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BIODEGRADATION (BOD/COD) TEST SUBSTANCE Identity:A mixturecontainingperfluorooctanesulfonatweh,ich may alsobe referredto as PFOS, FC-95, or as a component of FC-203A. (1Octanesulfoniaccid)(CAS # 2795-39-3). Remarks: The 3M productionlotnumber was notprovided.The test sample isFC-203A. Currentinformationindicatesitisa mixtureof 1.34% PFOS, 25% diethyleneglycolbutylether,67.85% water,2.66% Sultone foamer, 3% sodium octylsulfate0,.1% sodium laurylsulfatea,nd 0.05% tolyltriazole. The followingsummary applies to a mixture with incompletely characterized concentrations of impuritfes.Data may not accurately reflectthe biodegradabilityof the fluoruchemical component of the test sampie. METHOD: Method: Not noted. Type: Aerobic GLP: No Year completed: 1975 Contacttime: 20 days lnoculum: Source not given. RESULTS TotalOrganicCarbon (TOC): Chemical Oxygen Demand (COD): 121,000mg/L (calculated) 648,000 mg/L BiochemicalOxygen Demand (BOD): 5-Day: 1O-Day: 15-Day: 20-Day: 72,000 mg/L 407,500 mg/L 405,000 mg/L 427,500 mg/L CONCLUSIONS No conclusionsgiven. Submifter: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St. Paul,Minnesota,55133 DATA QUALITY ReliabilitKyJ:imischranking4. Valuesfrom a summary sheetonly. Study lacksdescriptioannd recordsofthemethod followed.The inoculumisnot propedycharacterizedT.here isno characterizatioofnthetestsubstance purityand the studylacksanalyticaclonfirmatioonfthefluorochemical concentratioinnthe solution. REFERENCES The studieswere conducted by the 3M Company, EnvironmentalLaboratory, St.Paul,MN, Lab Request number 2543, 1975. OTHER Lastchanged: 6/26/00 Ref:"'ENVIR.ASSESS. INQ. PRODUCT: qr_te4l.,-,(-,F C -?-a3 + 1 0 I-s PRODUCT ECOLOGICAL ASSESSMENT REQUEST FOR LABORATORY WORK DIVISION LAB REQUEST No. @,$L13 Name: Request Date: ProjectNo.: '7,3 Co(leNo.: Description: Purposeof Tests: REQUESTER Phone No Prob.No. -2=0!OMR@ C-*10 DiiteNceded/:/'?C LABORATORY Date ReceivedSample: Analyst: Date Completed: Hours Spent: y /!9 p PleaseCallRequesterIfDelaysAre Encounte - PHYSICAL & CHEMICAL PROPERTIES HeatofCombustioCnal/G(BTU/Lb.) Density Ash Other FC- 2- WATER POLLUTION PH COD Boob BOD.Ultimate TOC GC Oxygen Uptake DehydrogenasAectivit(yT,rc) Other 9.z'ow g /<54 7CF BIOASSAY SpecifOyrganisamnd Met@od: LEACHATE FROM LEACHING TEST PH COD BOD5 BOO. klitirmite TOC GC OTHER Bioaccuniulation Persistenr,;e DegradationProfJucts Recyclability Burnability Weathering -.PAY 0.7@D I AY!I .--DAY '@eo- 0 -------------- ?to, 0. -TV @oo ig mo4 %-c'r- i O@o/ !PL)6 ,oo 453 7 !92 cop 17 9-715CO 93$%Oo 7,0 6 co 70/coo 41%