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FORM NO.45A 201-B TRICHLOR TYPE 107 SHIPMENTS 1,2Trans -Dichloroethylene Carbon Tetrachloride CIS 1.2 Dichloroethylene Trichloroethylene Perchloroethylene 1 ,1 ,2 -Tr1CKLOROETHANE PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION LAKE CHARLES, LOUISIANA LABORATORY PRODUCT REPORT 1965 JAN FEB MAR APR MAY JUNE JULY AUG SEP OCT NOV DEC 1966 Avg . Avg. % 0.004 A 0O n n 0 0.09 , 0 0 0 ,0 (Q.Q1 % (0.01 0 (0.01 (0.01 (0.01 (0.01 0.01 (0.01 (0.01 (0.01 0.02 (0.01 (0.01 (0.01 % 0.01 0 00 0 0 0 0.01 00 0 0.01 0 .(Q.Q1 % 99.39 99.46 99. ift 99./,9 99.46 99.50 99.47 99.45 99.42 99.51 99.48 99.47 99..51 .99.48.- a (0.01 % (o.or 0 0 (0.01 0 0 (0.01 (0.01 (0.01 (0.01 (0.01 0 0.01 (0.01 (0.01 (0.01 0.01 (0.01 (Q.Q1_ (0.01 (0.01 0.01 (0.01 (0.01 (0.01 (0I01 (OwOL. GOL a 0.05 0.05 0.05 0.05 0.05 0.04 0.05 0.05 0.06 0.05 0.05 0.05 0.06 0.05 NPL % 0.14 0.14 0.13 0.13 0.13 O.U 0.14 0.14 0.13 0.13 0.14 0.13 0.13 0.13-- Appearance Clear Spot None Residual Odor Color Specific Gravity 20/20C None APHA (5 1.460 Distillation Range C Free Chlorine Low H 1 GH 86.1 87.7 None Water Content Cloud Ptint C (-10 Non-Volatile a .0011 pH % As NaOH Acid Acceptance % As NaOH Copper Corrosion 7.3 .0003 0.14 None Standard Stabi li ty CK TYL % .00? ADH Alkalinity .012 -----------------------1---------------------------------------------------------------- Clear None None 7 1.460 Clear Clear None None None None 87 1.460 1.460 Clear None None 5 1.460 Clear None None (5 1.460 Clear None None (5 1.460 Clear None None (5 1.460 Clear None None (5 1.460 Clear None None 5 1.460 86.1 87.6 None (-10 .0013 7.3 .0002 0.14 None OK .008 .012 86.1 87.7 None (-10 .0013 7.2 .0003 0.14 None OK .008 .013 85.9 86.0 87.5 87.6 None None (-10 (-10 .0011 .0008 7.1 = 7.3 (.0001 .OOOK 0.14 0.13 None . None OK OK .009 .009 .012 .012 86.0 87.6 None (-10 .0008 7.1 .0001 0.13 None OK .009 .012 86.0 85.8 87.6 87.6 None None (-10 (-10 .0015 .0020 7.1 7.2 (.0001 .0001 0.13 O.U None None OK OK .010 .010 .013 .013 85.8 87.7 None (-10 .0019 7.5 .0003 0.15 None OK .010 .013 86.0 87.7 None (-10 .0012 7.4 .0002 0.13 None OK .010 .012 Clear Clear Clear None None None None Non Non (5 6 6 1.460 1.460 1.460 Clear None Non . (5_ 1.460 86.1 87.9 None (-10 .0010 7.4 .0002 0.14 None OK .010 .013 86.1 86.1 66.0 87.8 87,6 _ 3ZJL None None Nogs . (-10 ("10 (-10 .0012 .OOU .0013 7.3 7.1 _ 7.2, .0002 .0001 .0002 O.U O.U- 0.14-- None None None OK OK- OK .009 .010- .009 0 a .012 .013_ SL 013020 CONF] PENT I lL r iubjec : to 1 rotec i ve 0 der Ot ITtfT Judici a 1 Di trict Court No. 91-11 5 TR1CHLOR TYPE 1,3 SHIPMENTS TRANS 1,2-DlCHLOROETHYLENE Carbon Tetrachloride CIS 1.2 DiCMLOROETHYLENE Trichloroethylene Perchloroethvlene 1.1.2 .Trichloroethane * % % % % * 1965 Avg. JAN FEB LAKE CHARLES, LOUISIANA ' LABORATORY PRODUCT REPORT MAR APR MAY JUNE JULY S GOL %. NPL % Appearance Spot Residual Odor Color Specific Gravity 20/20C Distillation Range Lot High Free Chlorine Water Content Clouo Point Won-Volatile pH % As Ha OH Acid Acceptance % As NaOH Copper Corrosion Standard Stability TVL aDh Alkalinity apha C C % % 1 - * cnH Sub j' C" tw -r,*A 1 ttiEHT Prote -iai n ,AL i Ttive istnt Order t"Com t- < if Mo 91-1 R5 S_,L nQnlonUoZil AUG 6EP OCT NOV DEC 1966 1 Avg. | 0 ;o.oi 0 -- (0.61 1 0 (0.01 0 - (0.01 1 ~0-- 0 0-- 01 99.99 99.98 99.98 99.98 1 0 0 0 -- 01 (.01 (0.01 (0.01 -- (0.01 1 *- 1 1 1 00 0 0-- --0 - fi 1 01 I 1 1 Cle^r Clear Clear Clear ClearJ Hone None Non None 'Jone None - NoneJ Nonel (5 C5~ (5 $ (5 J 1.466 1.466 1.466 - 1.4661 I 66.5 66.$ 86.7 86.7 1 87.1 87.2 87.3 87.3 87.2 1 None None None - None 1 (-10 (-10 (-10 (-10 (-10 \ (.(5531 ToDDl .0001 (.0001 (.00011 9.4 9.6 .0007 .0009 --- 9.4 9.6 .0008 .0010 -- - 9.5 1 .0008 1 1 - - - - *" 1 -- - - I - - - - -1 ---- 1 I 1 1 1 | I FORf.^R.45A201 .8 B; / TRICHLOR TYPE "5 SHIPMENTS ,2Trans 1 -Dichloroethylene Carbon Tetrachloride CIS 1.2 OlCHLOROETHYLENE Trichloroethylene P:rchloroethylene l .1,2-Trichloroethane % % % * * * 1965 Avg. JAN GOL NPL %. * PITTSBURGH PLaiE GLASS COMPANY CHEMICAL. DIVISION IAKE CHARLES, LOUISIANA LABORATORY PRODUCT REPORT FEB MAR APR MAY JUNE JULY AUG SEP OCT NOV DEC 1966 AV6< 0 0 15--------------- 99.50 0 (.01 0 (0.01 099.52 0 (0.T5T 0 (0.01 0 99.43 (0.01 (0.01 0_ 0 0 OQ./,g 10.01 (0.01 0 10.01 0 99.48 _ (0.01 (0.01 \- * 0 00 0. 