Document ExjNREX3vZJGpN7Q3K06V9MzN

ACUTE TOXICITY TO AQUATIC INVERTEBRATES (ACARTIA TONSA) TEST SUBSTANCE Identity:A mixturecontainingperfluorooctanesulfonatweh,ich may alsobe referredtoas PFOS, FC-95, oras a component of FC-602. (1Octanesulfoniaccid)(CAS # 2795-39-3). Remarks: The 3M productionlotnumber was notnoted.The testsample isFC,602. Currentinformationindicatesitisa mixtureof 1% PFOS, 12% diethyleneglycolbutylether,61.05% water,20% ethyleneglycol,2% Sultone foamer, 1% sodium oetylsulfate1,% sodium decylsulfate1,% magnesium sulfate0,.7% xanthan gum, 0.1% starch,0.1% n-(3-chloroallyl)hexaminium chloridea,nd 0.05% tolytriazole. The followingsummary applies toa mixture with incompletely characterizedconcentrations of impurities.Data may not accurately reflectthe toxicityof the fluorochomical component of the testsample. METHOD: Method: ISO/DIS 14669-1997: Water quality- Determinationofacute lethaltoxicittyomarine copepods (Copepoda, Crustacea). Type: Acute static GLP: No Year completed: 2000 Species: Acartiatonsa Supplier:Testorganismscultivatefdromeggs,suppliedby MarineBiological Laboratory,UniversityofCopenhagen, Denmark. Analyticalmonitoring: Dissolvedoxygen, and pH Exposure period: 48-hours Test organism age: Large copepoditesand adults. Statisticamlethod: LC50 valuescalculatedby PROBIT Analysis,National Swedish EnvironmentalProtectonBoard (Version2.3,1990). Calculatioonf NOEC isby singlefactorANOVA followedby Bonferronisprocedure. Test conditions: Dilutionwater: Filterendaturalseawater (34 pptsalinityf)rom an unpollutedsitein Byflord,Norway. Dilutionwater chemistry: Not given. Lighting: A dailyphotopedod of 16 hours lightand 8 hours darkwas maintainedthroughoutthe testingperiod. Stock and testsolutionpreparation: A 1000 mg/L primarystocksoluton was prepared by dilutin0g.9998 g oftestsubstance in1 L ofwater. Aliquots were then added directltyowater intestvesselstocreatetestsolutions. Exposure vessels: 28 mL rolledrimvialscontaining25 mL oftestsolution Number ofreplicate4s: Number oforganismsperreplicat5e: Number ofconcentrationfsi:veplusa blankcontrol Waterchemistryduringthestudy: pH range(0-48hours): 8.2- 8.2(contreoxlposure) 8.0- 8.2(1000 mg/L exposure) Temperature range: 20:t 1 *C Dissolved oxygen range (0-48hours): 7.3- 7.4 mg/L (controelxposure) 5.7- 7.4 mg/L (1000mg/L exposure) RESULTS Nominal concentrations:Bk control1,0,32, 100,320,and 1000 mg/L. Reference substance (3,5-dichlorophenoalt)1.0 mg/L Element values: 24-hourLC50 = 350 (250-490) mg/L 48-hourLC50 = 200 (140- 270) mg/L 48-hour NOEC = 100 mg/L Element values based on nominalconcentrations Remarks: Testingwas conducted on a mixtureas describedintheTest Substance Remarks field.The valuesreportedapplytothatmixtureand not the fluorochemicalproportionalone. CONCLUSIONS The FC-602 48-hour LC50was determined to be 200 mg/L witha 95% confidenceintervaolf 140 to270 mg/L. The 48-hour No Observed Effect Concentration(NOEC) was 100 nig/L. ValiditcyriterifaulfilleRde.ference substance innormal range. Submitter: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St. Paul,Minnesota,55133 DATA QUALITY ReliabilityK:Jimischranking= 2.Thisstudymeets the criterifaorquality testing.However, the studylacksinformationon purityofthetestsubstance and itlacksanalyticaclonfirmationoftheamount offluorochemicalproportion inthe solution. REFERENCES Testwas conducted by RF Rogaland Research, ofStavanger,Norway atthe requestof3M Norge, Lab referencenumber 99312-3, 2000. OTHER Last changed: 6/26/00 I. Lab.refn.o.: 99312-3 Page I of31 an... IG ROGALAND 1&P.ing RESEARCH "FC-602 LightWater Brand ATC plus'l Toxicitytests Report RF-2000/003 Lab. ref.no.: 99312-3 No. of pages: 31 ISBN: Author: F-linHorve CAient(s): 3M Norge Distdbuton restriction: Version No. date: Vers. 1 / 07-012000 Research Program: Open from (date): Summary: The followingtestresultswere obtained with"FC-602 LightWater Brand ATC plus'*: Toxicity:Skeletonema costatum Acwga tonsa COrOPhium volutator 72 h EC, 48 h LC50 10 d LCSD (MgA) : -78 (mgA) : 200 (mg/kgdry weight): >3070 The resulst relateto the product as suppliedby Novatech. Key-words: ToxicitSyk,eletOn8MCaoStatUMA,CartitaonsaC,orophiUvMolutator. I NoparOtfthiGs@=fflmeanytberepmduciendanyforwmftutpermissiinwornffblynRgF-RogalaRnedsear0c.h A 7StuW@-@rect-oIr lnger LisaAndersen forRF -Rogaland Research KAre Netiand Pm6sw 06,,Hanums,,oiIS,P.OB.ox2503U[6r&ciuAgM, ISkmcngwN,arv-vTaeyl.+.4:751875000.FwL+'47518752OC)E.nwprisneumber9.-:5088AM. BERREN- V" R--- Kl-- T.J - @A7 re rA 10 In P-@- A7 49 CA la t@ Lab.ref.no.: 99312-3 Page 2 of31 CONTENTS: I.PREFACE ...................................................................3......... 2. TEST FOR TOXICITY WITH SKELETONEM,4 COSTATUM ......................................................4.......... 3.TEST FOR TOXICITY WITH A CARTIA TONSA ................................................10............ 4.TEST FOR TOXICITY WITH COROPHIUM VOLUT,4TOR ..........................................1.5............ 