Document GKjMnoxO2q8zy5EdXzGm5G8B7

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PIGSE Coniack Custanes Seroice fo further Inform ih oh Scar 0 LIVE ACCESS Page 1 of 2 Seria) Naber: 931169 Frlaor /, res 1205 duitBd. 10. Bo 14 Sovchmpton, PA 19660514 Phone: 215355350 Fat: 215.355.7231wow acaboratrics om DEP2.SDWE-000136 QC Laboratories coalteo: cGhBoTr, wMITBMwIheEn OTYNoEF cManEce Roatan Tap: SF tesa (10): 1 PaEmrer tvs Analytical Report 250.hwo: en , 3: tov. vo: 1555 a Esete ws Test te ine H CpL0a amaorfc2us010wcountsaWthNoct cPeorralrts aLiimointe,of atsdEsEoTtrE ro ecYteTortin8sgllple,REi cron REE Ee tl Se Shiai =A Tesult marked with Jes "DRI" indicates Dthat 6the rersoullt lwass TRE TrE e lcaolcoulsatepd and erepornted omnn a dry leigh basis. on TPE equSiirreSd hsotS dieng tiL n8e daL tess otTherwLis0 e noAt e am1e37s.0s7 Ow: nsE: nPe0do1ww.nas57,70s.0s02n0P6h5T6PS6R0I,Aiss 00.00 eSRD r S TE S SeTi n fo es maiprs, "risHE BBEaUan vpwur rs Perl Tine 4s 10CorToicotn does and resus bless ontact Coston Gritce fo finer \forRiachton scag LIVE ACCESS. rae zor 2 Sori aber: 1169 Tloarsr JMes DEP2-SOWB-000137 Tm C --_-- C ~~ ANALYTOAL REPORT ProNPFoS Analyse ots: oonvazs: ek smin ra uasyt 7aet%argesein Febmary 2008 SE ------ f-- CO WTA RAI wont vee?owe000138 Table Of Contents StandardDeliverables Report Contents TpSictaaCoornfndeshaiLsreStdemrDiaendlditDhveeoRrelpaobritleoosvcrhp.gTarhe acopnseidererdcomgprrta cssllpass cid his TobeofComer re chen TaofbConltenets + CaseNarrative + Executive Summary - Detection Highlights + Methods Summary + MethodAnalyst Summary + Lot Sample Summary * Avalytical Results + QC Data Association Summary + QC Evaluation andlor Data Reports + Chainof-Castody Total Number of Pages TestAmerica 1 DEPZ.SDWB-000139 CasDeoANTa7r02r9a1tive iTpnreesastceAcnmotererddiacniancatDhewiisntvrheeptrohreutlmiwezeterhsooUadSnsaEilPnydzAiecaadtpefpdor.rotvhDeoidlpmtaeortnahmfeoatdcestrosrnslaailsnltdaendafolonyotttinchoaetlemwseoatrrhke.odpTsrohsveuidsmeamdmaporlnyecspaacghe datasheet to assist in the interpretationof the resus. d``TcahotemaprhieaasnvutelswbierehelnaatbreoeorvnailleyowretyodtpfhroerotcsooacmmolppsliewaisntcihneatwnhiiysterxtechpeeoprlttaiabononrdsatnmooertyeedGaAbleIlGroeCwq.upilraenmaenntdshoafvNeEfLoAunCd.i 0Allbe. LPilmeiats(eMnDoLt)e ahnadt sNhoonu-lDdebteeccton(sNiDd)erreesduNlsDhaattvehebeMeDnL.evaUlrulaetsesd odtohwenrw0isethneotMeedt,hroedsuDlettsefcotrion Sols have been dry weight corrected "This raport shall not be reproduced except in ul, without the wien approval of the laboratory. `"SThaempfolleloAwrirnigvarlepaonrtdcRoencteaiinpsthe analytical resus or three samples received 1/17/06, cacocnodridiionngattoadtoecmupmeernatteudresoafm3p1leC.acceNpotaanncoemaplrioecsedwureerse. enTchoeunStaemrpaldedsurwienrgesraemcpelieverdecienigpto.od ``ASntaalyntdiacraldsstandards were prepared using the acid form ofthe compound perfucrooctanoic acd (PFOA). PFOS is a commercial prepared and cerlied solution. aPneriinltueomraoln{s1t,a2n.d3a.r4d-"fCo.rjqoucatnatintcaitcioanciodfwPaFsOAn.lroPdourcfelduoarlot-h 1-e{x1t,r2a3ct-iCoanosctteapnaatnedswualtsounsateedwasas PinFtOrSo.duced at the extraction step and was used as an intemal standardfo quantitation of `SE`Tahmexpslaetmplre praesecntaetnddiinAtniaoslyrsenpiosrt was analyzed fr the target analyte by TestAmerica Denver SOP DEN-LC-0012A. aFnordiwtatserexstaiamcptleedsuasi2n5g0S0mLi.daplhiqausoet eoxfteraaccthiosnalmepclheniisquaeciwdiifhiemdewtihhan1olmLcoonfdi6iNonHeGdIGs1ol8ution Scaermtprildegeiss.paEsascehdstaomuplgehisthsepickaretdriwdigteh,tthheeiannfearyntalesstaarnedaerldu,tepdrwioihto4exmtLracotfiomne.thAanfoelr.thTehe fina volume is brought 10.5 mL using methanol and the extract is analyzed by LOMSIMS. MTheeMettQhoCdhSBalomanpkldiessprocessed reagent water siked with surogate and prepared vith each bmiatch of 20 samples ofthe same mari. Tha method blank was non-detect at ie reporting cEoancchenbtartacthioin plerveeplasroefdLwaibtohraatLoarbyoCroanttorroylCSoantmrpolleSswaemprleewi(tLhCiSn).conTthreolrmociosv.erios of two Testhmerica 2 DEP2.SDWB-000140 An"laiTmhlieyttL,iCbcSiaalpseeCrdociemngmthe,rnefctoorsvPeFrOySa.ssoTchiiasteisdawnitihdQicCaboarttchhat8d0a1t7a44m6aywabseobuitassieddehtihgeh.QC contol SaTuhnceh,bPocFonOuoSltdesdnaomhtpabtleotrhdeeulpiRlaibPclOaytcewaaarsnatlceyadslic.sulfaotreOd bCasbaetdchon80va1l7u4e4s5bsehloowwetdhearnepRoPrtDinrgosiumil,ofan2g0.asIt No ther anomaies wero observe. Testanerica 5 DEP2.SDWB-000141 EXECUTIVE SUMMARY - Detection Highlights Daar7oass eamETER 12512560-1 01/15/08 11:45 001 eerroons 12512560-2 01/13/08 08:30 002 perroosn 12512560-3 01/15/08 09:30 003 ePrroosn RESULT RpErROeRTING wwe o0l.o0t7s o00o1l0 wualet o0.o0n6 0o0w1 uuge o0.o0l5 oowo uween wAewmniLorpTICNL oDEmN --11cc--0000122 DDEeNn 11--001122 EDeww "-110c--0000122 Testhnerica 4 DEP2.SDWB-000142 METHODS SUMMARY Den70291 PnuaeTER 1c/ms/us, eron References: EY OSpeevreartninTgrenPtrocaebdourraet.ores, _ awwLerincoaL Da -1c-0012 Denver, Facility Standard wPeRmEiPoApRATION TestAnerica M DEP2.SDWB-000143 METHOD / ANALYST SUMMARY pam70291 mwvTIcaL memo omewssr DE 16-0012 Jaqueline Bonnett References: Dan SOepveerartniTnrgenPtrocLeadbuorrea.tores, Denver, Facility Standard ner om 003601 TestAmerica DEP2.SDWB-000144 SAMPLE SUMMARY Dan170292 wos smvPLER CLIENT SwLe tp KXPePPQQV3 000012 L122s5i1z2s5e6o0-1z KPPO4 003 12s12560-3 nToemms(9c) oeargson ee 58 A --_-- RAahshitdssrNDp"rneeestlcst o1gn0 d em1 hd. Rkoformltgprsse. ce ehrtead reatpboes ct6. ista,sdt, Pi,s,s. etar1. orryes ex oi, ects, 56 ol, opt, ho, ot oSue mi