Document G53gzbX5ydKNvEwgXEddm7Yw7

+ C QCLaboratories Analytical Report Eo-- RyR SEE nSEeI c pI SHroRan:s eme e ETE OL i SORE SL roe ne m EBmr sBmnar wore m AEm D EE. Prog No: C0927. UNITED WATER _ CITY OF ORANGE PASID No: 0717001 oe oe mPEoeTi mgBmmer ins " tee ATTTACRHyEDArTE--D: SH Tes -- = a WEa eemE PEE ho weer SmHeAmTTEmRm , B apJiEBL of atS e onnE ceonmfserteCftoetotoo mceicatoypee, SEE l iL as moni ma oh me SB ARTEEEN ed tfh StSTeAber RTh TTtR eA A mrpse = A result marked with "ORI" indicates that the result was calculated and Teported on a dry weight basis. a E L the FeS EsS noCiooaamSLeonnemFLeSEtIp eeO nt onOBseUsetE BBmhEo06trMs,nGrone ge rar Seri mater: ssn Torso JMores 0SdatiBd, 0. 814 oon, 546.54Ps1555.50 21535575 tron nerzsowRaoss QC Laboratories Analytical Report SF cnt ws cvs, wor rn i ces I nea o vo: i. Yo: 6574 Proj te [eo E----r---- UNITED WATER _ CI OFOTRANYGE SID No:0717001 F rpPFmeOAnl ets F AiTnTAmeCuHeEeD F Rwee eTeteonte ASHHEEE RBAeR e E n usotnemcorepgnaycn, rm heh CE EE rr Shand tnpee ry ee 32 5 CIlcta02,0Areer on ry ei soils, i scram Ecietes Mata aa [ParmeterEporft Sare0 Eh r1e55t08 CLoL0LL31M,0 PAIGE.FL S795 11223,CT P-0768,0E PA-OLB.KY tt 0228.40 Bory rorympereo, 206.69 PAOGBiOos IsaSyiP.h G3 RPTE ly Ris tEhS e aElo!e R GJPAE"WRaximRadm CIoS nvtaminanmt1,0Lv0eves]o"r fwolroapgsaravEuieteerarr.i,P"LwsFelS cruosstiemE er sspectR ific paermirt R laimiiot,s. -G5744,) an ero Yes Lo cTiotion kes an Femi eit eoiar CotsSa cE Ty. FeROSS prov "Siig Lie access. wera Sort rs 5501 Thassos DEP2-SOWB.000159 rTeesltANmeerniccaa ANALYTICAL REPORT PFOAPFOSAnatyais Lots: oaposozsz NikiSmith SQ1o3C0u5tLdaabmooprtosnatoCrriooosccm,.sy TestAmaria borsore, nc. ProjectManager Po17r,20t08 C akoys) 55 amonSt rt CORE SGI STL vemos DEPZ.SOWE.00160 . Table Of Contents Standard Deliverables Report Contents ThSetGaonvdeiaLsrSedarnDadenoldditDhveeeRrreaapoblslceCposcvekopga.geTairsecroenpsoirdtecreodtmprlle te meta oie.Theron eo Tableof Contents * Case Narrative * Executive Sum -Detm ectia onHir ghligy hts + Methods Summary * Method/Analyst Summary * LotSampleSummary Analytical Results * QCDataAssociation Summary + Chain-of-Castody Total Number of Pages Testamerica BN DEPZ.SDWB-000161 CasDe8DN0a4r02r6a2tive pIdrnTaaetassaetsnahcmtoeeertdicitconaatDshowesiinitsvhrrteotiprnhourtetdthimweioeztIarenhsteoUeadrnSnpsraiEelntPydactAiziceoandaetpfeoopfdrt.othDvheieolrdpueamtrsieoautnmhsfeo.atdcesiriosrnfsaallneldadnoalanyotttimhcoeatlmowseoatrrhkeo.pdTrsohsveiusdmaemdmeporlnyecpsaosgse `IachotmoaprhleiasauvnlettwbsiertoehlnaltraobeoovnrialetywoertoydtfphrooretscoaocmmoplplsliweaistnihcnaewtnihyitsehxtcpheoplrtatibaoonnrdsanmtooetreyetQdabAlolIlrGeoCq.puliraenmaenndtshoafvNeEfLoAunCd,tsAblle LSPiolmleiiadtss(heMnaDvlLea)batehnoadntsdNhrooynu-wDedaiblgeohcctocno(rsNriDed)certreeedsd.uNsDhaatvtehbeeMeDnLa.vaUinuisetsosddoowlnthotehneonMteestw,hmoaidiDnoeetesscertion Thisreportshallnotbereproducedexcept in ful,withoutthewriten approvalofthe laboratory. a{toadteompcersuaoamfEtp2uml.e3traCce.aceeNpotnanancoiemparlotiacecasdwudormroesen.etnTschfooeusnavtmepsrleedssdwureirngerSeemsspelheedai4cn t4aa1.s,)scoceamnd S`(tAnPaaFnlOydAta)ic.radPlssFtOanSdiasrdascwoemrmeeprrecpialrperdeupsair.negdatnhedaccerk.tiffoiremdsoofltuthieocn.ompoundperfluorooctancic acid inP2PtFnerOrtoSfdo,lunucaoelrdaost-tnta-hne{dea1xr,td2r,faoc3rt,iq4o-uns"alCo,npJioaactnctdoiaawdfntwacPasiiFsucOosiAnen.tdrPaoosdrufaclenudoirnaott-et1mh-ae1le,sx2tt.ra3an.cd4t-aiCrodnfJsootrcetpeqaunnaantdtowistaualtsiiuoonsnoaefidaassu.s `DTEShaomsxepalmetpnlSerOpvrPaeDseEeNcn-trLaetCdn-id'0niAt0n1ias2oslAry.osnpiosrtwasanalyzedforthetarget analyteby TestAmerica F`acosnaarrdmtwprtaliidetsigeeesrsxp.tsarEasamascpctelheeddssutashmripon2ul5gges0hiomtlshLisdepapilhkiaeqsduwoeitoetxfhtertaahcceithinsotanetmmepacllhensiitsqaauncediawdriidft,ihpemrdeiwtoiht1ahon1eoxmltciroanocdtfiit6oino.HnACetd!lesGo1lt6uh.etion finalvolumeisbrought 0 5 mic.aurstirindggmee,tthhaenaonlalayntdetsahreeexetlurtaecdtwsiatnha4lmyzLedobfymeLtCh/aMnSo/lM.SThe bTaiMhtec.hMeeotfth2Go0CdshBSalamapmonlpkelisdseopsfrotcheesssaemderemaagrexn.twTahteersmpeiikheoddbwlitahnskuwrarsognatoenaontdapcrteptareed wreiptohreiancyh `EcaocnchenbtartacthionslperveeplasroefdLwaibtohraatLoarbyoCroanttorroylCSoanmiprolleSsawmeprleewi(tLhCiSn).coTnthreolremictso.verofitewso TestAmerica 2 DEP2.SDWB-000162 ATPnhraeelpyStatinacdnadlLaCCrcodoOmnpdmeiertainottnissn.gPTrhoecaedlurte (eSOraPr)awoatfissaitledtobeernleodsswl.ightyfor thesesampiosinthesample Tu`hpeuSsnalmsaPperlcteeimpsoDnwiefp1rf0ee.rp1le.rn3ec.pee1ps0e:.dTfhoellsoewsinagmtphleensowremraelnportoacceidduirfiefedoranSdOaPWDaEtNe-rLsCO-a0s0i1s2,WRaexvcisoiloonm4n