Document Eqyj1vEjz3vDqmmv0rwdZ02Zn
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/
( ) KY-908-D <G) FWP 10/05/82 COMTYP JOB NAME: 3KY908DMG
, STANDARD HRS.
TIME______ _ M
rOCATN CG CODE PQ
LOT
DRY* WEIGHT
DRY CONT
NO. PKG
PKG WGT
TOTAL WEIGHT
ACTUAL USE LBS
14 YC-3 93 Hlo3
14 YC-3 93
-JC>^
14 YC-3 93 J-Zh&Z Si ~
14 YC-3 93
____
______ _____________ ___________________ ____-______ *______ 1TM_______________NON-BLEEDING_____
EQUIP
USE | N- 1 ACCT
MENT
NAHE * KROLtJR* YELLOW-LIGHT
LBS I CODE l . LBS
-T-
I
" BEFORE US^
SV MAKE SURE N-28-D LINE (HYDRO-
CHLORIC # ) IP: ANY IS BLANKED OFF.
RUN 60*(990 G) WAflRv IN V-203. SET AGITATOR ON
ig h SPEED.
WEIGH IN DRUM 6 POUR IN' \SQDIUM SILICATE)
420
) I 420
/| DUMP IN AND STIR,5 MIN XCHROME YELLOW) -
.63X50!
-B| 3150
I RECORD; ,/START.Xt, FIN--A4 Ju^L-
i
4 4 ADJUST TO 75* (1275 G) -*NOTE :Y'-VOCUMES: HIGHER
J^TfiAN 75* MAY CAUSE DUSTING IN EXHAUST HOOD.
SH Wim-AGITATOR ON LOW SPEED PUMP V-203 THRU
'iJtfMG AT 2400-2600 PSI INTO V-205
J
6H WHEN V-203 MT, WASH COLOR THRU HOMOG WITH MIN
OF HOT WATER AT- 2400-^600 PSI INTO V-205
CORD; V-205 VOL Jg.9,,* & ADJ TO 60` <2100 >
SPEC! HOMOG STRAINER 6 CLEAN IF NECESSARY $ ,
C*
I I I | | I |
RUN i 07"(5?4"GJ"WAfER_fNf0_vi^^sf$fT"AGITATOR ~~
| PUMP V-205 THRU HOMOG AX 4800-5200 PSI INTO SV.
I RECORD; TIME START Eli* Jb**OTAL MINUTES . NOTE; IF HOMOG PRESSURE FALLS BELQ& 480r PSI, | .3-WAY VALVE WILL RECIRCULATE SLURRY TO V-205
WHEN V-205 MT, RUN IN 5* (240 G'X WATER/*, PUMP;1 THRU..HOMOG AT 4800-5200 PSI INTO SV /.
TEP 0 . - SET FORMULA sLECtORs_f6 POSITION
(V-243) I OR POSITION 7 (V-244) . >
V.PRESS SV/tAM RESET PB - SET 22 TC IN AUTO
'EMOTE'^fTEMP IS SET AT 190-194*F)
RECORD LEVELS 6 SET R/M COUNTER *1 AS FOLLOWS:
A. 11 LG 7/._% PRESET
95 GAL
:r (LIQUID ALUM)
SET STRIKE FLOW CONTROLLERS AS FOLLOWS:
3FC10 (N-27-D CONTROLLER - SULFURIC ACID 60%)
IN MANUAL
0.65 GPM
2FC2 (N-27-D WATER) IN MANUAL LOCAL 5.2 GPM
^3pR1^r'(N-27-D/WATER) RATIO
0.8
fe'l (N-32-D CONTROLLER) IN MANUAL 0.87 GPM
8FC2Sr'<N-32-D WATER) IN MANUAL LOCAL 4.8 GPM
8FC20 (N-32-D WATER) IN REMOTE
8FR10 -i>K32-D/>UATER ) RAT 10
< .1
218 32-D
LOT* ,,...,, . COHTYP JOB NAME :. 3KY908DMG PACE 02
DATE PRINTED:10/05/82
EQUIP MENT |
I PACE 2 CG 03 KY-908-D
^
USE
N- i ACCT
LBS
CODE LBS
320 SV
SP CP"
I sflPFRATfiR rffP pt[ /
RECORD LEVEL 2LG<lx.%"3F <35% FOLLOW SOLUTION
|`>H MAKE-UP PROCEDURE FOR N-27-D T*
ADJUST SV TCU47* <2400 G) r'-
L*? I RECORD,.m' JtT. ADJ TO 11.0-11*2 WITH N-7-D
| | (CAUSTIC SODA SOLN) AT 5% <10 PARTS WATER TO 1
| .^IPART N-7-D)
'-VJf-
>^s!EPHON INTO SV. RECORD: PH3. - ASSUME 50%
OPERATOR STEP PB
^_r__ I I
7-D I.JS2L
r,2T?*Tj^S^_STER''06/397~AFTER-HEAf-Up--RECORD~_PH
SV !52^^.-9WITCH 3FC20, 8FC10, 4, 8FC20 TO AUTO
'|
SP ; ^rr^?8jC^'n'P'PRrATnp rirp pp
I
\ SP STEP 10/43. WHEN 3FC20, 8FC10 4. 8FC20 FLOWS f
ARE IN LIMITS, SWITCH 3FC10 TO AUTO' 4, PB
I
5 28^ I SP STEP 11/44. WHEN 3FC1 4, 3FC20 FLOWS ARE IN |
.^HTlfolTS, SWITCH 3FC2 TO REMOTE
I
| OPERATOR STEP PB
3><T)URING STRIKE RECORD: -
/* |
I SP STEP
.;
I
I V-243/V-244
; " PH ,, RANGE
TIWE;.,, I
I 13/46 (30 MIN)
JgsJ? 9.3-10.0 -JjJt'k- f
I 14/47 <60 MIN)
V. JM 913-10.0
J
i 15/48 (2 HRS)
:
9.3-10.