msmoee 0011//1155//0088 0181::3405 01/15/08 09:30 Testanerica DEP2.SDWB-000145 oc raboratories Client sample 1D: 125125601 are DLoatt-eSaSmapmlepl4e.d...: 0D1S/A1L57/002891-1010:145 DWaotrke ORredceeriv#.e.d.:.: 0K1E/P1Q7U/I0A8A PPrreepp DBaattche.i......:: 80011/71474/608 Dilution Factor: 1 `AAnnaallyyssiiss TDaitneel.:: 0211:/2221/08 Method... DEN -LC-0012 Matrix.........: WATER Peaomna.nETER Pros smsour RuuvroRTING oars 00..00173 0o.o01o0 gg/nm s13u0m4noopaRtoen 1304 PROS cpeonvcearry 10"n5 RecovsRy u(m5w0rt-s200) (50 - 200) Testamerica DEP2.SDWB-000146 oc Laboratories Client sample 1: 125125602 LDoatt-eSaSammpplleedf....:|: 0D1E/R1I5T/002391-0080:230 DWaotrek ORrecdeeirve4d....:: 0K1F/E1O7I/I08A Matrix.........: WATER PPrreepp DBaattchei...|..:. 0810/11774/408 Dilution Factor: 1 aAnnaallyyssiios DTiantee....: 0211:/3291/08 Method.........: DEN -LC-0012 PamaeTER } meso RuEprORTING mars veeosn o0.o06n1 0o.0w00 wwaasit `Tsaucmseoapnrtosa. } 13c4 pROS pREaRcCoevnety P2S06 RLeactovsery ((5500 -- 270000) Testamerica DEP2.SDWB-000147 oC Laboratories Client sample 10: 125125603 DLaotte-sSanapmlpelIe..d.:.: D0E1A/I1I50/20981090:0330 DWoartke ORredceeriv4.e..d..: K0P1P/Q17I/L0A8A Matrix. .....c WATER PPrreepp Daattec..h. ...:. 80011/71474/608 Dilution Factor: 1 `AAnnaallyyssiiso DTaitne.e..:: 0211:/5251/08 Method... DEN -LC-0012 epnrroaneTER ros mu0.0r65 olo1s RuEproRTING ous o0.0w10 ga//tu `3suammoabnRtoan 1304 PROS RpEeRcCoEvNETRY 160s2 LReocrorveery 5(500 -- 220000) TestAmerica 10 DEP2.SDWB-000148 swiss oor 002 003 QC DATA ASSOCIATION SUMMARY Daa170291 sample preparation and Analysis Control Wumbers wm awewmwiroTnICN. WATER DEN -Le-002 WATER DEN -Lc-002 WATER DE -Le-o0a2 LBeAACcHk W BorTepM A sowrass so1rass sows mo ow sourase sorrase sours Testhnerica 1 DEP2.SDWB-000149 METHOD BLANK REEORT mre MClBieLnott-TSoatmpl#.e..:: RDIEAAI1T700209010-446 Work Order #...: KEPSOIAA ADnialluytsiiosn DFaatcet.o.r:: 011/21/08 PPrreepp DBaattec.h..4.......:: 80031/71474/608 Matrix.........: WATER Avalysis Tie..: 19:30 spraomnETER pros sesur iREaROrRTING wuts wemop PwS 50..00100 gn/atr DDEENN 1160--0000122 suim3cReoapartoen 1304 pros RpEecrocveERy B2y6 RLaemceorvsemy ((5500 -- 220000)) Cnhoome): rn i vic 1 0a -- Testnerica 12 DEP2.SDWB-000150 LABORATORY CONTROL, SANPLE KVALUATION REPORT oc C1l0i5enLtot-LSoatmp#l.e.l.:: RDSIAAL7700209010-446 Mork Order 4...: KPPSQIAC PPrreepp DBaattec.h.