Document EO1N1d56kXO0EL8kxGkYvL1V
r Exygen ProFcoRneseRaerscths.
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Attachmen2t
AL224-1776-
Air Sampling Fluorochemical Report
|
DuPoonntt WWaashsinhgtoinWnoWrorgkks s--t--oAiArinrSaSmapmlpilinngg PiProgram RoRouunndd 5
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Exygen Research Report No. L0001400
-
Testing Laboratory
|
Exygen Research
3058 Research Drive
|
State College, PA 16801
[
Requester
z Michael D Aucoin
|
URS Corporation
Barley Mill Plaza
-
|
Building
Lancaster
27 Room
Pike and
Rt1216401
`WilmingtoDnE,. 19805
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|
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ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
|-
Page 1of7
Xe Blifeom, usa
000205Wi R25
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Summary [Seven solid media samples were received by Centre Analytical Laboratories, Inc. (dba Exygen
Research) (Exygen) from DuPont Corporation. The media represent samples of air collected on OVS tubes. Please see Table 1 for a completed listing of samples received and field air volumes [collected Sample WWK-A-AMS4-ES had sampler problems during collection. No results are reported for this sample. `The samples were analyzed for Perfluorooctanoic Acid (C8 Acid) using liquid chromatography (- / mass spectrometry (LCMS). The method employed is entitled "Method of Analysis for the |" Determination of Perfluorooctancie Acid (PFOA) in OVS Airtubes by LCMS" (James Miller, r Exygen Research, February 17, 2003).
~The OVS tubes were separated into three fractions for specific fluorochemical analysis. |" Fraction A consisted of the fier, backing material and plastic ring. Fraction B contained the _ first bed of XAD resin and the PUF backing. Fraction C contained the second bed of XAD |" resin and PUF backing. Fractions A and B were extracted with 1 mL of methanol. Fraction C
was not analyzed but saved for possible future analysis. Perfluorodecanoic Acid (C10 Acid) [ove added as a surrogate spike to each fraction prior to extraction.
Instrument operating conditions can be found at the beginning of each analytical run. Raw
I" instrument data is given in Appendix A. Chain-of-custody information can be found in
Appendix B.
-|
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
1
-
Page 2067
000206
|" Results Summary
|
SAaimepVloeldum1e)
c(omAgcmid
|
WWWKk-AAa-AiMHS!1-ES5550A
111444888000
Z<o0..N000A0000077
[
AAS 5(To) T CC ow
[.
TwncAaaMmRiIssSi2eEssSeSA
11r44e55d99
<00.0r00y000707
AAS ES a) ----
00007
I
rAR-- ISE 8
11445600
WkAES C
1480
<00.000000707 NA
I
ENE Tot) EY A
-
w WKAaAS 558A
11448622
Z<o0.0000000077
|
WVIANKSARMS5S(ET5oa) --1462
<G.N0A001
|
AAAS-- EES 8
KAASESC
1147799 1479
Z<o0..0000000077 NA
|
A RSG. To) CC --1
0.00074
NA ~ Not Analyzed. fraction was below the quantaton mi, therefor the backup ration doss nt equi analysis
| 1. "<" is defined as not detected at or above the reported level.
| 2. Sample results have not been corrected for blank results or control spike recoveries.
| EE 3. Please note the following descriptions of the OVS sample tube fractions:
|
A5 F[r Exaactrm
Cc
[2nd set beads extract (not analyzed)
| ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
;
Page 3017
000207
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000208
|
Ir Surrogates
A surrogate spike (C10 Acid) was added to all OVS tubes to give a final concentration of 500 ppb in the extract.
B Surrogate spike recoveries are given in the following table. There are no set criteria for surrogate spike
[r er r Ta recoveries. Advisory ranges are 75-125%.
oa
| WmmWKoAeAnMSe1e-EetS A | |G500
aw500
[| | mmmeoaweessssse | |a|ig ===
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|
WppWeKra -eAo-AwMeeSeS-ssESsB. | 5Ei|0G0
oa-=3u15
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1foo0s:0 273 6=i233;"
| = * Surrogate recovery outside of advisory range.
ALDATACONTAINED IY 1S REPORT ASGENERATED YF RESEARCH
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[Example Calculation [ For sample WWK-A-AMS2-ES A C8 Acid,
= [1020 ng/mlof C8 Acid x (1 mix) (1 ug/ 1000 ng) x (1 mg/ 1000 ug) } / (1459 L) x (1 m3 / 10001)
= 00007mg /m3
Signatures
|
Pe ( We,
Paul Connally, LMS Team Loader
ZL 1m
|
John M. Flanerty, Vibe President
Oe La MorisCongoDsta
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James Miller
2esloy Dato ish
Date
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ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
.