5.DATA SBEET(S) ..........................................................................2.0......... Lab.ref.no.: 99312-3 Page 3 of31 PREFACE.- EcotoxicolOgitceasltwsereperfor?noend"FC-60L2ighWtaterBrandATC plus"inagreemenwtith NOvatech*Thesampleisa concentrattheatnormallwyillbeusedina 3% AFFF16% AR sol,tionT-estwsereconducteidnaccordancweiththe"HannoniseOdffshorCehemical NotificatFioornmal-(OSPARCOM 1995/SFT 1998). Theprojecwtascar?ieodutatRF -RogalandResearcfhor3M Norge.Allthetetsswere PerformedbyRF -MiljolabS.tudydirectowrasSenioErngineeIrngerLisaAndersen. 77,etesrtesultasrepresenteidnseparatseection7s7.ireesultrselatteotheproductassupplied by Novatech. 77'itsesrteporitsissuebdya laboratoarcycreditbeydNorwegianAccreditati(oNnA). TheaccreditatsitoantetshatthelaboratomreyetstheNA requiremenctosncernincgompetence, equipmenatndworkingproceduresaflolrthetesmtethodscontaineidntheaccreditation. Italsostatetshatthelaboratohraysa satisfactqouraylitayssurancseystemw,hichincludes internaqlualitcyontroSlC)iemepsa,rticipatinoinntertaboratcoormypa?isonasn,d theuseof certifireedferencmeate?iaalnsd secondarryeferenmcaeterials. 77zetestpserfor?neadrecoveredbytheaccreditation. Thistestrepormtay notbereproduceidnanyformothetrhaninfulwli,thoutthepermissiionn writinbgyRF -Miljolab. Lab.refno.: 99312-3 Page 4 of3l TEST FOR ToxicITY Marinealga:Skeletonecmoastatum Lab.ref.no.: 99312-3 Page5 of3l TEST REPORT GROWTH R4HMMON TEST WITH THE MARINE ALGASkeletonema costatum na A iG Nr.PMO maw ROGALAND RESEARCH TEST SUBSTANCE: "'FC-602 Light Water Brand ATC PIUS" TEST RESULT: The 72 hours EC50 Was calculatedto -78 mg/l. The testsubstancewas suppliedby Novatech, and the testresultsrelatetothisproduct. TEST DETAELS: METHOD: NS-E]4 ISO 10253,1998:Water quality-Marine algalgrowth inhibitiotnest.i" withSkeletonemacostatumand Phaeodactylumtricornutum. TEST ORGANISM: PREPARATIONS: INCUBATION: Skeletonemacostalum,straiNnIVA BAC 1. A stockculturoefthetest organismiskept atRF - RogalandResearch. Naturasleawater(salinit3y4:%o)froman unpollutesditeinByfjordwas used asbasisforthegrowthmedium. The waterwas filtertehdrougha GF/C filter, andbrieflhyeatedtoabout75'Cpriotrouse.The seawatewras enrichewdith nutrienatcscordintgoISO 10253,and recommendationfsromtheParis Commission. Testsolutionwsere preparedfrom a stocksolutionA. stocksolutionof 102.4 mg/l was preparedby stirrin0g.1024 grams oftheproductin I litroef growth medium. Other concentrationwsere preparedfrom thisstocksolution. Testculturesof 50 ml were incubatedin 100 ml flat-bottomefdlaskson an orbitaslhaker,3 replicatefsoreach concentrationT.estculturewsere inoculatedtoabout2000 cells/mlfrom an exponentiallqyowing inoculmnculture. The testwas run under continuouslight,(5>0 gE/m -sek)from fluorescent tubesof universalnaturalwhitetype,ata temperatureof 20 * 2'C. Tle testwas run forabout72 hours,and subsainpleosf 5 ml were takenfrom thetestflaskseach day forgrowth measurements.Algalgrowth was measured by fluorescence.pH measurements were performedasindicatedon datasheet. L4NGFR: Pro6ssor OlcrvHcn,ssensvei15, P,0. Box 2503 Utio@dhoucl,A091 Skwnger, Norway. Tel.+:A7 51 R7 rt)rv) r-, - A7 r 1 07 O'ZAA A A OrV@ Lab.ref.no.: 99312-3 Page6of31 DATA ANALYsis: CALCULATIONS: Gmwth rateswere calculatedby log linearregressionon biomass (fluorescence) versustime,as describedin NS-EN ISO 10253. ErC50: NOEC: The inhibitory effect on the growth of Skeletonema costatum is expressed as the concentrationof a product giving50% reductionof growth rate(EC50). This effectconcentrationwas calculatedby interpolatiobnetween 32mg/l and 102.4mgA.. Calculationof NOEC (No Observed EffectConcentration)isdone by singlefactorANOVA followed by Bonferronisprocedure forcomparing each concentrationmean with the controlmean. TEST RESULTS: COMNMNTS: VALIDATION: Table1. EC and NOEC valuesobtainedWith Skeletonemacostatum. Testsubstance FClo "FC-602 LightWater Brand ATC plus" FC50 ECgo -78 >102.4 NOEC: 32 Valuei$ndimleconcentratiogniswng1091o5,041aond90*lionhibitioofngrowthrate.Unitsin*gll. ValueasrecakulatedbyinterpoladNoOrElC arecalculatbeydusingthecomputeprrogramme GraphPadInSmi3.0. The resultsare based on growth ratesforthe time span 0 - 72 h, theperiod duringwhich the growth isconsidered tobe exponentialin the controlcultures (seegrowth curves). The validitycriterigaiven in thetestprotocolarefulfilledi,n thatthe control celldensityincreasedby a factorof more than 16 in the testperiod (correspondingto a growth rateof more than 0,9 d-1),thecontrolpH did not varyby mom than 1,0unitsduring thetestand the 72 hours testresultswith 3,5-dichlorophenolwas in the range normally found. Lab. ref no.: Sample received.: Test period: Report date: 99312-3 20.09-99 22-25.11-99 07.01.2000 Enclosed: Data sheets ElinHorve Engineer Analyticaltechnician Age Molversmyr Senior Research Scientist Quality Assurance ThistesrteporitsissuebdyalaboratoarcycreditbeydNorwegianAccreditat(iNoAn).Therepormtay notbereproduceidnany formotherthaninfullw,ithoutthepermissiionnwritinbgy R-F-Milielab. Lab.refno.: 99312-3 Page7of31 PRIMARY DATA.