Document EvXrn3Mez48k3Rkpq09jbJvLg
CHART SPEED 1.0 CMVNIN ATTEN: 8 ZERO: 5f*
"5TAT
i:Ig3feCT
5E5t-----------------
1 HI NATICK
oc
tt'
W " TIT;. Hi HEXH3 IN AIR AT SOLVENTS
v4V
23:16 24 F EH -*r
v'4
CHANNEL NO:
PEAi< PEAK NO NAME 1 2 3 4 5 6 7 3 HCE 9 13 11 12 13 14 15 13 HCED 17 19 19 20 21 22 i4> J-i 24 25 28 27 23 29 30
... ,, 3.1. , __
1 SAMPLE:; #91 AGAIN
METHOD: HEXES
RES JL ~
TIME
Til'll
area
SEP
| / .
UG
CHIN j
OFFSET
COUNTS CC v
C S ; C
0.00 03
0.458
3 4 17 6 uv
13.6 3
0.0003
3.506
77205 V'.,'
2 . 83
0.0300
0.568
6 49 08 vv
2.91
0.0300
0.653
38990 S'V
2.23
0.0300 3.0000
0.76 2 1.241
1427410 2724
TV V
3.93 3 , 5 .3
0.0000 0.0008
1.497
725
1 . 6 ft 7 --------.C.CS3 ___________302
HE IIB
2V .9t:5?
0.0000
147
3.0000 C_ZZ2TST7""
0.0000
2.723
1 263^700^ ^"' 1 R A
VV T
153 T
5 17 5
?
0 V 0 1 . 2-3
0.0000
2.72 7
384 T
0.0000 0.0000 0.0000 0.0002 0.0000 0.0000
2.798 2.967 3.011 3.069 3.260 3.475
-6 .601
255 103 ` 140
108 855 10072
T .3 7
i
1 T T
> ?
.V '>
3 24t .*5`.Ti0>*r 7.2 0
T o' 7 , i ; '
0.0000
0.0000 0.0000 0.0000
<2EH5S~ 4.74 1 5.301 5.362
VV 7 6 3
104 T
7
139 100
IIV VV
o o
* 33 3 .5 J
0.0000 0.0000
5.451 5.632
152 vv . > 3 . 3 155 v*.' ' "o 0 , '73
0.0000
0.0300 0.0000 0.0000
5.650 6.452 6.504 6.574
107 V2
9 . ?0
766 1 1514 DO A 109598 1207
HV vv vv
0 o.
13
50
>
0.0000
6.689
CONFIDENTIAL 1942 vv *? ' 5 13V
0.0000 _;_e_-s.3.aTM.,
7t .1--.0, 8 ---- --
8790 vv -------- ----;----
33 34 35 36 37 38 HCBZ 39
TOTALS:
0.0000 0.0000 0.0000 1^3. 0.0000 0.1094 0.0000
0.1104
9.144
9.702 10.568 10.816 11.015 1 1 .iJJS,..-- _ -e.ics ^T2T464
--- -------- -C .649
a3 39219 84164 1 1033 6448 3063
- 50093^
4762993
V/ w - ? j2 V V >1 04 vv vv w vv *> VV 7 6
DETECTED PKS:
El
REJECTED PKS;
12
DIVISOR: 1,30080
MULTIPLIER: 10.0000
NOISE:
7.3 OFFSET:
21
RACK: 16
VIAL: 6
INJ: I
SAVED FILE: HEXES039
RUN LOG: COL : 120 LIMIT:275 IN,J A: 25 0 INJ B:73 ION :300 TCP :4 AUX :2 FLOWA: FL0WB: DET A:ECD DET B:FID R NG A: 1 0 RNG B:10-8 VOL A:2 VOL B:1 X$TA;0.03 A-'STB:0.01 GC XE:NONE TCFIL:0
RATE :2S.0 FINAL:195 STAT :RESET
vt* *'
TIME: 0.00 0.00