0 0 000 0 Appearance Spot Residual Odor Color Specific Gravity 20/20C Distillation Range Lot High Free Chlorine Water Content Cloud Point Non-Volatile pH % As NaOH Acid Acceptance % As NaOH. Copper Corrosion Standard Stability TYL adh Alkalinity apha C C % * o01L nU1lotUnZoZo , i' 511V1 jp COMF -t to JucKc ldehti Protec ial Ui <\L; L-ive sine1 r^pr rni r U No yi-i +5-------- Clear Clear Clear Clear Clear None None None None None tone None None None None - 6--------------- (5 "5 5 (5 . 1.461 1.462 1.461 1.462 1.462 86.4 88.4 None (-10 .0001 9.4 .0008 0.10 None OK - 0.013" 86.6 87.3 None (-10 .OOOl 9.4 .0007 0.11 None CK -- 0.014 86.6 86.6 87.4 87.6 None None (-10" (-10 .0002 ;.oooi 9.6 ".OOIU .0009 0.12"' 0.10 None None UK OK --- 0.014 0.014 86.6 87.7. None (-10. .0001 9.5 .0008 0.11 * Non OK 0.014 1 TR1CHLOR TYPE 11C^SHIPMENTS 1Trans .2 -Dichloroethvlene Carbon Tetrachloride CIS ti1.2 chloroethylene Trichloroethylene Perchloroethylene 1 1. .2-Trichloroethane * % % % * * 1965 Avg. JAN pea PITTSBURGH PLAlE GLASS COMPANY CHEMICAL DIVISION LAKE CHARLES, LOUISIANA LABORATORY PRODUCT REPORT MAR APR MAY JUNE JULY 0 AUG SEP OCT NOV DEC 1966 Avg. 0 to.01 0 98.91 n 0 0 (0.01 0 98.95 0 (0.01 00 (0.01 0.01 00 99.22 99.00 (0.01 0 00 0 (0.01 0 99.02 (0.01 (0.01 GDL %. NPL * 0.12 0.14 0.07 0.11 0.11 0.26 0.26 0.22 0.26 0.25 Appearance Spot Residual Odor Color Specific Gravity 20/20C Distillation Range Loi Free Chlorine y/ater Content High Cloud Point Non-Volatile pH % As NaGH %Acid Acceptance As NaOH Copper Corrosion Standard Stability TYL ADH Alkalinity apha C C % * sl ov n10nU?4Ji , CO 4FIDE 'JflAL: Sub ject j Prot ecti vf "Ortfe of 14 :h Jud Lcial Pistr: ct Co IL L N 9T- TT43 Clear - 5 - Clear -- - (5 - Clear None None 5 1.450 Clear Clear -- None rr-- None 5 ~~ 1.460 - (-10 7.7 .0003 0.25 - - 0.014 0.024 -- (-10 7.2 .0002 0.2S " -- -- 0.015 0.02/* 86.3 87.7 'None (-10 .0012 - t-10 - 7.4 7.4 .0004 .0002 0.19 0.22 Non - OK - 0.011 0.017 0.016 0.028 86.3 87.7" Non ~TW- .0012 7.4 .0003 0.23 None OK 0.014 0.023 * FORM N0.45A201-9 PERCHLOR TYPE 209 SHIPMENTS Trichloroethylene Perckloroethylene - 1,1.2 TRICHLOROETHAHE U -TETRACHLOROETHANE EPE . 1965 Avg. % % % % * Appearance Spot Residual Odor Color 20/20CSpecieic Gravity Distillation Range Lo* Hi gh apha C Free Chlorine Water Content. Cloud Point C Non-Volatile gm/100 ml pH HOLME % Copper Corrosion Acidity ml of 0..01 N NaOH Flask mg/30 cm* Soxhlet mg/30 cm^ Condenser mg/30 cm* Chlorides ppm SL 013024 1 JAN FEB PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION LAKE CHARLES, LOUISIANA . LABORATORY PRODUCT REPORT MAR APR MAY JUNE JULY 6 - ,uNLit- SWT1 t\l --------------- S ib-jert -to--Pt JcCCtJ of irTTti 3 ItfTTTTc J 1/131 I N O'.--- 1r--1( \ *Ai T er * nil f t AUG SEP OCT NOV G to.oi 99.93 99.94 TU^T" co;di 0.02 0.03 0O O 99.92 ^oT 0.04 0 Clear Clear- Clear -- -- 69 --- - 10 - - -- -- CD------------- to 7.0 6,6 _ (0 -- -- to * *- - -- - -------,, -- LEC 1966 I Avg . 1 0 to.oi 1 99.92 99.93 1 (0.01 (0.011 0.05 O.QL 1 0 01 1. 1 I Clear Clear I None Non 1 None 8 1.625 120 122 None to .004 6.5 .010 -- -- None 1 8I 1.625 I I 120 | 122 1 None | 1to .004 1 6>8 | .010 1 1 1 1 1 1 - 1 -1 *1 1 1 1 1 1 1 1 1 1 FORM NO. 45A20 J -9 A PERCHLOR TYPE 208 SHIPMENTS Trichloroethylene Perchloroethylene 1.1,2 Trichloroetbane U -Tetrachloroethane EPE % % % % % f 96 5 Avg. JAN (o.oi 99.90 (0.01 0.03 0.05 0 99.88 (0.01 n.07 0.04 PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION LAKE CHARLES, LOUISIANA LABORATORY PRODUCT REPORT fcb MAR APR MAY JUNE JULY 0 99.88 (0.01 0.07 0.04 0 99.86 (0.01 0.08 0.04 0 99.87 0.01 0.08 0.04 (0.01 (0.01 99.89 99.92 (0.01 0.01 0.03 0.01 0.04 0.04 (0.01 99.92 0.01 (0.01 0.04 AUG SEP OCT 0 99; 93 (0.01 (0.01 0.04 0 99.86 (0.01 0.05 0.05 0 99.91 (0.01 (0.01 0.05 NOV otc 1966 Avg . 0 __ Q___ 0.01 99.87 99.87 99-89 (0.01 (O.tQk (0.Q1. 0.03 Q-.Q5- 0,04. 