Document J3o2192vZE1yL3XV408346ee6
BIODEGRADATION (BOD/COD)
TEST SUBSTANCE
Identity:A mixturecontainingperfluorooctanesulfonatweh;i,chmay alsobe referredtoas PFOS, FC-95, or as a component ofFX-3106. (1Octanesulfoniaccid)(CAS # 2795-39-3).
Remarks: The 3M productionlotnumber was 015G. Thetestsampleis FX-3106, PO# S5233-004, EAI 85548, Sumitomo 3M Japan. Current informationindicatesitisa mixtureof2.31% PFOS, 2.6% diethyleneglycol butylether,83.38% water,10% ethyleneglycol,1.36% Sultonefoamer,0.2% xanthan gum, 0.1% 2-biphenylols,odium salt,tetrahydratea,nd 0.05% benzotdazole.
The followingsummary applies to a mixture with incompletely characterized concentrations of impuddes. Datitmay not accurately reflectthe biodegradabilityof the tluorochomical component of the test sample.
METHOD:
Method: Standard methods. Type: Aerobic GLP: No Year completed: 1985 Contacttime: 20 days lnoculum: Stalesewage, Chemolite.
RESULTS Chemical Oxygen Demand (COD):
220,000 mg/kg 240,000 nig/kg(Replicate)
Carbonaceous-BiochemicalOxygen Demand (BOD):
5-Day:
4,700 mg/kg
10-Day: 63,000 rng/kg
20-Day: 72,000 mg/kg
CONCLUSIONS
No conclusionsgiven.
Submifter: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St. Paul,Minnesota,55133
DATA QUALITY
ReliabilityK:limischranking3. Study lacksdescriptioannd recordsofthe method followed.The inoculumwas notproperlycharacterizedT.here isno charactedzafionofthetestsubstance puritya,nd the studylacksanalytical confirmationofthe amount offluorochemicalproportioninthe solution.
REFERENCES
This studywas conducted by the 3M Company, EnvironmentalLaboratory, St.Paul,MN, Lab Request number C2282,1985.
OTHER
Lastchanged: 6/26/00
11-25-85
ENVIRONMENTAL LABORATORY FINAL REPORT
LAB REQUEST
REQUESTER NAME: EAR/MTE DEPT: 0535 PROJECT NO: 9973010100 DATE RECEIVED: 13-24-85 DESC: FX-3106 LIGHT WATER-ENVIRONMENTAL
NO- C2282 SCREEN
CONTRACT LAB:
CONTRACT.LAB
COST:
0
3M E-L HOURS:
10
EST CHPLT DATE: 11-29-85
DATE COMPLETED: 11-26-85
PO #SS233-004 FOR SUMITOMO 3K EAI 85548*
----------
SAMPLE DATE
CODE
DESCRIPTION
- - - - - - - - - - - - - - - - - - - - - wm -
-----TEST
RESULT
1
FX3106 LOT 0156
BOD-OS (CARBONACEOUS)
4700 MG/KG
BOD-10 (CARBONACEOUS)
63000 MG/KG
BOD-20 (CARRONACEOUS)
12000 MG/KG
COD (DICHROMKTE REFLUX)
220000 MG/KG
FISH ACUTE TEST
COMPLETE
2
DUP OF #1
COD (DICHROMATE REFLUX)
240000 MG/KG
CONTRACT LAB SUBMITTED BY
DATED -@-------
tonmental LaboratoryBOD Work Sheet ,iksC,ontrols,and Standards
Lab Req. No.im-
A"t
Y" asource
cotestarted S@W Corcefflmtlon
mmftmion inhibtt(Cwone.
DistilleVdV#lff
N
Nonsooded Ollutlai-Wsater Blank
Bottlet4o.
Initi0a.l0. (Al)
BOD Run No. I,-
Analyst IncubatorTemp.
Date
Day BOD
Twnp.
Readlngs
Dat/e /(o.
Des
Temp.
