Document J3Gpo4Q9ELyBdn7q9jZ88okNa

5AnSaollyutmibciaalServices- Created with AnalyspitReporter Printed: 180212010 4 02.00 PM Project Data File E0v2a1n7's10PrSoajemctpslPeFsCsshwoirf RIenssutrlutmTeanbtleName __ AGP2)15701000shocrto BET TAS [SampleName Ra1000664.03 [`Acqmuisitiion MsethocdJ|e2Pir/F1C8/ho2i01n0en5l.e39x.vS3d0haAoimrM sr|SWDiaelmiupgtilnoetniTFoyavpcatenorumeJ[7[ o0o0Unknown||| Results Summary A Ramee | istame | saves | ABER praos | CHS | igi Praat [proent | 13CPFBA | vara| 5463400 van | 126 (120)| [sssmm| 11064000 ammo we |we| | = worms | sooo |awuz| mmm | wo| we | PrHxa 1 13C-PFHXA | 6199200 |5.23(5.31) 14747000 | 24.40 [Propat| 13cPrroa | 6196200 | 610620)| sedss00 25.00 No No | PFHxS 1 { 180-PFHS 3800700 | 6.22 (6.32) 28400000 26.00 No S_180-PFHS 13C-PFDA 4384200 | 6.21 31) 3800700 1.07 S13C-PFDA | 13CPFDA | 4384200 | 7.50 (165)| 4384200 1.00 No { [ &N 0 FoEoh le zz Page 137 of 169 22 [Sma AnalyticalServices' weswmmary PCrraeasted0vith2Ana0lysP01R2&p0o00rtiert [[apsrsos [[rPrmiosn s [emormn [[sepaemw|| wwoomm ||vwoo ||wcoawwmw|| wvww || [|ommeen[|mmoemwo|| wwoo||ezweawe|| vvwe || [sme |wom |vo |vam|_| Page13801 169 22s 8 lamba AnalyticalServices" PrCirnteeadted18w/i0t2h1A20n1a0.l40y..03R3e.p0o0rtPeMr QuanStita--tivePeakReviT ew w iol iz= wl a oB2a1sP3e0ir/n1ae6o8]M0is0saed | oB2a1s17e3.i00n.1e97s720Mi0sased Cl a3E I= i3 -- -i = KQi00066405 TF == Joi zl | Ba2sP6e3rli0Pn2ee1As90Mi0sased | oB3a1s15e3l0.n2Pe7cF00TvAsDsaed ol c=l I= Ih oBa2s0e9pl0ri8ee0c.sT0Mi0sased | oB4a0s13e80l0/n-1e0Pc3FM0HiSs0saed | oB3a1s3e0Rl2nH6e8Ac.10Mi0sased | Ba3s115i30Cn/-g2P1Fo0H0MxiADsased il 2 i iE "1 = a 2 36P3r0H1O6A9T0 08 oBaseline Missed | 13135C0.2P7F0T0A0a cBaseineo Missed | 2p9r90i180.008 Saseine Misses | 4031.6070037.0SDa Basen o Missed :: 3 E :7 3 2 : 3 oBs4Ss0e_3.l10i81n01e0-3MF.Fi0HsDSsaed | oB5a11s3e5Cl0-n4Pe7cF0hO0iAsbsaed | Ba5sS1e_5l1.i03n4Ce7.0oP.MF0iDasAsed | Ba5s11i530nC4g-7P0F0OMAiDsaeed 0 Before O After Page 139 f 168 226 LS RColoumtbiaa services: PrCinrteead:ted18w0i2th22A0na1l0y4s:P0R2b:p0o0rtPeMr TeooneiRraEtEiopoe CroenSfoiap rmmeatip on en--e--K-- Q100r0-- r664--- 0e3 m-- p m --m -- ow Tw = = i72] | io-=n | E b - e EbeZs wb = --| Re | SEA c21B3a0Ps1F1eE6cAl32M0iis0nsaeed | 2630P1F2P1e9A02 Da cBaseline cMissed | 200.p0r19E9S.02 Da BaselciMinsseed | 31P3F0H/I1A12800a Baselc Miisnseed Wrong Pea Wrong Peak Wrong Peak Wrong Peak T on ii= b5ee t4= pSio = Teenie - >J A -t Ba3s63e,lP0iF1n3He1P9A.M02isDsaed | Ba30s9P.R0e1H9lIc9.S0iM2iDnsaseed | Bas5Se1_l51i.n30eC4.o7PM0Fi0Ds0Asaeq | NA BaseloMiisnseed = Wrong Peak Wrong Peak Wrong Peak Wong Peak NB. PFBA and PFPeA do nol Fave quallyng on ransiions. O Before OJ After Page 140of 169 25 Columbia 4 Analytical Services PrCinrteead:ted18w/i0t2h1A2n0a10ly3:2R4e:p0o0rtPeMr Project Data File Ewar's ProjectsPFCs 021710iSamplesLong wif InRessturlutmTeanbtleName __ 02171000ng AP 5000 1b 100101] =oo] DA [SampleName Tiai000654.04 2/1772010 11:02:27 PM PFChinctextong dam UinjectionVial [48 InjectionVolume [5] Sample Type [DilationFactor 5.00 | [WeighttoVowme[000 | Results Summary {AFnalyytePeak [shame [isan FaaiyrleyRT| Anitree oT Caaic. Scoonne Modified? 13cpron | 34s4200 | 126(138|) asazso0 26500 No PENAT TICPFNA | 2401200 | 20820)| 11713000 | 44900 No PFOS 1 13C-PFOS | 8020900| 2.13(208)| 39909000 46.500 No PFOA 1 PRU 1 PFOS 1 PFOOA 1 PETA Y | 13crron | 2emm600 [aison| asesio0 | iran No 13C-PFUNA|115010| 394605)| 2760000 22.900 No 13CPFOS | 8020900| 3.04 207) | 6762300 No 13C-PFD0A| 163200 |as57(458|) tessio0 | 17.100 | No 513608|) 8s2130 19C-PFOA| 163260 | 557(551) | 741830 590 | No | No +hl0 ZF . yr Page 14201 170 226 Login oS Analytical Services wesewmay Sroesren [rsoesme motes [ermoes frroosmz cron [rss mam| seo | we |omwm|v | Toowweam|| 0em [[owwe[|oomoem| |_|| | own[| wwe | | [Toaowmweeornm|||wweoem|||eww |||oowwmoeemmn|| | vvww||| [|oevmuum| wwmwe|| wwo||omoowmen|| _wm | vem |ame| we|oem| vw | 4CAonlaulymtbiciaal Services Created with Analy Reporter Printed: 18/02/2010 3:24:00 PM TT Quantitative Peak Review 7% - ie BY = 7 KQ1000664-04 i i= GBa1s2e.Pi0Fn1O6e9Ac.T0Mi0sased| oB7as.1e30iC3n-e7PcF2OM0Ais0sed vane 3 TE | cB4a6s2ePl0En4Ne1cA901Mi0sased | ines oB4a6s1e83i0Cn4-e2Po3F0MNAsDsaed 7 lic eg i==l ioa iz= fo"| oBa4s9el9Pi0rn8eO0S0TM0i8ssed | = oBa15s03e3Cl.-0nP8e0Fc.O0MSi0s8sed nie | cB5o1s2eP.lF0n4De6cA51M0i0s8sed | FE c B5a1s1e53l0iC4n-e7Po0F0OMAiDsased : liza io i= i IE % 1 wb pe 563P0F5U1R9A0T 0a Baseline Missed| 5615360.2P7F0U0nA0a Baselinec Missed | 599p0r8o0S.T008 cBaselnec Missed | 50133005.8pF030S08 Baselinec Missed THN ian ta re 3i4 ii 7 iHi =I ia 7 wl oi wl JA = oBa1s3e.P0iF/nO5eO6oA8.M10is0s8ed | oB16a1s35eC0l/-n1P6eF9c.Db0OiA0ssaed | cBa6s3eP.l0Fn6Te1cA9h10i0ssaed | oB6as11e35iC0n-e/PF1oDM60i9DAs0ased i= i Zz 1 i cB7a1se3Pl.Fi0Tn6ee6cA810Mi0sased | o B6a1s15e3l0Ci/-n1eP6F9D0M0iA0sased O Before OJ After Page 144.1 170 28 LSS Analytical Services BCriweitwhAanalitysbReapaovaridter ee rm Segoe lon Ratio Confirmation =2 I TE eee KQ1000664-04 - = il l= ol ad : iE | [= | STAT| 41P3F01O3A6920 0a Baseline oMsced | 46P3r02190 0a Bssoinec Missed | 4p59r.o09S820 Da Baselo Miisnseed | 512P0r26O92R000 cBaselc Miisnseed = Wrong Peak =Wiong Peak WrongPeak Wrong Peak cl is | | I se ff Tl ad 7] fl Te A EN eer re be wl wt Ba5s6e2lP.iR0n2Ue6T9MA.a20 c0aed | cBa5s9Po9Fi.nO0eS9c02.M0is0sed | oB6a1s3eP.0lF1nD1e6Oc9A.M20is0saed | cB6a63.sP0F1e6T9oA.i2Min0saseed Wrong Peak =Wiong Peak Wrong Peak Wrong Peak 7 i-- 71P3E0T1oR62900a BasWeiloinneg PMeiasksed 0 Before O After Page 145.0f 170 20 4CAnoalluymtibciaal Services Grated vin AnapsReprer Printed: 18/02/2010 4:02:00 PM PORnroesajcreoucnFmtie.Tleanbtletame OG4E6wzaa1irn5rr'0isr0ooP0mrcooajneimciptssa\sPFmCos.nit Sample Name KSGralGGte0e8 [AAccaquuiissittioonnDeattheed|| F270e2070t56e53csaomF [nectonvia {a6 [ecE tioT nVans[5 --| |[DWieiosnhtFtaocvtoourme[1J 00 oo]| T--RehsurltseSu[mmsarmy e[isan [RERRRTETT Proat Ticeren | wo |12502m| moaseo || Gau cone 1960 | wear| FFrrroesatt | ommes|ssmoonn |4[rasoezceno||v sewne ||owo em|| wwoo Prin PFHXA 1 || ora| 13C-PFHXA | mo 6081700 | [ees| 5.22 (5.31) emo 14167000 | Frist sors | sso [sea| awn | [sworrs | nceron| ssw [sme| saw | S_13C-PFDA 13C-PFDA 4128300 |7.50(7.65) 4128300 am23.90 |wNe o ae " tm | we 1.00 | No. a0 7 ule 1! Page ator 1m 20 AnalyticalServices Created with AnalysPRborter wesommay [AnalytePeak Name bran: rez RT (ExpRT) EE [ERED sam RatioConfirms = IB [ms een|e |e|amam| w| [sermt omen|om| |own| 8 SAnoalluymtibciaal Services Created with Analy1R1eporter Printed: 18/02/2010 40200 PM Quantitative Peak Review =7 = T= lif.1 cl hs: KQ1000664-04 - TE 7 Ll - i=- il 2130P/F1B69A.T0 Da oBaseinecMissed | 211730C1-P7F2B0A08 oBaselinecMssed | 263P0F1P2e1A90| Da oBaseinecMissed | 311530C2-7P0F0HA0a Baseline o Missed HY alto geas us = sage i] i: I= i oBa2s0e0Pl.nr0ee60sc0TMiDsased | Ba4s10e83l00i-1n1eP0cF3H0MSi0sased | 313PE0H2X6A91008 cBaseinec Missed | o B3a1s1e53l0Ci2-neP7F0cF0MiiADsased li an wong +o pe i== lio bizd i 53 AAA J A te RL oB3a6s3eP.l0F/nH1ep6A9c.10Mi0sased| oBa3s11e53l0Cie-2cP7F0F0KMiA0sased | cBa3s9eP9iR.i0Hn8Xe0Sc0|Mi0sased | oBa4s0e13l80i0/n-1eP0F3H0SM.iDsased gp ty tog agg Pea 3 i oo I i- iL=oi i ul i - a _ 4S0_3.108100.3F.F0H0Sa cBaseline cMissed | 511530C4-7P0F0DA0a ocBaselineoMissed | $S1_51.30C4-7F0F0D0Aa Baseline Missed | 511530C4-7P0F0OADa Baseline o Missed 0 Before O After Page 143of 169 222 5 GAlnamlyttiiceal ServicesTM PrCirneteadte1d8w0i2th2A0n1a0l4y0P2e0o0rePMr P Ton Ratio Confirmation B KQ10h 00664-y 04 ------ f-iilT | =| cl--w ioa | LI= seL o g- ] T= eis ch21a3Ps0F1eE6A9c20as0aed | 2 Wiong Peak B2o6s3Pei0En2Pe1e6cA20V0isaes | ca2s5e0PiF1nB9S9M20i0sased| o S3as1ePl3Ri0nHeI1A12M90is.ased rong peak Wiong Peak Wong Peak FrS-- = - : Lo I I| [J J Fo lt i| iste ste ba56sP3iF0nH3P1MA020a0s8ed | Wrong Peak oBs3s9cPi6Fn0HeG/S0M2iDsased | = WongPeak oB5aS1s_e51i03n4Ce.7cP0F0MDi0As8sed | =Wiong Peak NA SaWseiloineg PMeiasksed 5 FFBA and PFPA Go nol have Qualyng on Tamsions 0 Before OJ After page 144of 169 2 Columbia 4 Analytical Services PrCinrteeadt:ed18wi0t2h2A0n1a0ly3:.2H4.d0o0nPeMr DPraotjaecFtile GE2v1a7n1s0SParmopelceisotPornCgs i InRessturlutmTeanbtleName__ A0P2I1751000000ng 30 Sample Name CkRa10I088T4.1 [Acauisiionbate P7eG2i0in1c0i1oi0o3n5g4d3aPmH ion Vil 45 |r SampleType E -- |WeighttoVolume [500] (ET re | we [EE wen Results Summary Bnatyte Peak Tae AT ie ane : PFOA 1c3CrPFnOA|| z4454w200 | [124z(1e.3n6)|| 4w21w08e00 | _18w.w70o0 | No | [ror vero| wore [arrom| oem o won| orron| moe [aman| somo ras PTFrUon1 [roms PrTeAT vermou me[sve vows | wm || eTarCrnrUN|A| s125e630 | 3s91e(e60n0)|| oaze00 26000 wNo l [oro | ooo [asm| wows |wom| we| 15cPFO0A | tesa |ssTsh|s|e team| Ne A = Zcelte Page 13001170 2 Loghmis AnalyticalServices STR Created with Analysp porter rCsSWOmary [mre rn |r ge [roeesrmon avmwa || mwomn|| wweo||omre ||| erovse T[oammaann||ow+e ||wwee|[oomweomm||wve|| [eros |ama |wm | we|oman| | [[crooowrs [sswoamm ||oawne||wwoo[omws| || | [rconsco [Twaamreess ||oowwen|| wwee ||oommaorm|| vm]| [rrmose T[osweemr ||aoownn||oew ||oowmeesm|| ooww || 235 4 Columbia AnalyticalServices CrweihAanalty Kepordter Printed: 18/02/2010 3:24:00 PM 1 A | A Quantitative Peak ReviCew RT Li i | | - FI = 3 KQ1000664-01 iA1 A i i 2 A Ba4s1e3lP.i0Fn1eO6Ao3M.1i0ssaed | Ba4s11e3l7Ci0n-3eP7F2O0hAi0s8sed | oB4a6s3e.Pl0En4N1e9cA.01Mi0s0sed | oB4a6s81e.3i0Cn4-o2P3oF.N0MAiDsased a 2 lias loge Ei= A i| o- A i = | A i A cBa4s3e9P.l0nF/eO2Sc0.1M0i0sased| oBa5s01e33l.Cn0-e1P0cF0OMS0isased | oB5a1s3e,Pi0Fn1D6e5Ac.10Mi0sased | oBa5s1e15l.3i0Cn4-o7P00F.O0MAiDsased xl i = = = i= cl i ne Bl 1 3 oB5a6s3eP,lE0n5Ue1R9Ac.10Mi0sased | oBa58s15e3.lC0i-2nP7e0Fc.U0MRiA0sased | Cline, longgeas B5as9e9Pl.iF0nDe2cS001MiDsased | Cline, Ba5s01e33l.iCn0-e1P0-F0OMSiDsased Wag pen A i i- i on i| 1 1 A 1 _ oB5a1s3ePl0Fi/Dn5Oe6Ac910Mi0sased | oB6a1s15e3.0lC1-n1Pe6Fc3D.M0OiAsDsaed | cB5a6s3eP.i0Fn6Te15Ac.T0Mi0sased | oB5a1s15o3.i0C/n-1eP6F5o.D0M0iADsased = i gry TM ---- Ca c B7a1s3eP.lF0in6Te6E9A<.10Mi0sased | Ba5s1e1l53i.Cn0-e/P1F6DM09i0A.sa0sed O Before O After Page 13201170 236 8 lumpia AnalyticalServices" Crewin AsnatsSeqgodter Printed: 18/02/2010 3:24:0 PM H EE EE, lo n Ratio = xConfir ma ti 7on ER = = KQ1000664-01 El : ol li TAF i -- e413ee0r8i8e0a00e rong Pear |<4s6e5s0os2irs1i8co0i0n8sed | cB1m5e8ei0rn9oa0sc0?s08a | oS5a1sa3ei0n2re8co00i0s8ed wong Pon tong Peas rons Pea iLd 3 r I|nee Ef; ae = fT: te sal I 56o30r2n89200 566v0e9s52Da 613p0r1o8ai52008 = casP0e1r6i8z0 0a eSoenstpeeake | cowmeoinngcMPueasted | Biasosinnse oPaeskes | oBaisoeinnsecpMeiasksed Ty i o7B13Paarnseeoeids2Mionsaseed rons Poa O Before O After Page 13301 170 27 -- 4 Analytical Services rcosets ssneartl FTMproeeoaamtntaIs [SameleName CTT E oaSn rears -- TT -- Tiaro006e2-01 [injectionVolumeTs 7 2P/r1C8K/n2e01t0ex5:s2h0o:r25dAaMm [DSiawmtploenFTaycpteor |100 | Results Summary ant rene [wen [RENE avaemes Peron Frost | ormon| en | woe| som [smaen| [ames| emer | maw | PHA 1 Prvs 1 scr| Tm [srs om | sae | 13C-PFHxA| 7118300 | 5.24(5.31) | 14328000 100PFHS | aovsn0 | 623650| ame | [GORE ean ww | veo | we we | | ~ 2050 No 1730 No sneer S_180-PFHS | cron| 13C-PFDA mn 4426800|| soem| s23631) wm 4033900 | to1.13 | Nwoe |{ A,x 77sZz l w pap 20000 LlAn@aulymtbiicaalServices: PrCinrteeadt:ed18w1it0h22A0n1a0l4y:t02:p0o0rPteMr wCSummary [PFrroawzs [rroomans [[orsmosrrsen [srormmn | stsaonma|| weomm || Nwee||tmoe o||avwem s || [asammoo||vwarseen|| ea||swnooow||_vw || [mwumm||wwowrew||wa||wsoowsm|| _ve | [sme |rom | wo|wmosm|v] Page 130.f 169 20 8 Solumbia AnalyticalServicesTM Quantitative Peak Review =- = z3 =| i 3 Created with Analyst1Re9porter Printed: 1810212010 4:02:00 PM KQ1000664-01 == Ey sm (et ii 2130P/F1B6A910 Da 21137C.-01P7F2B0A0a 263P0E2P1E9R01 Da 31135C0-P2F7HK00A0a cBaselinoc Missed | c Baseline Missed | cBaselinecMssed | c Baseline Missed * Aas I] z=l 5 | o. i i ix 2Tam - 209P0R8B0S0|02 40138001-0PF3H0S08 313PR0H2I6A90| 08 311530C-2P7F0H0XADa --cBascWianenMaissed | ~c~ BasewluingepceMaissed | Bi aselp ine: Missed | cBaseolinnegc MiPeassed ,2 - - I Rea}| I| i=J |= 363P0F/H1O6A910 0a 311530C/-2P7F0H0XADa 309P.F0H/X8S001Da 40138001-1P0F3H0SDa ceBalselnfeeaMissed | LcBnaselineoMissed | sBamsheline oMissed | BaselineWaoggMoinssed LZ Eo Lo : )= If| Ih uf 1]- 4S03_.108/010.3P.F0HDSa 511530C4-7P0F0OADa 5S1_51034C-7F0F0O0A2 5151.30C/4-7P0F.O0ADa oBaseline Missed | oBaselinec Missed | Baseline oMissed | c Baseinec Missed 0 Before O After Page 1310f 169 200 Columbia Le services: PrCinrteead:ted18i0t2h12A0n1a0ly4:0A2p.o0r0tPeAr i | i= | lonSTRatio Confirmation = of bobyf - pr 7 = KQ1000664-01 i "|lodei | iI== ls 213,P0F1B88A.Z0 0a 2630P1F2PE1A920 Da 205p.r0e9s902 0a 313P.F01H1G92.A00a BasWerloinnegcPMeiasksed | oBaseWlrionneg PMeisksed | cBaseWliionnegcPMeissksed| c BasWelrionnegc PMeiasksed Tew === icf f- = ! Fee-s 2 Tope 363E.0H3D19A.02 Da BaseloMiisnseed | 30P9.F0H9A9S020a oBaselinecMissed | 5S1_1530C4P7FO0DA0a oBaselne Missed | NA oBaseolMiisnseed Wrong Peak Wrong Peak Wrong Peak Wrong Peak NG PBA and PFPeA do nol have quallying on Fansiions 0 Before O After Page 132.0 169 201 5Antalymtipcal Services" PrCinrteead:ted18w0it2h22A0na1l0yd3t:2f4d:p0o0rtPeMr PDraotjaecFtle EGv2a1n7'1s0:PSOaRmpClIeEsPLFoCngS wif InRessturlutmTeanbtleName __ PG2|1751000l0ong rb [Sample Name--TKaTrroeoeoO6U64O02E ``nAAjcceqqucuiiissoiinttiiVooinnalDWaetteho[d|P6Fhneioxcongdam [injectionvorme [5 |[WDeiilgtomntFoavcotowrme[100000 [ARneaEsiusletPseakSum|marny m | nen nate RT Er Gate Gone PFOA1 | "iscoron | asooeon| 125139)| sz82700 wo | Pra Tchr | zoo | 207@on| sso | 20am | [Prost | mceros | som |2r0@os| remo | teow | T[F eFrruor tn| omo| 8rrcrwruomn | rao Siem| | ssson| sme | siamo reo [ros soros| sown an PFOOA 1 13C-PFO0A |183|845814550)| 1852500 17.000 PFTAT 13CPFDOA| 183610 | 512(506) | 1273900 20.400 13CPFOO|A 183610 | 558.(551) | 997460 21300 | || No | No me | wo | ~ No No No Ee Eo Page134.0f 170 22 AnalyticalServices Created with Analyt-A8porter RCsSummary ferro rs [[poooner [[rsoosesmn [sroonrses [poms rroows:s [rms [mreew||wow |owra|[ maw| ow vemoram||wownn|| wwoo |oomons |||| [Jaomweem||svw || wvo[|oomoomn|| ow|] |zen|www|e oman|e sowom|om | we |oom| | aun| oon| |omen|ow | omen | we |e omew|ow Columbia LS Rote services: PrCinrteead:ted18i/t0h2/A2n0a1l0ys3:p2R4E:g0a0riPeMr Quantitative Peak Review -7 J7 i1 H-- KQ1000664-02 == Eg El= 7 io7 i2 413P01F1O6A901 0a Baseline c Missed | 41173.C0-3P7F2O0A0a Baseline Missed | 463P0/R4N1A8T0 Da oBaselnec Missed | 46183.C4-2P3F0NADa Baseline c Missed hg . saben "one cons peas i==) i| i: 1 ilCl 459P.0F/O2S0.100a 50133.0C/-8P0F.0OS0a 512.P0F14D6A6.10 0 511530C4-7P0F0OADa CBausaeceMlisnseed | Baselianeg Missed | "oBaseliannegcMipesn sed | cBMaasnegooleMiissnseed A <= - : i =I Ih i z "l ul a - 563P,0F/U5R1A0.10 0a 56153.C0-27P0F.U0RA0a 599P.F0D80S010a 50133,0C/-8P0F.0OSDa Baseline Missed | oBaselinecMssed | oBaseinecMissed | Baseline c Missed i i. i| i pl A p - - 613P0F/D5O6A910 Da 511530C1-1P6F9D0O0Aa 663P0E/6T1A810 0a 611530C-1P6F9D0OADa oBsselne oMissed | oBaselnecMissed | oBaselinec Missed | c Baselineo Missed = i = 713.0P0F6T6e0A.T0 0a oBaseine o Missed =i i AL 61135C0-/PF1D6D8DA0a | 0 Baseline Missed 0 Before O After Page 136 of 170 204 8 umbia AnalyticalServicesTM PrCinrteead:ted18w/i0t2h/A2n0a1l0yd3t:-2R4.p0o0rPtMer fon Ratio Confirmation TT = KQ1000664-02 : = iE iq afr "A uf ipi _--_-- 4130P1F3O6A920 Da 463P0E1N21A92008 499P,R0O9S92.00 513P.0F1D22A69D.0a oBasWerlonnegcPMeiasksed | oBasWeloinngecPMeiasksed | BasWerlionnegCPMeiasksed | c B<asWeloinnegc PMeiasksed Tl J = TT] i 4 iol ld ef 563P01F2U6A902 Da 599.P01F9O9S.20 Da 6130P/F1D6o9A02Da 663P.F0T/I1A629D.a0 c BasWerlionneg PMeiasksed | BaseWlrionnegcPeMaisksed | cBa<sWerloinngecPMeiasksed | cBaseWlrionnegoPeMaiks.sed - io 4 - 71P3F0Te1A62900a BasWerlionnegPMeiasksed O Before O After Page 137of 170 2s 8AnSaollytuimciaalServices" PrCinrteead:ted18v/i0t2h/A2n0a1l0y42E:o0r0tPeMr DPraotjaecFtile 0E2wa1n7'1s0SParmopjleecsiSshPorrCts iff Result Table 021710hor6tb instrument Name __API 5000 [[SAacmqupilseitNioanbmaete |K2a/1r180o2Co0J o10ss5o -s2E25P5u 7AAT I SampleType Union| Dion Factor [100 | injectionVial [|46WeignttovoumeJoo | Results Summary [Rnaamieyeie Peak [tame[waa R[aReATRT|| anprea esnseas || C3GuClolne | wednes =X T3CPFBA | 6053100 | 126(127|) 12880000 nN pres 1 180.PFHS 1020)|amo| 1770 No | PFHXA 1 13C-PFHXA| 7357000 | 5.24 (5.31) [errpat 13CPFHA| 7357000 | 613629)| [Pr1eis| 180rrs | 4oa4700 | 623602)| S_1BO-PFHS | 13CPFDA| 4520200 |623(631)| SIICPFOA | 13GPFDA| 4520200| 7.51 (768)| 14912000 5578000 21886000 4044700 4520200 20.60 i 2150 1790 No. No No | No Kpie Zs2gl 24! Page 133 of 169 26 -- AnalyticalServices" mm CrweithAanalytBeepordter IRC Summary ere |ms | n| [rs oom[wow| we|owen| r[essos n osmeonm||wwew|| owwe |owwomeann||ee]| 5 uAnmalbytiicaalServices PrCinrteeadt:ed18w/i0t2h/A2n0a1l0y4s0PE2p0o0rPteMr Quantitative Peak Review A " 7 7 IE KQ1000664-02 7 7% i i i i| - ul ot | B2a1s3e.l0Pi1Fn6eB9A.10MiDsased | c B2a7s1e.3l0iCn1-e7PoF2iB0As0saed | 263P0F2P1e8A0102 oBaselnec Missed | Ba3se11l35iCn-0eP2Fc7HKM00iAs0ased /= Iii es Hl | A] pres 7 A] 180-PFHS PPG 1 ~ B2as0e9li0n6e0M0i0s2sed nog ea | B4a0s3el0i1n0e3c.M0i0sased | oB3as1e3i0n2e690Mi0s8sed | EE uaa goa 311530C2P7F0H0XA0a BaseilinnegceMnissed i. i3 is i3 363P.0F/H1P69A.10 Da oBaselcMiisnseed | 1331C5-0P2F7H0X0A02 Baseline Missed | 309P.H0A/S8E001Da Baselo iMinsseed | 4013800/-1P0F3H0SDa Baselc Miisnseed AY 7 aggPea tuo pen cogs ea kiz=o Fp=olt [Eol=l kEol= 4S0_3.108100-3P.F0HDSa cBaselne oMissed | 51135C0-4P7F0O0A02 cBaselinecMissed | 5S1_51.30C4-7P0F0D0Aa Baseline: Missed | 511530C4-7P0F0OADa oBaseine o Missed 0 Before O After Page 135 of 169 28 AnSaollyutmibciaalServices" Created with Analy2R8eporter Printed: 18/02/2010 4:02:00 PM Ton Ratio Confirmation KQ1000664-02 Tw TEE oT -iN |1"=f "|i = do=== |== ut zl a ef 213P0/F1E6A9Z0 Da BaselcMiisnseed | 263P0F1P2o1A902 Da BaselciMinsseed | 209P0F/E9S9200 oBaselinecMissed | 313P0H11A90208 cBaselc Miisnseed WongPeak Wrong Peak WrongPeak WrongPeak ITr], 1doh bE -- i ee sm Teipendnite i By uz \ 363P0R/H3G19A0Z Da cBasecMlisnseed | 309P.0R/9H9.X0S20a Baseline Missed | 5S1_51.30C47P0F0DDAa BaselcMiisnseed | NB FFWBraonndg PPFePakeA do nol have qWuraolnfgynPgeaokn Frarsiions Wrong Peak NA Baseline Mssed Wrong Peak O Before O After Page 136of 169 29 5 Solumbin AInnaelmyatreSANananamdlee:yrticalServicePTsro"rornon AcSqauaisrtiion Date Acquisition Method 2117T20O1C0 A30.4w3i PFCHnetexLodnagm Pract Evans rojecsiPRGS AlgaotruimtahnmtUNsaemde Regression Equation; = 0.0508 x + 0.00146 (r = 0.9989)" PrCirneea:ted18wi0t2h2A0na7l0y 323e4po.r8te5r A imeliGuan APY 5008 oors [one Tm Nn | wn] I 5i [; en ose T[ eo Thee hnan | whewn 70 Tv 70.158 102 Nan NaN Cs 20 Ts T8413 eee es | nwenn NwaanN / 4| | Hi ty3 4N pr rd PP _ re - _7 Ao ZF Luge Page tof 170 250 4CAonlaulymtbiicaal Services Created wih AnalyspRagorier Printed: 18/02/2010 3:24:00PM. AInntaelmyatleSNtaanmdea:rd: ADcaqtuaiFsiilteion Date Acquisition Method Project Regression Equation: P1E3NCAPTFNA o2/Z1i7/T2I0O10Ca6:L3o0g:13wiPlM PFCKinetexLong dam Ewan's Projects\PFCs. Result Table AIlngsotrriutmhemntUNseadme = 0.109x + 0.00371(r=0.9976) / T2T71000nG 105 AIPnIel5i0Q0u0an oo : 5 [ 10 % sm 4 "i : [+ ow--n[]dor | Nn |nn | [ [ w e e [ [w w e eoe [[wNaane ns [NNNv]] [e |e e Ws a [NaN] 1 Ee [es[NnTwn] |v[mem | ves[WN [Nn] 7 >. 