0.05 0.05 0.04 Appearance Spot Residual Odor Color Specific Gravity 20/20C APHA Distillation Range Low H 1 GH C Free Chlorine Water Content, Cloud Point C Non-Volatile gm/100 ml pH HOMME % Copper Corrosion Acidity ml of 0..01 N NaOH Flask mg/30 cm'1 Soxhlet mg/30 cm2 Condenser mg/30 cm^ Clear Clear None None None None 68 1.624 1.624 Clear Clear None None None None 88 1.624 1.624 120.8 120.8 120.7 120.6 121.7 121.7 121.7 121.6 None None None None -3 (0 (0 (0 .0007 (.0001 (.0001 .0007 6.7 6.8 6.8 6.8 0.009 0.008 0.009 0.008 22 (1 1 76 76 21 12 66 64 Clear Clear None None None tone 73 1.624 1.624 Clear None None (5 1.624 Clear None None 6 1.624 120.5 121.5 None (0 .0002 57S 0.009 12CJ.T 120.6 12C. 5 121.5 121.6 121.5 None None None (0 (0 To (.0001 (.0001 .0003 6.7 578 79 0.009 0.009 0.010 2, 2 2 3 21 1 1 66 7 8 7 3 8 11 Clear None None 5 1.624 Clear None None 8 1.624 150.6 120.6 121.6" 121.7 None None To (0 (.0001 .0005 6TS----- 6.9 0.009 0.011 43 11 77 78 Clear None None 9 1.624 120.6 121.5 None (0 .0007 6.7 0.010 3 1 7 8 Clear None Non 11 1.623 120.5 121.4 None (0 .0005 78 0.010 3 1 7 9 Clear Clear Non None ^one None 9 _JZ___ 1.624 1.624 120.6 121.4 None (0 .0005 6.7 0.010 120.6 121.6 None (0 .0003 6.8 0.009 ___ 1_ 1 6 7 3 1 7 7 Chlorides ppm 0.05 0.14 0.14 (0.06 0.09 0.09 0.06 o7o5 0.06 0.07 (0.06 0.07 0.06 0.08 . ------------ 1---------------------------------ociL nU i1 OoUnZoOr 1 "YYNFTr RUT T A . R ih jess* t- fr Pi nf- oof of 4Lh .1 i r i ; 1 ni e r j r-f No, ( I -1 J 4 li r t FORM N0.45A2014B .* PERCHLOR TYPE 203 SHIPMENTS TRICHLOROETHYLENE Perchlorocthylene 1.1,2 TRICHLOROCTHANE U-Tetrachloroethane EPE . 1965 Avg. * * % % % Appearance Spot Residual Odor Color apha Specific Gravity 20/20C Distillation Range Low H16H C Free Chlorine water Content. Cloud Point C Non-Volatile gm/100 ml pH HOME % Copper Corrosion Acidity ml of 0X1 iJ NaOH Flask ms/30 cm* Soxhlet mg/30 cm2 Condenser mg/30 cm2 Chlorides ppm SL w l JUZD L JAN PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION LAKE CHAHIES, LOUISIANA LABORATORY PRODUCT REPORT PCS MAR APR MAY JUNE JULY . -- 6 ^ ` ^ '' ;: ; ' ' ;" ' ` r' ' AUG SEP OCT NOV DEC 1966 AV6. 0 0 0.02 0 00 99.88 99.94 ^oToT" ToTST 0.06 0.02 (0.01 0 0 99.92 to.oi O.Q3 (0.01 * Clear Clear - lone - None 89 - 1.624 - - (0 - ~87H -- 120.7 121.2 None (0 .0011 8.6 - Clear Non None 8 Clear Non None 8 I.626 1.625 . 120.6 120.6 121.4 121.3 None Non (0 " (0 r.ooici UOOIO 8.6 - --. -- *-- - - 22 32 10 6 87 2 2 8 8 0.30 0.06 0.18 4 * ----------- tTT li lDuH r"TTTLj ! --Stm- set--fe- )--rtw OT--TTTl h--Jufl . C J O 1 ---------------ft ) i n i .1i'Ai El j rf -- i_______ PERCHLOR TYPE 20? SHIPMENTS TRICHLOROETHYLENE Perchloroethylene 1.1,2 Trichloroethane U-Tetrachloroethane ' EPE >965 Avg. * * % % * ** Appearance Spot Residual Odor Color Specific Gravity 20/20C Distillation'Range apha C to* High Free Chlorine Water Content. Cloud Point Non-Volatile gm/100 ml C PH HOME % Copper Corrosion Acidity ml of 0J>1 N NaOH ' Flask mg/30 cm* Soxhlet mg/30 cm* Condenser mg/30 cm2 Chlorides ppm - -- JAN oorL nU i1TJnU9Z7/ .... _K .VJ PITTSBURGH PLaTE GLASS COMPANY CHEMICAL DIVISION : LAKE CHARLES, LOUISIANA \ - LABORATORY PRODUCT REPORT. F E6 MAR APR MAY JUNE JULY -V: A. AUG SEP 4 OCT NOV 0 99.79 0.61 0.07 0.04 -- -_ DEC -- -- - 1966 Avs. 99.79 o;ur 0.07 0.04 m , m * x - 4 - fi nf bnect 4th J ONFID !NT1AL to Pr idicia itet'ti CrLsT ^--V>*H= .r. iic^e4* ( or nilFfe No. a .-114- 1 Clear OK, "OK---------"5-----------1.623 -- - - Clear -- OK- OK -6 - 1.623 120.5 121.3 None TO .0004 8.3 -- -- -- --' - 120.5 - 121.5 - None -- (u -- .0004 3.3 -- .009 175 -- ' - TT-- -- 2. - 4- - 1.4 U 2. 4 TJ705~ * . - 0.06 FORM N0.45A202-13 . HEAVIES STILL BOTTOMS Trichloroethylene 1.1,2Trichloroethane Pfrchloroethylene U-Tetrachloroethane S-Tetrachloroethane Pentachloroethane Hexachloroethane K * * % K Heavy Unknowns ^ FeCl2 Non-Volatile ppm 1965 Avg. to. 01 (0.01 18.73 5.01 38.80 27.22 2.39 JAN 12.56 3.96 38.12 32.62 3.19 PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION LAKE CHARLES, LOUISIANA laboratory operations report FEB MAR APR MAY JUNE JULY -- - 1 L.Ll. 13.49 3.14 2.54 34.87 29.67 34.35 35.42 2.74 3.21 (0.01 0.01 (0.01 (0.01 8.02 10.52 2.40 3.19 40.14 38.07 34.21 36.03 2.42 2.34 (0.01 (0.01 12.76 3.26 32.55 37.37 2/75 (0.01 0.02 19.94 3.15 25.19 34.71 3.90 AUG SEP OCT NOV - (o.oi - _ (0.01 0.01 (0.01 18.34 22.96 T7T7T 11.06 3.75 3.56 4.09 /a. 68 22.72 20.55 25.83 28.20 36.00 32.99 32.74 39.26 4.95 '4.92 5.58 5.56 DEC 1866 Avg. (0.01 0.01 0.01 ,0.01 13.93- 14.64 3.65 .. 