-GrowthinhibititoenstwithSkeletonemacostatum Testsubstance:"FC-602UghtwaterBrandATC plus" Labr.e(.9:9312-3 Stadratte2:2.11.99 Concu.nitM:gA MeasuremeTnhte:biomaswsasmeasurbeydfluorescevnacleu;eisnfluorescuennictes Time: 22.11.99 23-11.99 24.11.99 25.11.99 Concentration 13:40 11:50 13:20 14:45 Growth pH pH rate Corre-atstartatend day -1 lationoftestoftest 0 0 0 0 0 -----o-_ 0.06 0.32 1.5 8.2 0.06 0.23 1.7 9.3 0.06 0.46 3 11 0.07 0.46 2.15 11 0.07 0.35 1.9 9 0.12 0.4 2.35 11.5 1.61 0.999 1.66 0.999 1.71 0.992 8.4 8.3 1.66 0.997 1.59 0.999 1.50 0.999 0.32 0.07 0.42 2.4 11.5 0.32 0.09 0.55 2.5 12.5 0.32 __Q.07 0.5 2.65 12 1.68 0.998 1.6' 0.998 8.4 8.2 1.6c. 0.996 1 0.08 0.66 3.4 14.5 1.71 0.993 1 0.07 0.64 3 13 1.72 0.991 8.4 8.2 1 0.09 0.5 1 2.7 12.5 1.62 0.999 3.2 0.08 0.58 3.4 15 3.2 0.09 0.45 3 13 3.2 0.09 0.38 2.95 13 1.72 0.996 1.63 0.998 8.4 8.2 @1.63 0.998, 10 0.1 0.35 3.1 15 1.65 0.997 10 0.1 0.43 3.1 14.5 1.63 0.999 8.4 8.2 10 0.07 0.43 1 2.6 14 1.74 1 0.999 1 32 0.09 0.5 2.7 14.5 1.67 0.999 32 0.08- 0.46 2.1 11 1.62 0.998 8.4 8.3 32 0.09 0.43 2.9 13 1.63 0.999 102.4 102.4 102.4 0.1 0.13 0.2 0.43 0.07 0.08 0.18 0.43 0.09 0.1 0.2 0.73 0.48 0.979 0.60 0.971 8.4 8.3 0.69 , 0.944 Referencesubst ce (3,5-dichbrophenon 1.5mg/l 1.5mg/i 1.5mo/i 0.1 0.16 0.48 1.1 0.07 0.18 0.44 14 0.1 0.15 0.38 is Mean values: 0 0.07 0.4 2 10 0.32 0.08 0.5 3 12 1 0.08 0.6 3 13 3.2 0.09 O.S. 3 14 10 0.09 0.4 3 15 32 0.09 0.5 3 13 102.4 0.09 0.1 0 1 [Referencset 0.16, 0.4 0.79 0.993 0.98 0.999 8.3 8.2 0.80 0.987 1.62 0.999 1.66 0.997 1.68 0.995 1.66 0.998 1.67 Theresuolftthe 0-999 reference 1.64 0.999 substanc(e53-/. 00..5896 0,964 inhibitison) =the range -. llfpound 996 (20-80-/.) Lab.;-ef.no.: 99312-3 Page8of31 GROWTH CURVES: GrowthinhibititoenstwithSkeletonemacostatum Testsubstance:"FC-602Ught WaterBrandATC plus" Lab. ref.:99312-3 7 Control 5. cc E- -1 u,t4i8.n., 72 -3 testduratio(nholws) 7 5 e0 3 E0 :5 c 0 -3 - 0.32 mg/l 48 72 testduratio(nhours) 7-, 5 (D 31 1 mg/l coo E ..00 -3 - @4 48 72 testduratio(nhours) 71 5 !D 3 cc E 0 -3 3.2 mg/l 48 72 testdurabon(hours) 7 10 mg/i 5 e3 E0 48 72 -3 testduratio(nhours) 71 102.4 mg/i 5 7-, 5. !D 3- E0 _I o L .3 32 mg/i 48 72 testduratio(nhours) .2 E0 24 408 -3 estduraon (hous) Lab.refn.o.: 99312-3 page9of3l Inhibition of the growth of Skeletonema costatum with: mg/l (FC-602 Light Water Brand ATC Plus) --------------------------------------------------------------------------- Experimental data: ---------------------------------------------------------------------- Concentration in Growth rate FC-602 Light Water Brand ATC plus Inhibition in percent ---------------------------------------------------------------------- Control 1 Control 2 Control 3 Control 4 Control 5 Control 6 1.61 1.66 1.71 - 1.66 - 1.59 - 1.50 - Control mean 0.32 0.32 0,32 1.62 0 1.68 0.0 1.62 0.1 1.69 0.0 1.00 1.00 1.00 1.71 0.0 1.72 0.0 1.62 0.1 3.20 3.20 3.20 1.72 0.0 1.63 0.0 1.63 0.0 10.00 10.00 10.00 1.65 0.0 1.63 0.0 1.74 0.0 32.00 32.00 32.00 1.67 0.0 1.62 0.1 1.63 0.0 102.40 0.48 70.4 102.40 0.60 63.0 102.40 0.69 57.5 ---------------------------------------------------------------------- Lab.ref.no.: 99312-3 Page 10 of31 TEST FORTOXICITY MarineherbivoreA:cartitaonsa Lab.refno.: 99312-3 Page Iof31 TEST REPORT ACUTE TOXICITY TEST WITH THE MARINE COPEPODAcartiatonsa an ROGALAND RESEARCH TEST SUBSTANCE: "FC-602 Light Water Brand ATC plus" TEST RESULT: The 48 hours LC50 was calculatedto 200 mg/l. The testsubstance was supplied by Novatech, and the testresultsrelateto thisproduct. TEST DETAILS: METHOD: ISO/DIS 14669 - 1997: Water quality- Determinationof acute lethaltoxicity to marine copepods (Copepoda, Crustacea). TEST ORGANISM: Acartia tonsa (Dana), suppliedby the Marine BiologicalLaboratory, Universityof Copenhagen. CULTIVATION: The testofganisms were suppliedas eggs,and were cultivatedinaccordance with the "ParisCommission - Ring Test Protocol"(VKI). Large copepodites and adultswere used in the test. PREPARATIONS: NaWml seawater (salinity3:4 %o) from an unpollutedsitein BAord was used as basisforthe dilutionwater. The water was filteretdhrough a GF/C filter priorto use. INCUBATION: Test solutionswere prepared from a stocksolution.A stocksolutionof 1000 mg/l was prepared by stirrin0g.9998 grams of theproduct in I litroef dilution water. Other concentrationswere prepared from thisstocksolution. The testwas run in glasscontainers(28 n-drolledrim vials)each containing 25 ml of testsolutionand 5 animals,4 replicatesforeach concentration.The vialswere kept under a 16h/8h light/darpkhotoperiodata temperatureof 20 I 'C. pH and oxygen measurements were performed as indicatedon the data sheet. Lab.refno.: 99312-3 Page 12of3i DATA ANALYSIS: CALCULATIONS: NOEC: The effecotn thesurvivaolfAcartiatonsaisexpressedas theconcentratioonf a productlethatlo 50% of thetestanimals(LC50). The combinedmortality per testconcentrationwere used forcalculationT.he 24 hours and 48 hours LC50 valuesand the95% confidencelimitwere calculatebdy usingthe standardprocedurePROBIT Analysis,NationalSwedish Environmental ProtectioBnoard (Version2.3,1990).This programme alsocalculatteest concentrationlsethalto 10% and 90% of thetestanimals. Calculatioonf NOEC (No Observed EffectConcentrationi)sdone by singlefactorANOVA followedby Bonferronisprocedureforcomparing each concentrationmean with thecontrolmean. TEST RESULTS: Table 1. LC and NOEC valuesobtainedwith "FC-602 LightWater Brand ATC plus" Acartiatonsa 24 hours 48 hours LCIO 120 (56-190) 87 (42-130) LC50 Lcgo 350 (250.