-E2 A WWK-A-AMSFBLK-E2 B WWK-A-AMSFBLK-E2 C
WWK-A-AMS1-E2A WWK-A-AMS1-E2B WWK-A-AMS1-E2C WWK-A-AMS2-E2 A WWK-A-AMS2-E2 B WWK-A-AMS2-E2 C WWK-A-AMS3-E2 A WWK-A-AMS3-E2 B WWK-A-AMS3-E2 C WWK-A-AMS4-E2 A WWK-A-AMS4-E2 B WWK-A-AMS4-E2 C WWK-A-AMS5-E2 A WWK-A AMS5-E2 B WWK-A-AMS5-E2 C WWK-A-AMS6-E2 A WWK-A-AMS6-E2 B WWK-A AMS6-E2 C
Control Spike A
Control Spike B Control Spike C
L0001308-1 L0001308-2 LOG01308-3 L0001308-4 L0001308-5 L0001308-6 L0001308-7 L0001308-8 L0001308-9 L0001308-10 L0001308-11 L0001308-12 L0001308-13 L0001308-14 L0001308-15 L0001308-16 L0001308-17 L0001308-18 L0001308-19 L0001308-20 L0001308-21 L0001308-22 L0001308-23 L0001308-24
Date Received Description
Air Volume Sampled (L)
11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 : 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03
Frit extract
1 st set beads extract
2nd set beads extract
Frit extract
1st set beads extract
2nd set beads extract
Frit extract
1 st set beads extract
2nd set beads extract
Frit extract
' ,
1st set beads extract
2nd set beads extract
Frit extract
1st set beads extract
2nd set beads extract
Frit extract
1 st set beads extract,
2nd set beads extract
Frit extract
1 st set beads extract
2nd set beads extract
Frit extract ,
1 st set beads extract
2nd Set beads extract
.:.
;
.
,
.
,
.,
0
'... 0
0 ! "
.
'
.1475 1475
. 1475 .
1468
, 1468
1468
1462
1462
1462
1437
1437 1437. ,
:
.
.
1456
M456' '
.
1456
.
.
1422
.
.:.
'
:.
'
,
1422" ,
1422
,": ''0
'"
'
'
,.'0
,
- 0,'-
,'
.'
.
'
.
Table 2. Chain of Custody
Sample ID
WWK-A-AMSFBLK-E2 A WWK-A-AMSFBLK-E2 B WWK-A-AMSFBLK-E2 C
WWK-A-AMS1-E2A WWK-A-AMS1-E2B WWK-A-AMS1-E2C WWK-A-AMS2-E2 A WWK-A-AMS2-E2 B. WWK-A-AMS2-E2 C WWK-A-AMS3-E2 A WWK-A-AMS3-E2 B WWK-A-AMS3-E2 C WWK-A-AMS4-E2 A WWK-A-AMS4-E2 B WWK-A-AMS4-E2 C WWK-A-AMS5-E2 A WWK-A AMS5-E2 B WWK-A-AMS5-E2 C WWK-A-AMS6-E2 A WWK-A-AMS6-E2 B WWK-A AMS6-E2 C
Control Spike A Control Spike B Control Spike C
Date Collected
11/12/03 11/12/03 11/12/03 11/12/03 11/12/0311/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03 11/12/03
NA NA NA
Date Received at Exygen
11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03
.
11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03 11/13/03
Date Extracted by Exygen
Date Analyzed by Exygen
11/20/03 11/20/03
NA 11/20/03 11/20/03
NA 11/20/03 11/20/03
NA 11/20/03 11/20/03
NA 11/20/03 11/20/03
NA 11/20/03 11/20/03
NA 11/20/03 11/20/03
NA
,
11/20/03 11/20/03
NA .