3.45-31.16 30.5933.64 34.9k4.15 3.81 1.85 1.80 1.76 2.16 1.70 1.59 -.94 2.63 3.53 3.74 3.41 2.67 2.83 2.48 54 29 0.90 0.33 51 45 "55 58 65------- 52 0.38 0.41 0.58 0.53 0.66 0.72 57 89 USB 50 70 ~S8 0.88 1.02 1.39 0.76 1.01 0.72 HEAVIES. STILL REFLUX (PER STILL FLED) Trichloroethylene % 1.1.2 Trichloroethane Perchloroethylene % U.Tetrachloroethane % S-Tltrachloroethane % 1.31 2.15 96.49 0.03 0.06 -- -- - _ -- -- -- _ - -- -- *-- - - - 0.04 -- - 3.43 -- -- -- 96.42 -- -- - 0.01 -- - -- - - 0.04 - 3.43 - 96.427 - 0.01 -- DRIED UNSTAB. PERCHLOR Trichloroethylene 1.1.2 TRICHLOROETHANE Perchloroethylene U-Tetrachloroethane % % % (0.01 (0.01 99.95 0.03 -- (0.01 99.93 0.07 (0.01 99.92 0.07 (0.01 (0.01 0.01 to. 01 99.91 99.91 99.94 0.08 . 0.06 D.02 (0.01 99.96 (0.01 (0.01 (0.01 99.95 (0.01 - to. 01 99.95 (0.01 - to.oi 99.92 0.03 (0.01 (0.01 99.95 0.02 -- (0.01 99.93 0.02 -- (0.01 99.83 0.07 (0.01 (0.01 99.92 0.04 H?0 ppm 30 pH 6.7 --N--a-I---T-e-s--t!--.--O--x--id--e-s---------------p-p-m----- Nee. 28 6.7 Nee. 28 6.8 Nee. 28 6.7 Nee. 28 6.7 Nee. 23 6.6 Neg. 28 6.6 Nee. 28 6.6 Nee. 28 6.7 Nee. 128 6.7 Nee. 31 6.6 Nee. 28 6.5 Neg. 28 6.6 Nee. T28 6.7 Neg.__ oOiU QU 11 w30W2fcRv COMF1 TENTH L: ----- O_ af *. ub jec" i 4tn \ :--ter-F tidici rerterrt rl--ETtt i ve Oi tr ic't ?3eT court %---- FORM N0.45A 202-14 DRIED UNSTAB. TRICHLOR Carbon Tetrachloride Trichloroethylene 1.1.2 Trichloroe thane Perchloroethylene % % % % 1965 AVG (0.01 99.99 (0.01 (0.01 PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION LAKE CHARLES, LOUISIANA LABORATORY OPERATIONS REPORT JAN FEB MAR APR MAY JUNE JULY ToToT 99.98 99.97 99.96 0 (0.01 0 (o.ot -- 99.99 (0.01 (O.OT (0.01 99.99 (0.01 (O.OT (0.01 (0.01 99.99 99.99 (0.01 (0.01 AUG (0.01 99.9if (0.01 -- SEP OCT NOV (o.oi - 99.97 99.98 (0.01 (0.01 - 99.97 (o.m DEC (0.01 99.98 (0.01 0.01 1966 AVG (o;oi 99.98 (6.01 (0.01 H;>0 PH NaI Test . Oxides PPM U2 6.8 ppm Nett. 50 6.9 Neg. 51 6.9 Nee. 51 6.8 Neg. 51 o Neg. 50 6.7 Neg. 50 6.7 Neg. 50 6.7 Neg. 52 6.9 Neg. (50 6.8 Neg. 55 6.8 Neg. 51 6.6 N*>p. T50 Neg. 6.8 Kg., u U f J029 1______________________________ --COOT 1DENT Ab Sub je ct to pratei :t i vc-- 0 : 14 th dud it i'di-n .stric No" 91-1 "T3------ Crtii r t FORM N0.45A ?m.t SL 013030 GENERAL DEPARTMENT Perchlor (St,a.) Production T/D Shipments T/D nrTTsm?? tms i Ftl cHlOR ( STAfa . ) Pftootjc r i dN T/D Shipments T/D Inventory- Tons CONFIDENT) Ar. PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION f U'h ^ro,:decistitvroictorCrWou LAKE CHARLES, LOUISIANA PERCHLOPETHYLENE-TRICHLORETHYLENE DEPARTMENT OPERATIONS REPORTNo, 91*1145 Court 1965 Avg . JAN FEB MAR APR MAY JUNE JULY 65.5 8l.7 86.5 89.9 65.9 87.1 89.5 83.7 60,8 85.4 91.2 97.0 57.2 71.2 125.0 68.0 1693,2 2061.7 1928.0 1708.= 1970.0 2460.6 1394.6 1882.5 69.5 83.2 88-0 79-9 72.3 85.9 93.9 68.6 66.0 84.9 67.2 92.4 79.4 88.7 76.3 96.4 1486.0 1518.2 2101.4 1713. 1501.5 1414.0 1942.3 1080.3 AUG SEP OCT NOV DEC 1966 Avg. 80.7 76.8 58.6 73.2 68.6 78.5 63.3 124.0 42.0 41.4 114.2 81.7 2421.9 1006.2 '1519.2 2473.0 1059.C 1823.8 60.3 62.6 57.2 45.6 59.8 71.4 71.1 65.1 62.2 141.8 49.4 81.2 1849.9 1777.9 5045.0 2157.5 2480.4 2047.7 Unstab. Perchlor Production T/D EDC Cl 2 T/T T/T Tri - Eth.Bot. T/T NH^ Las./T 65.7 83.4 0.737 0.728 0.474 0.447 -- 13.1 15.5 88.0 0.727 0.462 10.3 90.7 0.717 0.422 8.2 66.3 0.776 0.463 -- 11.3 87.3 0.742 0.496 -- 15.3 90.3 0.732 0.484 - 13.6 84.3 0.759 0.485 - 17.0 -3275- 78.9 0.746 0.781 0.489 0.473 - 17.3 12.6 60.2 0.872 0.560 - 15.1 71.5 0.814 0.484 23.9 69.3 0.794 0.490 -- 22.9 79.4 0.766 0.480 * 15.3 Unstab. Trichlor Production T/D EDC T/T Cl2 T/T Tri-Eth.Bot T/T NH., Lbs./T 69.3 32.6 0.931 0.919 0.301 0.282 -- 15.2 9.3 88.6 0.918 0.292 _ 10.6 82.1 0.905 0.267 15.9 68.1 0.954 0.285 -- 10.0 90.3 0.937 0.313 - 7.7 78.3 0.924 0355 - 7.6 68.7 0.976 0.306 -- 6.3 61.9 1.011 0.331 -- 