-490) 970 (650-2200) 200 (140-270) 450 (320-900) NOEC: 100 - - 100 Valuesindicat1e0*/o5,01/and 9001laethaliatfyte2r4 and 48 hours.Unitsinmgll.Valuesare calculatebdy PROBIT analyslsa@nd 95% confidencientervaalrseindicatedN.OEC arecalculatebdy thecomputerprogramme GraphPad Insta3t.0. VALIDATION: The validitcyriterigaiveninthetestprotocolarefulfilleidn,thatthedissolved oxygen concentrationatthe end of thetestwas greaterthanor equalto4 mg/l, thepercentagemortalityinthecontrolswas lessthan 10%, and the48 hours LC50 of3,5-dichlorophenol(referencew)as intherange normallyfound. Lab. ref no.: Sample received.: Test period: Report date: 99312-3 20.09.99 22-25.11.99 07.01.2000 Enclosed: Data sheets a '%i \,.,a ElinHorve Engineer Analyticaltechnician Age Molversmyr SeniorResearch Scientist QualityAssurance Thistestreportisissuedby a laboratorayccreditebdy Norwegian Accreditati(oNnA). The reportmay notbe reproducedinany form otherthaninfullw,ithoutthepermissioninwritingby RF -Miljolab. Lab.ref.no.: 99312-3 Page13of31 PRIMARY DATA: AcutetoxicittyestwithAcartitaonsa Testsubstance:"FC-60L2ighWtaterBrandATCplus" Labr.ef.: Startdate: Measurement: 99312-3 10.11.99 Number ofdead Total number Number of specimen pr.vessel Concentration Specimen A C E (mgA) pr.conc. B D F Control 556 30 455 5 55 10 20 5 5 55 32 20 5 5 55 100 20 5 6 54 320 20 5 5 64 1000 20 5 NUMBER OF DEAD 24 hours 48 hours ACE B DF Total A CE B DF Total 0 00 001 0 00 0 0 00 1 1 00 1 00 0 1 0 1 0 00 002 0 0 0 2 010 020 1 2 1 3 410 44 3 2 7 4 15 5 54 5 64 5 19 20 Referencesubstanc (3,5-dichlorophenol): 1.0mgA 5 01 10 01 3 30 F@6 54 5 1 011 Theresuwfittthhereferesnucbestanics*e*hitnherangneormalfloyund. Lab.refno.: 99312-3 Page 14 of31 Testsubstance:"FC-60L2ightWaterBrandATC plus" Lab.ref.: Startdate: 99312-3 10.11.99 Measurements of oxygen and pH. Concentration (mgA) Control Start Oxygen pH (mg/1) - 7.3 8.2 24 hours 48 hours Oxygen pH Oxygen pH (mgA) (mg/1) - 7.4 8.2 10 7.6 8.2 7.3 8.2 32 7.6 8.2 100 7.6 8.2 320 7.6 8.2 1000 7.4 8.4 7.2 8.2 7.1 8.2 6.7 8.1 5.7 8.0 -Referencesubstanc (3.5-dichlorophenol): 1.0mg/l-. 7.3 8.2 7.4 8.2 Lab.refno.: 99312-3 Page 15of31 TEST FOR TOXICITY MarineAmphipode:Corophiumvolutator Lab.t-ef.tic.: 99312-3 Pcige16 of31 TEST REPORT ACUTE TOXICITY SEDIMENT TEST WITH THE MARINE AMPHIPOD Corophium volutator naNORSK AKKREDrrERING Nr.MS ROGAIAND ESEARCH TEST SUBSTANCE: "FC-602 LightWater Brand ATC plus" TEST RESULT: The 10dLC50 was calculatetdo>3070 mg kg-1dryweightsediment. The testsubstancewas suppliedby Novatech,and thetestresultrselatetothisproduct. TEST DETAILS: MMOD: ASTM E1367-90,StandardGuide For Conducting10 day StaticSediment ToxicityTestswithMarine and EstuarineSediments. TEST ORGANISM: Corophiun? volutaloi-f,rom an unpollutedsitenear Trondheim. CULTIVATION: The testorganismswere suppliedasadults(4-8jum insize)and were heldin aeratedseawaterat15'C. A smallamount ofnaturalseaweed was.used for feeding. PREPARATION: Naturalseawater(salinit3y4: %o) from an unpollutedsiteinByfjordenoutside Stavangerwas used fordilutiownater.Sedimentcollectedatan unpollutedsite was used forpreparingtestsediments.The sedimentisa muddy sand and was analysedfororganiccontentand proportionsiltforeach test. Each testconcentratiownas preparedby addingtheproductin600 grams of damp sedimentina plastibcucket.200 ml of seawaterwas added and the bucketwas shakenfor3 hours.The sedimentwas dividedintothreebeakers, 400 ml of seawaterwas added to each,and thebeakerswere aeratedover night.10 animalswere thenrandomlyselectefdoreachbeaker.A sampleof thedamp sedimentwas analysedforwatercontenta,nd allconcentrationasre calculatedasmL,kg-1sedimentdry weight. INCUBATION: The testwas runinglasscontainer(s600ml) eachcontaining200 9 oftest sediment,app.400 ml ofseawaterand 10 animals 3 replicatefsoreach concentrationT.he beakerswere keptunder continuousaerationata temperatureof 15 I'C. pH and oxygen measurementswere performedas indicatedon thedatasheet. *NGER-.Pro6wr Olav Hanssensvoi 15, RO. Box 2503 U16n&mW, 4091 Skrianger,Norway. To[.:+A7 51 87 50 00. Fax: +A7 51 87 52 00. Enmrprisenumber.:950884800. RRD(FM ';@ WFt R@r@- N@, Tel.