Page 7017
600211
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LOGY
000213
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ANALYTICAL DATA REVIEW SHEET
[
|
[
|
LC/MS
Tames Miles Analyst
Joron e2u 10n 0 fy Signature/Date
Tho m Foley
2 0 [LY
shy
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Reviewed by
ignature/Date
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|
|
|
0070
000214"
| sneences crvmemmansmamicn100.0
[sommes ani Method and Injection Ino Pact:
| Line Location Samplatene ~ Method Ing SampleType Injlolume Detafile
PDuvuisai]l smmmsuoE pmh | Rmm1am0 s11aSmemmmple
-
Puuaa:l Dmaonme 2 OB oLmoea
SDS uVuinagels DomoAiweNreEml fmHaadEde 11ooSReommmte
FBoRWaR}ll omlreeuiemenali fRee
SE 1
fseeme
|
1H13 oVVydiaaeel es14 Lmpm0ea0o0cu1e4te0er0:-ds2
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1h9 uvVinee mmmeoeteeetrn?, gSRIRnNS 11 Smbeielse
iva mole Re fe
Io3% voVivaaelalBBE oSDnohnoeemmt: R mRaedeol11 bsseaemmines
| ILovouvenaelsn tpwololehd soSleRo ]11 sebemmene
| BSBuoonuvs:e, mSmheoT rme, ofdeobb ]L1oamammn
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k caldbration part:
|
Line Location SampleName
Method Callev Update RF Update RT Interval
|
D2TPUUVviSaR:l]l MsMMteilM5e0opEpb RFB8e-ER1b0 13ffRhMepellealce Aepevenernannge
WfPUul dn:t mmmipurems, EISRlE]i2 jfMelmnees SSAeeennnn
BIPoouulnnl:l mMmuaimeimsmek ml Bslf33 hMbeeemmnme hdfeeenmns
|
34 Vial5 STD 750 ppb
FC8-10
5 Average Average
||1 13 13B2511Vo/i0a3lma6ssimSsTDoeu100s0mmssprpobrfrFRC8, -s10
56 Mmm Average ann Average 40 | 600215 sage 1 of 2
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!
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Calibration Table
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Calib. Data Modified : Friday, January 09, 2004 4:06:50 BH
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| signal 2: usp1 469, EIC-468.7:469.7
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- anol 1153 3150sa00i.T00o00n00o00000s 1a.s10o08mr0m3si0seeessd 3a5.0s0e33s07i04e0en03s3 il
33 1035050000.100000000000000 1Ts.ii6ia3mr4io2ir4vieeesrs S3& ae0to45es0re70ee7ss3
i. 6.937 2 351191053000:.00000000000000 133..15447137390096050103 S3.3e4d0de3se0hr1ie0er3ds 1
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Wore compound-opecitie sectings:
[7 compount; co ste
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Time Window
|[7 = Compoundi:nC1a0 surrogate
: From 7.298 min To 8.298 min
. From 8.141 min To 5.946 min
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| cooara 1/9/04 4:07:56 pusmitter 07Yt
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LC/MS SYSTEM AND OPERATING CONDITIONS
|
Client: Dupont
EXYGEN STUDY: _ L0001400
[
Instrument: Hewlett-Packard 1100 LC/MSD (LC/MS 3)
~
API-ES Interface - Negative SIM mode
|
Nitrogen: 10 L/min at 300C
Fragmentor: Variable; Vcap: 3500V
|
Computer:
r
Software:
Hewlett-Packard Kayak workstation
Microsoft Windows NT 4.0
Agilent ChemStation Version A.08.03
a
HPLC Equipment: HP G1379A Solvent Degasser
HP G1311A Quaternary Pump
-
HP G1313A Autosampler
|
HP G1316A Column Thermostat
HP G1946A MSD
[
HPLC Column: Thermo Hypersil-Keystone Betasil C18, 30 x 2.0 mm x 3um
Column Temp.: ~~ 35C
|"
Mobile Phase (A): 2mM Ammonium acetate in OmniSoly Water
Mobile Phase (8): HPLC grade Methanol
Im
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%A
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Post Time = 4 min.
