Document GzoYy3DJwOMyD3oOKVOXOroJY
CO Oi
3DE YE&p221"D
Li/ii/MA _y?Jp)
< DATE )
< LOT >
4448* LBS* < EST WT )
PROCESSES VpP ( ) YE-721-D < M)
APPROVED BY: FMP 11/08/82
COMTYP JOB NAME: 1YE721DMM
I 1 ivOBTAlN FOR S-12
I 2Ay OBTAIN FOR S-34 I zA.OBTAIN FOR S-38
I 4^4>0BTAIN FOR S-40
I 5 A,OBTAIN FOR S-44 1 &A OBTAIN FOR S-47
WEIGH IN: OPTIR 22. , MK
T-____
OP'TR l$3, MK____ T-______,______%
rr WUI'U/fci f
--_
___
USE ~T
"a c c t
LBS i N-CODE | LBS -- ii ------- ------- 1
68 i 108-A | 68
600 i 4-A ! 600
120 i 3-A i 120
195 i 32-D j 195
350 i 3-A ! _ J50,
61 i 711-BD4i^ ^'"44? 1
| WEIGH IN: OP`TR JL MK JZL. T-
OP:'TR
MK T-
\ 1* <500 G) WATER INTO V-358 \\0T\ RUN V-35? INTO V-351 6 PUMP IN V-351
111TO 55* <2600 G)
&&FT IN N-108-A FROM SI* *.
5 MIN 6 RECORD: PH_^/if<9.0-lA*0)
ADJ TO F'H 9.8-9*9 & RECORD: PH.._7if
ASSUME 50%
ASSUME 66%
RUiL-tNTO V-351 FROM BADGER METER
QPJR__I^___ , MKJSt____,
*
FROM V-351 TO V-358
FLUSH V-351 6 PUMPING LINES WITH 1000G
ER INTO V-358
ADJ TO 74* <3530 G) AT /7-69*F
RECORD: VOL_W* 6
| STIR 5 MIN ^RECORD: PH____ <7*2-7.4) &
G/ML J&Sl JL < 1 * 55-1 * 058)
| NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK
i LIST 6 ATTACH* TAKE 1 QT SAMPLE.
I RUN 20* <996 G) WATER INTO VPCBRD N-41-D STORAGE TANK TO PUMP FROM. CIRCLE ONE: 402 410 411 420 424 425
1 1 CHECK WITH CU SUPV: | ^STORAGE TANK MUST CONTAIN AT LEAST 1900 I GAL: 402=2^^44.0=20*, 411=38* , 420=20'
| 424=20* 7l425=557 J ^STORAGE'TMr^6tT HAVE STIRRED AT LEAST
I 20 MIN SINCE LAST ADDITION OR ADJUSTMENT | ^STORAGE TANK MUST BE ISOLATED UNTIL ALL | PUMPING FOR THIS BATCH IS COMPLETE I^T^SET METER FOR 300 G 6 PUMP TO SV |M,,
LOT:----- --EQUIP | MEMT| |
CQMTYP JOB NAME: 01YE721DMM PAGE 02
DATE PRINTED:i1/08/82 I USE I N- |ACOT I LBS | CODE | LBS
5v i^aTATAPPRox" ? g o ~g " w h i'l e~c o n t in u i n g ~ t o " pu mpT
51 | CHECK PH & DENSITY. RECORD BELOW. IF NOT CONTI I IN RANGE, STOP PUMPING 4, SEE SUPV.
"
-I____ I
--
i( I
I
I I * PH -.Mdt. <2,2-3.7)
U DENSITY: ^AMk G/ML <1 .270-1 .328) ' IF S--23 OK 6 WHEN S-22 COMPLETE, RECORD
I
I DENSITY M$e G/ML ON TRAPPED SAMPLE
IJPROH END OF S-22 PUMPING.
J$TUSTNG DENSITY FROM S-24, FIND METER SETTING FOR
"T I SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
I ACCOUNTS FOR 300 G ALREADY PUMPED IN S-22.
I CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
>II
#** TABLE ##*
Il
iI II Ii
1 WMM MM MM M.MM MM MM MMM..MM.M. M. MM MMMM MM M.s nm
1 G/ML SETTING 1 G/ML SETTING 1 G/ML
1 1.270 1259 1 1.291 1146 1 1.312
1 1.271 1253 1 1.292 1141 1 1.313
1 1.272 1248 1 1.293 1136 1 1 .314
1 1.273 1242 1 1.294 1131 1 1.315
1 1.274 1236 1 1.295 1126 1 1.316
1 1.275 1231 1 1.296 1121 1 1 ,317
1 1.274 1225 1 1.297 1116 I 1.318
1 1.277 1219 1 1 .298 1112 \ 1.319
1 1.278 1214 1 1.299 1107 1 1 .320
1 1.279 1208 1 1.300 1103 1 1 .321
1 1.280 1203 \ 1 .301 1098 1 i 'K'y?