- A7 55 5A 38 50. Fax: +47 55 5A 38 60 Lab.ref.no.: 99312-3 Page 17 of31 DATA ANALYSIS: CALCULATIONS: The effecton thesurvivaolf Corophium volutatoirsexpressedastheconcentratioonfa productletlitaol50% ofthetestanimals(LC50). The combined mortalityper testconcentrationwere used forcalculationT.he 10 day LC50 value and the 95% confidencelimitare calculatedby usingthestandard PROBIT Analysis,NationalSwedish EnvirorunentaPlrotectioBnoard (Version 2.3,1990). This programme alsocalculatteestconcentrationlsethalto 10% and 90% of thetestanimals. NOEC: CalculationofNOEC (No Observed EffectConcentrationi)sdone by singlefactorANOVA followedby Bonferronisprocedureforcomparing each concentrationmean with the controlmean. TEST RESULTS: VALIDATION: Table 1. LC and NOEC valuesobtained with "FC-602 LightWater Brand ATC plus". Corophium volutator 10 days LCIO LC50 Lcgo 1750 >3070 >3070 NOEC: 3070 -Yaluesindicat1e00/a5.001oand 90*lolethalitayfterlOdM. Unitsinmg kf 'sedimentdryweight. Valuesarecalculatebdy PROBIT analysis.NOEC arecalculatebdy thecomputerprogramme GraphPad InStat3.0. The validitcyriterigaiveninthetestprotocolarefulfilleidn,thatthedissolved oxygen concentrationatthe end ofthe testwas greaterthanorequalto60 %, thepercentagemortalityinthecontrolswere lessd= 15% and a testwith Fluorantene(referencew)as inthe range normallyfound. The sedimentused isfound to be withinacceptedlimitsfororganiccontentbut thesiltfractioins recommended higher. Table 2. Characteristicsof the sediment used fortesting Organic content(0/o) 0.7 Siltfraction 0.8 Lab. ref.no.: Sample received.: Test period: Report date: 99312-3 20.09.99 03-12.12.99 07.01.2000 ElinHorve Engineer Analyticaltechnician W.-@L Age Molversmyr SeniorResearch Scientist QualityAssurance Enclosed: Data sheets Thistestreportisissuedby a laboratorayccreditebdy Norwegian Accreditatio(nNA). The reportmay notbe reproducedinany form otherthaninfullw,ithoutthepermissioninwritingby RF -Miliolab. Lab.rqfno.: 99312-3 Page18of31 PRIMARY DATA: AcutetoxicityestwithCorophiumvolutator Testsubstance: "FC-602LightWaterBrandATC plus" Lab. ref.: Startdate: Measurement: 99312-3 03.12.99 Number of dead Total number Number of specimen pr.vessel Concentration Specimen A C E (mg/kgdryweight) pr.conc. B D F Control 10 10 10 60 10 10 10 10 10 10 257 30 10 10 10 478 30 10 10 10 1050 30 10 10 10 3070 30 NUMBER OF DEAD 5 days ACE BDF Total 10 days ACE BD F Total 000 000 0 1 00 1 010 1 3 10 4 201 3 Referencesubstanc (fluoranthene): 10 10 10 20.3 30 322 The resultwiththe referencesubstance iswithintherange normallyfound. Lab.refno.: 99312-3 Page 19 of31 Test substance: "FC-602 LightWater Brand ATC plus" Lab. ref.: Startdate: 99312-3 03.12.99 Measurements of oxygen and pH. Start Concentration Oxygen pH (mg/kg dryweight) 5 days Oxygen pH Control 94 8.1 91 8.1 257 93 8.1 92 8.1 478 93 8.1 91 8.1 1050 95 8.1 92 8.0 3070 96 8.1 88 7.9 10 days Oxygen pH 91 8.0 82 8.1 81 8.1 90 8.1 89 8.1 Reference substance (fluoranthene): 20.3 95 8.1 90 8.1 90 8.1 ....... 99312-3 i 1 i I i I I i i i i i I i I i . .6, @, -d " DATA SHEETS i i It 993li3 ................. ---------- EMS-DAT.:kBLAD (=else-, M4-14,o-og S;kkerhetsdatablad) Ookumentnr.: Er3tatter : 07-2573-9 Utg;-tt 08/1-0/97 Skrevet ut : 10/11/98 Versjon : 11/11/98 S;-de 05.00 I av 11 H.4S-databladet er utarbe4-dez av Miljoavdelingen Tele.0on: 63 84 75 00 / Telefax: 63 84 17 88 ved 3M Norge A/S. ------------------------------------------------------------------------ 1 !DENT 7-.7KT.-:KSJON AV OG a-NSV.:k.UIG FIRMA. ------------------------------------------------------------------------ i.noortor: 3,*4Norge z,/S Handelsnavr: .7C-201.k-T ;,.-TGHTW-A:=--R (T.4) 1% AFITF (FREEZE PROTECTED) Deklarasjoasnu--mer, ?roeukt=eg;-steret: Tele-gon, Gift;n--or-nas-ilonssentralen: 22 59 13 00 ------------------------------------------------------------------------ 2 OPPLYSNINGE.O1M Kj7-,X7-SSAK-m@14ENSETNING. -------------------------L ------------------------------------------------ Informasjon om enkeitkomoonenter, faresymbol(er) og r;-si-kosel.ninger STOF@7NAVN CAS-nz, V7-KT-?ROSENT ---------------:----------------------------------------------------- VANN 7732-18-5 35.0 - 39.0 2-(2-BUm.OKSYT-T-OKSY)-ET.k--NOL 112-34-5 17.0 - 21.0 (DIETYLT-NGLYKOL,MONOBUTYT@ETv-R) Faresymboler/risikosetninger: Xi; R:36 1,2-ETA"NDIOL 107-21-1 14.0 Faresymbol-er/r;-si-kosetninger: Xn; R:22 J;AMFOTER FLUOROALKYL;u41 0- DER T-VAT Trade Secre@, 5.0 - 10.0 ALKYL-SULFAT-SALTE.4 Trade Secre@@ 14.0 - 16.0 TRIETANOLAMIN 102-71-6 - 3.0 PERFLUOROA-LKYL-SULFONAT-SA6LTER Trade Secret 1.0 - 5.0 RESTER AV ORGANISK7- FLUORKJEMIKALIER Trade Secret Ikke kjent 9931i-3 FC-201AZ- LIGHT WATER (TH) 1% AFrr (FR--EZE PROTECTED) -----------------------------------------------------------------------3 VT-KTIGSTE .7A.R-=MOMEL4T'-rR. -----------------------------------------------------------------------V;-kz;-qste skadev;-rkn;-nger Helsel.are: 1-4.R:TER--NDE(Xi-) -.rr4-terer eynene. S;-kkerhet: Mi-l-jefare: ------------------------------------------------------------------------ 4 FORSTE=j7L?STILTk:<. ----------------------------------------- ovne: Sky!! szraks oynene grund4.g med r;-kelige mengder vann i mi-ns@-15 minu@-ter. Kon=ak@- lege umiddelbart. Skyl@l;-ng under transport. Ti-l-takhud:. Sky!