4.4 68.1 0.958 0.290 - 10.2 58.5 1.069 0.343 11.3 43.0 1.093 0.325 21.6 59.6 1.003 0.310 - 13.7 70.8 0.972 0.304 10.7 Unstab. Product 02 T/T N2 T/T Catalyst Lbs./T 400* Stm. (actual) Las./T kwl/t mc Hvy. Still Bottoms t/T Unstab. Product Cl' Yield C Y1ELO % % 0.269 0.267 0.149 0.183 1.07 2.03 3924 3146 67.3 55.9 0.017 C.023 82,8 85.4 79.5 80.0 0.265 0.177 2.62 2851 52.1 0.002 85.8 81.3 0.271 0.192 2.27 2830 54.1 0.028 87.5 80.7 0.274 0.333 3.95 3174 59.5 0.002 83.1 77.0 0.264 0,261 0.292 0.223 0.240 0.303 1.03 2.83 1.75 2795 2710 2574 50.4 53.5 60.4 0.025 0.028 0.006 80.6 81.2 30.6 78.3 78.7 76.9 0.298 0.295 2.83 2953 67.4 0.029 77.9 74.7 0.309 0.271 1.86 2600 65.4 0.025 73.7 78.5 0.314 0.627 2.64 3542 78.7 0.018 69.3 72.8 0.343 0.598 4.99 4259 85.5 0.041 67.3 73.2 0.315 0.468 3.64 4032 74.5 0.032 73.4 78.1 0.289 0.325 2.70 3122 63.1 0.022 78.9 77.5 MAN HOURS/T STAB. PRODUCT Production Maintenance Salar1 ED Total Contract Man Hrs. Included MAN HOURS/T SHIPPED 0.662 0.469 0.663 0.441 0.406 0.251 jum_ 1.161 0.0?4 0.000 Bulk Drum 0.063 0.053 C.916 0.783 SALARt ED 0.031 0.029 0.435 0.247 0.249 0.931 O.OCO 0.049 0.644 0.021 0.450 0.621 0.334 0.578 0.265 0.263 1.049 1.462 0.051 0.039 0.047 0.055 0.627 0.953 0.023 0.028 0.440 0.251 0.189 0.380 0.024 0.542 0.474 0.200 1.216 0.000 0.543 0.552 0.194 1.289 0.000 0.053 0.077 0.070 1.388 1.316 1.199 0.026 0.025 0.018 0.573 0.754 0.238 1.565 0.032 0.612 0.647 0.242 1.901 0.000 0.379 0.888 0.278 2.045 0.051 1.061 1.304 0.272 2.637 0.205 0.672 0.937 0.256 1.865 0.000 0.608 0.617 0.241 1.466 0.034 0.086 0.077 0.113 0.073 0.059 0.068 1.016 1.292 1.501 0.959 1.144 1.069 0.032 0.024 0.042 0.022 0.021 0.026 FORM N0.45A 210-2 MATERIAL BALANCE CARBON - TONS Total Carbon in Feed Carbon in Uiystas. Product Process Loss by Difference Accountable Process Losses Blowdown Reactor MlSCELLANEOUS Sue- Total Unaccountable Process Losses Carbon Loaoing Loss Total Carbon Losses PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION LAKE CHARLES, LOUISIANA PERCHLORETHYLENE- TR I CHLORETHYLENE DEPARTMENT OPERATIONS. REPORT 1 96 E JAN FEB MAR APR MAY JUNE JULY AUG SEP OCT AVG. NOV DEC 1966 Avg. 851.1 1047.8 992.1 1075.C 853.9 1152.9 1044.0 997.8 955.8 948.8 891.6 798.1 675.4 638.6 606.4 ft67,9 644.3 903.6 821.9 767.8 714.0 699.0 618.0 510.8 175.7 209.2 186.7 207 1 209.6 249.3 222.1 230.0 241.8 249.8 273.6 557.8 898.0 971.3 659.3 740.1 238.7 231 .2 14.3 15.1 145.9 176.1 9.8 18.0 170.0 209.2 5.7 0.0 11.3 156.4 18.0 185.7 0.0 9.0 180.1 18.Q 207.1 0.0 14.0 15.8 177.6 225.3 18.0 7.7 209.6 249.3 0.0 0.0 13.9 200.5 7.7 222.1 0.0 12.9 209.4 7.7 230.0 0.0 15.9 205.9 20.0 241.8 0.0 17.5 212.3 20.0 249.8 0.0 13.0 240.6 20.0 273.6 0.0 17.6 219.7 50.0 257.3 0.0 14.3 204.4 20.0 238.7 0.0 14.2 200.7 16.3 231.2 0.0 9.3 3.3 6.4 22.5 -20.4 29.1 12.3 12.5 11.6 36.7 16.6 -23.0 14.9 10.2 185.0 212.5 192.1 229.6 189.2 278.4 234.4 242.5 253.4 286.5 290.2 234.3 253.6 241.4 CHLORINE-TONS Total Chlorine in Feed Chlorine in Unstab. Product Process Loss by Difference Accountable Process Losses Blowdown Reactor MlSCELLANEOUS Sub Total Unaccountable Process Losses Chlorine Loading Loss Total Chlorine Loss _ SL 4145. 5044.0 4822.0 5128.5 4054.7 5679.4 5198.8 4905.8 4762.7 4578.0 4331.8 3877.1 4340.8 4727.0 3449.6 4306.2 4136.5 4486,1 3309.0 4580.6 4219.5 3958.9 3709.2 3597.0 3152.6 2836.6 3388.5 3806.6 696.2 737.8 685.5 745.7 1098.8 979.3 946.9 1053.5 981.0 1179.2 1010.8 952.3 920.4 32.0 83.6 548.5 562.2 50.5 92.0 681.0 737.8 15.2 0.0 62.6 530.9 92.0 685.5 0.0 49.8 77.8 501.6 575.9 92.0 92.0 643.4 745.7 0.0 0.0 87.7 77.2 982.4 873.4 28.7 28.7 1098.8 979.3 0.0 0.0 71.5 88.4 97.0 84577-1 865.1 784.0 28.7 100.0 100.0 946.9 1053.5 981.0 0.0 0.0 0.0 72.3 98.0 1006.9 842.8 100. G 100.0 1179.2 1040.8 0.0 0.0 79.4 772.9 100.0 952.3 0.0 78.8 762.1 79.5 920.4 00 47.0 23.5 33.3 108.3 -87.6 132.8 60.9 60.2 ma 175.5 87.5 -115.0 71.4 50.9 743.2 761.3 718.8 751.7 658.1 1231.6 1040.2 1007.1 1113.3 1156.5 1266.7 925.8 1023.7 'ONFID fc'NTIAJ pi ihjnrt to Pr otect ve Or ler n f 4 Hi J 1 Dis rict :ourt No. 5 1-114. . -- FORM WO. ASA 2/0-3 SL 013032 s"bjoctC^uWM/S PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION Of 1U4tih! JiurficiParoi ClP)Lo-n.V: LAKE CHARLES. LOUISIANA iio* PERCHLORETHYLENE-TRICHLORETHYLENE DEPARTMENT OPERATIONS REPORT rfJer Cou^t REACTOR NO. 1 On Stream Time Disch. Press. Temp. F Vaporizer Liquor Dowtherm Out Highest Tube Lowest Tube Sec. Cono. Disch Catalyst Charged Catalyst From Centrifix Flow GPM EDC SCFH Cl2 At R 1 965 Avg. Hrs. T8oo* psia 9.3 248 506 825 796 23 Lbs. 21208* Lbs. 8720* 5.2 6399 2207 10303 JAN 669 10.0 268 ;,Q5 828 785 26 2331 1675 4.4 6418 1326 10252 FEB S72 13.0 258 442 827 797 51 1554 1675 5.0 7561 926 12220 MAR APR MAY JUNE JULY AUG 744 13.9 312 445 823 802 55 2501 2600 5.9 6976 936 11180 610 744 720 744 12.4 13.1 13.3 14.0 285 282 287 _ "288 462 474 505 497 824 "825 826 824 800 803 793 788 --- 72 75 2742 3747 t'T876~ 1773 2740 2430 1900 2080 6.0 4*3 4.9 4.6 7017 7454 7142 6300 1250 154 1776 1879 12086 11757 10514 10995 672 13.0 275 528 823 778 82 6130 6560 +.8 6184 1187 9499 SEP 720 12.6 280 471 818 791 84 1129 2000 5.4 6676 778 11182 OCT 744 13.1 255 474 822 780 65 2830 3000 5.3 6098 753 10540 NOV 662 12.4 280 _ Rm 817 780 _ 69 5710 57m 5.7 _ 6154 . 1465 10851 OEC 733 12.6 260 483 821 784 66 2360 2400 5.0 6006 1532 10623 1966 Avg. 8434* 12.8 283 481 824 .790 64 34703* 14660* 5.2, 6666 1197 11142 Vent Analysis CO; HCL Per-Tri Ratio Pfr \ Tri in Crude % 40.0 34.3 53.0 58.5 50.9 43.6 23.5 14.2 10.9 % 8.9 15.4 11.4 12.5 8.7 18.5 16.8 "370 13.7 1.01 1.31 1.02 1.05 0.97 1.02 1.12 1.51 1.23 % 82.15 33.56 34.68 86.32 34.66 86.95 83.86 84.66 31.35 41.9 33.9 38.8 16.5 16.4 10.1 1.31 1.28 1.63 _ 86.14 84.85' 88.72 49.8 37.8 -9.7- 13.2 1.30 1.23 88.05 85.23 REACTOR NO. On Stream Time Di sch . Press. 2 Temp. (f Vaporizer Liquor Dow the rm Out Highest Tube Lowest Tube Sec. Cond. D i sch . Catalyst Charged Catalyst from Centrifix Flow CPM EDC SCFH Cl2 Al R 2 Hrs. psi g. lrs. lbs. 7721* 9.1 254 506 826 79C 21 25350* 8870* 5.1 6600 2120 7C1 744 13.3 273 439 831 796 29 3059 1675 5.0 7664 1316 10846 672 12.4 272 471 326 799 35 2650 1675 4.8 7133 1079 10388 744 12-2 243 436 326 799 46 2478 2 600 3.6 6736 n-Lef A -- 602 725 12.9 253 443 825 799 13.1 283 158 "825 801 -- 4084 2815 4.3 7236 2174 2430 5.2 8221 1281 532 10671 11786 720 744 715 13.0 13.4 13.1 284 278 257 497 493 510 826 823 822 799 790 786 74 70 79 1361 2908 2380 1400 2080 2000 5.1 4.7 4.8 7695 6957 7164 2817 3042 2208 11218 10964 10280 711 755 13.0 12.0 264 250 339 567 818 820 780 785 82 60 1481 1685 2000 1500 5.3 5.7 6343 5330 1501 1519 10004 3415 618 10.9 744 12.4 517 478 819 821 757 721 62 63 5430 2150 5400 2200 5u___ 5.1 5324. 5905 1975__ 3003 3154 3539 8483* 12.6 _ _ 267 422__ 824 784 60 31840 27675* 4.9 6818 1836 10266 Vent Analysis CO; HCL Pfp-Tri Ratio Peri Tri in Crude % 40.8 -- _ 52.7 54.3 44.4 27.7 18.8 20.2 15.1 29.4 24.9. 31.9_ % 7.4 -- -- 4.8 11.7 9.1 4.8 6.5 16.1 12.9 6.7 6.1 8.7_ 1.02 1.08 1.30 1.59 1.03 1.02 1.41 1.47 1.32 1.15 1.38 1.89 1.26 1.32 80.60 31.30 34.47 86.63 85.52 84.94 86.76 85.73 S5.02 83.04 83.38 SULL 80.05 84.39 Totals FORM N0.45A 2Ordr protective - COUE^PITTSBURGH PLATE GLASS COMPANY .SfiSfl"S- JSicttrlCt CCHHEEMMIICCAALL DDIIVVIISSIIOONN LAKE CHARLES, LOUISIANA SL 013033 REACTOR NO. 3 On Stream Time Di sch. Press. Temp.F Vaporizer LrouoR Dowtherm Out Highest Tube Lowest Tube Sec. Como. Uisch. Catalyst Charged Catalyst from Centrifix Flow GPM EDC SCFH CL? A1 R 02 1 965 AVG. JAN Hrs. 8043* 744 8.3psig. 13.0 254 274 511 442 826 823 797 790 22 25 lbs. 24361* 1537 lbs. 9645* 1675 5.0 5.0 6489 7429 2091 1532 9707 11319 FEB MAR 672 13.2 275 452 325 798 35 2373 1675 5.1 7766 1045 11596 744 12.2 276 Zl66 #*25 799 42 2271 2 500 6.0 7103 800 11402 APR MAY JUNE JULY AUG SEP OCT 573 11.8 272 744 13.0 28? 452 435 824 827 799 "866 -- 2494 2057 2940 2430 5.a 5.3 7373 ~5354 1422 427 10938 12228 720 667 13.9 11.9 295 "284" 462 482 826 828 798 780 70 76 1430 898 1400 2080 5.0 4.5 7889 7143 1333 1441 10963 10613 735 13.4 274 493 821 775 82 2440 2000 4.9 7218 1116 10808 711 665 11.6 9.9 270 266 511 5LA 819 818 81 2162 761 75 1400 2000 1500 5.2 5.3 6364 6222 T% 766 10088 9019 NOV 720 12.6 280 482 819 728 70 2670 2700 5.6 5606 577 906? I DEC 638 11.1 266 506 815 776 .58 4090 4000 4.8 5605 1119 9761 1966 AVG. 8333* 12.3 277 476 823 781 61 25820* 26900* 5.2 7008 1023 10650 Vent Analysis Per-Tri Ratio Coj HCL Per i Tri in Crude % 40.2 % 8.0 - - - 48.8 30~ 19.5 19.6 19.0 20.1 15.1 9.2 6.7 16:5" 11.5 7.4 7.5 5.1 15.7 7.2 30.0 24.2 6.0 9.3 0.99 1.07 1.11 1.16 1.17 1.03 1.43 1.41 1.29 1.44 1.70 1.61 1.51 1.33 % 31.12 80.55 82.87 84.00 82.46 31.73 81.63. 