Document Gm3Oybaj8zzojq8ddZMKqZVbm
\_____
c.v
CG 46
CODE RT-53-1 -D PKG
W 2 S_1982
L2H73
T"5a t e ")
('Co t *?
EST. WT.
LBS*
<fS?
: D.V. 315, 317, 322, #223)
..
PROCESSES
APPROVED BY:
< ) RT-531-Dt (P) EUK-08/02/82
COMTYP JOB NAME"--40RT531DMP.;
STANDARD HRS* ___________ .1
TIME A tt ? SEMI-BLEEDING
EQUIP., 1 WENT J
NAME: NAPHTHANIL RED-LIGHT
| USE I
- I ACCT
) LBS, | N-CODE/I LBS
1 | OBTAIN 4-NlTRO--2-AMINOTOLUENE FOR S6
2 I OBTAIN 3--HYDROXY-2-NAPTHYLAMIDE FOR SI 8
3 i CLEAN, DRESS, CLOSE 24* CLARIF PRESS
15 FRAMES
/X & r> > (j f i/- ?& O
I I 504-C I r . i 150-c i -.
(700 G > WATER INTO -V-______.____
IN HYDROCHLORIC ACID FROM V-324
m____
DUMP IN FROM SI I 4-NIDRQ-2-AMIN0TftLUENE-
f7 li
i STIR 15 MIN TO WET^ - LOT_______
>J TO 42* < i470-G) .AT-S&rW-DEG-F- -
13X330-1-^57-A-i.gltjL
"SIPHON IN SODIUM NITRIT^IN
"
I-
. M_______X-__,
5/ZL..L 725-A 1 138
i^TSTIR 5 MIN 6 RECORD: CR_^_< + ), KI_j^__(+)
I
r
) NOTE: (1 > IF CR-, KI- ADD 204 ,*AS IS*
| INCREMENTS HYDROCHLORIC ACID ASSUME 32%
._! 28-D |;____*
I RECORD: CR_____! + ) KI__i__,,_< + >
,1- - --- I -'
j <2) IF CR+, KI- ADD 10* *-AS-IS*, INCREMENTS | -
I SODIUM NITRITE-
ASSUME 33%- -1
1 725-A 1_____
, 4 LRECORD: CR,,______< + ) KI__^_< + )
- ! '1.
I
` ` ` TSTIR 10 MIN AT^^f^F-MAINTAINING +CR, -H<14 ,i .;L:- |
| FOR SI3 RECORD: TIME START
--I - |
1
MISC
.3 _
SLURRY DICALITE FILTER AID IN 40* GAL. WATER I
I IN DRUM 6 PRECOAT CLARIF PRESS
!
5.
777--
DV WHEN SI 1 STIR COMPLETE-
4
\yr\ mmIP IN DICALITE FILTER AID
I1XTSTtJiCrR 30 MmIiNn AaTt 35-4d eg f
10 I 777-A | 10
a s s u me 33% 1, ____ _'( 725-A i______
f t MAINTAINING +K 1 roftAsL.._ ^
,,^__1 57-A
| (RECORD: STJARRTT. .
KI__L_____< + >
sun
l*m?r WATER INTO-V-
1
ii>^rSLURRY TRISULPHOIL SOAP D -IN' 25G WATER 6 - I 32. J :
'vr >J^PlTUR IN
- ^
....... 1
| DUMP IN 3--HYDROXY-2-NAPT:HYLAMIDE FROM S2 (
!
[ RECORD^ START^/^Jji^" T0 "ET-pii-
i
39- -A A
150--C I 536 -... - ~ 1 I
%
CQMTYP JOB NAME : 40RT531DMP
PAGE 02
DATE PRINTED: V/14/H^
EQUIP | MENT |
_ I USE I
I ACCT
PAGE 2 OF 3 CG 40 CODE RT-531-D <P> . \[ LBS I N-CODE i LBS
. 302
C144G) WATER INTO V-302-
I I' I
6 |2<l^PtfUR tN SODIUM HYDROXIDE
ASSUME 50%
-i 84 I 7-D | 42-'
' RUN IN ACETIC ACID THRU METER & STIR 3 MIN |
i- -# Jr-.
JUfeJdLjz f
h-\ 30-D [ 63 - *
^Oa^rRECORD PH^yjJ-<A*7-7.5) IF .NECESSARY ADJ TO!
f / ::'6Jr~7<5.. i ^
ACETIC ACID ASSUME 70Z
1 -- 30-D 1 ___ -:U.