TwhmaLesouffosfreomdrimicinacscaticediasddosoloufltuiatoiPnoinshipnrseetpepanedodobfSyHtmdPriaLuteCtaiXgnnrcga2ode.le2uw2mxa5ntm.eTrL,howefhsi8ca8hm%pdlfioefersrmwsiefcrraecoirmidstnesocetd1i0o2n0t1mi0mL.ew1si3wt.ih1t0h.6 fVoaetearc.hSceacrttriiodnge1i0n.s1t.e3a.d20owfas4amlLteorfemdebtyhaadndoiln,g 4 mLof 1% ammoniumhydroxide inmethanol Nootheranomwaerleobiseervesd. TestAmerica 3 DEP2.SDWB-000163 EXECUTIVE SUMMARY - Detection Highlights `Devotnz6z `PRRAETER 12604751-1 04/02/08 08:30 001 ovrroosn 12604751-2 04/02/08 07:45 002 reroos 12604751-3 04/02/08 08:05 003 Eroys meswT RLEReOrRTING mars 00.0030023 00001100 uugg 00l.0006ss 3 o0.l01a0 uug/gL 00001m6 oooo uugg nwoewernTICAL mBsN 11cc--00001122 BRNN --11cc--00001122 DDEBnN 1-10c--00001122 TestAnerica a DEP2.SDWB-000164 METHODSSUMMARY `DeDoso262 PAwvETER Le/ms/ms, pron References: mwLYTICNL semion De -1c-0012 EY OSpeevreartninTgrenPtrocLeadbuorrea.tores, Deaver, Facility Standard PREEARNTION memo Testamerica 5s DEP2.SDWB-000165 METHOD / ANALYST SUMMARY `Devosozez AALYTICAL mmo om -1c-0012 References: mews 00000 Jaqueline Bomett om SOepveerrantiTnrgenPtroLcaebdourraetores, Denver, Facility Standard aowsT on 003601 Testamerica DEP2-SDWB-000166 SAMPLESUMMARY `DeDosoze2 wwo t4 sswmmeicumewevesesr cuxe swe 1 XXKQXVK 000012 L1a2c6o0a4r7s5i1-z1 KKQVO 003 126047513 00000 0 oThrRtsi)droesotsr ede 8 trsnpom be kg id or itFs. TBeom getotbepprescgespdtt ri pa fci,febmle,, rn.petren, ci. em,pie A,ee,i,mh Beet,ra,,esr,eio,. m mrm moee 0044//0022//0088 0078::4305 04/02/08 08:05 TestAnerica 7 DEP2-SDWB-000167 oc Laboratories y Client Sample T: 12604751-1 we DLoatt-eSaSxapmlpele8d....:.: D04S/D0O24/002862-0080:130 DWaotrekORredecreiv.e.d...:: K04K/O0W42/A0A8 Prreepp BDaattche3...... 0841/00091/2018 Dilution vactor: 1 AAonaallyynsiiasTDimaet.e..:: 0040/:1421/08 Method.........: DEN -LC-0012 Matrix... WATER rPoaneTER ros. Resvur 00..0030082 3 RLBoRaOrRTING wars o0.0o10 wugo/i `TsaucmsRopgraoT"E 1304 pros. vaBRccovaEnRTY ans LRmacrosv.RY ((5500 -- 2700087) ors): Testamerica 5 DEP2.SDWB-000168 0 Laboratories Client Sample 1: 12604751-2 mic Doatt-eSaSmapmplleed#.......:: PrepDate... |: D0O4D/D0420/20682-0070:245 04/03/08 DWaotrek ROredceerivf.e.d...:: Roalysis Date. 0K4K/Q0V4I/Z0A0A 04/11/08 DPirleuptBiaotncPhac8t.o.r.: 83200121 oalysis Time:. 