80.75 84.04 83.15 79.15 74.81 85.71 81.74 REACTOR NO. On Sire am Time Disch Press. 4 Hrs. psig Temp, op Vaporizer Liouor Dowtherm Out H i ghe st Tube Lowest Tube cSt Cono. Disch. Catalyst Charged lbs. Catalyst trom Flow GPM SCFH Centrifix EDC Cl 2 At it ' lbs. 8130* 9.3 260 510 326 794 23 9110* 9145* 4.9 6043 2016 9934 744 572 708 13.5 13.5 13.5 283 287 300 422 442 460 827 824 ft?5 799 796 796 27 38 A 5 1548 1761 4911 1675 1675 5500 4.4J 4.7 5.1 7035 7109 6913 1322 993 1796 11317 11495 116#*n 555 12.5 284' 469 826 796 2515 3340 5.6 7260 912 11483 731 12.5 283 477 826 800 1753 2430 4.6 7349 545 10803 668 12.9 283 467 826 729 13.2 281 448 825 798 794 104 82 9610 2754 9600 2080 4.7 4.4 7353 7336 1933 1657 10721 10625 709 720 12.6 12.7 282 280 459 474 822 820 788 759 84 84 1610 3266 2000 2000 4.4 5.8 6765 5850 1175 874 10955" 10681 702 11.3 272 481 823 754 63 4053 3980 5.4 6330 1178 9046 686 9.9 270 525 817 744 66 310(7 3110 53 5325 1502 8989 671 8.8 247 498 818 757 69 6180 6180 4.1 5157 1431 8529 8295* 12.0 279 469 823 783 66 .43078* 43570* 4.9 6653 1235 ~ 10527 Vent Analysis C02 HCL Per-Tri Ratio P 1fh Tri in Crude % 40.9 - - 57.8 54.6 26.1 37.9 19.7 27.4 17.2 18.7 20.7 32.5 31.3 % 9.3 - - 10.0 8.7 14.3 11.9 8.1 9.5 8.0 17.7 12,3 11.1 11.2 1.03 1.15 1.09 1.24 0.96 1.14 1.33 1.45 1.35 1.33 1.59 1.38 1.96 1.33 % 31.66 85.63 85.79 87.80 85.16 85.74 88.96 86.47 87.47 82.45 82.12 81.64 84.96 85.35 *Totals NO. 45 A 2 10-5 SL 013034 REFRIGERA ItL/ Temp. F Warm (Out) Colo (in) SubjectCf0WNT,flL; PITTSBURGH PLATE GLASS COMPANY of CHEMICAL DIVISION LAKE CHARLES, LOUISIANA PERCHLORETHYLfNE-1 R !CHLORETHYLENE DEPARTMENT OPERATIONS REPORT protDe;c;t;i;voe order N- 91-H45 lct Ct 1 965 Avg . 6 3 JAN 12 6 FEB MAR APR 25 30 18 23 _ - MAY - JUNE JULY 58 60 39 52 AUG 67 60 SEP 70 62 OCT 47 40 NOV 50 43 DEC 51 41 1966 Avg . 47 38 DRYING STILL Temp. F Bottom Top Bottom Pressure psig PER -TR1 STILL Feed Reflux Bottom Temp. Overhead Temp. gpm gpm F F HEAVIES STILL Feed Reflux Bottom Temp. Overhead Temp. gpm gpm uF F 203 139 1.40 19.8 37.1 280 184 9.6 96.3 336 256 207 211 138 143 1.45 1.42 213 212 150 _ 162 1.51 1.43 210 178 1.15 21.7 34.7 286 188 22.0 34.6 288 191 21.6 34.6 288 192 20.7 34.0 287 192 21.6 34.7 288 192 9.5 97.9 345 262 10.1 96.6 344 265 9*8 89 r 9 347 264 8.8 79.3 347 261 9.3 86.8 346 "252 211 173 1.00 212 176 0.91 20.7 35.3 288 193 19.4 34.5 287 193 9.7 88.3 344 263 9.9 86.8 341 253 211 172 1.19 208 752 0.85 208 153 0.94 19.7 32.1 286 193 20.0 1773 29.7 32.5 287 289 194 193 * 8.9 93.0 344 263 3.7 69.7 332 261 10.5 78.3 342 263 211 156 0.90 17.2 33.9 287 190 8.7 84.2 347 262 210 164 0.61 210 161 1.11 17.4 38.1 290 193 19.9 34.1 288 192 8.2 97.1 344 253 9.3 87.3 344 263 Feed Reflux PER STILL Recycle To Wash Column Bottom Temp. Overhead Temp. gpm _sai_ 10.31 10.67 10.32 9.19 9.63 9.86 9.26 8.45 8.74 10.44 8.39 8.74 9.54 gpm 20.35 17.15 17.71 19.43 18.19 16.87 16.25 15.98 19.17 19.17 18.09 19.07 18.06 17.93 gpm .277 .256 .201 .118 .176 .192 .060 .002 -- 0.144 gpm 7.51 8.39 9.49 9.49 8.73 8.99 9.40 9.54 8.82 3.32 9.67 8.78 F 275 273 281 288 281 279 279 1279 283 283 282 282 8.31 9.04 281 281 uF 237 246 249 o/.4 244 245 246 257 247 236 250 245 245 246 TRI-STILL Feed Reflux Bottoms ' Recycle Bottom Temp. Overhead Temp. gpm 10.20 9,53 9.84 9.50 9.20 9.43 8.46 7 8.68 9.36 7.37 7.05 7.49 8.65 gpm 73.43 ,76.35 74.81 70.75- 71.33 72.02 70.14 60.48 54.85 53.68 53.99 56.50 60.10 64.58 gpm 8.38 9.62 10.15 9.83 - 9.33 10.13 8.96 8.19 8.90 9.53 6.33 6.21 9.35 8.96 gpm 1.482 1.499 1.249 1.369 1.349 1.320 .779 .818 1.490 1.507 1.531 1.430 1.253 1.304 F 234 240 241 239 237 237 238 234 233 231 231 232 234 236 F 140 141 143 145 145 144 146 147 147 143 142 146 354 144 f 9 W* FORM N0.45A 210-6 TRI TOPPING STILL Bottom Temp. Overhead Temp. F F W ^ PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION LAKE CHARLES, LOUISIANA PERCHLORETHYLENE- TR I CHLORETHYLENE i----------- DEPARTMENT OPERATIONS( REPORT 1965 JAN FEB MAR APR MAY JUNE JULY AUG SEP OCT A VG. 1% 193 201 201 200 200 199 199 200 199 197 190 193 196 197 195 195 195 196 195 195 194 -- ------ ------ NOV 196 194 DEC .196__ 194 1966 Avg. 199__ 195 NEUTRALIZATION PERCHLOR NH3 Flow To Stg. psig gpm A. . 