11/20-11/21/03
11/20-11/21/03
NA
11/20-11/21/03
11/20-11/21/03 NA
11/20-11/21/03 11/20-11/21/03
NA
11/20-11/21/03
11/20-11/21/03
'
NA :
11/20-11/21/03
11/20-11/21/03
NA
1,1/20-11/21/03
11/20-11/21/03
NA
11/20-11/21/03 11/20-11/21/03
NA
11/20-11/21/03 11/20-11/21/03
!
NA
,
3058 Research Drive
State College, PA 16801
RESEARCH
Phone:814-272-1039 Fax:814-231-1580
Login #: Project: Project Storage: Submitted By:
L0001308>1,418 P0000419 :;
f" ..
Michael D.Aucoin . :
Status:
Unreceived
Login Type: Started: Date Start: Due Date; Received Date: Received By:
Immediate Receipt of Samples
.. T
' - . -'. .... :
11/14/2003 8:43:13AM
. . ;',
11/28/2003
11/14/2003
AMMERMAN, MARK
Spread Sample:
Label:
Project Title/Type:^Apalysis%PFQj^ri^S^
Login Notes: Conform Notes:
' ;
;
' -
.
Conform COC: Conform Sample: Conform Request:
True True
.True
^0001882 Carton
Packages /Containers
Mail Date / Condition
'
Shipper/_IP
Temp. Control / Temperat
11/13/2003 2:00:14PM Package & Contents. Uncompromised
FEDEX 8363913020070200
RT 0.00
Direction / Handled By
RECEIVED AMMERMAN, MARK
Container #
Gross Weight
C0019829 C0019830 C0019831 C0019B32 C0019833
7.2 g 7.2 g
---------^2-ir
7.2 g 7.2 g
-7:2 g
C0019835 . C0019836
7.2 g, 7.2 g
G001083?---------7^3-
C0019838
7.2 g
C0019839
7.2 g
GQ6W6W----------7 .---2--
q
sj
C0019841
7.2g
C0019842
7.2 g
Wu l^/U r\J C0019844
7.2 y 7.2g
C0019845
7.2g
69849846--------f-s^s-
CO019847
7.2 g
C0019848
7.2g
cno.aaaAs------ 7 2 a
C0019850 C0019851
7.2g 7.2g
----7.2 g
'Niy scellaneous
Item Key None
11/14/2003 Loain.rpt
Container Type
Other
Other
Other
Other
Other
Other
Other
Other
Other
Other
Other
Other
.
Other
Other
.Other
Other
Other
Other
Other
Other
Other
Other
Other
Other
Preservative NONE NONE NONE NONE NONE NONE NONE : NONE NONE NONE NONE NONE NONE NONE NONE ' NONE NONE NONE NONE NONE NONE NONE NONE NONE
!COC
Mfg.J-ot
Description
0056
Report Version: Nov 13 2003 4:51 PM Page 1 of 5
Instance:
R0072755
Sample ID 1301308-0001 _U001308-0002 feeee^see'eeeaL0001308-0004 L0001308-0005 LOOOUOO eee& L0001308-0007 L0001308-0008 L000439&-e999L0001308-0010 L0001308-0011
L0001308-0013 : 10001308-0014
L8ee4388=eW8L0001308-0016 L0001308-0017 10004388^848L0001308-0019
. L0001308-0020 l nmi?n^no?4-
L0001308-0022 L0001308-0023
.