7 Pe iE i _ | _ y| _-_ ] _ 1 4, & SN Suse Page 20f 170 251 Columbia 4Analytical Services" PiCnrieeda:ted1w9it0n2An5a0ly1p:0K2ep4oP0nie3rn AInntaelrynatleSNtaamndea:rs AcDqauriasFiiteion Date APcrqoujiescittion Method Regression Equation jprroos1ck C21E7T12O0C10a6o:3n0.13wiPM PEvFaCn'HsnPerlojeoxcLsdoPaRnGmgS ARlegsoaritThmabUlseed Instrument Name 201075400016 =He0a9r989) / GIntli7cuan06 AP15000 oors EIE EY:0489 [TYew [we T 5 [sw e T Te e nheen [wwean 0 ! 1 TT T eT0e88s9 w 09 |Nwae N| Nan | [| 5 7 50229 10 | NN |Nan| :. { Pe~~ ~ +4 : re re 4 _ 1| _~~ Fa i1 7~~ |] _, |1 7 EEE A 7 cegle Pa3g1e70 252 [5 Glumbin AnalyticalServices" Prrimed:e18s03a2nt0a1305a4g3p0uorPetr AInntaelrynatle SNtaamndea:rd SAcaquisiitionDate APcrqoujiescittionMethod Regression Equation PTarcorAr1on 2S117T201C0 6L:a3n0:g4w3iPtM EuPaFCni'inPreojteectxsLPcoFanCmgs RAelgsoraitThammUesed Instrument Name ~0.108 0.000as2(=0550) T Inetiquo an AP1 5000 Co oT 05 eee 0482 Tw [wen % NaN |ww | |nen| | 1 Ta [ 5 70 [+ T [ee7s 0.077 |e Tot |NNn aN | |NNaa N|| ED5 T w mese [ess | NNawnw ||wnvev || ] P / - pi { _7 ; | _ 4| 7~~ iy Fe 1 wl pre ere Tee ny "5 Page 401 170 = 5Anoatlymtoiciaal Services" PriCnrteead:ted18v0it2h22A0na1l0yR3t.2R40p0orPteMr AinntaelmyatleSNtaamndea:rc AGcaqtuaisFiiteion Date APrcoqjueicsttion Method Regression Equation: PCFPU U1 20/2117172T001C0a6l:o3n0:g13wiPlM PEvFaCnn'cstPerxojteocntsgPdFaCms ARlegsuolrtitThamblUesed Instrument Name = 1.05 x + 0.0336 (r= 0.9994)" TI2tTe7l1i0u0a0nng rab API 5000 I 0s 1 0530 we Nat Nan |I 5? 7: 1.07840 I Tor NNaO N | [[ = 1o T ] e 20372 sr h102 an Nan | hen NaN Cs Tee ie s [nen | new 4 7 re " i rerd o 11 __ rd jl" 7~~ HE ] Lord J 7 i _ ] rd ee BSey 7 21st Page Sof 170 254 3 GAnoalmytiicsal Services PrCreeda:ted18wi0t2h2A0n1al0y3s.p2R4e.p0o0rtPeMr AInntaetrynaeSNtaamndea:rs SAcaquaisriition Date APrcoqjueicstition Method Regression Equation: TprioCshr1os E 2/172T0106:C30:13 PM PEFuCaHni'nePtrejxLeocnsgiPdFaCms ARlegsoraitThammUesed E InelicuT an Instrument Name AP1 5000 =-0.000414 x*2 + 0.11x8 + -0.00244(r = 0.9991) / T or v ows [ow | nw[ne | i hes eee we] [ 5 = TF r |e wsees T wwoe re [mn aewn[|Rieven|] Cs +| saw | vor |men | Nev] Hi pr Ei 7 4i 7 pl ii i | i 3il 7 _ >i rd 7 4 Sa Zi Pages of 170 255 4Columbia Analytical Services" Created with Analyp:B8porer Printed: 18/02/2010 3:24:00 PM AInntaelrnyatleStNaanmdea:rd BAcqauiasistion Date PrAcoqjueicstition Method PTaocoPnro10n T 2177T201C0630wP1iM3 EPvFaCnK'nsetPreoxjteoctnsgPdEaCms ARlegsoraitThamblUesed T Ineliouo an Instrument Name API 5000 Regression Equation: = ean 0.x+6-00 .0045 56(r = 0.9959) -- I os 51 T : e ow w mm m a| wmmw [T emsow m esn [Ns aa N | | Nwaa CC o T w r : 3 mmoerTv w he en wear 7 = _7 ~ 1 rd 7- Iidl i re >J3| i3 EE _Pe Pe ~~ - 256 ES es reste Pag7oer 70 Columbia LS services: PrGinrteead:tea18w0i2n2A0n1a0ny3s.2p4r.a0o0rPeMr AInntaelrynatleSNtaanmdea:rc: ATcqauisFiiteion Date APrcoqjueicstition Method PT3ECTPAF1DOA 2T/E1T7/O2C01A0L6o:3r0g:13wiPlM EPvFaCnK'nsetPreoxjLeoctnsgPdFaCms ARlegsoulrtitThamblUesed nEteliT cuan ab Instrument Name API 5000 Regression Equation: ean =0.x3 + 03 .06691 (r= 0.9959) * 05 [+[oa [ et [ Na [Nw| C -- w s T TT o wmaee n T T w vwme |m wwweeenn | hwwewa Cs T em wT ww | we] |wl re zl u 2 _ I{a ~~ } 7 ] 7 2 rd 1 yo x Awe cs este Page or 170 257 6AnGaoluymtibciaalServices CrweinAanatmaeBorater Printed: 1810212010 3:24:60 PM. AnaariyseSamaem:s PTeerernson hTequrstion ote E 21772C 01053043 RRooreinmeUsed CineliTouen PAreaouicstion Meinod CPuFsChpnreeeanstraacnmsg nrument Name AP 5000 Regression Equation 0000561202 + 02x+4002669 r=09999) ET = T oosws [w oT swehana ] hw Cs wo ew ses T w w wRean wwamn C Co sTT + 1 T mSomut w 7 hew[ wf pd :- 7 4 ot iHI d a 4A} 2 ~~ LT er il~~ re ~~ P rd _7 } pl A Z2ftraf Page 901 170 250 Columbia PAY ov-- PaCinrteeadt:ed18w1i0h27A2n0l10ys3h.R2e6p.0o0rPteMr PDraotjaecFtile Ea2v1a7n1s0CParlojLeocntgsPwFiCfs RienssutlrtumTeanbtleName __AGP211751000000ng ab [[AScaamupilsieoNnamDea8 ts |2A7ZETOE 30 TE PIT ioctoinoVnalWat[|1oFSneomgas TweSacmptloenTyvpae me [ [Un| ion [[WiegohtrtFoavcotlourmsf0 oo 0]| frre Ta| wii Results Summary [Anais Peak EE | Tate RT aes | gEle Cane | w-e br eorrens|| wao a [swom| m ww ||a weww|w s eo|| sera Troon] wn [sme] ww |ww| we ha Zz a Page 1001170 250 columbia LS Routeservices: Bovis pasrain4s Created with Analy- 8porter WeSammary [armenian arena) [| ares | ater| pW RoteCte| [ronz [omasm [| 0 |w |ewew[ we | [orepron [rorase| we |w[oorwes| Pprwz [remees [we |ow |owes | [ower mew| ms | we| wom| ow rTTw [ssorros [ama [aw |we[sna | ow | Prova [ames| we |we[owow[ow | jorreeotrron [a[woewaosn|| 0 er ||wmee||oowoaremy|| we | [sscerm [rosz [rove [sserrom [raz rae [orem | w | wm | wae | [omaen| 0|we| wos [we | [omuss| |we|owoam[ ne | [amuse [| me |we|owem| we | [ems [es |we[owes [we | [emes| mo | we[ooo [| we | ZteTstes " LSCSoluusmbeiravices CrewinAavaltystAertder Printed: 18/02/2010 3:24:00 PM 7 Quantitative Peak ER Review 7 1B 7 iTEsI a ard i| 2- EE, 3 4 Ml Aa fii | pth A 2B ne Bas1e3lP0i/Fn1eO8A3oT.V0i0sased| oB4a1s1e73i0Cn5-e7P2FM0OiA0sased | o4B6a3se0Pi4En1eN5AoTl0l0i0sed| oB4a61s38Ce0-P4loF2MNii3ADsn0aseed 32 23 ETNa ] PT Le FI aa [VW i] cinmmtingne] sa tlianinl ennd Be paw Coa4s9e9Pi0Fn2Oec0Sl0Ti0s8sed | cSs5s01e33iC0n-6eP0cF0OMSsDsaed | oB5s1s3e.Pi0Fn4De80cA.MT0isased| oB5a1s15e3l0Cn4-e7PcF0O0MAi0s8sed ]| nae tt 1 == i Tht is if = b=: I 220 ca56i3PnF0Ue5R1A001Mi0sased | oB5a6s1e53iC.n-0Po7Fo0UN0NiAs0saed | Ba5s9s6Pi0Fn/O0Sc0ThiDsased | Ba5s01e53l0iCn1-e8P0F0OMS0isased ; =A |[I AHd] w iVIE f 1 Teh Ba6s1e3Pl0iF5nDe0O0Ao.M10i0ss8ed | oB16s13s5Ce0-i/Pn1F6e8Oc.M00iA0saed | NY| li lbboy ofalalii] Ee1bod helndal] ge] REE A B7a1se3Pl0Fin6Teo5Ao0VT0i0s8sed | 0 Bsa11s53ei0Cn.1eP8Fo3D0OW0Aiasse "ghstd(1i k oB6s3ss0Pi8FnT1eA8oT0M0ss8sd | tana pea +1rd Ea Tedd oBa6s11e3l5Ci0-n1PeF6oDM3oi0As0sed ona oe 0 Before OI After Page 1201170 261 Columbia 4 Analytical Services PrCirneieadted16w/i0t2h1A2n0a1l0y3s:P2R4b:0b0orPeMr Ton Ratio Confirmation Lx= =| Hy7 I TJV en el"hp da fc iB 5 = | i. 323 413.P0E0G88A.?0 08 Baseline o Missed | 462P0E2N1A90 0a Baselineo Missed | 49P9R0O80S0?08 oBaselne Missed| 513P.0r2O8A92.00a o Baselineo issed WrongPeak =Wiong Peak Wiong Peak Wiong Peak i| --arr =E-) !i "i ifr -i itd Atak, Ba5s6e3lP.i0Fn2U6e9Ao.0M2i0sased | cBa5s9s3Pi.R0nO9eS0c2.0Mi0sased | c61Ba2s0ePl/Fi1nDe6O9A02Mi0sased | Wiong Peak o Wrong Peak Wong Peak i il i Lots o B7as1ePl3Fi0nTe1eA62M9i0s0ased Wiong Peak O Before O After B6a6se3Pl.iF0nT/eo1A62M9i0.sa0sed oWang Peak Page 1301 170 22 7ASnoalluytmibciaalServices- PrCinrteead:ted18w/i0t2h/A2n0a1l0f3s2tH4e.p0o0rPteMr Project Data File 0E2v1an7'1s0 CParloLjeocnsgPwFiCfs Acauisition Method _PFCkinetexLdoanmg ARlegsoulrtitThamblUesed 0n2t1e7l1i0u0oanng.1db Insirument Name__AP1 5000 [[AScaqmuipsiietiNoanmDeate [|P2P/1C7200116009&0 5257 id [C inTf--cTtzionviar Acquisition Method | PFCknetexLdoanmg [Sample| ows2aen Sample Type Dilution Factor [Standard| Sample Comment [7|WeighttoVolume [000 | re ore| | a Results Summary [Raatyis |Anat RT Fnaiyie | ExpCone|Cale.Core PFOA1 | 1251.9| 130PrOA| ams| areunen| odo | ote | PFNA1 | 206206)| 13C-PFNA | 2669800| 21049 | 0.00 | 0107 | PFOS1 | 21|0132 cPr0 os|97se)zi0| eserr | 0am | oom PFDA1 | 3103.06| 13C-PFDA | 2604200| 27648 | 0.100 00s | PFUNA1 | 392|6130CP0FUN5A |222160| 2665 | 0100 | oom = 14 | No | 107 | no 5 | no 99 No EE PFDOA1 | 454455 | 13C.P|F2D053o80A| 1436 | 0100 CE PFTAT |5076|1.3p0F000n| 30530| toass | oo | NA |NA | No| PFTeAt | 656651) | 13G.PFDoA| sas0|G22| 0400 | NA | WA| No| Af0 = EN Pa14gofe170 263 ooQO Columbia AnalyticalServices IRC Summary | Analyte Peak Name PFOA 2 | RT (Expected) | 1.25(1.36) Created with AnalystiRforter Printed: 18/02/2010 3:24:00PM 19544 1 No = on Ratio 1.36 5nceros aia | mew |we| mee -- rosz| asm arse ost Columbia 4 Analytical Services PrCed:r18ei0t2A2s0n1a0tf3iH2oe4p.a0r0dtPeAr Quaz-- ntitative Peak Review ; 7 iLzl: oof ia. i===-- ort PFC 0.10ppb 7 a Bim i-= oB4a1sP3e0lr1n8oo0c.TM0i0sased|cGs7s01e33l0n7.e2cp0MFi0As0sed | 463P04E1A8.T000 oBaseinocMissed | Ba4s6e18l30i0n4.e22.5F0IMAiDsased ge gg BA Mio Eil| | i x =FTseosolbsA nfl i| 49p9r0o18s0000 oBaselnec Missed | 5013500.00705050 oBaseinecMssed | 51P3r0o48A0T0 0a oBaseino Missed| c 51A 504700 Da Baseine Missed ha. gia Bree ere i=o Reef| iEZ i x= Cl =! pl 563P0ru51010 0a cBaselineo Missed | 56135c0-2p7F0Un0A02 oSseinec Missed | $68P.00850010a cBaseineotissed| oBa5s1e03ln30e.07b0GMDSe0ased i 3i Bers id iz es iE i =i iz hehe fd beJ..J . 