Pfe"nt0.0. (At)
0.0.Dopletion (At.As)
Average 0.0. Depletion
J3 C)
0.19
Seeded Dilutio-nVfatorBlank(optlonaq
Bottlemm
q
InitiDa.lO. (cl)
I
Prmwnt 0.0. (Cf)
C,
c,
0.0.Depletion (Cs.CO)
0
-
0
Avw"o D.O. Do lotion (i.-U.)
o,?-I-
Seed Controls ""I* No.
Sample Size
InitiaDl.O.
Pre"nt 0.0.
D.O. Depletion
-73 II @ 7q'3
yo_
(0
yo
V.
CW,wose-Glutami-A.cidStandard
BottleNo.
Smmpie Size
InitiaDl.O. (DI)
V3-
Present
-t.
7 c,' vf
TotaDl.O. lotion Dt)
)L :T.lo
DeTpoISettLloDous ard
c,17
Day
21 C
Paussium HydrcmlePnhthalatSetandard(aptionel)
BottleNo.
Sample SL=
lntiialD.O. (D.)
Prmwnt D.O.
TotalD.O. DToopietlDouno - 506 Day
D(oeletion
Standard
1
Day BOD
-2.103
Average Day
BOID
-vironmeiitLaalborstory aD Work Shoot -Ssmples
Lab Req.No.p-
An@"
Nit
nhibftConiL
ampwO"Crwo;-
am* 810%d
-
I //-/ - I?-:r-
1-7
600 Run No.No.
Analyst
3M
Day BOD Reading&
a
lniuaDlIILMM INIUWDilutioFiasaW
ofSampledilutetdo
mi withDiwater
(Dilutifoanctor I ifundiluted)
Bottle cope.of No. san*b,
SUaWnn"
lnilim p @l D.O.(Do) D.O.(Do)
TohdD.O. DgftdonDue c;rlotion -FaAMEMMS
-Day
Do)
CD-D'ST-
BOD
BOD
C)
10q
TO -;77
C,.
13,
y
cc
6,0391
oo 3 c.@
cl
o - o 71ir
f Li
-C,-o
o
3 -2 yi- o
Note: 1. Cone. Concentrati of sample (mVi 045P
BOO buttloo.
tedsample added to 600 Bottle.
2. Samplosialumi ;p 9 ample ordilu
3. Samples with% :0,1 and
tocalculateaverage 800.
Comments
.,nment.iLlaboratoryBOD Work Sheet .dks,Conti-olsa,nd Standards
,119M-A-PWO
Lab Req. No.o-
Y" & acum
c
We &mod
I //-/-t-@r
Sew owomtration
mmfwatim kwwbrtwe.
Dfttiliod
('Yl N
Nonseeded Dllub)n -Water Blank
800 Run No.P.
AnWyet InambomTonp.
- . Day SOD Reading$
Date
Dam
TOW
ow
TW^
.2o.3
Some N4L
bOtW D.O. (A,)
2.3
C)
Pr"ont 0.0. (As)
D.O. Depletion (Ai-A4
)r
A"mp D.O. De".tion (As.14
c. 38
Seeded Diludon-lnaterBlank(optionaq
notueNO.
wiw 0.0. (CI)
Pr"ont0.0. (Ca)
D.Oic!!PCI.O)U"
Avwsp 0.0. D"W"n
113
Smd ConWe Boni@No.
samplesin
lniuaDi.O. (Bi)
c-73
Pr"ont0.0.
0.0.Do ton
to
./o
0
Okico"-GlutomkA-cidStandwd
SolUe No.
I;GmpSiien Initia0l.0.
V5
Pfo"nt
Patmium Hydrog-enPhthalateStandard(optionso lot"*No. SampleSL= Initi0a.l0. Pro"nt0.0.
Tota0l.0. oTowso= As oeeletion
Day Boo
Avorqp Day
LBJ6
7-
211
cq
Total0.0. D@oiilotnio
Day
'T*:@*'U'OnndaDMBUOO
Avimgo D"
- Boo
.onmentalLaboratory
.00Work Shoot -Samples
dml@M-A-PW-
Lab Req.Note-
,%k'Wiefk,WdWoroConiL
LL - Y.2 @i /,O,/Sa
-/ /71-
L/
-
DSM ll&,M
800 Run No.o-
An&"
Day SOD Readings
I/
lnitDwilittion lnidDeUlutle-,%
ofSampdlieluttoed
miwitDhiwater
(DiluIt&iWoonr1Ifundilutoo
BottioCooOlfL No. smvb.
