Document EvqV1GbLrnVojmVbv3kQa1NQ0
S.L
Internal Correspondence
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% D. R. RICKER - 53-WN
CAONMAMLEYRTCIICAALLCRHEEPMOIRCTA#LS308
-on L.
D. WINTER - 236-3
one. ap rose St Aupesisop [ESTEE
ro-u43) ron raken SEA
I ate
STUDY #0681TB0398
Reference:
CCD Analytical Request #'s 16474, 16614, 17958
I ice A white powdered solid labeled
was received originally on
FC-143 Lot 37 October 28
(P-6052 Lot 94) (T-3141 and December 3, 1980
COC) for
several studies including the Study #0281CR0012. The sample
two was
year feeding study re-analyzed for post
(T-G998COC) 0681 TBO398
Riker study
with sample received from D. Ricker 29 Jan. 82. Sample was 100% solids.
`The sample analyzed as follows:
gs ste oi o~ofzse ersnae C7 hetd
0.6
et
CCgg AAcciidd (all isomers)
987.6
9w8u.4
Cio Acid
2
2
J vs iin operate ns negara Cx Acid
5
4
foe Elemental Dee Analysis: Ee
i
F
Cc N H 0 by diff. F
66.13
22.21 3.24 0.92 7.42
0
66.2
22.2 3.5 0.7 7.4 68 ppm.
65.9
22.2 3.6 0.7 7.6
68 ppm
MW = 431
03111
Lc
Can
Spectroscopic Infrared spectra
AGATA-L
and
1798-1
are
identical
and
match
reference
spectra. JR spectra
H
8386,
F
8388-9
(Pre) and
chain is
F 101634 (Post) are
79% stralght chain,
identical and
9% (CF3)EF~
oiPngecfearemnc1e27spbecatcraS.onoThSeranuies.
Gonclustons
FTCe-p1r4e3senpItioatetiv3e7 ohfascomaenrcaniaallysmiasterwiiatlh.in specifications, is stable and is
LA
LDW/he
de: EM. TG.arCtanseer -- 221188--22 WE.. GC.. NLaomGpormemcihotk -- 22108--235-02
W. H. Pearlson - 223-6SE
RL.o A3.. SPirooinksoi-pd 2-362-1288-33
03112