6P13r0o5c05.008 cBaselinec hissed | 6113500-1p5F8Bo0A0 oBaseinecVissed | 653P0r515T008 oBaseinooMissed | 6113500./pF15609DA0a Baseline Missed 7 3 a5 io| a =Fi oB7as1e3Pi0rn5Te8eo5TM0i0ssea| c 61135.021FB6090A0a Baselineo insed 0 Before O After Page 1801 170 265 PASACnoalluymtibciaalServices CrweithAanalytstizedfordter Printed: 18/02/20103:24:00 PM - RETES EeT on Ratio Confirmation PFC 0.10ppb aR i i: 1: - pv w] Feas a wu eo fi 2igAl n| -IF 2 p=oos n eer o B4a1s3elP0i1Fn3Oe6Ao92M0is0eaed | B4aP63sE0eN21lA9cM0iis0nsaeed | oBa4s9e9lP.iFn0Oe9S9o20Mi0s8sed | Ba513s.P0eF25lO9c2.AMi0i0snsaeed Wrong Peak Wrong Peak Wrong Peak. Wrong Peak TO] 3 J 7 io Thar A\ T WU Am=E lf =! Tk iEl=ssn 56P3.r0u269.2 0a oBaseloMiisnseed | 599.e0r9o9s0?Da 6130p1o16o920 0a BaseloiMinsseed | oBaselineoMissed | 663P.0r1a1c690.0a Basel: Miisnseed Wrong Peak WrongPeak =WrongPeal S WrongPeak i 1 sw o B7a1se3Pl.Fi0nTe/e1oA62M9i0.s0ased o Wrong Peak 0 Before 0 After Page 17of 170 26 4AnCaollyutmibciaal Services- PrCinrteead:ted18w1i0t2h1A2n0a1i0f34.f2e6p0o0rtPeMr DaPtroajeFcitle aEv1aTn1'0sCParoljeocntgsPwFiCts Acquisition Method _PFCiinetestdoanmg AlRgeosrulitthTmablUesed n2te7lTi0aiuoamng 0 Instrument Name__ API5000 [Sample Name `Acquisition Method T|2P1P7FCC20i0.i510n09e07t7e0x6Ld5oanPmgAE [- SSaammplpelCeomsment |[Tcuszese [[iinSnjjaeemccpttliieoonnTVVyoipalelume [[1 S5anda 3]|| |E WeightoVonume [0 T 00] Results Summary [A[nhpaorlnoyextet |[ arasE n|[ a amvcaonre~n [wseme|| rsApeAnalyte || ExspSeCowotnac||Cal[coc.aamCneoonc||s Aecacurac|ys| Pra asses| coma| wm| [prost[2osaon | creo | rose| a| wwe | ome osm |ams| wm | ne| |am |we o | Pron | aman| tcrron| zee| Pru1| 3850s, | riceruna| meio wom | as |oar| ww | wm | we | ne Frost |ssa| erro [reser| wae | Pron1_| 4stss|1ac|eorw o|sosn| oso | oso | wm osm |w|o we| | i | wo| Pri | sarees| tsorroon| zene | we | aso |ams| m1 | we [Prrent | ssowst| 13cproon| zste0 | soses | oso | caso | ss | ne AS ers 2 sie Page 18.0f 170 267 LS Gehmba AnalyticalServices IRC Summary ana es ame [E-- ares PrCinrteeadt:ed18w0it2h72A0na1l0ys3P2R4E0bo0rPteMr cai |'s13c_pFoa Prvaz sms | No 4396 ass | swt No | 033 fI r os we |em we | ows mem mw weTew i rwase emwees neewe eTee w Page 1901170 250 5 tumbia AnalyticalServices- PrCinrteead:ted18w1i0t2h1A2n0a1l0yp3t24RR.p0o0rtPeAr Quao ntitaF tive Peak ReviT ew T = IE ia.y = Iw PFC =0r.5ppb Bg i=Ti i o3l 413P01F1O6A901 0a 41173.C0-5P7F2O0A0n 463.P0E4N1A9.T00a 461830C1-2P3F0NAa ZoBasuelnegc Missed | oBasuelngeoMssed | roBase elineioMissed | Baselineimc Missed i= i3 i ~f i = pA = of 499P.r0O80S0TDa 15033C.-0P1F00OSDa 513.P01F4D65A.T0 Da 511530C4-7P0F0DADa Baseline c Missed | Baseline Missed | oBaselnecMissed | oBSaseline c Missed i= icl i=: i =ol 563P0F1U5R1A901 0a cBaseine c Missed | 56153.C0-2P70F.U0nA0a cBaseinscMissed | 599P.R0O3S00T 0 Baseline oMissed | Bas5e01l33i00n-1eP0cF0OMSDisased - cl i1 i3 | sor = =x 3 613.P0F5D5O6A910 0a 16135C0-/P16F9G.00A0a Baseline o Missed | oBaseinecMissed | I 853 - hd] 2 713P.F06T6O9A.10 0a 61135C0-P1F6DO90A0a c Baselinec Missed| o Baseline o Missed 63.P0E6T1A5.008 oBaselineoMissed | 51135C0-/PF1D6oD3A0a Baseline o Missed 0 Before O After Page 20 of 170 20  Gohumbia Analytical Services- PrCinrteead:ted18w/i0t2h/A2n0a1l0y3s:P2R4:o00rtPeMr fon Ratio Confirmation PFC 0.5ppb -l IE ] - J] i= t fis | iE i Zl | TK| etl 4130P/E3G6A9.20 Da 463.P0E2N1A8.2Da 499P.F0O1S9290.0 513P0F/O22A6900a cBasWeilonnegMPiesasked | BasWerlionnegMPiesasked | oBas=Werlionnecg PMeiasksed | BaseWlrionnego PMeiasksed 2= ] E7 E == I E==== uy = $k 563P0U/2T6A920 Da 599P.0F1O99S.20 Da 6P13F0/O1A6920 Da 663.P0F/1T6A9.20 Da BaseWlionnegoPMeiasksed | BaseWlrionnegcPMeiasksed | oBasWerloinnegcPMeiasksed| oBaseWlrionneg PMeiasksed i} T 1 he | 713P.E0T1E1R6?9.Da0 BaWseiloinnegoPMeiasksed 0 Before O After Page 21 of 170 270 8 Solumbia Analytical Services PriCnrteead:ted18w/i0t2h/A2n0a1l0yB5t:2R4p:o0r0tPeMr DaPrtoajeFcitle Evan's ProjecisPFCs 021710CalLongwif Acquisition Method _PFCkinetexong.dam Result Table Q2171000ng 1b IAnlsgtorruitmhemntUNsaedme __AInPte5l0iQ0u0an [S`AacmqpuilseitNioanmDeate | 2T/F1C7/120O1p0pb7.:08:07 PM I InjectionVolume [5 || `Acquisition Method _| PFCKinelexodanmg [Sample rcuszsec ESL ampleTya pe K[ -- T Sangad| [SampleComment | ~~ |WeighttoVolume [000 | Results Summary [|Niammee | peectetd) tama | toon2| "area | ExgpmGto)ne | Galeg.mGto)ne| Acc|ueracy PFOS1 | 208209)| 13C-PFOS | 760|0s4210z00| too | tow |103| to [Prunat | ss0|a1scopruena | oss | aessso | tooo | tose | 05|no| PFDOAT | 454|413.c-5PFD5oA |2s02e0 |tessso| tooo | oes 8 |no| PFTA1 | 5.07|513c0-P6FD)OA|200240 |setst| tooo| o0e0o w | Nn | PFTeAt | 5.53651)| 19CPFDOA| 200240 |7432| tow | osyt |8 | ho | 2 ZaFle Page 201170 on AnalyticalServices" Created with AnalysPREporter CSummary [ren| om [en| EER, | E[a rEoss | TwTan|ww|ow | ew | PASACnoallyutmibciaal Services- CrweithAanaityBtSeepordter Printed: 18/02/2010 3:24:00 PM Tz Quantitative Peak ReviSIew = i | It 3 TF - i= PFC = 1.0ppb --; i3 413P01F1O6A9T0 0a 411730C8-7P2F0OA0a 463.P0E1N41A9T.008 4661.304C2P3F.RADa oBascine o Missed | o Baseline Missed| cBaseinec Missed | oBaselineo Missed i: = i:=! i| lei 3| oBa4s9e5lPi.Fn0eO0S0c0M1iDsased | cBa15s03e3Cl.i-0nP1eF0cG0MSDisased | B5a1s3.eP0i1Fn4Oe68Ac.M10i0ss8ed| oB5as11e35lC0n-eP4oF7OM0ADis0ased i] | i J i i: A oB5a6s3eP.iF0nU5e1R8Ac.10Mi0sased | Ba5s8e15l3.iC0n-2eP70Fc.UM0NiA0ssaed =1 fF 4= F ho fx cl Af oB5a1s3eP.l0Fi1D5e8O9Ao.10Mi0sased | cB6a1s15e3.l0Ci1-n1P6oF8oD.00MiA0sased dow 1 i. | = | oBa5s9e9Pi.nR0eO80S01Mi0sased | o Ba5s01e33liC0n-8eP0F0OMSDisased =FET : g = Il =| L = Le meme] 2 | B6a6s3e.l0Pi6nE1e9T.cA0Mi0sased | oB6a1s15e3i.Cn0-e1P1FoD6MO8DiA.sa0sed oB7a1sPe3Fi0Tn6oE6cA810Mi0s8sed | o B6a11se35lCi0n-1ePo1F60M03iAs0ased 0 Before O After Pa26gof1e70 mn 4 lumbia Analytical Services" PrCinrteeadt:ed18w/i0t2h1A2n0a1l0ys3p:r2i4s:p0o0rtPeMr Ton Ratio Confirmation bo Jo -= i= ila PFC 1.0ppb i =" ao -ol i \ 413.P0F13O6A6.20 Da BaseWliionnegcPMeiasksed | 463.P0E2N1A9.200a 499P.0R1O99S.2 Da 513P.0F1O2A52 90.a0 BasWerloinnegcPMeiasksed | BaseWlrionnegoPMeiasksed | BaseWlrionnegoPMeiasksed sli ] tl sw -- : 3=] feet am =zl fla 563P.0F/U26N9A.02 0a 509P.0R18O9.S20 0a 6P13F0D1G16A920 0a 663.P0/E16T9A2.0 0a BaseWlrionnegcPMeiasksed | BaseWlroinngePoeMaikssed | BaseWlrionnegMPiesasked | BaseWlrionnego PMeaiks.sed iod1 fa 713P0/F1T6E9A.20 0a c BasWerlionnegoPMeiasksed O Before 0 After Page 25 of 170 274 AnmalbytiicaalServices" PriCnrteead:ted18w0it2h12A0na1l0yB3t:2#4p:o00rtPeMr PDraotjaeFcitle Acquisition Method aE2w1a7n1'0s,PCraoljleocntgsw\PiFfCs _PFChinetextong dam [SampleName To2r175201op0po7155 PI [[AScaqumipsilteio>nMethod[|cPiFCsiiznet5e0x_ong am [Sample comment | Results Summary Talis |Analyie RT AlRgeosruiltthTmabUlseed 0n2t1e7l1i0Qluoanng.rdb Instrument Name __ API 5000 [E imecTtonvar [5] DiSlaumtpiloenFTaycpteor |Sanda | [Weightto volume Joos | -- Faia le Gone| Accuracy Prat | vanaos| tscera| meso| vane| sooo|asso | ss | we| [rr | sss|wncoersun,n| surso | isos| sooo |s|a wr|o we| [Proont | aszass,| 1scoroon oon |sow| eso| mn| we Pra1 | soot| taceroon| aro | men |sow |sam | me |no| [prrent|sooon| nceroon|ar|sceamo| sao | sao |w|m we| 23& 7zsi 410 Pa26gof1e70 275 8 Sms ji AnalyticalServices" PrCinrteead:ted18w/i0t2h/A2n0a1l0ys3P:2R4E:B0o0rtPeMr wCsummary snr [src pron s_rsc.pria bros s_iceros [oomron oss |wo [| oe w [ws eer | E_E Tas |ww | e mw | wor omas| m 0 ow awa| mm | w 02 [amra|m mw | w [0 | swam | won| we|| wen | www[we [en | prea am|emes w | ow or 8 ASnoalluymtibciaal Services PriCnrteead:ted18w/i0th22A0n1a0ly3t:2F4e:p0o0rtPeMr Quantitative Peak Review - TT TE Tw PFC 5.0ppb = wr TT 2) = =| hx (J p= = 413.P0F/1O69A.10 0a cBassinecMissed | 41137C.-0P57F2O0A0a cBaselineaMissed | 463P,0E4N1A9.100a oBaselinecMissed | 4681.30C4-2P3F.N0ADa Baseline c Missed SI ged 5 oT So -- i s1 Io [el Fo Ho i Z| 499.P0F18O0S.01Da oBaselne Missed | 50133.C0-80P.F0OSDa cBaselinec Missed | 513.0P/F48D9.A0 T Da oBaselinec Missed | 5151.30C/4-7P0F.O0ADa cBaseline o Missed ho I3 ix I~ A 563P0F/U5R1A9T0 Da cBaselne Missed | 51635C0-2P7F0U0RA0a oBaselinecMssed | 599.P0F/D80S.01 Da oBasclnechMissed | 50133.C0-8P0F0OSDa oBaseline o Missed - kang Bea TI I. or aangBea el a | i. I || ol 613P.F01D5O69A.10 Da 16135C.0P/1F6D9.00ADa cBalseiloinecMssed | cBaselnAeYcMissed | i =i | eB LB -- 713P.F0T66E9A.1 0a 51135C0-/PF1D609DA0a oBaselinec Missed| o Baseline c Missed 663P.0E6T19I.T0 0a oBaWseoinnaecMissed | 61153.C0-/P1F6Bo9DA.a0 oBaseine0o MiPoassed 0 Before O After Page 28 of 170 277 5 Gahmbia AnalyticalServices PCimr8w1ei3n2aa0n1a0yts5P2ee4S6f0rdPeor lonToRatio Confirmation= = PFC 5.0p5pb = - ig I _" kt =| H =| ol i- ok 1. ct4n1s3ei0nr5e8io8v0a0s0es | ob4ee3ro0g2r1os8m00saes | Ga4s9s9pi0rng0o5so6a?m0a8sea | o S5a1sa5bi0rn2oei0oz0th0s0sed rong Pea tons pean Wong Peat Wong Peak N3EE I = E - E TM w| IE i - --| ob56e3Ps0re28U0v2a0saes | cB5w5eo5irn0g8io0m0o8es | oB5as1Pe3ri0one0v6io02i0s8ed| oSaas3sP0i1rn6eic0s0th0sasea rong Peak Wrong Peas Wrong Peak rong peas AE+ i i] go o B7e1aP3ne0er1eM6ze50ea0t Sion Pea 0 Before OJ After Page281170 as 4AnSaollyutmibciaalServices- PrCinrteead:ted18w/i0t2h/A20n10a3l:2H4e.p0o0rtPeMr Project DataFile Evan'sProjectsPFCs 021710CalLong wif Acquisition Method _PFCinelextcoanmg Result Table Algorithm Used CIn2t1e7l1i0Q0uaanng db Instrument Name__API5000 [SampleName FPC010900TEER I ecton via [5 -- ] `AcquisitionMethod _| PFCKinetexLong.dam Sample Type |Sanda | [SSaammpplleelCo>mment |TL~ CMS2:85E ~ |DWieliutgihotn tFaocVtoorm_e_[[010000 | | Results Summary [nNaamles ||ApnarimyiaenRyT| totame [waa [ Tn"aRiyeie |[ ECxpRCEoNnSe |CalaemCtoyne |opu| t-o [roar [1270.36 | 1aceron| sessann| rrssseo | tose | tome | 102 | wo| PPNA1 [203200| 13CPFNA |276|028sas0io00| to000 |sss| ss | no PFOS 1 13cFOs| 7se|s7ezoason0| 10000 | fos | 10 |no| PFDA1 | 3083.06) | 13CPFDA| 2754300 | 2866500 wi | or | ne | PRURA1 | 388606| 13CPFUNA|239|z5as7too0| 1000 | sam | ss | no | PFOOA1 | 4554.55 | 12C-PFDOA |201580|17u|asT0o000o| sero No | PFTIA1 | 5066.06 | 12CpFDOA | 201580| trisso0| fo000 | tia | iz | No| PFTeAt | 583651| 13cP|r2D015o80A| 7azi20 | tooo |to | a ot | no xAY FFs 2 1plee Pa30gof1e70 279 Lom RCSwmmary PrCereda:ted18wi0t2h2A0na1l0y 32R43.p0o0rtienr Caled f[erarz n s-tscpFos #50A% Prunaz Src prunA Pros 2 Pron? Fria 19 [|aowwaas || e0we | | owwe | o0m | |_wmaw | emo|| 03 [owe | ame |v | ots ava waa No oan [ssa wen | ow | ow | seen |w|w me | oa assy stato No 0) | mem | asso | we [om| Page 3101 170 250 /X Golambis Analytical Services PrCimedr: 1w5ei0t2h1Aa2n0a1l0tys3p24e.0o0rdtPM FE Quantitative Peak Review i bo | io ik J hl = x I: PFC 10EpRpb el i2 