Total run time = 14 min.
|
Flow Rate:
0.3 mL/min
-
Injected Volume: 5 pL
|
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600227 022:
Sample Nae:5TD 50 pob
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Data file Ci \HCHEN\1\DKEA\FC000002.D
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600225
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7 Injection Date : 12/11/03 5:21:50 BY
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Pri, 9. Jan. 2004
04:53:23 pm
0022
Page 1 of 1
26 600226
saammp ma 50 250 eon
:
|" InjectionDate :12/11/03 5:37:30PM | Acq operator: jmiller
SeqLine vial No.
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600227
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Fri, 9. Jan. 2000 04:55:23 pm
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Page 1 of 1
600229
sarple Haze: 1000 ob
I" Sample Info:
1
I
[ Injection Date : 12/11/03 6:24:17 mM
SeqLime +
1
[ pee wombs reacsocn
|
7.481 C8.
[|
]|
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| |
PC00414
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Fri, 9. Jan. 2004 04:55:42 pm
ubz
Page 1 of 1
G00230
sample Nase: 1500 ppb | SbaamtpelefilIen.fo:CH ECHE\SATI\RCIONES,D
B Injection Date : 12/116/:309:352 BM
1
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5
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600221
sample tane:solvent blank
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9
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|= =
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MSDY 489,EIC=488.7:469.7 (CHEMSTORN157 ABAS0T203 FC03 00008 80)
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Tei Endof Report eee Fri, 9. Jan. 2004 04:07:36 pm
Page 1 of 1
600232
[ Sample Info:
[I InjectionDate : 12/117/:100:352 2M
[ veoma + senso
1
Seq Line : 10
-
ee
|
10000.
ae!
Uo
I 000
- 2000
1
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|"
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++ "End of Report ter
Fri, 9. Jen. 2004 04:08:40 pm
9023
Page 1 of 1
600233
[SSameple Name:L0001400-23
:
Data file :C:\PCHEM\I\DATA\Chemstor\L1570512\A84S856\EC00001>1
IAIncnjasetcortpuimeoernnattDoarte |:| m130i20l/0l14e14r/03 7:26:27 BM
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1
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3 vel. | sul
[7 Anaiyaiia dMethod | GT:\kEICHEM\1\METHODS0\61:20161:05413 om
Le/Ms analysis of perfluorcoctancic acid.
| - = SDT 8513687357 CHENSTORY570 TaWHES Gio--ceAPFES, oy SWFarVr
| ow [I
H. ||o.|
I
r=
A SOT466, EOSABS z14887(CHEWSTORY {ISTOSTEUBTSR0S)B0A0P01NFoTg:ESSF- r, Vr pe 22C3io s4ura.t,
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rl 4000:
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0.00
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SDI 369, B1-368.7:369.7
TT
Te End of Report es
|| conus
Frio. gan. 2008 04:09:24 pm
TTT
o
JO30
rage 1 of 1
oo234
sample Name:10001400-1
| Sample Info:
1
Data file iC: \NECHEN\I\DKTA\Chemstor\11570627\AGS1712\FC000012.D
[7 SeprnaoifeecootpiaielorlnaitEeburte: BT| niRittiHeess remem wyShee e imei3}
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if
ve
sui
|r SEarcaRd,iyaMgeethohdethod |+roCao-y1H0R.CuHI1 ETHODS 1S2o11e03st0 om
LMS analysis of perfluoresctanoic acid.
I TO EGS T05CRESSTTEOa8RTFCEo0TET ES SHFri
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Tr---- Puoas1igofe1
600235
sample tame:10001400-2
[ Sample Info:
1
Data file :C:\HPCHEM\1\DATA\Chemstor\11570714\A854912\FC000013.D
[Ef Teshti ei owpda es erse a :
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[]- = TE EET CREO TOT
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TT Fri, 5. gan. 2004 04:18:39 pm
---- 0032 Page 1 of 1
600236
Ie Sample Info:
1
I Injection Date : 12/11/03 8:13:1P1M
SeqLine
4
{7 on, sonmoa + peat.