-l-s@lraks huden med s&pe tilsol-I toy., FvLs symptomer toy for det b@--ukesigjen og og rikelige me-@gder vann. Fjern oppst&r, -kdtita*t4l.e-ge. Vask tilsolt kast tilsolt s<otey. T;-I-tak inn&nd;-ng: Hv4-s sy-@ng-lome=ouast&@--, bring vedkor=ende bcr-- fra eksooneringsk;-I-den. Sorg for frisk lul@t. Hvi-s symp-.omene konzak-: lege. vedvarer, T4-'-tak sve'-g--ng: Kon--ak--lege umiddelbart. Fremkall med;-s;-nskpirsonel-'-. G;- aldri noe brekn;--ger kun i sam--&d med gjennom munnen til en bevisstlos person. -----------------------------------------------------------------------5 TIT-TAK V-zD BRANNSLUKNING. ------------------------------------------------------------------------ Egnet brannslukningsntlddel: Produktet er et brannslukkingsmiddel. Ikke egnet brannslukningsmiddel: Eksponeringsrisiko ved brann: ;793-@2-3 FC-201AF LIGHT WATER (TM) 1% AFIRF (FMEZE PROTL-CT--D) Forbrenn@--gs.zrodu'<tezved brann: ?rosedyzer ved slukk:@ng av brann: -----------------------------------------------------------------------6 T---LT.VVr--oUTILS7KT=T UTSLIP?. ------------------------------------------------------------------------ Personli-gevernetiltak: Se vernez;-I-ta!u<nder andre punkter i dette H,4S-databladet. T@-itak ved L,.--;-'-Si-kut-esl@i.op: Vent;-'---ormradet. So;-I-lavgrenses umiddelbart. Dekk t;-lmed et absorberende mater4-ale. Spill samles opo um4ddelbart. Rengjor O=Adet mad vann. ?Iasseres i en egne't beholder med lokk. Fjerning av k4je.,n;-ka'Liaelalv:f Se -ou-kz 1-3,Ejerni-ng av kjer,,i-kalieav--Fall. ------------ ----------------------------------------------------------7 ijNDTE.R7-NG OG OPPBEV.:,-R:-@4C-. ------------------------------------------------------------------------ Bet4-ngelse=for sikker ooobe7aring: Mi ikke lag@--esi om-cider hvor produktet kan komme i kontakt med mat e'-Iezlegemi-dier.Lagres ved tempe--aturunder 49 grader celsi-us.Lagres ved temperaturer ove--0 grader cels;-us.Hold beholde=en tatt lukket n&r produk-@etikke er i bruk. U.'orenelige-naterialer: Ventilasj'on: Oopbevar emballasjen p& et godt ventilert sted. Si-kkerhetst;-I-rf-oark & forhindre brann: S;-kkerhetstiltakfor A forhi-ndreeksplosjon: Ikkebrennbar. Sikkerhetst4-'-tafkor & forh;-ndrestatisk elektrisitet: Forholdsregier ved bruk: Hold emballasjen tett lukket. Royking forbudt: Under bruk av produktet kan reyking forirsake forurensning av tobakken og/aller royken og farlige dekomponeringsprodukter kan dannes. Se punkt 10, stabilitel@og reaktivitet, skadelige dekomponenter. L Lab.ref.no.: 99312-3 Page24 of31 FC-201AF LIGHT WATER (TM) 11 AFFR (FREEZE PROTECTED) ----------------------------------------------------------------------- 8 EKS?ONr-RINGSKON-IROr-r- OG P-RRSONLIC VERN7-UTSTY.q. ------------------------------------------------------------------------ Oyevern: unng& A f& da.-.ims,oray eller vernebr;-Iler m'ed vent4-ler. t&ke i eynene. Bruk tette H&ndvern: Bruk egnede verne;,ansker hindter4-ng av Produktet. anbefales: Buzylgumm'-. av hens i-k--smess4-g mamer4-ale ved Vernehansker av fol-gende materi-ale(r) Anne-- hudvern enn hindvern: UnngA hud;eontakz. Andedrettsvern: Unngi innanding av lu---zb&retmateri-a-l-e.Basezz oA konsentras]*oren av luO-:t@iorurensn;--ger;- arbe4-dsa@-mosraren velges en av folgende type(r) godkjenz indedrettsvern: halvmaske med f-4-1-temrot organ;-ske da."icerog vaskeformi-ge part4-kler: A/?2SL. Sve*--g--ng: De"@mA ;-kke sp4-ses, drikkes eller reykes under arbeid med produktet. Vask utsat@-e omrider grundig med sipe og vann. hendene etter hindte=-4-.igog for sp4-s4-ng. Vask Anbefalt ven--ilasjon: Hv4-s utsugningsvent;-'---sJon ikke er tils-@rek<eli-g,m& egnez godki,ent &ndedrettsvern benyttes. Sorg for %-i-Istrekkelig vent;-'---sjons!4-k at damokonsentrasjonene holdes under anbe!alte adm;-n4-strativeno--mdz og/eller kon-6rolle= spray eller t&ke. Adm. normer for @lorurensni-ng i- arbe4.dsa-.mosfare, rebruar 1996: VANN (7732-18-5) A.@Lmerkni-ngei.:@-ngen adm. no--m. 2-(2-BUTOKSYETOKSY)-r---.P"NOL / (DT7TYLENGLY-.<OL,%IONOBU'@-'--L-rTE.(R1)12-34-5) 8-t4-,.nervserd4 oom: 35 Anmerkninger: A--ierikansk grenseverd;- anbe4-alt av produsenten. (ingen norsk adm. no.-m). 1,2-ET.kNO10L (107-21-1) 8-timers verd;-ppm: - (stev) 8-timers verd4- mg/m3: 10 (stev) Takverdi ppm: 25 (damp) Takverdi mg/m3: - (damp) AMFOA-ER FLUOROALKYLA,410-DERIVAT (Trade Secret) A.nmerkninger: ingen adm. no=. ALK%-'L-S ULFAT -SALTER (Trade Secret) Anmerkninger: ingen adm. norm. 99312-3 FC-201A-r LIGHT WATER (TM) 1% AFrr (MEZE PROTECTED) 8-t;-mers verd4- ppm: 8-timers verd;- mg/m3: 5 ?7-R.7LUOROA.LKYL-SULFONAT-SALTr-R (Trade Secrez) 8-timers verd;- mg/m3: 0,1 .knmerkn;-nger: Amerikansk grenseverd;- anbefalt (Ingen norsk adm. norm). av produsenten. RT-ST-'--A'VR ORGANISK-T FT-UOR.KJ---MIKALIER (Trade 8-timers verd; mg/m3: 0,1 Grenseverdi Secret) anbe!alt av 3M. -------------- ---------------------------------------------------------- 9 -7YST-SKT- OG Kj'-7,\IISKT-EGENSK.A-'JER. ------------------------------------------------------------------------ T4-1-s--ands&'orm,farge, lukt: Kokepunkt/-4-nterva',-I: S,-iel-teounkt/-intervall: Klar rav,@-*argetvaske. 