S ^ *. - vlv RECORD PH^&i.# SODIUM HYDROXIDE . ASSUME 50%|
I -7-D
'
TURN ON V-zZtJ AGITATOR & ADD ICE, THEN OFF AGITATOR
m330I 57-A -| .
|
|
UMP DV THRU CLARIF PRESS INTO DV USED IN. I 1
S 23* MAINTAINING TEMP AT 40-45F* RECORD:
I ......... I
START:TOTAL MIN__^W__,, DO NOT USE V-303 - TOO SMALL
1-
1 WHEN S23A CLARIF COMPLETE WASH DV <S4) LINES PUMP & PRESS FOR 20 MIN OR TO A -CR -
I
TEST ON A SAMPLE OF. TOTAL PRESS EFFLUENT
WHICHEVER COMES FIRST* COLLECT WASHINGS IN
V <S23) RECORD: START_L^__CR__r-ri<-*OR+)
I WHEN S24 IS COMPLETE TEST DV/S23 ) ASSUME 33%
. f 725-A
ECORD: KI_JarL<+); TEMPiK!2?_L<40-45*: F)
,1 57-A
i WEIGH SULFAMIC ACID IN RUBBER BUCKET AND
I - - }
SE IN AND STIR- 5' MIN*
, - ' - -
I - 15. f . 395-D |
RECORD: KI.ljrm* MUST BE-- & IF NECESSARY I
-
J TO -KI,WITH SULFAMIC ACID
-
,| 395-D . 1
ADJ TO 55* <1925 G> At 40-45 DEG F
11X330* } 57-A
;
:
N 33* <330 G) WATER INTO V-260 INSfAl
{. I . "
1 ? 'If-P{
WHEN SIS STIR COMPLETE, POUR IN SODIUM'
|
i ^>M1?DE0XIDE` IN 3-4 MIN*
ASSUME 50% I
HSSI HEAT TO 128-132 DEG F AFAP & STIR 5 MIN TO I
1 ( DISSOLVE. STOP AGITATOR*
320
-I
7-D I 1 60- ....
IMMEDIATELY RUN V-J^ AFAP INTO CV# NO, / - f
AGITATION IN CV- RECORD: START_/J?.3 /*- I
MW----- *.------w
I
134 IN ACETIC ACuD THRU/METER ^S* ^ 5 .MIN i
*t i m____ 4._,,___ ..Il &j AAj x . t
RECORDv PH //*Sn10*5-11.0) ASSUME 50%
IF NECESSARY ADJ TO PH 10*5-11*0
J^RECORD: PH-j CM--
yf RUN IN V-302 AFAP
ASSUME 70% - * -?*>-
I ?8-82 DEG F AND RECORD: ' >
__,,d e g f a n d r e c __l _mj 5_..d e g F
I
jit
-1
30-D1 I '218s..-;' 7-D |___ r_
30-D UJth&z--
!.
V^-V'w-XV.
*y
40 J^SflR 5 MIN, DISCONNECT TRANSFER LINE AT CV I
V^ECORD: DIAZO__r)E__,, <+/-) -
r
; f l^BAS&_sa__(MUST BE + ) PHi^iffei<4.2--4*6)
I 41 WF^NECESSARY STIR^TQ - DIAZQ RECORD:
\f iTi'Oo Tt AaLl ^ MiN.j[i^nssrr?
} ia*ORfr: DIA20 **rLi. "MUST BE -- - -
T/
BASE
MUST BE + yvW a
\. *>
PH
<4*2-4*6)
^
t i i';^rr'.4 *
DUP050061172
COMTYP JOB NAME -40RT531DMP
PAGE 03
EQUIP-! ;MNT J
_ T. u |
T i PAGE 3
.. -Mi | |
OF 3
| i-- I,
CG
i'~r " i\ 11* i
1 r |` | n i i * . ` ` i r i.,i i - irr
40 CODE^RT-531~D <P)
i.i
; * 142 I^h TSo G WATER ATHOT
ATER HIXER ADD. BLANCOL N 4.STIR FOR-S43
<s
'' 260 ' .12
| 43 144 I' 145
i: j46 147
U-TOWR IN N-567-B SOLUTION 'FROM S42, yftEAT TO 194-196 DEG F IN .55-60 MIN AND
RD: HTj4____ DEG F AND REC^Zl.DEG F . S44 HEATING COMPLETE,' RUN IN ALUMINUM
TE SOLUTION THRU BADGER METER. NOTE:
E-IN LINE AFTER N-115-D SOLI N' RUN IN. 30 'MIN AT 194-196 DEG 'F ' - -`i. ;v
LOOD TO 80* <7928G) AND STOP AGITATOR
FIN^ 3/
OPTR
DATE PRINTED: 9/14/82
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DUP050061173
DUP050061174
9 DUP050061175