7] - 3 412.P0r16o9x.: 0a Baseline oMissed | 701537.20070A8 oBmselnec Missed | 46P2E0N41A3T008 cBaseinecMissed| 4681.304C7P3.F0ADa oBSaseline Missed To ix To i :2 To i=- Te i| zd 2 1 coa4s9t5Pi0Rn5Oea0SM0Ti0s8sed | cB1a5s30e3C0i-%nP0eF.cO0MS0s8sed | oB5a1s2e.Pl0Fn4eD69cA.h10is0saed | B5a1s1e53l0iCn4-e7P0FO0MAiDsased it '- I i= 1 a --] zl 5P63r0u51n0T0 0a Bainectissed | 5615300.291F0U0n0A0 oBassinecMssed | 55p6.r0o0t0 Da oBaseineaMissed | 5103c5.00F05DS0a Baseline o Missed bo io = aE = i i1 oB6a1se3PiF0nD5sO5Ao0M10i0s8eed | oS6s1s15e3lC0-n1Pe6Fc9DV00iA0sased | o6B5a3s0eP5inT1e9Ac.l0i0s0sed | Ba6se11l53iC0n-/eP1F6O9MOiDA.s0ased io i a El oB7as1e3Pi0Fn6Te5EA001Mi0s8sed | o B6a11s3e5lCi0-nP1eFo6D0M9i0As0ased O Before OJ After Page 3201 170 mn 8AnSaollyutmibciaalServices" PriCnrteead:ted18w/i0t2h1A2n01a0ly3::2R6b:p0o0rPteMr TfoomnRRaattiiooCCoanfimrmamtion i| i) =| oole 2ol fT3 PFC 10ppb T a fe || >| 41P3.F03O69A.2 Da 46P3F0N21A9Z0 Da cBaseclMiisnseed| oBaseloMiisnseed | 49P9.F0O19S9.20 Da BaselcMiisnseed | 513P0F26O92A0 Da Baselo Miisnseed WrongPeak WrongPeak WrongPeak = WongPeak iol 4 _ | - + - 4 [= + 563P.0F1U2R60A.20 0a cBaWrsonegclPMieiasnkseed | 4 Desi 509.P0/R9O9.S0 2 Da BaseWlrionnegoMPeiasksed | 613P0F/D1O6A902 Da cBaseWliionengoMPiesaksed | 663P0F/1T6I92A0 Da BaWsroenglo PMieiasnlseed 713P0E/T1e6A29.D0a BaWseolinneg PMeiasksed O Before OJ After Pa33g011e70 262 PAYAnealytvicalServices pCiedr2veit9hAan1altys0pespeodroes RForuaes Filen ethod_ FoPrratriFncEiaoonRnvgaStm nRNuiemoersrtiaUsaame _ o 4n5t1c50u0ao 0n FA[caSubaitmonbpsls etee7a6ez1mo0oe73075 [ ection | ["AScaqumisaitoion_Me[tthood u|sPzFCakisnretexLdoangm OSlameplne FTaycpteor [Sanda | sewer| wevoes Joo] Results Summary [TTAoinranlotynte1 |itoatsatrey|| sacvoreon[|oswvseuns|[ ss0o [|53EaxpoCaownnc|| toa0| 2i || Cale. Conc| Accuracy| verr| sent | 2maoe| vicera | ao| sams| mmo | mo| m | we| pros | zssamm| mceros | wo| taszioo|n mao | were| 5 |to| PFDA1 | 3.053.069) | 13C-PFDA | 2957800| 5644600 | 20.000 18.500 92 No PrURA1 | 380005| 1SCPFUTA| Toros1 | sweawn| neeros 20800| sa7ost0 | 000 | wo | 20400 | wwe | 102 | No sw vroant | ss |nops roon| eo | smo | mam |mew | ve| to| wert Perens | | soram| vcer|ozesotn| sszaen| 1ceroun|mst| reser| mmo | mow |z|m wr | moo | aw | sm | wo No| ANi30 Luise Pago340t 170 wn / AGnoaulymtbiciaalServices PriCnrteead:ted18w/it0h22A0n1al0y3s:e2p6:o0r0tPeMr RCSummary [remeron [eer eer me |r[vor| ES mon | wen|| owas | 0|e[ew] Pron 05009 0 oe [rSrocsrsrm roots pari) Taomweesn || | amen| wwwe e|eow | | wee|e| eewe ow | [ewo e ||w w wew e|on wwe o[aerm 8 AQnualmytbiicaal Services" PriCnrteeadt:ed18v/i0t2h1A2n0a1l0ys3:pR24a:p0o0rtPeMr Quantitative Peak Review PI EE = i i3= 2 in b=l PFC 20ppb q Tw fA= 413P0/F1O6A90 Da cBaselnec Missed | 41137C0-3P7F2O0A08 cBaseinecMissed | 463P0F4N1AT300 oBaseineoMissed | 4681.031C42-3P.0FRA0a Baselinec Missed = io = i 4P99r.0O/S8010Da Baseline o Missed | 50133.0C/-8P0F.0OSDa oBasslnecMissed | 513P0F4D6A901 0a oBaseliecMissed | 511530C1-6P7F0D0A0a Baseline c Missed 3 + I i i yl 563P0F/U5R1A90| Da 561530C/-2P7F0U0RADa Baseline Missed | oBaselinec Missed 7 ol bl= I:r =f Ix = 599P.F0D8S001 Da | oBaselinecMissed 7 t(i l a i " 50133.0C/-8P0.F0OSDa | Baselineo Missed 7 silx 613.P01F5D6O9A.100a Baseline Missed | 611530C1-6PF9D.00A0a cBaseinecMissed | o6B6a3s.eP0lF1Tn9Ge.Ac10Mi0saed | 61135C-0P1F6D090Aa0 Baselineo Missed i=l il> 713.0P0F6T8e6A910 Da Baseline c Missed| o 61153.C0-11P6F8D.O0A0a Baselineo Missed 0 Before OI After Page 36 0f 170 285 8 mba AnalyticalServices PCredr1w8ei0t2h7Aa2n0a1lt0y3 R2e4S:p0o0drPeMr TonRatioConfirmation 1 EJ i | PFC20ppb 7 s Io = 3 TL 17 7 CB4a1s3eP0iF3n8Oe3A.20Mi0sased | o4B6as3e0Pl2Fn1eN9Ao02Mi0s0sed | oBa4s0e5Pi0Fn8eO5SM02i0s8sed | cassie3Pi0FnOzA020M0isased || Wong Peak Wong ea = Witong Peak Wong ea HE 3 Zl _ 2q FEag ake e]k= 3 NLoe I1 = CB5as6eP3i0Fn2eU8A520Mi0s8sed | oBa5s9Pe0lF0nDe3S8c20Mi0s0sed | oB6a1se3Pi0Fn1Do8Oo5Al02l0is8sed| o Bca6s3eP0li/Fn1Te6A92.i0v0saed Wrong Peak =Wong Peak Wong Pea Wong Peak EI i zl } o B7as1ePl3iF0nTe1oo8A2M9i0s0ased Song Peak O Before 0 After Page 3701 170 286 5 Golumbia AnalyticalServices PDraotjaeFcitle o2F1a71n0sCaPrloljoRnGgSPiFtCS Acquisition Method _PFChinetextong cam [SampleName TP2C2500pp0b TIE [SSaammpplleeComment [|TCMS2:85G Results Summary Anais |Andyte RT PrCinrteead:ted18wi0t2h2A0na1l0ys3p..2/4B:g0po0rPteMr AlRgeosrulitthTambUlseed TInFeTliTQGuoanng ab Instrument Name__ API 5000 [SiiannjjmeepcctltieoonnTvvyioparelume 11 |5Strand 6]| [DWiifeuitgihotntFoaVcotlourme [[700000 || Anais | ExpCone | Co Gone Proa1 | soso| 1sceron | ssrioo| ross| samme |si|atesm|woo| [pronat isso| tossio|n soo | ssam | too| no| eroont | esas| 1ceroon| aso | tooo| samo | erro |s|s wo| LAJ F et Lug! Pa38gof1e70 27 nalytical Services Created with Analy porter rRCSOmmMary feos 1 sven 1 weTaos TF1 Freeesrn omam |e[we | am Ei hee a [oemeer aowmeen ||w weem o we[em w || [e rons |wen | wT w|e] f[aorses oowween ||wwwm||ewe |[oewm]] - 3 Solumbia Analytical Services PrCinrteeadt:ed18v/i0t2h/A2n0a1l0y3:24:p0o0rPteMr Quantitative Peak Review EI om Tp PFC50ppb 7= tx: ipue i= ipu 413.0P/F16O9A.10 Da 41137C.-0P27F2O0A0a 463P.0F4N1A9T.00a 46163.C0-/P4F2N3DA.a0 --cBdanseoligneeceMaissed | o oBaseie necMissed | noBaiselgneoMissed | cBaseoinnegceMaissed i J A ix A i: i: I 499P0F8O0S0102 GBaselianneac Missed | 50133.0C/-8P0F.0OSDa 513P0/F4D6A910 Da 511530C4-7P0F0OA0a Basecliunpe Missed | 7oBaseblonenc2gMissed | oBaseulnego Missed i-] ioo I-= i-l A 563P,F0U5R1A9.10Da 561530C1-2P7F0U0NADa 599.P0F/D80S.01 Da 50133.001-8P0F.0OSDa BcBiaseiliYnec Missed| oBaseinec Missed | l oBasa einea Missed | CoBasueinee c Missed zi | = El Il i Iz - 613P.0F1D5O69A.10 0a 611530C/-1P6F9D00ADa 663.P0F/T618.0 0a 51153.C0-11P6F9D00ADa cBaselinec Missed| oBaseline oMissed | oBaseinec Missed | oBaseine c Missed i Io oS oi 7P13F06A6901Da 61153C0-/P1F6D9O.0A0a oBaseline Missed | Baseline o Missed 0 Before O After Pa40g0f1e70 289 LSAnSaolymtimcael Services" prCireeda:ted18w0it2h1A2n0a1l0ys3t:i2R4B:f0o0rtPeMr FE fon Ratio=Confirmation; [a. i o2l 1 - -- = PFC 50pp=b Lfiso aNLi: ) = re t4r1t5Po0Fen5OgA8eZP0o0o0sk | oB4e6sro5Pio0Enn2Ngg1Ae02Pm0os0osk0es | oBa12v9ie8Pio.Rnn0eO0sS0i20Pa0osaea | c5a1rs3Po0eFn2s8O02AP0Mei0sa8sed IS! L 2) "ew LE J am i fo F 2 g =| [3= === 3 c5r6ioP5Fm0U2sTe8Ap92e0so0 | ow5S6oeP6nR0nO9gS0o2p0me0as0kes | oB6ao1s3sPn0iFn1Dge6O0oAPM52es0askaea | cacest3Peo0FninTg6nAc0P20Mei0ask0sed iE 4 o B7a1sJ 3i1ng60o0s0e0d rons peo 0 Before O After Page 4101170 250 4Columbia AnalyticalServices CrweinAanaitfi Reepordter Printed: 18/02/2010 3:24:00 PM PDraotjaeFcitle Tozat7sI0PCaolRoanRgPwRiCS Acquisition Method _ PFGiinetoxtong dam AlRgeosriatThmamUesed EinteTliauOan Instrument Name __ API 5000 [SampleName P27C20210p0mb017cv01 PHL [ectnonjvalec1[t55 ionvome|| [Sampled IPTFCkiCnetexwLongs.damz7y| D`SiaumtpolneFTayspteor Qual Control [100 SampleComment | | WeighttoVolume 000 Results Summary Analyte Analyte RT - `Analyte Exp Conc |Calc. Conc | Accuracy NParmeoxT_| nade| (Expected) 11SaNoarmreon | swe| 1S Area seAriesan | mov |mao| (ng/mL) (ng/mL) {ro%r) | hl PRNAT | 200205| 150PFNA| 2503600| seaaro0 | 20000 | z000 | 108 | no Prost |20s|z13coerons | raion| seseaeo| zoom | maw | tot | wo PRUOAT| 531006|13c|eTerss u|avniosa0| zoom | zara | mie | ne Prost | sasaan| opros| eestor| weereeo | mow | maw | wot| no| Prat | sareos| tsorroon | so | zie | move |s|e wos |o no | Prrext | ssaasn| nceroon| mise wom |maw| wos | vo | *3N 7 2 (0 Page sof 170 201 Te RS nalyticalServices Serre CSemO@y eer rrecrsn [foopoemes sooron mow |wee|ow |e| Toomweanm | amam [|ow0e | mew || | wWew ||ow ww| we || | oowmean||wmeonr||owwe||ow | pros | pros 2 [oraz Prone | 389(387) 5658600 No YES 0- soem | mn | te oem | mo | ne | ve | 5AnCaollyutmibciaalServices- prrinetaedt:ed18w0it2h12An0a1l0y 32H4e.p0o0nPeMr E E Quantitative Peak Review_ =m ow p = TF i4 i PFC 20ppb ICV ap - oB4a1s3e.Pi0nF11eO69Ac.10Mi0sased | 41137C.-0P37F2O0A08 cBaslnec Missed | cB4a6s3e,P0i1En4Ne19Ac.T0Mi0sased | o B4a6s81e.l30iC4n-e2P3oF.N0MAiDsased Cag J ny EY S sea i= zl oBs4s9e9P.l0Rn/eO3S0c.1M0i0sased "oo x] I=2 | 563"05o19y.0 0a oBaselne c Missed i pi | oBa15s03e3Cl,-n0ePc0FM0OiSDsased og 9 i- acon | oB5a6s5e.i0n2e70cM.i0s0saed iE i= a zl | oB5a1s5eP0l/nF4eD5A910MiDsased | Ba5s1e15l.3i0Cn4.e7P0cF.O0MAiDsased = aog22a 7 ling ea =! oo Ip ra2 rest Tonics | Bas5e9l5i.n0e0o0Mi0sased | oBa5s0e3i.n0e100MDisased 3 i Fl 3 ix i i ; ix i Fi fi | 4 5P13F.0D15O6A9.10 0a cBaseine oMissed | 61153.C0-1P6F9D.00A0a oBaselineoMissed | oB5a6s3sP,i0En6Te1Ac9.M0i0sased | o B5a1s15e3l0Ci/-n1eP6oF9D0M0iA0sased reg To i= | i3 oB7a1s3eP.iF0nT6oe6cA8.1M0i0s8sed | B6a1s15e3l.Ci0-n1ePc1F6DM09i0A.s0ased O Before O After Pa48gof1e70 203 8 Gumbia PrCinrteeadt:ed18w1i0t2h1A2n01a0ly32s4i.d0o0rPtAMr Analytical ServicesTM e TonTERTatio Confirmation r eres PFC a 20ppb ICT V eer :C--O 54d = Po] A 1 Ir1EE - iL1 ol |i=hen ah i:F3 ee Sl c B4a1se3Pl0iFn3Oe6AM92i0s0s8ed | B4a6sP3e,lE0iN2ne1A92.0Mi0sased | oBa4s9e9Pl.Rn0Oe9S9c0?M0issed | B5a1s3elP.i0Fn2eD8o92A.Mi0sased Wrong Peak Wrong Peak. Wrong Pesk Wrong Peak 5EaR ERo-T i EH = e 7 EEde ; Lose of 5 a B5a6s3e,l0P1iF2nU6eR9c.A0M2iDsased | 5B9as9e,lPi0FnO9eS9c2.M0i0ssed | o6B1a3s0Pe1iF6nDe9Oo.A0M2i0sased| cBa6s6e3lP,i0nF/ec1T62M9i0.s0ased = Wrong Peak = Wrong Peak Wrong Peak o Wrong Peak i1 1| < B7as1eP3lFi.nT0eEc1A62M9i0s.ased Wrong Peak O Before 0 After Page 49 of 170 204 PASACnoalluymtibciaalServices- Ainntaelmyatle SNtaamndea:rd P1r3Co.APtFBA ADcaqtuaisFiilteion Date 2/T18I/O20G10A1S2:a04n:5i7tAM APrcoqjueicstition Method EPvFanC'KsnPerotjeectxsSPhdFoaCrms Createdwith Analfit7R4eporter