-4....:+ 80011/71474/608 AAnnaallyyssiios Tbaitne.e..:: 0119/:2461/08 Dilution Pactor: 1 Matrix.........: WATER rpornTER Pros mPREcRoCvEENRTY =2 RmEmCOsVERY (009 - 113200)0 wDemmwo-n1G-0012 Dm rc-002 `Tsaucmssoapartosn 3c Pr05 er excar v Recovsy 75 ((5500 -- 2200001) o_ we_ : _____________ Testhmerica 13 DEP2.SDWB-000151 LABORATORY CONTROL, SAMPLE DATA REPORT nee C10lSienLtot-%Soatmpl.e.f.:: DRS&AA117700020901 446 Work Order B...: KFPSOIAC PPrreepp BDaattec.h........:: 80011/71474/608 AAnnaallyyssiiss Tbaitme.e..:: 1091:/4261/08 Dilution Factor: 1 Matrix.........: WATER PArmoanETER vros semrovew wawnsoumRED wuts oEacaNT mcoveRy hemion _ 00..220000 o0.1z02 agr/tt a21 DDev 1-16c--00001172 si3ucmemoraaoTaE _ 1304 pros samreccoveny 7a RLaemceorvsery ((500 -- 2200000 wwe: pnde cpr TestAmerica 1 DEP2.SDWB-000152 LABORATORY CONTRO, SAWPIIE KVALUATION REPORT nei C1lCi5enTtot-LSoatmp8l.e..l:: RDOENA1I700209010 446 Mork Order 1...: KPPSQIAD PPrreepp DBaattec.h..4......:1 #010/11774/408 aAnlaylyssiiss TDiamtee....:: 2001:/0221/08 Dilution Pactor: 1 Matrix... WATER ppraomnETER eros PREERCCOEVNETRY 11270 a RLRaCwOrVtEsRY 609--1213000) iwewmo1n0-0012 pan 1e-0012 sTaucmsooraoras 134 p05 semRmcoaErRrY nTo RLEaCwOVsERY ((5s0o -- 2700007) pow: Spdme ey cn TestAmerica 15 DEP2.SDWB-000153 LABORNTORY CONTROL, SAMFL DRTA REPORT C1l0i5enTtotT-oStam8p.l.e.:: PPrreepp DBaattec.h..4......: Dilution Factor: ernmosnseTaR ros `ssucmemoaparToen. 1304 prOS DRIIARLLIIO0209010-446 801 011/71474/608 _ Mork Order f...: KFPSOIAD Matrix......_.: WTR AAnnaallyyssiiss .TDiantee...:: 0210/:2021/08 mspoiwkeer MwEAoSUnRED vwzs pmReccoEvNeTRy memo o0l.o0220000 0o.l0ozmsza wvaaflti 712s RDrNs 116--0000117 sseerccoavTy n02 RLepcaoTvssry (G5o0 -~ 720000)7 + Sn reak so ceo Testamerica 16 DEP2.SDWB-000154 MATRIX SPIXS SAMPLE EVALUATION REPORT npc 5LotL-oSta-mSpalmepl.e..4:: DDeIAALI7700227991-001 Work Order 1...: KFENTIAC PDraotpe DSaamtplee.d....:. 0011//1176//0088 07:05 DAantaelyRseicseiDvaetd.e..:: 0011//1271//0088 PDirleuptBioantcPhac4t.o.r.: 81017446 Matrix........: WATER PeaoanETER veos suT3mcoeaparToEn 13ce pros oCrs(9) t:eret fo ig RPEmCROcVNETRY 1055 ed LmmeacoTvsaRy 005 -- 112mm eRemcRocvaerr P1Y03 ed _ ebionn1.6-0017) Dax 10-0012 RLeocrorvsery ((5500 -- 3200000) SE Testhnerica 1 DEP2.SDWB-000155 MATRIX SPIKE SAMPLE DATA REPORT none 5IotL-oSta--nSpalmeple...:: DDA8ALLI100229719-001 Work Order f...: KFRNTIAC PDraetpeDSaatmepl.e.d....: + 0011//1167//0088 07:05 DnantaelysRiecseiDvaetd.e.:.: 0011//2117//0088 PDriolputBiaotnchFacit.o.r.:: 81017446 Matrix.........: WATER eparRonnETER oros sTaocmeowprnosn 134 PROS wor): _ ASMnOtUrNLTE SAPNITKE AMEMAOSUENDT UNITS M0W.0060 00.1220000 00.126185 uvga//1k RaeEcRocvasvrty 6103 RpEeCrOVcEeRY METHOD. P1Y05 RDss 116--000027 RLeactovsaRy G(5o0 -- 720000) Testamerica 18 DEP2.SDWB-000156 [THE | lo Fra ol EE 1ooTd= HcH 2 3 Ho E5 ER5E NT sy g : HRE)iEg si HeS| aHlar STH O"D BL F Re Sl 5g ] kh 2 Ki SEI. PTRR S A QL [] HEshEat 0we `H|elHijmusEs FE Ep | ln Lh 3 HE Sess gH |e HH So = sR R 1 MH - 282 E[ iIY z2 8HE 2g rk [IS 1 i: $ restrmmrion @ 3 lH q ii H iH NB |. 3= ran nero fio E eae f3iilszzfseszrssE2ir:z|s8 gil c8 2: ff) 88 iH 20 oepzowaorsr