Initial
as"hw*
LO. (D-)
pro"ni ILO.(Do)
-z-z
C).
;Z. 41o
lo
-6-60'rqL-,T-O 7.-.c@
70 -f,Yo . --
17.1 15,6391 q oc) z-
Tot0m.0. OgftUDaune
Do
to $Moab
(IL-04
(004
C,
-77
17
Day ROD
;ey SOD
I
r e.,@wev
L170
1'6
R.-@ro :ric.C;
Note.1. Conc. Concontratiofsample(mwl
600 bott[*L
2. Sampi4Siinia mi; gp "mple ordilmuitges@dampleaddedto600 Wftlo.
3. Samphewith% 2-0o,W1 DDSt2 usedtocalculaatveerag6e00.
Comments
.snmenialLaboratoryBOD Work Shoot dks,Conlrols,and Standards
IOM-A-PWO
LabReq.No.0-
Analyst
yoApo
umftuom lnm tw Cold.
C
Daig gtwted
//-
BOW Concmtmtion
Of C' tiIWlledYWON
NOngeoWWDilutiWo&ntSBrlank
-----------------
800RunNo.0-
Analyst gnrugaw Tornp.
Dais
3M
DDaa@YyBODD RRieiaadiinnggiis
Des
Bo r
Due
T&IW
BottNlOe.
InitiDa.lO. (Ai)
PrftontD.O. (As)
0.0.DopkMm (As-As)
AwWop MO. Do IoUon
C)
SeededDiluti-olnvateBrlan(koption&Q
ooftwNO.
UdUalD.O. (Cs)
PrftontD.O. (Cm) izC)
0
@)OI@ LC)
----------------0.0.Depletion (Cl-Co)
Avwap 0.0. Do"tion
fteCdonimis BottlNeo.
?0
SampleSin
ini0t.i0a.l Pro"niD.0
0, D.O.D@Volion
to
Okico-GsleutleAciSdtand&W
notthNo.
&unpiosin
Ini0t.i0a.l Pro"nt (Di) 0.0.(Do)
7 TotalD.O. Depletion
C,C) DTeOpSlteatnidoDanured
20 Boo D sy BOO !Dy
Ll
1?1
Li
14.1/
Pobwum HydmgoiiPhthalatSetandar(doptionad NO. Se.,nplSobe initiDa.lO. Pro"ntD.O. (Do)
TOIW 0.0. 0,?Iotion
DTeopletioDnue
Standard
1(7
1 el
2 2,,--
BOD Day
so,
Averap BOD Day
ilronmairitLaalboratory ,00 Work Sh"t -Samples
Lab Req.No.imC2
WalmiCcwim
6-4o"lio-r@
$term
800 Run No.w-
Z (,)--
A"Yu
..@...3M.
. Day SO[) Reading*
lrdtwDilution InitiOalllutkwFieew
ofSampledilutetdo
miwithDiwater
(Dilutifoanctora I Itundilutoo
Bottle Conr-of lkwfpw
"aM PWIW
Initial
plow
MMM4)
M&04
/ol
50
70
?010
6,639) oc)-
ToldD.O. D"Iotim
(01 Do)
D"W*Uonova ZIC, TO(S0w0a4nk - DOD 1ow
-A1n0-o-w, .D" MOD
3 '3 (2 0,T 3v) ry6oO"C C";v
q, 7y
all
a 3?-.lo
600 Note:1.Ccmc.:Czoncentmtif ampl(eMVI
botti".
040 2.SampiSti,znilmi;N0 O=ploordilutseadmpla*ddetdo600Bottle.
3.Sampicweit0h,NOIWW 006-12usetdocalculeavteeme130D.
Comnwnts