Printed: 18/02/2010 4:02:00 PM ARlegsourltitThamblUesed teifTiQiuGasnhon Instrument Name API 5000 Regression Equation: fiean =0.x 1 + 00 .005 66(r= 0.9890) / ewcmeoumy |eorvaus [ou chatpgmy |#ho|oswom|ewerr] [ [o o T s r T+ oeamsT Ter|e NNaanN |[Nhaav N|| 1 Ls Toes Tee es es NaN | aw Nan han [ veews 7 w wo[mv en [[mheww | J ' ~~ 5 [i wer re [en | nen vl| _Perd Id __ u ~~ i Hl _7 ] rd 1 xS ZLsisle Page1 of 160 25 8Coalutmebidaservices: PrCinrteeadt:ed18w/it0h2A/n2a0l1y0st4R0d2d.0b0rtPeMr AInnatlerymtale SNtaanmdea:rd: Gaia File Acquisition Date `PArcoqjueicstition Method P13FCPPAF1HA 22118T2T0I1O0CA1S2h0a4R:5W7i AM PEwFaCnK'isPnreojleecxtSsPhdFoCarstm. ARlegsourlittThambUlseed 0I2n1el7i0Q5uahn 195 Instrument Name API 5000 Regression Equation: Wean =0.0 x+00.04000991(r= 09983) or Cos ow [mr[Nn [oN | vest [wes [maw [Nn |] 1 Te sr 539 [es 108 Na NN | NaN | Nan I 0 I 1128 Tz Nan NaN [s wT] 1 v e18s75 | [ee r [WNeanv|| Na wn ii i 7 il] rd" 5d re LE 7 i 3 _~~ i _ i pd i ~~ 3iH,er A r rrr ; al 0 9 usjm Page 20f 169 206 8 olumbia Analytical ServicesTM Created with Anahi7R6eporter Printed: 18/02/2010 4:0200PM AInntaelryntae SNtaamndea:rs ADcaqtuaisFiilteion Date APrcoqjueicstition Method Regression Equation P1r80a-sP1FHS 2G/a1r8T/2I0O1C0a1S2h:a04r:5w7iAM EPvFaCni'nsePtroejxeSchtosrPtFdCasm ARlegsourlittThamblUesed GTSho db Inteliuan Instrument Name~~ API 5000 = 00019112 + 0.36 x + 0.00745 (1= 0.0975) Mean [ov [os FT + [7 ow |e ea Te New | nw | Ney han L[ s Tve se T TT e e NNaeny |wheann | 10 [ wae 7 es [wea | Nn 20 [7 Ls Tv wee Te[maw[New| se [we wan |mw] 34 _-- | 7 4 _ }] pe 3 iiu _ : 3il rd 3 pd | ~~ we "b4t0 "pe "at Page 3 of 169 207 5 AGnaolyttaicnal Services PrCinrteeadt:ed18v0it2h12An0a1l0ys4t:f0R2G:B0o0rtPeAr AnIantleyrntaleSNtaamndea:rd AcTqauriasFiitlieon Date `PArcoqjueicstition Method Regression Equation PTaCr-P1FHA C2118E201C0 12A:04:57 AM PEvFaCnK'sinPreotjeecxtSsPhdFoarCmts ARelsguolrtitThambUlseed Instrument Name = 0000207 x2 + 0.102 x + 0.00867 (c= 09985) TInieliGQsuhaonr ib API 5000 Cor os [v 7 oe s [ee ee w [|MewNw [Nawa [[ ! [r s te swv Teewes Nan [ON man Nal 0 I 1065 [or [wee Te [Na NNaaNN | Cw + 1 S05 Torna he] i:l 3 ___ 3 4 | ~~ ! rd i 7 i re ]} rd la XTad40 "27glo Page dof 169 208 PASColumbia AnalyticalServices Created with Analys} Heporer Printed: 18/02/2010 4:02:00 PM Project Ewan's Projects\PFCs. orca [sores| cue chgmy | accomer| sm [ov] [o3s] [[ 7 eomewTh e eww n || nheann|] C r s T+ + Si0o8r [ [o ir e | mNaann | nneenw|| [[ 0 Cw[w es T T ee e | |e nms aavn | nnaan | = t 5040 [or | nen | nan] of 7 _ 3 _ i ~~ a rd x ra ER =Slr" gee x a os 28le A ami AnalyticalServices" Fe a79 Created withA. nalystRporter afneaunamee:, Faehmeonn ivatoen rego pTries TSaRcahC1o30e057nAM mST earn--F n--e E AC5o0oT 0t A y= 00017024 03ax +000 r= 05681 = I osi : vo iT - [ow2 = m= e = a Nan |Nawen| --[0 CT i: w io1ss wow wenwe] | -- 3|] 7 x] _-- _ ii 3 i _rdvd 3 rd 1 Hy 1% Sale repeat 160 20 8AnSaollyutmibciaalServices- Created with Analyst.8R0eporter Printed: 18102120104:02:00 PM Project Data File E02v1a7n1'0s.CPraoljSehcotrstPiFfs Result Table G21710shodrbt InstrumentName __AP! 5000 [SempleName6 [Ac`qAucaiusiistitiioonnDMaettehod||2P/F1C8K/n2e0t1e0xS1h2a.r0t45d7aAmM [infectionVial [+ Timectionvoume [5] SDaimluptlioenTFyapcetor [100 | [WeighttoVolume [ooo | Er | en[ei Results Summary [ER e-- s|Gg | rer| PrHXA 1 [Preis 1 BCPFHA| 0 | 532531)| 7208 180.PFHS EET) No No | Ao " 200% 1 Page 9of 169 301 AnalyticalServices" Created with AnalystBforter weswmmay [rroass Loowmoom|| emna || [|wwoomm|| vvee|] ron ome |0 | omon| [[reesrm [sms TTLooomwmoesn|||0 o 0|em w [oowmweeenn||| wwx | 5 olambia Creat with Analpy5R2eporter Pred 1802207046308 Pt AnalyticalServices ssTsEm E RsIeesccmseemm eessre Quantitative Peak Review 1B iEzSEl A..=. -- EuIPiFTtll hif=Z 32 e ce d = I 7S ] hn l S cBa2s1h o5Pi1Fn8eBc8AMT0i0sased| 3oB2aor1s17s30iC1n-7eP2Fo0BMAsDsaed | J oB2es6oP3iF0nPe1ea9AM01a0s0ed | RBe4is11a35rCi0-2PsF1H0Ae0asd I:3 | FLC ah Let== Divi Hl LkiH 3, po LYPT wen | Ndi, o2Ba6s9oP0inR3eB0S0M0i8ss pe ed | o4B0a3s10s87i01-n0PeF5oH0MSs0.s8ed "i | SoHB3as1o3Pi0nH5e6Aa8M10a0s0ed | S S3a1135sCE 9-a5PF7oI0pX0iAe0sed b7l| Z Hi n i sn Bee "Ph LA 3 Zr ait r]n Bir] itil da]i) 36P3r0r1p6h00 0a oBssolnoclisse | oB4a1s1e5al0cn2po7io0ib0iiAs0s0ed | oBe3s5dp5ie0nre8s0M0]i0s8es | o4d01e380s/01.6s58i07n0ace T T To Flier Lahn of Dnt To el Toba] andi] Tobmadiac dma | CY] -- = | oB4aS5s_3i1.i08n70e1-0P3F0MHi0Ss0sed | oB5a11s35aC0i-4nP7eF0cO0MAs0saed | Bas$Se1_l21i03n4Ce7-0oP0MFDaoAsned | oB5es11e53i0Cn4-e7P0F0OpAi0e0ced 0 Before O After AS Pa11ogf1e69 a0 LS CSolaumbiaservices CrweithAanalytsptR.ee6p3ordter Printed: 18/02/2010 40200 PM Ton Ratio Confirmation iB zl zl 3 5 ESz hem||i=2 tl a t|i:Shy h . i3=] 4 rns 2130P1F6E9A20 0a oBaseline oMissed | 2630P1E2P1E9R02 Da Baseline Missed | 209.0P1F8E9.S02Da Baseline oMissed| 31P3R0H1A12000a Baselinec Missed Wong Peak Wrong Peak Wrong Peak o Wrong Peak ls = Hl 363P.F0H1D3A1.2 Da oBaselie oMissed | 309P.F0/H9G9.S02Da Baseline oMissed | 5S1_5.1034C70F.F0D0Aa oBaseinec Missed | WongPeak Wrong Peak oWrongPeak NB PFBA and PFPeA Go nol have qualifying on Fransiions O Before 0 After )NA BasWerloinneg PMeiasksed Page 1201169 304 4Columbia AnalyticalServicesTM CrweitnAsntased Printed: 18/02/2010 4:02:00 PM DraonwaeFrite Acausiion GEETaT CaShT att ethad__prCunsiphdoanm ARooreihmeUsed nGeloicuon n Insrument Name__ API 5060 [SampleName 2P/F18C/200.1100p1p2b35.38 AM [ec[ tio onVe olumc e 1[t 52s onvial|| `Acquisition [SampleD Method | | PFCKinetexShodratm owsoaea [Samplecomment Sample Type [DonFactor [Sanda [100 [Weontiovome Joo | || ES --------/ eT Results Summary TNoarmoent ([Exrpaecstaedn)|rc1e3Nraemen|saswaieo| Amrseai | owg/mL) |osg/mLs)| sm | Wtor [preent |sz|wa scerms a[sa0 ss [saws oe | wm | [pprresit1||ssaaanna|| cwoormemnsa |aswsoieoo|| rsown ||oaww ||oomo|| wwmw || wWeo| [prris1i||ceoaaewsnaen|| vwocpormeis ||sstioomn|| wsewisms || ooww || eowo | wm | | w SsTiIi gasaan| ropron |sere | ase | te | | [Sise S rasass | vceron|swe| swam| ton | tev |w|o wo | Heo [cddt ) sos AnalyticalServices" ; IRC Summary | Analyte Peak Name [praaz PFPeA 2 RT (Expected) 1.24127) 70291 T 3.52(3.60) | 43417 85 Created with Analyd Reporter wm fon Ratio No 1.00 No AACnoalluytmibciaalServices CrweinAanaltysPedorder Printed: 18/02/20140:02:00 PM Qu= antitam tive Peak ReviT ew F B = : -3 i =3 io:s Ii.- PFC 02= .10ppb == 21p30r11i65T008 casting oMased | 2117s0c7p7F2E0A08 oBaseinac Missed | cB2a5s3ePl0enp2ee1cr010Mi0s8sed | 311530027F0F0ADa oBaselneo Missed -| |g 3= == i i: = It 3 l 3 lA | 290P9r08e0t008 otesgine oMissed | 40r3a0010p5i0S0a oBaseine Missed | oB3a1ss3Pi0Rn2Ie8cA0M0is0saed | 31153002p7F00iA0a oBaselinec Missed i| 2 E i 363P0/1p6901 0a Baseline oviseed | 31Ta5c0P27T00A08 oSaselne c Missed | oBa3Ps9se5i0nr2es0c0M1i0sased| o 4013800.1p0F5RS.D0a Baseline Missed hy ime "hinges Brier bi ox3 BE iE:l i2 E - -l ol be ca6ss3_s01i1800s.37o.7v0HnDse8ed | 5115a0c4.7PF0O0A08 oBwelinecNissed | cB$aS1s1e5ia0n4ce7Fo07M0iD0sAased| 5115a004.7P0F0DADa oBaselinec Missed 0 Before O After Page 15.01 169 207 Columbia 4 Analytical Services" Created with Analy8R7eporter Printed: 18102120104:02:00 PM Ton Ratio Confirmation rxE o3 iz i= " Lu mgr" |7 A PFC 0.10ppb L=z | ei Temas 2130P/F1B6A920 Da 263P0F2P1e9A02 Da 2090P1R9E9S.20 Da 31P30H/1A218D0a BaseWliionnegcPMeiasksed | Bas=eWlrionnegoPMeiasksed | oBa=sWeloinngecPMeiasksed | c B=asWelrionneg PMeiasksed = cesT Le | oes feed f I "Ld =| 3i Ti sie 3P63F.H03O10A.20 0a 399P.0H1I99S.02Da Baselinec Missed| oBoselinec Missed | 5S1_81034C7P0F0DDAa NA } Baseline oMissed | Baseline o Missed Wong Peak Wong Peak Wrong Peak Wong Peak NG PFBA and PFPeA do not have Qualiying fon ransiions. 0 Before O After Page 16of 169 308 8ACnoalluymtibciaalServices" Created with Analy Fiborter Printed: 18/02/2010 4:02:00 PM PDraotjaeFeitle Eav2a1n7'1s0CPraoljSehctosrPwFiCs Acquisition Method _ PFCKinhoerttdeaxm ARlegsoaritThambUlseed C InefiEQuanT Instrument Name __API 5000 [Sample Name PFC05500 [recov [5 | "AcquisitionDate 2/18/2010 12:43:13AM [nject[5ionVolame| "Acquisition Method [Sampled | PFCkinelexShortdam [lcwszsse Sample Type [owonfacor [Sample Comment |__| WegioVouume [1E 00 r| Jom | Results Summary N[ambe r||ar(aExsnpedcatetnd)| ssceren | swoon| wooArea | osong/mL)| oa (ng/mL) (%) orrvn||saarssse|| ceorrioan [s|summooe|| tmewma|| awsno ||o os||w wn || wwoo| Prous1 | se |wos prws| am| amo| oso |ow |ws| te SSiTmo evan| ceron | swam| wm|1m| oss | sw | o sSfEcC: [mass| verron sa|maom| too |T wo | wm | : *a0 Ze 2 Pa17gof1e68 208 AnalyticalServices Created with Analy Adporter IRC Summary _ rr [C|owsem|aee| wm -- sracer usw |s|w we | ooo 8 lAnualmybtiicaal Services Quantitative Peak Review =7 7= il7] ioc: PriCnrteead:ted18w/i0t2h/A2n01a0ly4d:0R2b:p0o0rPeMr Ts~ i:ol PFCO.5ppb = Ea == 2130P/F1B6A901 Da :Baselionego2Missed i== bo 209.p0r/8e0s.T0 Da GBaseliEneaMissed il=l| 363P0F/H1O6A901 Da oBasellianenc eMissed = i3 | 211730C1-P7F2B0A08 Baseline cMissed | 2630P1F2P1e9A01Da oBaseline Missed | 31135C0-1PF2H7XD0Aa0 oBaseline o Missed A oa ea oc aong Peak Ii E=] LC i3 2 i= a 3 zl | 40138,00-/1P0F3H0S0a Baseline Missed | oB3as1e3Pl0iH2n6eA9cM01iDsased | o3B115a30Cs1-2Pce7F0HMi0XiADsnaseed -- ap aa yp on| ~) isig= z] i:33 | 311530C1-2P7F0H0XADa Baseline Missed | oBa3s99eP.iR0nH1e8X0oS.M01iDsased | oB4a0s13e80i0/n-1eP0MF3iH0SsDsaed py Wg Wao pea | zo oo 1 i. to 4S0_31.8000-3P0FHDSa oBaseline c Missed | 51135C0-4P7F0O0A02 Baseline oMissed | 5S1_51034C7-0PF0DDAa Baseline oMissed | 511530C4-7P0F0DADa oBaseine o Missed 0 Before O After Page 19 of 169 an 4ACnoalluytmibciaalServices" Created