0.00 0,00
0.00 0.00 3.00 3.00 0.00 0.00 3.00 0. 00
3,00 0.00 3.00 0.00 0.00 0.00 0.00
^ *"06/ ' : * 3.00 3.00 13.23
CHART SPEED
ATTEN:
8
1.0 CM.'MIN
ZERO: 5S* ___
1 MINVTICK
1VI
1?vt 7.106
DO A 109599 CONFIDENTIAL
l-jjj
RECALC TITtE: HEXES IN ft IF Hr SOLVENTS
CHANNEL NO: i
PEAK NO t ;
3 4
5
PEAK NAME
7
3 HCE 9
l1 #'
12 13 14
15 13 HCBD
17 13 19 23 21 22 23 24 25 25 27 23 23 33 31 32 33 34 35 35 37
33 HCBZ 39
SAMPLE: #91 AGAIN
RESULT
Jj tl n . n ;i 0 0
0,0000 0.0000
0.0000
0.0000 0.0000 0.0003 0.0003 0.0000 0,. 000.0/. '0.0000' 0.0303 0.0000 0.0000 3.0003
0.0002 0.0000
0.0303 3.0303 0.0000 0.01300 0.0003 0.0000
0.0000 0.0000 0.0Q00 3.0000 0.0300
0.0000 0.0003 0.0000 0.0300 0.0000 0.0003 0.0000
0.0003 0,0(300 0.1094 0.0303
TINE (MIN) 0.458
0.506 0.568 0.653 0.752 1.241 1.497 1.687
'2.*723 2.737 2.798 2.967 3.011 3.069
3.263 3.475 3.895 4,741
5.301 5.362 5.451 5.632 5.650 6.452 6.504 6.574 6.689 7.108 7.267 8.864 9.144
9.702 10.568 10.816 11.015 11.115 12.464
`
TOTALS:
0.1104
23: IS
2 9 VEH 79
rETFOD: HEXES
TILE OFFSET -E-G 63 f* i* ."**, - e. e e i
-G .505
AREA EOUNTS
3417 6 77285
64908 38990 1427413
2724 725 332
12 622*30
^SM53 384
255 103
140 108 859 1007 2
933350 1 04 139 100 152 155 107
766 1 15 14 1207 1 942 3793 4789 133302 39219 84164 1 1033 6448
3063 16498 500937
SEF CC DE
B7 yV V V/ V/ t
r\ 3 B.-3 ;* >
T T
i T T
n
'V
T V/ T Bl V! sw V7 V13 I! 7
V
V7 V7 V* ' . V i` V / V7 S' / V7 ' 77 '77 S' / 7/
IT i -( 55
rt 3 ^ 5 '4
>, n
5 , N:
`;
~.*! . J
7
r\
*? 7
-m 5. .771 10*
* 1 -'j ^
i i-t
7. i
. 5;
? 7 1.33
N
.3 ^ 3 . `` 3
3 7 '*
9 . -i
13 5 3 >
>
5.1:'
1*. 5 ? * t f .5 J
2 9 3'? ? 11.-5
1** . i I
t.-ii
i , 3 3'
-G .6 49
4782993
( ; 11
j ! :
1 -1 . ,.4 `*3'" y
\
'
DETECTED PKS:
51
DIVISOR: 1.(33000
P EJECTED PKS: MULTIPLIER: 10.0(
12
DO A 109600 confidential
CHART SPEED 1.0 CM/'MIN
ATTEN: It
EERO : 5%
1 Mr! N/T1
"aTAT : llT/l
f
14.472
' 'it''--'.
A
I T L E ! HEXES IN AIR A" 30 L VENTS
HANNEL NO: .
SAMPLE: #91 AGAl
EAK HO
l c. 3 4 5 6 7
3 3
10 11 12 13 14
15 16 17 18 19
20 21 22 23 24 25 26 2?
28 79
PEAK NAME
HCBD
............