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000237
[_SoSmabmpilee Niaene::L0001400-5
2
Data file :C:\HECHE\L\DATA\Chenstor\11570979\ABS5264\FCO000.15D
I oITnndjgeucortpaiemoernnattoDrat|e :|i: 1mpo2io/lv1le1el/rd03 8:28:44 PM [oe il [7 hAenqa.ivaEMiensthnWoedathod ;x CFEoC\BT-A1P0C.H4EN\1\NETHODS\0142:10160:35.1
Lo/us analysis of perfluorooctanoic acid [ SDTEC TART CENSORS | ow I'l ow
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Fri. 9. den. 2004 04:13:29 pm
TTT
034
Page 1 of 1
000238
fate RATES? I DSaatmapleFilIenfo:G: CHEI\I\DANChanator\LLSTLOSTAARGLOS6\RCHOD014. 1
r iki IB op pIenejeoactpn ioennDeatre ::1}m12/e11r/03 8:44:20 BM
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7
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pp fei. 5. san. 2008 08:14:06 pm
a 403s gos 4 02 2
600239
_ Ssaammppllee Nnafmoe::L0001400-8
:
.
1
Data ile :C:\HECHEM\I\D11A57T34A31\\ACB8h14e72m\FsC0t00o017r..\D
I1] s | [" Injection Date : 12/11/03 8:59:56 BM
Seq Line
|
~
dATicolqtuotOiipmoeenrnatto|r
i+ tjpCmoiDlAllear
vnigal vNNeoel.i.
[ | cAnqa.iE vaviesthMoen athod |+ CAr:c\aRE-PtC0H.EmM\I\METHODS\10231:10063:.541 pm
10/45 analysis of perfluorooctancic acid.
r |
SOT, E3587887 CHENSTTOSRTT HGaTATEFGO0MB0TT) APVES,
ars
2am.ca
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17
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SoTo"AcSiudrrogat 303.30.051
T13a35 eo9w89 sMoooii 436609,, mBr1o0--d3e6n8.771:63699..77
r
[ nd seoousa
"End of Report ter
Fei 9. dam. 2008 04:25:41 pa
TT
uo36
sage 1 of 1
6002~,40
[ Ssamiplce Nmaimoe::L0001400-10
1
Data file :C:\HPCHEN\1\DATA\Chemstor\11571274\A863680\FC000018.D
I IAIcnnqjsetcOrtupimeoennrtaD tora :: 1t 2mEC/iO1l01le 4/eL0r43 9:15:38 PM
vsIienajq.lLNiNoon..e ::
1I81
Dilution
iY
mil vel. :
sul
A ---- [A=nalysCihsanMgeetdhod : C1:/\9H/0E4CHEM\1\METHODS\I0261:10063:5.1% pm
Le/MS analysis of perfluorcoctanic acid.
-
MSY359,EC=I8873887 CHENSTORTTST27
0) APeEgSSW.F,rag Var
Me Tn [lm
|
15000-
|
r 12500
10000
I 7500
|
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| = [=
[7 ~e ese a i ot e sies 5 i
16000
8323-10Surge
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|
[|e
i
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ompound Amount (ng/ml)
[=ioacSuirdropac 418027.44.405
I R.T. 78.342586
Area 111741254536
|
5
i
pe
signal sSpDll 346693,, BBXICC--436688..7:74:6336197.7
I
"ind ofReport ter
Lae msomson osm
mueo3ryezs gored
_ Sfamiplre eNasde:i0001400-11
.
Data File {C:\HPCHENto\r1115\73O62N1ATBBA32\64C\FChB0e00m19s.D
[eeMeiTrniNee rbere ER fAeE iTnS Ion ER five Hh
TsereiNeel ml
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[semegeaworemosthod s| cCR5oS-eAtPO0Wn ETHOD1I 211S03.\
1
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Teen rage 1 of 1
000_742
Ii
SSaammppllee NIaafnee::ST 500 ppb Data file iC: \HECHEN\1\D\1K15T71A392\\ACRGhS66e4\nFCs00t00o20r.D
s
r I TInojE eercotmpieeornnattoDrate i|:| fJ1fo2ao/ln1e1et/ns03 9:46:5M2 wSWeqavLiNeenee i
su20i:
S heeia,yaMes| thoMdethod +| z\cRaP-C1H0E.Nn\1\NETHODS\12o1i100031.5110 om
L/S analysis of perfluorooctancic acid.
J - So ECT ar
as7caAsPeES aS Fri
[|| we
|
-|| oe
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r.
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"MSD 489,EIC+468.7:489.7 (CHEMSTORN 15713A0B2BS664FCO00020.0) APNogI,S-IM,EFraSg:V,ar
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8.334-C10Sumogate,
[7] 12000.