10.5 10.8 10.6 7.24 8.47 8.70 10.2 9.8 8.72 9.8 11 11.9 9.04 9.39 9.31 Tri chlor NH3 Flow To Stg. , psig 10.4 7.c 8.9 7.9 7.5 7.5 ~J7T~ 9.7 gpm 7.55 9.92 10.49 7-17 8.74 9.15 7.97 7.63 13.2 13.4 12.2 14-0 8.46 8.27 8.18 7.90 7.9 6.7 10 8.1 9.87 7.35 5.59 5.72 13.8 11.5 7.63 8.62 7.6 8.0 6.39 8.21 '^ ' SL 013035 -------- & CONF 1DENT1 AL: 'f To Prote< tive ( irder 1 A l-h Tnfl i C i al D: stcici Cour * Ho. 91-1J 45 1* 1 FORM N0.45A210-A PITTSBURGH PLATE GLASS COMPANY PCONFIDENTIAL! Subject to Protective Ordei CHEMICAL DIVISION LAKE CHARLES, LOUISIANA of 14th Judicial District Court .Ho 91-1U5 TERMINAL DATA 1965 Avg . JAN pee MAR APR MAY JUNE JULY AUG SEP OCT NOV DEC 1966 Avg , CH1CAGO Shipments To Perchlor Trichlor TRI-ETHANE"*^ Tons 321 288 264 0 1290 1301 62 1424 133 0 0 0 1356 420 "285 0 379 276 00 0 371 1675 0 611 1042 684 1403 0 0 591 628 502 0 1672 439 0 0 134 137 539 534 Shipments From Perchlor Tri chlor 'TRI -ETHANE Tons 504 696 451 816 352 1226 563 606 440 710 298 189 1048 356 471 7077" 755-- T55 "477'" 719 349 644 392 553 "570 "559-- 888 312 475 539 252 417 701 653 522 826 "563 731 718 419 "427 631 EOM Inventory Perchlor Trichlor "TRI - ETHANE Tons 510 825 ~25 MC KEES ROCKS 682 354 931 139 932 308 354 1444 487 1992 166 49 1798 92 94 1316 1097 746 120 "I50U 839 125 730-- 270 435 1372 834 575 135 T08 1573 T53 117 43 44 68 1011 545 "255 Shipments To Tons Perchlor Trichlor tri -ETHANE" * rmj---------------------------------------- ------------------------- "Vapor Chlor" 790 1368 552 21 Sh i pments From Perchlor Trichlor 'TRI-ETHANE" "Vapor Chlor "1TM' Tons 626 738 579 27 EOM Inventory PtfCHLOR T R1CHLOR 'TRI -ETHANE" & "Vapor Chlor Tons 454 455 590 40 SL 013036 1395 0 0 0 941 175 1007 0 1432 1498 1309 0 0 873 556 0 398 123? 525 0 336 1005 482 8 516 1133 "725 21 1607 1224 1080 43 732 1133 592 6 848 672 736 0 101 1234 980 34 856 103 252 14 594 1256 150 29 1308 119 880 0 459 317 698 0 0 1439" 470 543 0 474 0 1404 768 0 923 0 883 0 0 0 0 0 00 500 1594 378 0 0 0 0 0 635 727 455 0 843 1812 737 0 529 481 595 0 "570 491 392 0 578 425 822 662 505 341 00 586 499 160 0 194 668 664 883 326 154 06 756 126 724 716 484 703 00 1740 592 574 0 1159 666 513 0 1276 68? 768 266 10m______ 00 1001 1193 60 0 339 663 455 6 -- FORM N0.45A 2TO-B | PITTSBURGH PLATE GLASS COMPANY CHEMICAL DIVISION LAKE CHARLES, LOUISIANA TERMINAL DATA 1965 Avg. JAN FEB SUPPLEMENTARY REPORT _____ -- MAR APR MAY JUNE JULY AUG SEP OCT NOV DEC 1966 Avg. P1TTSBURG Shipments To E- SO Shipments From E. 50 EOM Inventory E- 50 SAN PEDRO Tons 1361 Tons 1734 Tons 1392 2497 0 3300 1857 1732 2143 1055 2342 257 0 1703 2040 2087 1448 2662 3355 0 2005 2149 697 1806 3400 1726 2592 0 2355 2681 2227 2297 2087 3028 405 1067 " 3080 2350 1640 1744 2194 1567 Shipments To Perchlor Tr 1CHLOR 'TRI -ETHANE " E- 50 Tons 432 154 222 699 743 656 479 2000 0 0 0 0 1115 0 0 2153 0 153 0 0 753 0 498 3155 ~wr~ 0 57 0 00 2364 0 756 47 481 1243 0 98 T4 0 631 507 0 3152 0 49 0 0 1184 0 770 2400 496 131 154 1372 Shipments From Pe rchlor T R1CHLOR TRI - ETHANE" E- 50 EOM Inventory Perchlor Trichlor 'TR 1- ETHANE " 'Ey E- 50 Tons 518 234 151 964 542 285 726 755 292 226 451 732 255 . 334 162 67 365 287 131 960 2625 575 2226 862 Tons 829 354 817 776 542 740 622 625_________ 1030 943 1204 580 91 203 664 1174 418 335 407 1133 964 179 773 1847 424 421 235 1142 347 434 163 1166 545 959 96 111 536 146 742 1930 424 577 189 1841 385 477 187 3669 560 464 147 1174 321 631 155 1142 433 341 234 994 459 445 194 1615 533 898 963 641 1383 714 235 263 773 314 611 367 176 465 315 158 287 465 337 547 3296 2432 3801 1585 SL 013037 CONI 'IDENT AL: Rh jf= ct to Prote ;tive Drdsr Cl F 1 4tL Judii :ial D stric t Com t No 91-1 ,45 -..................... r......