with AnaiysPRSforter Printed: 18/02/2010 4:02:00 PM seg eeSF e eee e mp erree lonT RatiT o ConfirmationFT = PFC 0.5p=pb ot + El = i io 1 | joke po i} io 15 o B2a1s3elP0i/Fn1Ee6AM92i0sDsaed | B2a6se3Pl0Fin2Pe1ecA90M2i0s8sed | cBa2s6e8lP.iR0nE9eS9c?0Missed | Wrong Peak p-- Wrong Peak up gl Wrong Peak B3a1s3ePl.Ri0nH1eI1c9A.M20i0sased Wrong Peak hz i = cose f Tepid 3 eemiAz zl erie x S1aCFROA a Ba3s6e3l,i0n3e19o.0MiDsased | c B3as9e9l.i0ne99c0M0is0sed | oB5a1s5e.i0n4e70.0Mi0sased | Baseli)ne Missed NB FF=BWAroanndg PPFePakeA do nal have aWuraolnlgynPgeafokn Tansiians Wrong Peak Wrong Peak 0 Before OJ After Page 20 of 169 az 5AnCaulymtbiciaalServices- Created with AnalyspisR2eporter Printed: 1810212010 4:02.00 PA PDraotjaeFcitle Acauisition Method 0E2w1a7n1'0s CParoijSehctosr\wPFiCs. _PFCkintexShor dam AlRgeosrulitthTambUles:ed 0i2m1e7l1i0csuhaonrt.rdb Instrument Name __AP1 5000 [Sample Name `Acquisition Method TP26C72T601p0pb12524A8 | PFCKnetexShodratm [[iinnjjeeccttiioonnVVoilaulme [[ 5 4]| Sample Type [Sangad| [[SSaammpplleceodmment |[lows-- zescJoi|wviewt ghttoo voumn e[Jo1F m0 acer|| Results Summary [ANpnaarmloyeatte || AtpnlaaalysytceaRnT|| rvocrearmoen[|wowmroeim.nm|s`Ai[nalAayte | too| tas |tos | [nl Exp Conc | my | |Caic. Conc| i | Accuracy owne Pros1 | Prat | a1owz| szseon| topes |aeaso|n cera| ssi| fosssw|o sie | 100 te | | toe | 10s tot| tot | | Ne| re | Sido: [S Taaaas| 1orron | ssrrao| swam| veo | tm | sw | we Flo 2 "C"4 28 Pa21gof1e69 a [ns nmi AnalyticalServices J = IRC Summary Created with Analyst Reporter rou Twn |we[ow|e| [Pris2 2363) arosa0 No 03s 4ASnoalluytmibciaalServices Created with Analyspi9R4eporter Printed: 18/02/2010 4:02.00 PM Quantitative Peak Review 35 T= E= = hE Hx I zl 2130/P1E60A.T0 0a 21173.C0-1P7F2E0A0a pcrBaseline Missed | < Baselaine oMissed iol Icl == 7 if = PFC 1.0ppb 2 sm i = 263P0E2P1e8A002 31135C.-0P2F7H0DA0a | ScBAasLelnTecMissed | oBaseWinaegc Mienssed i== 2i 269P0F/B8S0102 oBaseline Missed | 4013800/-1P0F30HSDa cBaseineoMissed | 313P01H2A6910 0a cBaseinecMissed | oB3a1s1e53i0Cn-2eP7Fo0H0MXiADsased FI FE Tor To Iio o iHi 2 = = iF:S a pon | zl 363P,0F/H1p69A.10 Da oBaseline oMissed | 31153C0-2P7F0F0KAa oBaselneMissed | 399P.R0/H8X0S.01Da Baseline oMissed | 4013800/-10P3F0HSDa Baseline o Missed Sr ings ea Wop pea Was pea Izsl iboix hz= 3{ ih 4s0_31.08100F3F.H0s0a oBsselinecMissed | $1135C..0P47F0O0AD8 cBaselinecMissed | 5155_013407.0507DDAa oBaseinecMssed | 51153C.-0P4FO7AD0a0 oBaseine o Missed 0 Before O After Pa23gof1e69 315 LSSCoolusmebiravices: PrCinrteeadt:ed18w0it2h12A0na1l0ys4t.8R2g9g0ortPeMr fon Ratio Confirmation To po -El i==| i 2 PFC 1.0ppb 7 = |=e : fi = = lsd 213.P0F/1E6A8.20 0a 263P0F2P1o9A2008 209.P0F1E99S.20 Da cBa=sWerionnegPMeiasksed | oBasWeloinngecPMeiasksed | oBaosWerlonnegcMPiesasked | p-- =| iporE-- - i| |== = IE 3 313P0FH1G1A90202 Ba<WsoengloPMeiiasnkseed Tih ite 363P0F/H3p1A902 Da CBaseloMiisnseed | Bas33e9lP.i0Fn1H9e9G.SM20isased | Ba5_1s153e.C0lPc4FM7iDi0snA0saeed | NA BaseloiMinsseed Wrong Peak Wong Peak Wrong Peak Wrong Peak NB PFEA ana PFPeA Go not have Qualfying on Fransiions 0 Before 0After Pa24gof1e69 a6 Columbia OS ervices- PrCinrteead:ted18w/i0h2/A20n1a0ly030SgoPorHer Project Evan's ProjecsPFCs Data File o21710CaShorwif Acquisition Method _PFCKinetexShortdam [SampleName | PFC 50990 [Sampiel> | tcwsz50 [Sample Comment | Results Summary |Nnaamiyeie | AEnxapleyciteeRdT)| SV-- Result Table, GTO ho db Algorithm Used InteliQuan Instrument Name__AP! 5000 jection Vial 5 STanmjepclieonTVyopteame [[S5unda || | biltion Factor WeightioVome Joo] oo AAnraleyate | ExpoCioln)c|| Ca(lncgiGmob)ne | Accuracy Mod? PFPoAT |3.83|109CP6RH0AA | S300| ararao|n sep |sas | 108 | Ne | fSehee| sma| 1aceroa|asw|szeoa0o| 100 |tot| tot | we S13: AtAyeP Pe Lisi Pa25gof1e69 a7 4CAonlaulymtbiicaal Services Created with Analydt Reporter Printed: 18/02/2010 4:02:00 PM IRC Summary | Analyte Peak Name Perea Pros? roe: RT (Expected) Area Modified? wom | mem | we mes | www | we ase Tssas00 | enem | wom[ow | --_-- fon Ratio 100 Too 03s an Columbia 8 Soservices: PriCnrteead:ted18w0it2h1A2n0a10ly4:02:p0o0rtPeMr Quantitative Peak Review I == Tm PFC 5.0ppb 5% bil i=| rozo I = Lor zl : x . Ba213s.P0e/F1B6lc9A.MiT0i0snaseed | Bas21e13l7Ci.-n0eP1F7MB2iA0s0s8ed | 2630P1F2PE1A80| 0a oBaseliecMissed | Ba311s53C.e-0Pl1cF2HMi7XiDA0sna0seed .z = 5 E i i: i i= 209P.r0e8s001 Da Baselines Missed | 40138001-1P0F3H0S02 oBaseine Missed | 513P.0H26A9.10 0a Baseline cMissed | 311530C-2P7F0H0XADa Baseline o Missed alge ep age eg IiZ 2= = = LD i 363P,F0H11D6A910 0a Baseline c Missed | 31153C0-2P7F0H0X0Aa oBaseinec Missed | 3P09R.H0/X8S001Da oBaselinecMissed | 4013800/-1P0F3H0SDa Baseline c Missed SR = bingype cog tog peak i i. it 3 i. i. i= = li = 4S0_31.8001-0P3.F0H0Sa oBaslinec Missed | 51135C0-4P7F0O0ADa oBaselinecMissed | 5S1_51034C7-0P0FDDAa oBaseineoMissed | 5151.30C4-7P0F.O0ADa oBaseine oMissed 0 Before O After Page 27 of 169 a9 3 Anoalluytmibciaal Services PrCirnteeadt:ed18w/i0t2h1A20n1a0l4y:0B2d:p0o0rtPeMr fon Ratio Confirmation PFC 5.0ppb ibof1Lt 124 i:=;oI 33 h i bW2il e i ocTleesfe || 213.P0F/1B6A92.0 Da Baseline c Missed | 263P0F2P1E9A02 0a oBaselinec Missed | 269P.F0E9S902 Da c Baseline oMissed | 313P0F/H1G1A802 0a Baseline Missed Wrong Peak Wiong Peak Wrong Peak Wrong Peak Tn = = bool |: = A ta EE a I These 363P.0R/H31O9A.20 0a 309P.F0/H9G9.S02Da 5S1_51034C7F0F0OADa NA BaseWlrionnegcPMeiasksed | oBasWeliionnegcPMeiasksed | BaseWlrionnegcPMeiasksed | Ba=seWrloinngoePMeiasksed NB_PFBA and PFPeA 00 nol have qualiying ion ransiions. 0 Before 0 After Page 28 of 169 320 8AnoallyutimcablServices" PrCinrteead:ted18w/i0t2h/A2n0a1l0y4sP0F2b0r0tPeHr Project Data File E02v1a7n1s0CPaoijSehcoirstPFwiCfs Acquisition Method _ PFChinetexShdoarmt RAelsguolrtitThamblUesed CIZntTeTlTi0QsuaonR 195 Instrument Name__API 5000 [AcqSuisaitNimoanmDepa_tel__e|TP2F11C8/1200p1p0b 1:11:52 AM "AcquisitionMethod | PFCkinelexShdoarm [S[amSplaeCmompmlenet d|| LcMS285E [mjec[6tonviar| [iSnjaemcptlieoTnyVpoleume [5 | | WDieliugtihotntFoactVoro__l[10u0 me [000 | Results Summary [NAanmaeis ||A(nEaxlpyetcteeRa)T Anraeins | ExpgCimobn)e|| Ca(lnegiCmotn)e | AGGUAEY| ogy PFBA1 | 1.26.27)| 13C-PFBA | 4346600| 5019200 | 1000 | 1100 | 110 | No | [Prpeat | 3.53050,| 13CPFHcA| sa00500| s7asso0 | 1000 | ma |mz| No PFES1 | 4194.26)| 180PFHS | 2737500 woo | maw |m|3 we| PFHAA1 | 5.25.30) | 19C.P|F6H35x05A00| 5773500 | 1000 | 1070 PrHPA1 | 6.14.23)| 13CPrHeA| sis0s00| Z097s00 | 1000 | oso | 10s | No | PRHXS1| 6.2063|0 180PFHS| 2737500 oo |w |ow m | we| STI | szsean| naceron sere| zoe| 100 |o|s sz| we [Ssesec | sees|T rscproa | seratoo| seraieo |T 00 | 100[00 [ve| i0 e2l( e Pa29g0f1e69 El PAYCF oluvmbiaP---- Printed: 18/02/2010 4:02:00 PM IRC Summary [pram om | we |we| wo 8 umbia PrCinrteeadt:ed18v/i0t2h/A2n0a1l0y4s:P0R2M:0R0rtPeMr Analytical Services" op Er eee Quantitative Peak Review -------- eee ET PFC 10ppb eeeemere? 7 To 3 = Ea oe =! ow = i 5 i= = 2130P1R6B9AT0Da 211730C1.7PF2B0A02 26P3F.0P12e1A9.10 Da 311530C2-7P0F0HA0a soBanseigne c Missed | oBasecliuneec Missed | A oBaselT inec Missed | cBaseliWnoe n: Mipeassed i i i: i= 269.P01r80e.s0 0a 40138001-1P0F3i0S0a 313P0E/H2A6A910 08 Baseline o Missed | oBaselinec Missed | oBaselinec Missed | 311530C2P7F00HA0a Baseline c Missed 2 I = il lw rl 2 ih: 363.P0F/H16P9A.010a Baseline o Missed | 31153C0-2P7F0H0XA0a Baseline c Missed | 399P.F0H/8X0S.01Da 403108101-0P3F.H0IS0a oBaselinec Missed | Go Baseline o Missed i:a ii= iloo - ' a 4s0_3.108/010P3F0HDSa 511530C4-7P0F0OADa 5s1_51034C7.0FF0O0Aa 511530C/-4P7F0O0ADa cBaselne Missed | oBaselinecMssed | oBaselinecMissed | oBaselieo Missed O Before O After Page 31 of 169 2 Columbia LSE services PrCinrteead:ted18wi/t0h2A/n2a0l1y0R-47:O0520b0rtPeMr Ton Ratio Confirmation ETRE Tas HE 2 i==f x = PFC 10ppb = = e - a E, F= = whey 2 213P0F1B1A6920 0a cBaselne c Missed | 263P0F1P2e19A02 Da oBaseline c Missed | 209p.r0e9s9?00a Baseline Missed | o B3a1se3Pl0iHn1e1Ao902Mi0s8sed Wrong Peak Wrong Peak Wrong Peak - Wrong Peak PC 5 7 iJ | <= t| SE - ---- 363P0FH3p1A902 Da 309P.0H/9Y9S.02Da 5S1_51034C7P0F0DDAa Baseline c Missed Baseline Missed Baseline c Missed 6. PFBWAraonnag PPFeaPkeA da no Fave qWuraolnfgynPgeafokn Tansifons. Wrong Peak 0 Before O After ) NA Baselinoe Missed Wrong Peak Page 3201 169 24 8 m Analyb ticalServices PriCnrteead:ted18w/i0t2h/A2n0a1l0y4s0pR2U0b0rtPeMr DFartaatie cE 2rr1ocaa ort wi Acquistion Method _prCknetexsnor.dam AC gorthm Used T netiuan Instrument Name__ AP! 5000 [Sample Name TPFC20Zo0pmoTIE [r[ neoctinonVahame 7 [5 ] [[C S`SAaacqmmuippsietio >on Methodm [|LoPwFsCm aKsnsertexSa hdoarmt ]E [SawmWpilgemTyopveoume [ JS E oaogna] s| [rans erro [FRrmeiissrults[|SEurmatemaarRyT[ener[omwes[Fnr0asiws ||[mGCalorey|[|aGwemmCane|| i||w|| Torrent [ssa| cr|sam a | ww|om| on | sw | w eros | ass| swore |zwi|toosooo| mao | mao | m0 | we [priont|ese | cera|sunwn|swam | moo|we| | wo| so: 2 7"5ile Page 3201169 a2s Analytical Services IRC Summary Created with Analy Reporter (ores [Eprors Torun ssrscoorema mam |ow[ww sceamn| we om |e wm | |one sem | mmm | we | 2m |s mem |e | ewms|m | vwee || oosm 5 Soma Analytical Services PrCimedr: 18we1i0h2a2n0a10yts4f028e.6e0drPt i Quantitative Peak Tp Review ho | |lx i| PFC C2R 0ppb ==| oB2as1e3Pi0na1oi68T0Mi0s8sed | oB2a1s1e7ai0nc1ep7Fc2EN0iA0s8sed | oB2oPs6se3i0pn2ee1c8Mts0s0ed | B3a1s1e53l0i02n0e7cF007MAi0sased i IE i- i= cBa2s0e5pir0nee8s0MT0i0s8sed| o4Ba0s31el0ai1n00e3Fch0si0s0sed | oB3sP1se3ri0rn5ee68Ao.1M0i0ssed | B3as11e3l5i00n6e3cF77M0Ais0ased ie2 izl i -h iz3 | cB3aP6s3er0lH/n1gc6oA9v01is0s8es | oB5s1ss5Ti0n2e7cA0t0isDsaed | oBa2s5e5ei0n8ed0c0h0s8sed | B4a01s3s0e01.6lop5FM0iiSDsnaseed iE = = i3 El x z zl oB4as3s_3e1i08n10o0oF3lH0iSs0ed | oB5a1s15ea0l4cn7ep0oi0iAs0saes | cBaSss1e15l30inc4e77070M0i0Assed | oa5s1e15ia0cn4.e7po0E03MAiDsased 0 Before O After Page 35 or168 ar 4 umbia Analytical ServicesTM Created with AnalypRoEfrorter Printed: 18/02/2010 40200 PM fon Ratio Confirmation = TEE i= | i--- PFC 20ppb a oT i== a t-at4 z TL 2130P/F1B6A9200a 263P0E2P1e9A0208 209.P0F1E98S.20 0a oBasWerlonnegoPMeiasksed | BaseWlrionneg PMeiasksed | oBaWrsonegclPMieiasnkseed | Tem 7 = to i of == | | pu] ol pot 36P30F1H31A920 Da 399P.E01H9I9.S020a 5s1_135c0F47D00A02 cBWarsoneglPoMeiiasnkseed | 0BaWosneglcPMeiiasnkseed | BaWsroengloPMieiasnseed | NB PFBA and PFPeA Go nol have Qualfying fon Fansiions 0 Before O After 313P0R1H11A92008 Ba Wsroenglo PMieiasnkseed Trop NA BaWsroenglaPiMeianskseed Page 36of 169 28 Columbia GR services PrCinrteeadt:ed18i/t0h21A2n0a1l0y402S00FPrM DaPrtoajeFcitle Eav2arn7'1s0CParioSjehcotrstPwFiCs Acauisition Method _ PFCKinelexShortdam AlRgeosrulitthTmablUesed~~ IGnTtliTQOusahnon Instrument Name__AP! 5000 [SampleName_ TP2F2C0510p0ob130 A [ijectionvialaTs -- ] [[SAcaqmuipsiiteio>n --ie[thLod o|PvFsxz5netexsho| SDrailmupdtlioeanTFyampcteor Results Summary [nRianltts [|RAnesymsyRT sve[ome[0A0nais [|EExRpCTone[| oCalme Coyn || A"ccurac||y vo | PRHAA1 | 5.25631)| 19CPFHXA| 6177700| 23062000| 50.00 |s0d0 | 101 | No | 5780" S13: 1 pv 55 Lust Pa37gof1e69 329 Analytical Services CrweithAanaltysFReepordter RCSummary rows en | ew[we |e porsAsz amEeTnE |E we |C | ew ras oem |ww|e| ew | - 8 lmbia I Analytical ServicesTM Quantitative Peak Review 5 Id zl Tm i il i:- p zl -- PFC Ei o-T J m :i a 2130P1F6B8A.T0 0a 21173.C0-1P7F2B0A08 26P3F0P2e1A8100 a GBaseline peMissed | BaselianencgMeissed| o Balsealinge oeMaissed ;= isl bl : hx ix I- i 206P.r0a80s01Da 4013800-1P0F3H0S.08 313P.0R1H2X6A9.10 0a = oBaselinauen Missed | oBaselnine tMissed | 7o Basteilicnoego 2Missed i=l i i: i 363P0E/H1P6A001 Da 13135C0-/P2F7H00KA0a 309P.F0H/X8S0.01Da Baseliange c Mieassed | m Basey line cpMeissed| o Basellinaeo aMissed Lo : i3 ix i hs i 4S03_.108/010-3F.F0HDSa 51135C.-04P7F0D0ADa 5S1_51.30C4-7P0F0D0A oBaseline Missed| cBaseline Missed | c Baseline o Missed O Before O After s1w8i0th22An0a1l0y40F2o0o0rPM ) 5 P27F00ADa inenczMissed P27F00A0a ine2c Missed P10F3.S008 inwe rc Missed 7P4F70O.0A0a ne Missed ge 39 of 169 ES 4AnSaollyutmibciaalServices- PriCnrteead:ted18wi0t2h2A0n1a0ly4p!012R.e10po0rtPeMr lon Ratio Confirmation TE ibu | i- | PFC 50ppb [7 J iJ:I =Fk 1- 4 B2a1s3eP.l0Fi1nB6e9AM.2i0s0saed | o2B6a3se0Pl2Fi1nP9eeo.A0M2i0sased | c2B0a0s.e0lP/iFn9eE9.Sc02MDisased | Ba3se1l3Pi0nH1e1Ao90M2i0s2sed < Wrong Peak Wrong Peak Wong Peak Wiong Peak. A i| a ME e iE oe empiri o B3a6s3eP.l0Fi/nH3e1A0A.20MiDsased | . o Ba3s0e9P.l0iH/n8eY9S.0M2iDsased | Ba5sSe1_l51i0n34eC7F0oF0MDi0Asased | Na Baselineo Missed = Wrong Peak Wrong Pea Wiong Peak NB PBA and PFPeA do nol have qualiying on Transitions. o Wrong Peak O Before 0 After Page40.0f 169 32 8 S Columc bia services: PrCinrteead:ted18w/i0t2h/A2n0a1l0y4s0PR2E.H0B0riPeMr DPartojaeFcitle o2E1wa7n1'0sCPariojSehcotsrPwFiCfs! Acquisition Method _ PFCkinetexShortdam AlRgeosrulitthTmablUesed 2InTt7el0isQuhaont 100 Instrument Name__API 5000 [|SAacqmupilsietNioanmbeate ||2P1F8C22001p0m11-08V87 Ath [menjcetctoonnvVoatrame [5 5 ]| [SAacqmupisiietlio>n Method _|| LPFoCvhsizn7e3texShdoarmt Oto Factor [100 | [Samp| leComment [WeinttoVome Joo | Results Summary oAnmais | A|nopataidyyieRT| sronn [se FTReE T|SB G o || onSo eocomo)c Nets prant | 1232n| 1SGPFEA | 40160| sists0| 00 | 2060 | 103 | No Pron | 3530.60)| 13GRF|RSTA a0 | foa0000 | 00 |2110 |106 | No| [Prost |aa0azs)| 1e0prns| z7s|staaztnso0nn [200| wa | 102 | mw Primal | 5256.90 | 1CPFRXA | St00a00| fo7e00| 00 |zid0| 07 | No PrHpA1 |6466.29| 130PFHXA|S1asi0| amees0|200| a0 | 107 | No PFHxS1 | 6.25632| 180PFHS| 2789400 | 17097000 | 2000 | 2080 | 103 | No S30 [eas@an| naceroa | azetono | zzssaon| 100 107 107 | No 5S1e3e6 [rssaes|rscpron |saetonn|azeiom | 1.00 100 00 | No I a ZA,Pj9le Pa45gof1e69 3 ee nalytical Services: [mmm rRCSOMWQOQRry [wren| mi Created with Analyst Reprer we | JE fore ewem| vw |we] [[oomormman |smwuamn|wwwww ||w wo |w Tw ] . Columbia LS SBRservices: Quantitative Peak Review = = ra i. | i 3 | = i Created with Analy1R1ep4orter Printed: 18/02/2010 4.0200 PM PFC 20ppb ICV 57 i3 213P0/F1B6A3T0 0a 211730C1-7PF2B0A08 263P0F1P2e1A901 Da 311530C2-7P0F0rADa oBaSseolinnegc Missed | cBaseeineyoMissed | onBasleliynec Missed | 7oBaseloinneogMissed i] i3 A 209P.r0a80s01 0a 4108300-1P0F3H0S08 cBaselaigneggeMeissed | BasolhiniecpMissed 2 5 i i a zl 363P.0E/H1p69A.10 0a 13135C0-2P7F0H0XA0a oBaselinoc Missed | c Baseline Missed eR bol Px To a 13 = i3 El A SL " 31P3F.0H12G6A9.10 08 311530C-2P7F0H0XADa | oBaWsoeinngeceMaissed | E oBasea ineo Missed | lL: i i: 2 a 309P.R0H/X8S001Da 40138001-0P3F0HSDa | Baseline Missed | Baselinec Missed 3 Feet Fa iE hz fz 4S6_3108/01-0P3F0H0Sa 51135C0-4P70F.O0A0a 5S1_51034C7.0P0FDDAa 511530C4-7P0F0OADa Baselinec Missed | cBaselneoMissed | oBaselinec Missed | oBaseline o Missed 0 Before O After Page 4701 169 ES Columbia 4 Analytical Services Created with Analy1R1ep5orter Printed: 18/02/2010 402.00 PM Ton Ratio Confirmation TE | -!I EE i. I 7 = PFC 20ppb ICV. = Lo . lh o-r]i Ho[ "i he SB 2130P/F1E6A920 Da 263P0E2P1E8R00a 20P9F01E99S.02 Da 31P3F0/H1G21A09a0 oBaseWloinnegcPMeiasksed | BaseWlrionnegoPMeiasksed | cBasWelrionnegcPMeiasksed | c BasWeloinnegcPMeiasksed [EC " Heo k3l i He ssErm i[i 53 | Peper 363P01F3H1p6.A2 0a 309P.F0/H9I0.S02Da 5s1_51.30C47F0F0D0Aa NA GBaseWlrionnegcPMeiasksed | BaseWlrionnegoPMeiasksed | BasWelrionnegcPMeiasksed | BaseWlrionnego PMeiasksed NB PFBA and PFPeA do nol have qualiying on ransiions 0 Before 0 After Page 48 of 169 33 5AnualmybtiicaalServices PriCnrteead:ted18w0it2h12A0n1al0y3R2a4g.0o0rePrM DPraotjaeFcitle 0E2v1a7n1s0CParlOLRoCngEPwFifCS Acquisition Method _PFCkinetextong dam ARlegsourlittThamblUesed GIzntie7lii0Qiuoanng db Instrument Name _AP1 5000 [SimpleRame [PC opm Gov ``AAccqquuiissiittiioonn MDeattehod | 2P/F17C/k20n1e0t7e:5x3.L2do8anPmgM [SinajmepctlieonTVyopleume [G5uay Control | [ SampS loCa ommem nt | p|Lcl us_ 2.e 85F _|Weignovoume [000 | Results Summary [Analyte | Analyte RT Fae | Epcot|Cae on [Rees| oq? Name [pront | (Expected) 122036 |1 3cP|FsaoOstoAo| awArreeaaoo | 2(n0g0/m0L0) | (ntga/dm0L0) | (9%2). | Mo Prat |2010s| ticera | aso| srooun| mmo |mo| wm | Proat | sasaon| nceron sora| wom | swe | | we| Pru1| samaon| ce|rteenm | ermin|e maw | maw | sz | no | Prost swam| neeros ossooo| zoom | reso| 01 | no | Proon1 | sssse|rac|eassro| smo | mm | 4 Print |so|n1iceo roon |as|sorom| mm | mame | we | wo rE ec Lode Page 4201 170 7 AColumbia a. AnalyticalServices" RCSummary Createa win Anais: Kponer Printed: 18/02/2010 3:24:00PM Lr] [s.1ac.pr0n [oocrma prose [rorwoenzrros [sooceron [roma | 19pm Froty ie) [oscrrom [PFT rome a [_tzsas [somo| we | ow [owes | 0 | we|ow | [[2|oassso@|iwom| ves | esseeo | mew | wNeo | wwee | [secon| mews | Ne | we | [[o [| wmowe|ewn o| w [omen | ssw[we | ve | ss |asuen| ae | we | we | [emus |wom [we | we | Page 4301 170 sss Columbia Services Prcnted.r1u81ne02n2a0a130se3c4a0nrPH QuaCnEtitative Peak Revi= ew m i = = a 41P3r0o1n601 0a 41173.C0.0P7F2O0R08 h o Baselip ne Missed | oBoseiniegclsissed =p "PFC 2I 0ppb CCV. i ] ioa | 4620P4E1N9AT008 Baseline Missed|o 4618300.4PF2I3AD0a Saseline c Missed ia hay il i iE i= il pu a uA | 4p03r0o8s0002 coaseineoMissed | 15033C.0P/F80O.0S08 cBaseinechissed | $1P2.r0O14A69T0 0a cBaseinecMissed | 51153004.7P0F00ADa c Baseline c Missed =ipe Ae ony ime izzl == i= i: = 5P63r0U/A51A9T0 0a Baseline evivees | 561a5c0.2P7F0U0M0A8 oBaseing o Missed | 509P0r8o0s0t08 Baseline Missed| o 5013300./p8E050S0 Baseline < Missed a4 x1l bua Ha 7 I= he h- - 12P.o05o6n910 0a oBasineoMssed | 6115a0c/.1p6F9Bo0A0a cBaseinectissed | 620P6T1A90T 0a cBaseinechissed | 611530/.1p6F9B0oA08 Baselineo Missed i i= 713P0E6T6E0R0] 0a Baseline cMissed | 0 B6a11s5e3l0Ci7-n1Pe6F09DMO0iA0s8sed 0 Before O After Page 4401 170 a PASColumbia Analytical Services Greatea win Anais #honer Printed: 18/02/2010 3.24:00 PM fon Ratio Confirmation PFC 20ppb CCV. 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TH EI - | - Ih 213.P01F6B9A.TDa 211730C1-P7F2B0A02 263P0F2P1e9A01 Da 31135C0-P2F7HX0A0a oBR aselina e Missed | cBawseolningecMissed | cBaiseigneceMnissed | aoEBaseine o Missed 8 i lc i: A. = = Ih 200P.r0/e8s00TDa Baseline c Missed | 40138001-0P3FH0SDa oBaseinecMissed | 313P0RH2X6A001 Da oBaselnecMissed | 311530C-2P7F0H0XADa oSaseliec Missed iizE3 i[2 I-Cl zcl > 363P.0F/H1p69A.10 Da oBaselinec Missed | 31153.C0-1P2F7H0X0A0a cBaselinecMissed | 399P.R0H18X0S.01Da oBaseinec Missed | 40138001-0P3F0HSDa oBaseine o Missed oie ip pe dupes |i: i:& i:8 ii: _Ba4Ss0_e3l1,i80n01e-0Pc3F0MHiDSsased | 511530C4-7P0F0OADa cBaseinecMissed | 5S1_51034C7.0P0FDDAa oBaseineoMissed | 51153.C0-4P7F0O0ADa oBaseline c Missed O Before O After Page 43of 169 343 LS lamba Analytical Services prCinrteead:ted18w1i0t2h1A2n0a1l0y4d.0Ha2s0o0rtPerM fon Ratio Confirmation "PFC 20ppb CCV Sm ew = po A- B! e | wl| i | ho i =| ol | J Tie 2130P1F6E9A20 0a 263P0F2P1e9A.2 0a 2090P/R9E9S.02Da 313P0R11H02A0 0a BaseWlrionnegoPMeiasksed | BasoeWlrionnegcPMeiasksed | cBasWerionneg PMeiasksed | o BasWerlionnegc PMeiassed oi 616. l[s iow]ml a pl 5 a[ -s 8ZH ho - oz N i Third 363P0F3HR1A902 Da oBaselne c Missed | o B3as9sP9l.Fi0nHe9Xc9S0M2iDsased | Wrong Peak 5 Wrong Peak B5aS1s_3e.l10i3n4Ce70F.F0MDi0Asased | NA Baseline o Missed Wrong Peak Wrong Peak NB. 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