I
wn
[7] o=n
| - 2000
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1
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3
Compound souns (ng/ml) RT. aves
signal
| Soh"Sura rogard31a6.10
i35e3s0 T1a3ss0ss wMoenni saeess,. mEircewwsdsee.s771i3d6e9e7r
I
| conse
+++ Endof Report t+
Fri, 5. Jam. 2006 04:36:03 pm
0039
Page 1 of
600243
~ gFuosotles Ytaegaas swimens Dhar
.
OV ----
JEdeoe rgpgerimrner +A ap: myiesr FmmoeEma uFdiy:
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ro
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TE rei. 5. sam 2008 6162 pm
0040 age 1 0f 1
000744
I Sample Info:
`
1
(TM Injection Date : 12/11/03 10:17:54 PM
Seq Line :
22
Acq Operator + jmiller
Vial No. :
21
[fram I
ER
Lous analysis of pereluorooctaneic acid
- .-
--AT IU
[| =
1
rlo-
fe.
|
MN
[A[[J |E o| =woewoen Ss e S------ esr. cross; | - |
"MSD1469,Ei
7469.7 (CHEMSTOR\I 1571627\AB69120FC000022.0) APNIog,-SIEM,SFr,ag: Var
| 2000.
[i comms --se--me or wr. ven
st
I
I" --
*** End of Report ***
reel ie =
TTT
00re4g1e 1 0 1
conzas
Sample Name:L0001400-14
I sample Info:
1
Data file :C:\HPCHEN\1\DATA\Chemstor\11571685\A871296\FC000023.D
ET -- I AIncjqecOtpieonrDaattoer:: 12jm/i1l1l/e0r3 10:33:26 BM SveiqalLitno.e ::
223
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sul1
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(=Le/s analysis of perfluoroctanoic acid.
-
NSO 383, E0-36873857 CHENSTORTTSTISoSar
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[=
0
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r=0
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"MSD 469, EIC=468.7:469.7(CHEMSTORN 157 1685\A8T1206 FC000023.0) APNogI,S-IM,EFraSg:V,ar
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10000:
[7] os
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80302060 507448
1
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M"SSDDII 436699,, EX1CC--436688..77::436699..77
r
-
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"+ Ea of Report +r
Fri 5. gam. 2006 04:20:44 pm
uo42
Page 1 of 1
0600775
y_ Sample Nane:50001400-16
}
2
! Data file :C:\HPCHEM\1\DATA\Chemstor\11571858\A873664\FC000024.D
I hIdoniajreocotmpieeornnattDoart|e ii| 1s3jom/oi1od1al/te0sr3 10:43:00ow SweSaaNttiemee 1 2382
[-coiqtucieotnrea i+ seston
nie
su
[ArniiyeetsdMethod || C3 s \NPCHEN\1\NBTHOOS\10211010632.50 om
L/S analysis of perfluorooctancic acid.
[
SET O TS TCHESTORETAT OT RES eFS R
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|
-
| "0
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r== | r- =mw
I om ST 8EAE 8CHENSTO 57 AETSRGAFGO00245O38].APCI1E0S8Noo,SW FirVar
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r
-
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veh, 5, san. 2001 01:21:32 pm
00s43ero
000247
ample ame 10001400-17
| Sample Info:
1
Data ile sc: \HRCHENVtLor\\11D573N75T6\AABB\S05C6\hFCOe00m025s.D
Iherenre |Mjearilynera
Ewredle
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"MSD1469, EIC=468.7:460.7 (CHEMSTOR\ 1673A75B8BS056\FC000025.0) AP NegI,S- IM,EFraSg:V,ar
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0044 ra1gofe1
600248
[_seSmapmprlee Nsaamie::10001400-19
:
Data file :C:\HECHEU\I\DATA\Chemstor\11S72016\AG75456\2C000026.D
| AIIcnnqsjteOrcputemieronanttoDrate : i212m0/i01l41l1/e40r3 11:20:07 PK VSIineajq.lLNiNoon.le :
3261
| HE iT
3 vel. : sw
AAcnaa,lysMies tMehtohodd:| CF:C\BA-P1C0H.E1N\1\METHODS\121103.4
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0:06:51 pm
Le/us analysis of perfluorooctanoic acid.