I
I 16/49 <2 HRS, 25 MIN): JQsg 9.3-10.0
l 17/50 < FINAL 3 HRS) "_feS 7.5-8.5 ZJ&sES^
| NOTE: IF PH NOT IN RANGE, NOTIFY SUPV 6 NOTE
I
I IN LOG. IF FINAL PH >8.5, ADJ TO 7.5-8.5.
!
i, RECORD: PH ____
' ASSUME 77% I
iXI SIFT IN (BLANC FIXE N)
1
I 27--D ! ____ 128-AI 55
385 ,6
DD 42* (320 G) WATER TO V-385 ADD 6 STIR FOR .2 MIN FOR S 57
ASSUME 50% | 260
387 7
L3??"T*"DURING-sfRIKE~CHECK~LEVEL~IN'"v-387'
132 | IF LOW LEVEL LIGHT IS NOT LIT, GO TO S-35
|33 i IF LOW LEVEL LIGHT IS LIT, VERIFY BY CHECKING
1 THAT LOW LEVEL PEG IN VAT IS- ABOVE SURFACE
134 1 IF VISUAL CHECK CONFIRMS LOW LEVEL * FOLLOW
1 STEARATE MAKE-UP PROCEDURE.
'
j
\ 1 1 1
i35>'tXRUN IN 251 <244 GAL). DO NOT MAKE UP THIS
l
i 1
i SOLUTION MORE THAN 30 MINUTES IN ADVANCE. 1 DELAY BETWEEN END OF STEP 41 HEAT-UP AND
I START OF STEP 48 HOMOGENIZATION SHOULD BE
> LESS THAN 30 MINUTES.
i I 1 !
388 IM>-TURN ON STEAM K AGITATOR
I
0 Wf^ADJUST TO 32* (317 GAD AT 178~182*F *
I
13# L-SET BADGER METER FOR.466*
I
I39n PUMP IN FROM V-387 THRU UNDERSRFCE DISTRIBUTORS|
I | AS FAST AS POSSIBLE (ISOBUTYL STEARATE, BUTYL I
i .^.STEARATE, EMCOL P-10-59)
/I
1|440<f>j SHUT OFF PUMP
f STIR 30 MIN AT 178-182*F FOR S 48
I
M421 DO NOT SHUT OFF AGITATOR
378 44 44
I 7-D { 130
I
I i ;: 1 i *7 1i 1i
1l 1 | ,VV. 1 -1 I I '"7
V* c,-
cSfer I 169--A | 378 1S5-A| . 44 160-AI . 44 'I
DUP050060013
1__ - COMTYP JOB NAME: 03KY908DMG PAGE 03
DATE PRINTED: 10/05/82
k PAGE 3 CG 03 KY-908-D
USE LBS
uSq IWHEN S2i~E0MPLiTE~HEAT SV TO lil-So DEG F IN**
r ^>-5 TO 10 MIN
",
CLOSE WATER XINE & DISCHARGE VALVES AT STEARATE
PUMP
'.
>::t v .
OPEN V-388 DISCHARGE VALVES TO STEARATE PUMP
INLET
OPEN WATER. VALVE AT STEARATE PUMP 6 RUN WATER
,.IHRU HOMOG AT 2900-3100 PSI, TO SEWER
JHILE HOMOG WATER AT 2900-3100 PSI, OPEN HOMOG
DISCHARGE VALVE TO SV AND CLOSE VALVE TO
SEWER
Imme d ia t e l y o p e n s t e a r a t e p u mp d is c h a r g e v a l v e ,
TURN ON PUMP & HOMOG V-388 TO SV AT 2900-3100
PSI- MAINTAIN SV AT 198-20*F-
WHILE HOMOG V-388. TO SV, -SHUT OFF WATER VALVE
- AT STEARATE PUKT ASAP
WHEN HOMOG COMPLETE, RINSE IN V-388 WITH HOT
*T WATER FROM HOT WATER MIXER
|5^| WHEN S50 COMPLETE TURN OFF HOMOG & STEARATE
r j p u mp
1^>STIR 5 MIN AT 198-20#F
Wj, SHUT OFF STEAM
WHEN S53 COMPLETE, OPERATOR Pg
SP STEP 23/53 RECORD PH_j Ij T_(3-3-3-7)
IF NECESSARY, ADJ PH TO 3-3-3-7 (DOWNWARD ONLY)
6 RECORD: NOTE: USE LIQUID ALUM, N-115-D- ADD TO SV VIA
BADGER METER- STIR 5 MIN AFTER EACH
1>
ADDITION-
ASSUME SOX
LSTi RUN IN N-7-D FROM S-3 IN 10-12 MIN h< STIR 5MIN
'HCORD: PH<4-2-4.4) t IF NECESSARY, ADJ
TO PH 4-2-4-4 6 RECORD:
ASSUME 50%
(DILUTE 10 PARTS TO 1 WlfH WATER) ASSUME 78%
SIPHON N-7-D INTO SV
ERATOR STEP PB
PERATOR STEP PB
SP STEP 60 - BATCH COMPLETE
START
FINISH
TIME SP 'TEP TIME SP STEP
I _______ 1/ocs^r________
OPERATOR
N- lACCT CODE I LBS
I
I I I I
I I I I i I
115-D
7-D 27-D
|______
I I I______ I
i
I
I I f
DUP050060014
DUP050060015