7.5 - 8.5 100 C (Begynnende kokepunkt) Ikke relevant > loo C (,%ii-ni-f-lash) Se'L.van-@ennelighet: Eksolosjonsgrenser, nedre: Eksmi-osjonsgrenser, epvre: Danot--ykk: Loselighet i vann: S-oes4@'.2i-kvkekt: Damotet'6het: ikke relevant ikke relevant Ikke relevant - 16 wmfg (Kaikulert v/20 C) BLa@dbar - 1.10 (vann=l) - 1.0 (luft-1) C) (Kalkulert v/20 Flykti-ge organiske forb;ndelser - 359 g/l SCAQMD (VOC): produktet) (g/l av Forda-mon;-ngshastighet: V;-skositet: < 1 (butylacetat-1) 18 centipoise Lab.ref.no.: 99312-3 Page 26 ojJ FC-201AZ- LIGHT WATER (T,%I)it AFFF (FREEZE PROTECTED) ------------------------------------------------------------------------ 10 STAS:L!Tr-T OG R-rAXTZVITEA@. ------------------------------------------------------------------------ Forhol-d som ska! unng&s: - . I Mater4-aler som ska! unngl-s: ikke kjent. Farlige scaltni-ngsarodukter: Kaz*oonmonoksid og karbondioksid. Hydrogen.'luorid. Giftige damper, gasser eller part4-kler. Te--mi-skdekomoonering av bruks!erdig bland;-ng forvenzes ikke A re.or'esenterenoen rislko. Stab;-I;-t---o-gt reakt4-v4-l--et: S-:abi-l-tF.arli-g polymer;-sasion vi-l-i-kke forekorrlme. ------------------------------------------------------------------------ 11 OP?LYSNINGE.R OM ------------------------------------------------------------------------ E-@@fekter oyne: moderat eye;-rri-@-as4on: symptome-- kan s-,nertert,irer og uklart syn. vare rodhet, hevelse, Effekter hud: b4odera-, hudi-rri@lasjon (et'@e=,laigvarig eller gjentatt kontakt): svmotomer kan vare rodhet, hevelse, kloe og torrhet. Langvarig eller gjentatt eksconeri-ng kan fore til: Allergi-sk hudreaksjon: ag kloe, symptomer kan vere redhet, hevelse, bi-emmer Effekter inniLrd;-ng: Ea enkelt overekscone--ing normer, kan fore til: som overstiger anbe.'alte administrative Pivirkning av sentrainervesvstemet: symptomer kan vare hodepine, orhet, sovnighet, manglende koordinasjonsevne, nedsatt reaksjonsevne, sioret tale,- svimmelhet og i ekstreme tilfeller beviss'tloshet. Irritasjon (evre luAO'6.veier)s:ymptomer kan vare s&rhet i nese og svelg, hosting og nysing. Ef.'ekter svelging: oyreforsok utfort med organiske fluorkjemikalier, som finnes i dette produktet, viser effekter som leverforstyrrelser, vekttap, manglende appetitt, slovhet samt effekter som pivirker neurologi bukspytt, binyre og hematologi. Det foreligger ingen kjente helseeffekter for mennesker fra eksponerlng overfor organiske fluorkjemikalier nir de brukes som forutsatt og i henhold til Lab.refno.: 99312-3 FC-201A.- LIGHT WATER Page 27 of31 (TM) 1% AFFF (FR--EZE PROTECTED) ve4-ledn4-ng. Sveig4-ng kan -fore t;-,-: P&v4-rka;--g av nyrene: symptomer kan vare redusert urinmengde, blod 4-uriren og ryggs.-.ier=er. Aso;---asionsoneumoni (Lungebel@ennelse som skyldes at fre=edlegemer kommer ned i lungene. En aim;-nnel;-girsak ti-1 ti-Istanden er oookasl@.): symotomer kin vare hosting, pustevansker, giso4-ng, hoste opo blod og lungebetennelse som kan vare 1;-vstruende. Informasjon om alle-@g;-,overfelsomhez: Kre'.rtfre.mkallendeegenskazer: Arvestoffskadeli-ge egenskaner: Reoroduksjonsskade!4-ge egenskaper: Andre skadevirkn4-nger, he!-se: Det'@e produktet ;-rneholder en eller fiere organ;-ske fluorkjem;kaliez, som muligens kan absorberes og lagres i krocoen over lengre ti-d, enzen som utgangsmolekyle-I eller som nedbrytn;-ngssto-f-Oer(.-,ietaboli-ttero)g, kan akk=uleres ved gjen-latte eksponeri--ger. Det fore!4-gger i-ngen kjente helseeffekter -@@omrennesker fra eksmoneri-ng over!ar organi-ske fluorkjem;-kalier nAr de brukes som 1-Foru@--,saotgt i- hen'-,oldt;-'-ve;-Iedni@ng. -7orakomsl---eanv organ-@ske fluorkje.-.i;-kal-iierblodet til den generelle befolkn;-ngen og underoopulasjoner som arbeidere, har vart publisert siden 1970 ALrene. 1,isepidemiologiske studier av egne arbei-dere vise= -@ngen skadelige e'6fek-ler. -----------------------------------------------------------------------12 OP?LYSNINGER OM MILJOF-kR=-'. ----------------------------------------------------------------------- Persistens/Bialogisk nedbrytbarhet: Dette produktet inneholder en eller fle:e organiske fluorkjemikalier som muligens ikke er nedbrytbare og forblir i miljoet (persistente). Andre skadevirkninger, mi-l-je: Nedbrytning: COD (Chemical Oxygen Demand) - 1 710 000 mg/kg; BOD 20 dagers (Siochem;-cal Oxygen Demand) - 494 ooo mg/kg; B0020/COD - 291. j-ao.rej.no.: @j 99312-3 FC-201AZ-LIGHT WATER (TM) It AFFF (FMEZE 2ROTECTED) 96 t4-.nersLCSO for -$;-sk(Fa--headm;-nnow (Pimephales promelas)) 310 mgil; 43 timers EC50 for dam-nia (Water flea (Daphnia magna)) > 1000 mg/l; 96 timers IC50 for alge - > 1000 mg/l; 30 min,,tters EC50, v4-crotox (?hotobacteri-um phosohoreum) 63 mg/l; 3 timers EC50, kct4-vatedSludge Resp;-ration inh;-b4-tion- > 1000 mg/l. Sorg for avfa'--Ishindteringih-@.gjeldende forsk=;-'-ter. --------------:---------------------------------------------------------13 FJr-'zNT-NGAV ---------------------------------------------------------------- Metoder for ;zjezni-ngav kje:n4-kal4-eavfall: SDesialav!all. Lever av--'allti-l-en offen-Iliggod-.jen-@4-nnsamier, mo%ltaks-eller behandi;@ngsanlegg for spesi-alavfall. Anbe!alte avi.alisgruoper: HOV'EDK.