Le
Matrix GAS GAS GAS GAS GAS
GAS. , GAS
GAS GAS GAS GAS GAS GAS GAS - GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS
ogm
Fraction OVS Tubes OVSTubes OVS Tubes OVS Tubes OVS Tubes OVSTubes OVS Tubes OVS Tubes OVS Tubes OVSTubes
OVSTubes OVS Tubes OVS Tubes OVSTubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVSTubes OVS Tubes OVSTubes OVS Tubes OVSTubes OVS Tubes
Samples
Sample WWK-A-AMSFBLK-E2 A WWK-A-AMSFBLK-E2 B WW.-A-AMGrDLK-C2 C WWK-A-AMS1-E2 A WWK-A-AMS1-E2 B
WWK-A-AMS1 1:20 WWK-A-AMS2-E2 A WWK-A-AMS2-E2 B WWKAAMSa 1:20 WWK-A-AMS3-E2 A
,
WWK-A-AMS3-E2 B wwi<"A-AMS3-ea-eWWK-A-AMS4-E2 A WWK-A-AMS4-E2 B WWK-A-AMQ4-E2 C WWK-A-AMS5-E2 A WWK-A-AMS5-E2 B -WWK-A"AMGG-E2 CWWK-A-AMS6-E2 A WWK-A-AMS6-E2 B -WWI^A-AMOG-CJCControl 1 A Control 1 B
.
Centrol 1-8--------
Date Sampled
^Ja C.. s'et-T"i-o.iA_
'
fc>--(-r c, <^ .A t- 8 o^ly,
Date Received 11/13/2003 11/13/2003 11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
11/13/2003
Date Due 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003 11/28/2003
11/14/2003 Login.rpt
0057
Report Version: Nov132003 4:51PM Page 2 of 5
Instance:
R0072755
R0072755
^0001308-0001
Container
C0019829 / Other / NONE
L0001308-0002
Container C0019830/Other/NONE
L0001308-0003
Container C0019831 /Other/NONE
L0001308-0004
Container C0019832 / Other / NONE
L0001308-0005
Container C0019833 / Other / NONE
L0001308-0006
.A Container'. : C0019834 /Other /NONE
L0001308-0007
Container C0019835/Other/NONE
L0001308-0008
Container C0019836 / Other / NONE
L0001308-0009
Container C0019837 / Other / NONE
L0001308-0010
Container C0019838 / Other /NONE
L0001308-0011
Container C0019839 / Other/ NONE
|||001308-0012 11.
Container
11/14/2003 Login.rpt
ogin
Bottles
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
Report Version: Nov 13 2003 4:51PM Page 3 of 5
j05d
instance:
R0072755
R0072755
C0019840 / Other / NONE
^0001308-0013
Container J0019841 /Other / NONE
L0001308-0014
Container C0019842 / Other / NONE
L0001308-0015
Container C0019843 / Other / NONE
L0001308-0016
Container C0019844 / Other / NONE
L0001308-0017
Container C0019845 / Other / NONE
L0001308-0018
Container
(HiC0019846 / Other /NONE
LU001308-0019
Container C0019847 / Other / NONE
L0001308-0020
Container C0019848 / Other / NONE
L0001308-0021
Container C0019849 / Other / NONE
L0001308-0022
Container C0019850 / Other/NONE
L0001308-0023
Container C0019851/Other/NONE
;|j|Q001308-0024
i
Container
C0019852/Other/NONE
11/14/2003 Login.rpt
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
u059
Report Version: Nov 13 2003 4:51 PM Page 4 of 5
Instance:
R0072755
R0072755
11/14/2003 Login.rpt
Report Version: Nov 13 2003 4:51 PM Page 5 of 5
u06u
Instance:
R0072755
R0072755 IIIIII11IIIIIIIIIIIIIIIIIIIIIIIIIIIIII
CHAIN OF CUSTODY/ANALYSIS RE
RESEARCH
Exygen Research Sample Receiving 3117 Research Drive State College, PA 16801, U T: 814.231.8032 F: 814.231.1580 ' exygenresearch.com
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Piease fill out this form completelyto ensure
Project Manager (Name & E-mail Address):
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.
Project Name:
f\-s r
P.O. #:
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LAB USE ONLY
Relinquished by
Date
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////^^7/-7
OTHER INFORMATION L>\m i
Cooler ID # ftoc^L^ Cooler Temp. (C) M
Recfeiv^d by
Date
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Precise Research. ; Proven Results.
Sample "Condition Upon Receipt55 Form
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Protocol#
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