01:21 Method... DEN -Lc-0012 Matrix... we EPAroRnNER ors s0m.s0o6u6r olooss 3 wREaPOrRTING gars o0.o02t0 umgg nseueemAmoaTs 1304 PROS Nora(s) : RPEECROCVEENRTY.. %qo RLoEacrorvsERY ((5500 -- 220000)) Testamerica DEP2.SDWB-000169 oC Laboratories Client sample 1: 12604752-3 mie DLaotte-SSamapmlpel4e.d.:.. D04I/D0O24/002862-0080:305WDoartkeORredceeriv1e.d..... K04K/Q0V4O/Z0A8A PPrreepp BDaatcthe4...0.: 0842/00031/2018 Dilution Pactor: 1 aAnnaallyyssiiss DTaitmee....:: 0041/:2315/08 Method... DEN -Lc-0012 trix... WATER raomnma EY se[sxour 0.016 wREaROrRTING mers 00.00100 gwa//mn s23u0RsRoParoTn 13c4 pros eRBuRcCoavNimTy 0"8 LREocaovrkRY ((5500 -- 220000)) TestAnerica 10 DEP2.SDWB-000170 Some on 002 003 QC DATA ASSOCIATION SUMMARY DeDosoze2 sample Preparation and Analysis Control Numbers mic emworTpICN, WATER Dev -1c-0012 WATER DE -1c-0012 WATER Dem -1c-o012 BaATcCaH Y BoArTpCH Sms mows 8100121 s100064 8100121 8300064 8100121 s100060 TestAmerica 1 DEP2.SDWB-000171 METHOD BLANK REPORT 8ClLoti-LSocatmpa#l.e.t.#:: DRGODDSO00020602-121 WorkOrderf...: KIHTIMA Analysis Date..: 04/20/08 PPrreepp BDaatcthe......: 80240/00192/108 Dilution Factor: 1 rPoen nn ros `asucReRoGpArToEx. 1304 2ROS R3esour ww RpEaCrOcVaERY 0301 L`RoERrORTING mors 00.001100 ugg//ti RnmacosvRy ((5500 -- 220000)) re ------ Matrix.......WA.T.E:R Aoalysis Time..: 23:50 bemnmoLG-0017 DEY -1c-0012 Testhmerica 12 DEP2.SDWB-000172 LABORATORY CONTROL SAMPLE EVALOKTION RERORT mc C165lLoitL-oeSatm#np.l.et.d:: RDOODDOOLS00206020-121WorkOrder ...: KIXNTIAC PPrreepp DBaattec.h..#......:: 08140/00152/105 oAamlaylynsiiss DTaiteee....:: 0004:/0131/08 Dilution Factor: 1 Matrix... WATER rPoawnETER ros RPeEcRoCvEeNrTy 5=n8 LREaCOsVERY (0 -- 51200)0 ebmTwio-p16-0013 pms -1c-0012 `1s3ucmesopcraoTns frogey orisn)epee he nig7 pi de cotem emEcRocvmeNsTy 1028 8 7 hd pRBactovsERY ((5500 -- 220000)) -------- Testamerica 13 DEP2.SDWB-000173 LABORKTORY CONTROL SAMPLE DATA REFORT rie C1l6i3enLtot-LSoatmp8l.e.d.:: DRI8DDO0L900206020-121WorkOrder 4...: KIOTIAC PPrreepp DBaattec.h..1......:: 0841/00031/2018 Aonaallyyssiiss DTaitmee....:: 0004:/0131/08 Dilution Factor: 1 Mateix.........: WATER ernonema eros sweomew MEmAoSUmRED. oats mReRcCoEvNeTey wemion 00..220000 00..118967 aafrrn. E5S8 em 16-0033 ms -1c-0012 smTaRcokaPArToEn 1304 ROS. PmaSRccvEENRTY 10n8 RLEpCaOTVsERY ((5500 -- 2200007) nooTnR(se) pert reein= lo t decr otes Testamerica 1 DEP2.SDWB-000174 LABORATORY CONTROL SAMPLE EVALUATION RERORT mc CLClSieLnott-LSoatmp#i.e.l.:: DRS8DDO0N300206020-121 Work Order A...: KIXHTIAD PPrreepp DBaattec.h........:: 09140/00192/108 Annoaallyyssiiso DTaitmee....:. 