RESULT L`G 0.0000 0.0308 0.0000 0.0003 0,0000
0.0000 0.0000 0.030O
0.0000 0.0000 0.0000 0.3000 6.0300 0.0000 0.0002 0.0000 0.0000 0.0000
0.0000 0.0300
0.0000
3.0000 0.0000
0.0000 0.0000
0.0000 0.0000 0.0000 ^ n* 3 C?f?-.,
7 IMF Ul IN 0,452 0.495 0.37 1 0.656 0.766 1 . 244 ) . 500 2j 154 ' 276T5T 2.715 2.739 2,754 2.974 3.051 3 - E67 3.257 3.270 3.319 3.486
4.767 4.336 5.047 5.215 6.193 6.438 6.501 8.869 -P , ,
23:41
24 FEE 7'4
1'ETPOD: HEXES
t !TE OFFSET
AREA COUNTS
1 7485 126 47 5 24 9 2 39 132 1287070
972
1420200
ltd
186
517
158
31 1
.83
100
882
33 1
198
..1.02-92 -T v.80
134
16 6
31 1
302
DO A 109601 CONFIDENTIAL
3032 5834
2 140
147225
A. 5.
1 . ,80
5i 3.? HCBZ 33 34
TOTALS:
0.0000 0.4000 0.0000 0.0000
0.43.02
- G . 3 50 S .433
DETECTED RLE:
a,-:.
REJECTED P K 5 :
14
DIVISOR: 1 02008
r1'JL T I PL I ER : i (3.0000
NOISE:
HI. 4 OFFSET:
10
SACK: 16
VIAL: 4
I ti.j; .
SAVED FILE: iJEXESD40
RUN LOG
COL
120
LIMIT 2 75 INJ A 250
INJ B 68
! On
300
TCD 4
AUX 2
FL 0 WA
FLOWS
DET A ECD
DET B FID
RNG A 10
RNG B I 0-8
VOL A 2
VOL B 1
A/STA 0.03
A/STB 0.01
GC XE NONE
TCF1L 0
3T AT INJECT
RATE 25.0
F I HAL 195
STfT RESET .
TIME: 0.30
3.00 3.00 3.30 3.00
0.00 0.30 0. 00
0.00 0.00 0.00 0.00 0.00 0.00
0,00 0.00
0.00 0.00 3.00 3.00
5.30 8.30
57/
'V
667 13
VV
2 3 .. ;3.3
2 3 6 7 S vv *7
603 12 vv >> 32 4..
42834
vv
3
^-2^4
T
J c_ i
478 3 150
C
c
I
i)
Cv'W.V
'vM 'p* '
it
DO A 109602 CONFIDENTIAL
{
i !' I
10.476
RECAlC TITLE: HEXES IN HIP AT SOLVENTS
CHANNEL NO: l
SAMPLE: #9 1 P.GAI
PEAK
NO 1
PEAK NAME
5
4 5 6
*7
3 '9
10 1t . 12 13 14 i5 \b 17 I3 13 2^3 2i
HC BD
15
24 25 26 77
23 23 S3 31 32 HC 32 33 34
TOTALS:
'RESULT
T I HE
UG /MINI
0.0003
0.452
0.0000
C . ^9 5
3.0000
0.0300 0.0003
0.571 0.656 0.766
0.0300 0.0000
1.244
1 . 500
0.0000
4
0. O'llBAT'
- '>0.0000' ' 2.715
0.0000
2.739
0,G300
2 754
0.0000
2.974
0.0300
3.051
0.0002
3.06?
0.0300
3.257
0.0000
3.273
0 - 0000
3,319
3.0000
3,48i,_
0.0000
0.0300 t
4
------ 1
0.0300
4.83c
0.0300
5,047
0.0300
5.215
0.0300
6 . 19 3
0.0000
6,43 o
0.0000
6.531
3.0000
8.869
0.0303
9 . 13S
3.0000
S . 739
0.0000
10.4?6
0.4000
0.0000 ^-T2T4b4
0.0000 ^ i 'l-r4 / 2
3.4302
4, b f" E T or At.
r EL
ciA'
V' V<
ri
Uc
D 1,
-t . G S3
134 7i
; :V- :
302 3 0? 2 5834
1/
*1 ii. \ %.
? 1 40 147225
4 i t- 1 2
W ^` \
8 6/7 i 3
V .*
2 3679
V'-
2 5TB----- --------- s4i3> 2
V>
5 4 283?"> V.
--..... eg 4^ 1
--C . 433
V 8 1 15C?