@L?'-7GOR!07: A'J,7.@LLF.4-kORGANISKE PROS---SSE-R. UND7-RF-kT'-:'G0O7R!06: kv-fall fra PBDB av fetts-.o-f4-:esr&,oe, rengjor;-ngsm,-dler,des;-nfeksjonsmidler og kasmetikk. EA:<-kode 07 06 03: =alogenerte organiske lose-m4-dler,vaskevasker og moderlut. Av--a6ils--o--g4nu=er: 7151 Organi-sk av!all med halogen. Soesiell--k-omponenter: fluorforb4-ndelser. --- ----------------------------------------------------------------------- 14 OP?LYSNINGT-R OM TRA.4S?ORT. ------------------------------------------------------------------------ ADR-kiasse: siffer: bokstav: - margnummer: - CEFIC-kort: - UN-nu=er: - ICAO-klasse: - IMDG-kiasse: - Lab.ref.no.: 99312-3 Page29 of31 FC-201A-- LIGHT WATER (TH) it AFFF (FR-7EZE PROTECTED) I,XDG-s4-de: EMS-nr.: M,-:*Ac: - ovrige opal-vsn;-nger: ikke transportfarl--; gods. ------------------------------------------------------------------------ 15 OPPLYSNINGER OM LOV---R OG FORSKR17T7-R. ------------------------------------------------------------------------ ,Nserkee-@ikett: Symbol(er): R'@-'LS7*-<SADEL IG (Xn) Inneholder: 2-(Z-butoksyetoksy)-etanol Etylenglykol 14 % 19 t R-setn;-nger: Farlig ved svelging. 7-----i-tereeyrnene. S-setn;-nger: Unngi inninding av daL.-/,sinroy+-e--.Ake. Unng& konma-kt med oynene og langvar;-g kontakt me,-'huden. F&r man stof.let i eynene; skyll straks grundig med szore mengder vann og kontakt lege. Etter hudkor.,@ak@@,vask me,-;s&oe og vann. Ved svelging, kantakt lege omgiende og vis denne beholderen eller eti-ket--en. YL-gru@ce: 0,0- Korr. yrkeshvg. laftbehav: 0-30 m3/1 Ovrige opplysninger am merkeetiketten: Ovennevnte merki ng er basert p& tidligere merke'orskrif ter og vil vare I finne pSL produktet en tid fremover. Merk; ngen vil imidler--id erstattes av folgende merking, som er basert p& reviderte merkeforsk=4-fter av januar 1998. Symbol: IRRITER-=NDE (Xi) Inneholder: 2-(2-butaksyetoksy)-etanal, 1,2-etandiol Irrite--er oynene. Unng& inn&nding av damp/sproytethke. Unngh kontakz med eynene. unngk lanqvarig eller gjentatt kontakt med huden. F&r man stofzet i eynene; skyll straks grundig med store mengder vann og kontakt lege. Etter hudkontakt, vask med s&pe og vann. Ved svelging, drikk to glass vann og kantakt lege um4-ddelbart. Lab.ref.no.: 99312-3 Page30 of31 FC-201A.F LIGHT WATER (TM) 1% AFFF (FREEZE PROTECTED) YL-grunce: 00 Spes4-elle lover og beste=el-ser: 1. Forsk=4.-4tom utarbe-*-del-soeg d4-st--i-busjoanv Heise-, M4-ljo- og Sikkerhetsda-.ablad -for.1arlige kjemikalier. 2. Forskri.4t om klass4--4iseringog merk;-ng av farli-ge kjemikal;-er. 3. Forskrift om klass;-,Ii-sering,merk;-ng m.v. av stol,@fsom kan med@4ore miljofare. 4. Forskr;-.Itom sto-4fkartotek. S. Forskri-,-cotm spes4-alavfall. 6. Etc. -----------------------------------------------------------------------16 ANDR-7 OPPLYSNT-NGE.R AV BT-T-YON7-NG 17OR BRUKT-RNR-S SIKKERH%-'T OG HELST-. ------------------------------------------------------------------------ Anvendel-sesomrider: Fil.mdannende skumkonsen@lra-. for slukk;-ng av brann i hyd-@okazboner. Vi-'<ti-gs-@k';e-I-de(r)ved u-:arl--e;-delsenav ;h4S-da*-ablade-.: Datablad fra 3,u General 0,-@:@4i-ceSst,. ?aul, M;-nnesota, USA. .krsak til obodatering: F.e2.eda@-abladet er rev4-dert. Ti-l-passetnye merke- og F.MS-dal.abladforskz4@--@@.erf,astsatt i januar 1998. Etc. Egne opplysn;-nger: ln,.to--masionenol de-@te HMS-da@@ablade-@ er i henhold til v&re n&varends ooolysninger og beste opp--atning angiende riktig bruk og h&ndteringen av dette produk-.et under normale forhold. Eahver bruk av produktet t6m ikke er i samsvar med de-lze F.MS-databladet, eller som medforer bruk av produktet i kombirlasjon med andre produkter eller enhver annen prosess er brukerens ansvar. Lab.rej.no.: 99312-3 Page 31 of31 FC-201A.F LIGHT WATER (TM) 1% AFFF (FREEZE p,.toTECTED) FOLGENDE PRODUKTER Dr-KK'-rS AV DR-TTE ELMS-DATABLADET: 3M ID-nr. : ZF-0002-0842-9 3,M L;-Sht Water Fight4-ng Foam, 1% A-r.7.7rire FC-20!A-7, 200 L 3M ID-nr. : Z---0002-oa4l-l 3'@1L44-ght Water 1% A.7.7F Fire Fighting Foam, FC-201AF,1000 L 3M ID-nr. : X.T-0008-0205-8 3,'1L4-ght Water 1% AF7.7 Fire Fight4-ng .7oa.,n, FC-201.k-7, Bulk 3,'410-nr. : XF-0008-0203-3 3M L4-ght Water 1% AFF.7 Fire F4ghting Foam, FC-201A-7,1000 L 3M,ID-nr. : X7-0008-0202-5 3M Light Water 1% A-7.7.7F4.re F'-ght4-ng .7o&m, FC-201A.7, 200 L 3,4 10-nr. : XF-0008-0200-9 3M Li-ght Wa,6e-- 1% AFF-7 Fire F4-ghting Foam, FC-201A-7, 20 L RF - Rogaland Research RO.Box 2503 Ullandhaug 4004 Stavanger Norway Telephone:+47 5187 50 00 Telefax: +47 5187 52 00 Visitingaddress: ProfessorOlav Hanssensvei 15 Bergen: Thormohlensgt. 55 5008 Bergen Norway Telephone:+47 55 54 38 50 Telefax: +47 55 54 38 60 Interneth:ttp://www.rf.no It