0004:/2161/08 Dilution Factor: 1 Matrix.........: WATER rProanmmTER ros RPEECROCVEENRTY 58s RELCmOrVTEsRY 0093-2B0O) DMieTwHo-D1e-0i Dew -1c-o012 `1s3u0m4RopeRAoTaE 1304 PROS. Caworne(ss)vepoe heei [-- od rshd mRERcCoEVNETR.Y "us RLEpcaozvsERY ((5500 -- 220000)) TestAmerica 15 DEP2.SDWB-000175. LABORATORY CONTROL SAMPLE DATA REPORT me CLlCiSenLtoLt-oStas4p.l.e.d:: DR88DDO0M0O0Z0602-121 Work Order F...: KHTIAD PPrreepp DBaattec.h..4......:: 80140/00132/108 AAnnaallyyssiiss TDaitme.e.:.: 0004:/1161/08 Dilution Factor: 1 Matrix....._..: ATER raoRnm.ETER mseoxweT 0.0200 Pros 00200 Smcamceoeoppnrrtoosn oe . iworiR(s)vepeed ioregarhem MpenoSUwRED. 00..0021956 PERCENT RaEsCOVERY. By ie outs mPsEcRoCvENeTry ovaarti 0 Recovery L(5o0 g- i200s) (50 ~ 200) oMmeems1on6-6033 ome 10012 Testamerica 16 DEP2.SDWB-000176 MATRIX SPIXE SAMPLE EVALUATION REPORT wc MCl5ieLnott-SLoatmpl#.e..:: DDOODDOOL400226622-001 WorkOrder ...X: QKUXVQWLIAADC--MMSSD PDraetpe DSaamptleed......:: 0044//0052//0088 08:30 ADnaatleyRseicseiDvaetd.e.:.: 0044//1014//0088 DPirleuptBiaontcFhact.o.r.:: 19200121 oalynis Time..: 00:55 Matrix.........: WATER EenSvSveTER eos. cPEoRvCEeNrT y 99ss 5" mLEmCmOVzEsRY. 7(700--113300)7 09--1210200) mp L=mperTs 0.44 (0-200 15 (0-200 owememi-o1p6-0013 mDEsW i_1cc--o00m1z2 mw -nc-0m2 `BsoumaRopuraoTn. RBmcRoCvaENRTy m RLneacrorvsery (50 - 200) 2304 pros 0122 ((5500 _- 220000)) a (50 ~ 200) oraebso)e:e rr hr ie 8kr eee eeS eerereememeesemt Testamerica w DEP2.SDWB-000177 MATRIX SPINE SALE DATA REFORT we Cl5ieLnottL-Soatmp8l.e..#:: DDOEDD0OA400Z26622-001 WorkOrder#...: KKNxQqWvIAACD-HsSD DParteep SDaamptleed......x: 0048//0023//0088 08:30 DMoaatleyoReicseiDvaetd.e..:: 0044//0111//0088 DPirleuptiBoantcFhac#t.o.r.:: 81100121 malysis Tie.: 00:55 Matrix......W.A.T.E:R TPraoennTER eos MoOnUmNiTs sMeTa 00.00330 00.22100 00.00008822 00.221100 vveonmt ours 00.222350 wuaai 00.129925 uwgo/uL msscavmeay ep Emon 555 o.e4 Dmoow 116c-o00m1z3 I8 15 vmea 1oci-c0o0m1z2 soTimcmeopmrrone 1304 PROS sorsm)s.e ret herio 82 `raacsocveery nnzz a0 ed RLeactosver ((500 -- 2700007) ((5500 -- 220000) TestAnerica S25 18 DEP2.SDWB-000178 1B TINT | welll lie SRIF EE {sR xH 1S i ing (SREB Sa ge HHEE3 LEEfHRiIRTET];TEot En1il K Hl: fs i| off 0 RiN IB eenceT teFieeen)|| 6I[ls ed mg {eh ee Li Ripe SEE LL 3 1| Ni - AH