1 1.281 1198 1 1 .302 1094 1 1 .323
1 1.282 1193 1 1 .303 1089 1 1.324
1 1.283 1187 1 1 .304 1084 1 1 .325
1 1.284 1 1.285
1182 1177
f g1rr.3^0o5TL il
1073b
I 1 .326 1 1 .327
1 1.286 1171 1 Trirr TWo 1 1 .328
1 1.287 1166 1 1.308 1066 f 1 .329
1 1.288 1161 1 1 .309 1061 1 1 .330
1 1.289 1155 1 1 .310 1057 I 1 .331
1 1.290 1151 1 1 .31 1 1053 1 1.332
SETTING I 1049 J 1045 | 1040 |
1036 1 1032 | 1027 1 1023 |
1019 | 1015 I 1010 | 1006 | 1003 |
999 | 995 | 991 | 987 |
983 | 979 |
975 I 971 I
967 |
1| I|
I|
1i 11
1|
|i
i .. 1 \ '"'1 I| 1i
1i 1| 1j
1i 11 ri ii
ii ii ti ii !\
II II
II J 41-D I 4094
iI 330X,, I 57-A |__ :_
I 33-d I____ JJt-1 ?-D | .2.
II
iv
DUP050059729
LOT* .
*EQUI!;` ME NT |
_ C.OMTYP JOB NAME: 1YE721 DMM
i
PAGE 3
DATE PRINTED:i1/08/82 I USE | N- | USE I LBS | CODE | LBS
EN 1 QT SAMPLES OF S-19 & S-31 SOLUTIONS 6 TITRATE TWICE NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
9.5-9.9 OR IF THE TWO TITRATIONS DIFFER BY MORE THAN .1 ML N-1-D (IF YES, FLUSH ALL EQUIPMENT & REPEAT TITRATIONS). DO NOT
PROCEED IF N-10-D TITRATION IS OUT OF RANGE ADJUST V-358 FOR A TITRATION PH OF 1.00 Ttt-K FROM FINAL IN-LINE TITRATION, RECORD/LOWEST,
ML N-IO-D
HEN S-32 TITRATION OK, STRIKE V-358 THRU BOTH
UNDERSURFACE DLSTRimTORS INTO SV IN 44-J6 MIN
RECORD : START JXiS&mgSr TOTAL MIN^J^Jl IL ,
NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
BUBBLES APPEAR IN SIGHT GLASSES
\
IMMEDIATELY DUMP IN N-4-A FROM S2i SET TIMER \
15 MINUTES
i
DURING S 34, WASH IN V-358
2 MI^JL- RECORD P:`HH_,,J6_Z._(1 -7-1 .8)
I I F'BXS,
( MUST BE + >
J^P^StlR TOTAL OF 15 MIN FROM S-34 &
RECORD: TEMP_7/___F (67~73#F>
*DUMP N-3-A FROM S-3
3 MIN
|4<2^01JR IN N-32-D FROM S-4
MIN
IN IN LIQUID ALUM USING BADGER METER
3 MIN 6 FLUSH ALUM LINE WITH WATER
iw4<^^KrvDUuMnPr IN N-3 FROM S-5
145 I STIR 4 MIN FOR S-49
|Kh I RUN IN HYDROCHLORIC ACID USING WEIGHT &
39 ONTROL PANEL
MK
7 MK
47 | JNJRING S-45 SIFT N-711-B FROM S-6 INTO V -390
jr Wt ITH AGITATOR ON IN 1-2 MIN
| SSTT3IR 1-2 MIN TO MILKY SOLUTION
302 9
SV WHEN S-45 COMPLETE, IMMEDIATELY RUN IN N-711-B 8 SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV
WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
UNTIL FOAM SUBSIDES.
HP IN BLANC FIXE N WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
275 128-AI 275
OP OF PAGE 1
RECORD: CODE R 2 MIN * j
LOT ___
ORD: PH__#iC___(5.8-6.0)
IF^IECESSARY, ADJ TO PH.5.8-6.0 6 RECORD: PH-_____QH.&..
ASSUME 50% ASSUME 66%
7-D 33-D
FLOOD TO 153' (7298 G) & STOP AGITATOR
OPTR
DUP050059730