--I I ^ ? 4 14 ',
V ; 1 L. o
7 D. > - g ' 1
^ ^ ^* 8.Gj
" 2 6.,-'O'
DETECTED PK3:
43
REJECTED PKS:
DIVISOR: 1.33000
1ULTIPLIER: 10.3003
NOISE:
10.9
OFFSET:
10
14
DO A 109603 CONFIDENTIAL
4
i RECALC .j T I T'L E : HEXE
CHANNEL NO:
PEAK
NO 1
2 3
4
5 6 7
9
PEAK NAME
IN AIR AT SOLVENTS
SAMPLE: #91 AGAIN
RESULT LG 0.0000 C.0000 0,0300
0.0300 G.00O3
0.0003 `. 0300, 0.0302
TIME
cmin) 0.452 0.495 0.57 1
0.656 0.766 1.244
2^:4* 24 LEE1. 79
NET hO.: HEXES
T! I" E OFFSET
AREa
counts
17 485 12647 52492 . 39132 1287070
SET1 ce
I.V V-/ V. V VV VV
T
I i
DO A J09604 CONFIDENTIAL
II
v, ?, 7 5 . .3 .j 4:
Vi
11 1?
13
I4
II HCBD
1b
17
18
t1
23
21
22
23
24
25
26
27
23
29
33
31
`11 3 2 HCB2 33
34
T0-HL5:
. - .V
l- d-JUU 3.0300 O.0000 0.0000 0.0030 0.0302 0.0000 0.0003 0.0000 0.0003 0.0000 0,0000 0.0000 0.0000 0 - 0000 G.0080 G.0000 0.0000 B.0000 Cl. 0000 0.0000 G.0000 0.4000 0 0003 0.0000
S.4002
.715 . 739 , 734 . 974 35 1 .06 7 3.257 3.270 3.319
/<T3 . 981
4 . S36 5.047 5.215 6 . 19 3 8.438 6.581 0.869 9 . 13 3 9.709 10.476 11.270 j J4.
14" 4/2
-".93
-2--iS0_ .4 33
DE TEE TED DIVISOR: 1 0.i0io0
REJECTED PHI:
1A
.IUlTIPLIER; 18, 000
NOISE:
10.CUTSET:
10
123 196 517 159 31 i ! 00 882 33 ) 193
t?;i5s
1 34 r6S " 3 11 382 3 83 2 ' 58 7 4 2 l 4G 147223 4Js : 2 867 3
1
T T T 1 1
1
1 1
1i
1 T r | h! . \' '."4 V1 V',,> ^ ' V,1
47 8 1 . 5 0
1.0 0.
0, '-
? / h 0 :. 5 j
37
'J (
i
^1 -^
^
-
f:
,,
; 17.1C
>: |, -
54 i
- 'fm
- V V.
'HM U/&-
clli
V '. ...
'-'ii'-'-X,
"v ' , -1 vX
' vi
CO 1
:
:>s:f:'.
: '- -:-yvv.;. i`
7-1
'V .v
T'TT::'.'
j-.
Ifc.'Jr1- 'r 0
'
-V4V-". :
. " r* ,-v -: *
--.V
V^
111 j a z> . ION s30C
TOO : 4 AUX : 2 FLOWA: FLOWB*. DET A:TOD DET B:FiD
RHG AMO RNG B: iO--E VOL A:2
VOL B: 1 A.'STA : 0.0'
A/STB: 0. Cli
GC XE;NONE TCP IL:O STAT :INJ-:t
RATE :25 0 * INAL: 195 STAT :RUN END
J . sJ0
0 00 3.00 0.00 3.00 3. 00 0.00 0.30 3.00 0.00
0.00 3.00 0.30 0.00 0.00 0 - 00 0.00 '3 . OO 0.00 10.02
ii*.".
DO A 109606 CONFIDENTIAL
RECALC TITLE: HEXES IN AIR A f SOLVENTS
G : 05
T'LI!