[ SDT88 ICATE GHENSTOR 7ST SS GR03 APaESHSFa,Vr
Ls
r= [=wo
[| ==
= ro
w | "wntIY 50 ECA :497
|= [| = 12000
|
(CRESTOR 1I572 RATSSGFC0:0020) APES Noo3, SW.Firvar e311 cto surat
r= | a
Io
I
1
3
Compound Amount (ng/ml) R.T. Area
signal
| S3h6" euatrosar 2To6n8o.s10
8a13a10 laisisy WHaebbii 4366s5,, BEilcc--3a6e6h..77:i3a6659..77
r TT
endof report ee
[. -- trait ee
TTT
00r4e5 1oc1
000241 9
Sample Name:10001400-20
| Sample Info:
Data file SC: \HPCHEN\1\D1N15T73A83C8AOhBGoB4m0\sFCtO0o00rZ7\.5
1
[edy edgreemee sa Jjeees
rpnal
Ea:n
Lape}
RE
sul
[[7 siSca,aevesnaaeanon +| Craernb-soonn vETHOOS 121103 1
LC/HS analysis of perfluorosctanotc acid.
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r=
=
| 20
| ow | i
|" 160.
sai cts i
2
45
5
|
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) APNIeg,-SIME,FrS ag:V,ar
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|
wo
[7] wo
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A
I.
7
7
7
7
corpound_peoune nara) RT. Aves
stant
(F SeeSe [EFaL, amnEi sas, mEenma maei
| | esnere
TT --T Fri. dan 2008 08:28:17 pm
0046
sage 1 0 1
600750
. samoie Nene: 500 pp
| Sample Info:
.
1
Data file SCo\HPCHEN1\DATA\Chemstor\11572055\AST7760\FC000028.0
[7 AhtoimGpoaemmncors |Riominde ilesr Gaim iSeienhee
5:i
J ire
Hove Lo sw
| MEodiRye-- iLa Evachoa | C\HRETCHODHS 1S2Ee1r1o0eL3is1t pm
1e/m snayass of pertluorsoctamoic acid.
r ao 8ET CHENTOR SOETOvEam oaTES oS
[7] oo
7
Ml =
[7] ~ wo 1
|
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|
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WSO460,EIC=468.7:460.7(CHEMSTORN! 1572085WB177601FCO0002810) APNegE ,SM,S Frag, :Var
ao I] ao
ao [-7l] . i i
Icorpound__ amount am2i) m5. 4 area 6
si8gna1 mir
EN
Si ee he a mee 36
| 1-
| ecooura
R Rap S
Fri, 9. Jan. 2004 04:24:29 pm
0047
Page 1 of 1
0025
600251
sample ame:Solvent blank
| Sample Info:
1
"Data file :C:\HECHEM\I\DATA\Chemstor\11572153\A879744\FC000029.D
[ haIonurjeOmcpteeironantDoarte :| 1sje2mo/io1la2it/es0r3 12:06:43 AX vSeaq tLNienee
TT 5i
[- sDeiqiwcivoonres irencto
Dhl sul
[Rei divatE s Wathod | CSo\RiECHEN\L\WETHODS\1S2i11r0035.64 pm
L745 analysis of perfluorooctancic acid.
[
S55,ETT CESTOR 67 AST RFG00E30 APES: og SW Farar
0
[| =
[ wo
"
1
| mo
|
~ 180
I ~ : 7 |
"MSD 469, EIC=468.7:469.7 (CHEMSTOR\I 1572153AB767441
|
3 0) AL NegE ,SIMS ,Frag, :Var
[l=
| 180-
rom
[| =
| 155
I Compound Seis
2
4
amount. (ng/mi) AT Area
Tol
loro
WA
5
8
min.
signal
Won 369, Ec3gs 7369.7
r
|| scooaza
+++Endof Repowerr t
Pei, 5. gan. 2008 08:24:59 om
4043
rage 1 of 1
o0070552
| J Sample Info: --
i,
1
[ dInojemctmioen Date mh : 12/12/03 12:22:15AM nSeeq Line
30:
[7 fr
EI oe,EwoAre L+ reIEsRoEnentwie
|
EIEI RE i.
Tacs onc
| 1200
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"MSD 469,EIC=468.7:469.7(FCO00030.0) APNIog,-SIME ,FrS ag:, Var
|a-ooon er. cross| | [| md
|
[| -m=
[=
I
3
I
coped soos arnt wr. aves
wien
r sr
"++Endof Report +++
0049
000253
sample Name:STM 100 ppb
| SDaamtpaleFilInefo:Co\HECHEA\I\DNTAVECO00031.D
1
[ Injection Dat:e 12/12/03 12:37:48 AM "SeqLine
1
-- maeonen `Acq Operator + mi jmiller
gLaEn Vial No. :
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