CHANNEL NO: 1
SAMPLE: #91 hGAIN
METHOD : HEXES
PEAK NO l 2' i
PEAL NAME
4 5 6 7 S 9 10 11 HCBD 12 13 14 15 16 17 19 19 20
21 22:
23 24 25 ' 26 27
28 29 33
- ,- 1 32
33 34 35
36 37 33 39 40
41 HCBZ 42 43 44
45 46 : 47
43
*
TOTALS:
RESULT L; 7 0.3S30 0.0300 0.0000 0,0303
0 - C "i 3 0 0.0003 3.0 000
0 . 0003 iil 3300 0.0300 0.0336 3.B00O 0.000 G 0.0000 0.0003
0.0300 0.0303 0.0000 0.0000 0.0000 0.0000 0.3000 0.3303 0;0000 0.0300 0.0000 0.0303
0.3000
0.0000 3.0309
0.0000 0.0000 0.0000
0.0303 0.0300 0.0309 0.0300
C. 0.300 0.QO03 3.9300 C . 03 1 5 3.0300
0.0000 3.0000 0.0000 S.0003 0.0003 0,0000
TIME chin: 0.46 2 0.495 0.57 1
0.65 6 0.766 1.24!
1.339
i*^aa-- S~~27l5J,
THE C7 V 6ET
3.262 _? 4 7 ....
.112
V --dj, ; Iji *f*j'
i
6.039 6,43 3
6.451 6.52b 6.559 7,334 7.454
7.556 7.6 2 i 7.995 3.057
3.095 3.141 8.607 8.855 3.369 8.980 q j 2 t;
4`
9.301
9.660 9.685 9.332 10.043 13.100 10. i 3 9 10.2G2 i 1 , 326
11.912 JJ a f.a----
.444 ^ --r 4.0 JZj
14,103 i 4.2 1 5 14.354
f 11
*
5 ,206
O.005 1
C 3 18
6 EEA NTS C L 7/
17 76 12:30
1:1 ' V
53266 3 906 0
V' ` \,
'299 4 Q \ 31! -y 2b
V 1 -r
'^
--------
^T
i 'o
14263 5Ol0 ------ --rrr fl
fI } - i
2 08 7 j o j-- l:
/ v;
'234712:D V
i 3J
b
? ?
4j
100 12 43 , E v
*
539
\ V*
: 32 16 I 78 7
V Vr, 3
I*'
o23 12 3 4 1814
V'v
9 67 0. 2440
119 4
26 . 2 5 19 4
V' 1.
v/y *, \ >
1 S ?65 35 2:0
V' \*
t-
1935-*- VVV
2 44 B 5 2672
/ tt
1 9245
\`/
6297
1`V
7262
\J
1 14 6
'> '/
7
?'
w
627
7 /
B26
N J '7
6 C- 6 t ' / 7
228
I:
235 v / O
. v v T:
(i ,
016 1C ---------b/7~"
4S0 325 :5
DV V '/ '` ,
VS
y
? o -? ' 'i , } ?
5 342 0
DETECTED PKS:
57
REJECTED PCS:
DIVISOR: 1.00000
MULTIPLIER: 10.0000
NOISE:
15.9
OFFSET:
28
CHART SPEED 1.0 CtVMIN
AtTEN: 16
2EPO: 5X
' M '-1 r (
DO A 1<?9607 CONFIDENTIAL
CHART SPEED 1.0 C rv:i i N
ATTEN: 16 C E R 0 : *'4
moIwm'wi
1 M1NXTICK'
--ov* -*f.
-iuE FULL
Sfc .1 v : " . :Si
4.24E 4.76'
JL-QZa.
---ell ---- .575
--56S-SS . 6 t_- i
9.677 I E . P52
i?:?6S
-i-i i 4 s a
v 4q : 3" 3b8 i -1 .3G1
TTwTTi
'--4 '** '
` M >r * -%, ' /. .{*
DO A 109608 CONFIDENTIAL
RECALC TITLE: HEXES IN AIR AT SCI,.VENTS
1*. 06 2 E TET 9
CHANNEL NO: i
SAMPLE: =49i AGAIN
METHOD: HEXES
PEAK NO 1 2 3
*j*T
3 6 7
8 9 10 11 12 13 L i*
PEAK NAME
HCBD
RESULT
11G 0.0000 0-0000 0.0000 0.0000 0.0000 e.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.4859
TIME
TIM-
AREA
SEP
(MIN)
OFFSET
COUNTS CC D E
0.448
16694 i! */
0.493
10776 VV
0.574
2774620
'
0.767
4240080
\*V
0.915 ! . O08 1 . 242
1053010
3 1 1964G 2018760
Vt * \"
N
1.290
2206170 VV
1.5U
66 32630 Vv'
2.032 yg 1
^rr77? "
246 2 440 V7
57 2 3 0TSTO VV
38818
T
3.036
-G.114
280321
v /
....... _______________
--.---- -*
ii l V*, r
i
i
to **> , " '? 0 '* *T* `.u ? ft* "C
7 ,'3/7 ty
l
4*
<X
/
t-ait :
! _ Tr U L L
7l `
: u ^ 1.1
C i" - '1 \ L. ` * 0
?-' ' ' J
F-EAC t% n '* 8
-
_
4
3
' -4 t4
. Z M(. d J
14
1-
1 20 1
13 I9
.? 1 ^1
: J -3 t. 4
5
^ i* i< 7
ib 44 ^ j -z ',
; , r4 l" -'l ^ ,J L ~f ,' 8
I:OC
Of: r:-_T.
j
AAr! 1 L c il 3 : -I C-.-. ' '
1 ET h CO : ^J.r' -,H2
7 =f.. 1 f
<,, 1; lu
: : 3,:
Li . 0 v.'
t . GGOG :... c ?.o::-
'. . DOSO
C . i300D O . .'30 *0
0.0000 7 ,:l 'H?10
0 . C J0 A
S . 000 .3 L. 1 ^ w T' 1 !
0.0-3O 3 t.).. 015 3 j Ci. <21300 f. 0.30.3 0 Ci .3 0 0 0.0300 fj. 0000 0 0 300 0 G 30 'J 0 0.300
0.0003 0 0 3 01,3
0 0003
G 0-300 0 , GOO'.3
O-O 300 0.O 300 r: /* `urn
' .i-E
:1 H
,-:'Er,
3i
,i. 1
G F- F ~ E '
1. r_ U;T ... C .' .
: 4 4 :' t * , ^ a j;,
AC ? t 10"' ti
T '
C 2' : `7
j' r 9 V 6 0 ^ 4 !j. 1;J Gj
\{ \' 1
i; , r ; .. 10 A
' aO
^ C;
^04
* 1 '* . '
1 *7 - '
i 2 3 4* 1a
' tTj `
20 i 7S0
2 2 06 'O
6 2 0 217 0 Z' A -. A 4-i. ' '
l" ` t it.'
'*
--TT; 5 T T*^n---- ........
3 2- r.
0.114
'T .;i
,57 220 10 Z>
i&8 1 2
1
;o C " 2 i
\
" J. 1 Q: ~
* m<ze 1
<cOO~
4^415 4 . 76 1
5. iat
0 . 4 .; 0
2.C06
1^
3 10
4
z> y t t ,
1S 167 1
. ' ' }
1 55 '.SC
-
/ j 6
\ ` -f
8 . -T '+ r--j r- t-* 17
0 C 2 .-
-,.!
C . '! Li 3
f .' 0 1 t 7 6 020
1 2 2 'J 8 2
1 5 7 4 s .5 2 7 1 '15
'!
* \" t
7.0.3 A j. v', 4
qb577
612 3 3H
DO A 109610 7 3&3i>
i, ,
'T 9 : 2 b ii2
CONFIDENTIAL
.........
\ * - ' \ ,
0 ' ` 1-. i: ,
* ' "
.j , ; -J* - T'
7 j t, . '
' c }:,
^ -\
\
*O
K' '
. -1 ; '? 4l .> ij ^ \
'
-;
' v '
` - t :_ ;'
. ; -- %
8 1'^
I i, ! )7
'4
<
1 Cc
; is
.-! t
8 : 6 4 75
-- 9,566
~2S------ 9.365
~J
;
f: j
1-3. 169 B '- 41'
n C7H -1^3
OTsT : RESE F
__ (
fI FuE: H EX:
2 n-VlNEL i-iQ
-4.' U
1 >
PE6K' Nrt'lE
3 4, 5, 6 *
6 9 10 i1 ` 2 HCBO i ,y 14 < c*
i3
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00 A 109612 CONFIDENTIAL
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