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From: American Laboratories and Research Services, Inc. P.0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Comapny P.O. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03421 Sample location: VISTA Vista Sample Loc. SP-7-3-2 Collected by: K. MCCALISTER Collection date: 03/21/90 Time: 15:15 Laboratory submittal date: 03/22/90 Time: 23:10 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 16:02 Parameter: TCLP Metals Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 08:00 Ed Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.35 mmpy Date started: 03/29/90 Time started: 19:05 Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP Date finished: 03/30/90 Analyst: BB CWH 000010.U3 Vista Chemical Comapny Page: 2 April 3, 1990 Sample I.D. AA03421 (continued) Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/02/90 Time started: 04:00 Ed Degrees F Date finished: Analyst: JKP 04/02/90 Parameter: Reactivity Method reference: SW846 3rd Ed Result: see appended report Date started: 03/23/90 Time started: 01:00 Date finished: 04/02/90 Analyst: BB Parameter: Oil and Grease Method reference: EPA 413.1 Result: 65000 mg/L Date started: 03/29/90 Time started: 12:30 MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA Parameter: Moisture content Method reference: SW-846 Result: 54.05 % Date started: 04/02/90 Time started: 14:30 MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene IsobutanolMethylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Det 580 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det 44 Not Det Not Det Not Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CUH 000010114 Vista Chemical Comapny Page: 3 April 3, 1990 Sample I.D. AA03421 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1.4- Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6- Trichlorophenol 2.4.5- Trichlorophenol 2.4- Dinitrotoluene 2.3.4.6- Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4- *D 2.4.5- TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det Not Det Not Det Not Det Not Det Not Det 130 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Component MDL .1 .l Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 3.00 Component MDL .005 .01 CUH 000010115 Vista Chemical Comapny page: 4 April 3, 1990 Sample I.D. AA03421 (continued) Data for TCLP Metals (continued) Component Name Cadmium,`TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration Not Not Not . 02 Det Det 4 Det 04 Component MDL . 01 1 . 01 .2 . 005 . 01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. Reviewed By: James W. Pinson, Ph.D. President CUH 000010116 From: American Laboratories and Research Services, Inc. P.O. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Company P.O. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03422 Sample location: VISTA Vista Sample Loc. SP-9-7-6 Collected by: N. MCCALISTER Collection date: 03/21/90 Time: 16: Laboratory submittal date: 03/22/90 Time: 23:10 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 16:46 Parameter: TCLP Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 08:00 Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.35 mmpy Date started: 03/29/90 Time started: 19:05 Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP Date finished: 03/30/90 Analyst: BB CWH 000010117 Vista Chemical CompanyPage : 2 April 3, 1990 Sample I.D. AA03422 (continued) Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/02/90 Time started: 07:00 Ed Degrees F Date finished: Analyst: JKP 04/02/90 Parameter: Reactivity Method reference: SW846 3rd Result: see appended report Date started: 03/23/90 Time started: 01:00 Ed Date finished: Analyst: BB 04/02/90 Parameter: Oil and Grease Method reference: EPA 413.1 Result: 18000 mg/L Date started: 03/29/90 Time started: 12:30 MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA Parameter: Moisture content Method reference: SW-846 Result: 80.17 % Date started: 04/02/90 Time started: 14:30 MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene Isobutanol Methylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Det 680 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det 92 Not Det Not Det Not Det 31 Not Det Not Det Not Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CUH 000010118 Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03422 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1.4-Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6-Trichlorophenol 2.4.5-Trichlorophenol 2.4-Dinitrotoluene 2.3.4.6-Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4-D 2.4.5-TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Component MDL .1 .1 Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 4.00 Component MDL .005 .01 CUiw 000010119 Vista Chemical Company Page: 4 April 3, 1990 Sample l.D. AA03422 (continued) Data for TCLP Metals (continued) Component Name Cadmium,TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration Not Not Not Not * 02 Det Det Det Det . 02 Component MDL . 01 1 . 01 .2 . 005 . 01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. CWH 000010120 From: American Laboratories and Research Services, Inc. P.0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Company P.0. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03423 Sample location: VISTA Vista Sample Loc. SP-11-3-8 Collected by: N. MCCALISTER Collection date: 03/21/90 Time: 17 Laboratory submittal date: 03/22/90 Time: 23:10 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 17:34 Ed Parameter: TCLP Metals Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 08:00 Ed Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.35 mmpy Date started: 03/29/90 Time started: 19:05 Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP Date finished: 03/30/90 Analyst: BB CWH 0000.10121 Vista Chemical Company Page: 2 April 3, 1990 Sample I.D. AA03423 (continued) Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/02/90 Time started: 16:00 Ed Degrees F Date finished: Analyst: RLH 04/02/90 Parameter: Reactivity Method reference: SW846 3rd Ed Result: see appended report Date started: 03/23/90 Time started: 01:00 Date finished: 04/02/90 Analyst: BB Parameter: Oil and Grease Method reference: EPA 413.1 Result: 58000 mg/L Date started: 03/29/90 Time started: 12:30 MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA Parameter: Moisture content Method reference: SW-846 Result: 46.87 % Date started: 04/02/90 Time started: 14:30 MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2-Dichloroethane 1.1-Dichloroethene Isobutanol Methylene Chloride Methyl Ethyl Ketone 1.1.1.2-Tetrachloroethane 1.1.2.2-Tetrachloroethane Tetrachloroethene Toluene 1.1.1-Trichloroethane 1.1.2-Trichloroethane Trichloroethene Concentration Not Det 1000 Not Det Not Det Not Det Not Det Not Det Not Det Not Det 23 40 Not Det Not Det Not Det 110 Not Det Not Det Not Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CWH 000010122 Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03423 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1,4-Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4-Dinitrotoluene 2,3,4,6-Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2 ,4--D 2,4,5-TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det Not Det 79 Not Det Not Det Not Det 41 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Component MDL .l .l Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 3.00 Component MDL . 005 . 01 CUH 000010123 Vista Chemical Company Page: 4 April 3, 1990 Sample I.D. AA03423 (continued) Data for TCLP Metals (continued) Component Name Cadmium, TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration Not Not Not Not .01 Det Det Det Det . 01 Component MDL . 01 1 . 01 .2 . 005 . 01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. Reviewed By: James W. Pinson, Ph.D. President CUH 000010124 From: American Laboratories and Research Services, Inc. P.0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Company P.O. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample X.D. AA03424 Sample location: VISTA Vista Sample Loc. NP-1-8-6 Collected by: N. MCCALISTER Collection date: 03/22/90 Time: 10:15 Laboratory submittal date: 03/22/90 Time: 23:10 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 18:19 Parameter: TCLP Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 08:00 Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.35 mmpy Date started: 03/29/90 Time started: 19:05 Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP Date finished: 03/30/90 Analyst: BB CUM 00001012b Vista Chemical Company Page: 2 April 3, 1990 Sample I.D. AA03424 (continued) Parameter: Igmtability Method reference: SW846 3rd Result: greater than 140 Date started: 04/03/90 Time started: 03:20 Ed Degrees F Date finished: Analyst: JKP 04/03/90 Parameter: Reactivity Method reference: SW846 3rd Ed Result: see appended report Date started: 03/23/90 Time started: 01:00 Date finished: 04/02/90 Analyst: BB Parameter: Oil and Grease Method reference: EPA 413.1 Result: 44000 mg/L Date started: 03/29/90 Time started: 12:30 MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA Parameter: Moisture content Method reference: SW-846 Result: 76.87 % Date started: 04/02/90 Time started: 14:30 MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene Isobutanol Methylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Det 860 Det Det Det Det Det Det Det 10 Det Det Det Det 62 Det Det Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CWH 000010:126 Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03424 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1.4- Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6- Trichlorophenol 2.4.5- Trichlorophenol 2.4- Dinitrotoluene 2.3.4.6- Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4- D 2.4.5- TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Det Det 690 Det Det Det 240 Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Component MDL 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Component MDL .1 .1 Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 3.00 Component MDL . 005 .01 CWH 00001.0127 Vista Chemical Company Page: 4 April 3, 1990 Sample I.D. AA03424 (continued) Data for TCLP Metals (continued) Component Name Cadmium, TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration Not Not Not . 03 Det Det .3 Det . 02 Component . 01 1 .01 .2 . 005 .01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. Reviewed By: James W. Pinson, Ph.D. President CWH 000010128 From: American Laboratories and Research Services, Inc. p.o. .Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Company P.O. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03425 Sample location: VISTA Collected by: N. MCCALISTER Vista Sample Loc. NP-4-3-2 Collection date: 03/22/90 Time: 13 Laboratory submittal date: 03/22/90 Time: 23:10 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 19:04 Parameter: TCLP Metals Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 08:00 Ed Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.35 mmpy Date started: 03/29/90 Time started: 19:05 Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP Date finished: 03/30/90 Analyst: BB CUH 0000101 Vista Chemical Company Page: 2 April 3, 1990 Sample I.D. AA03425 (continued) Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/03/90 Time started: 01:30 Ed Degrees F Date finished: Analyst: JKP 04/03/90 Parameter: Reactivity Method reference: SW846 3rd Result: see appended report Date started: 03/23/90 Time started: 01:00 Ed Date finished: 04/02/90 Analyst: BB Parameter: Oil and Grease Method reference: EPA 413.1 Result: 32000 mg/L Date started: 03/29/90 Time started: 12:30 MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA Parameter: Moisture content Method reference: SW-846 Result: 72.82 % Date started: 04/02/90 Time started: 14:30 MDL or sensitivity: .1 Date finished:. 04/02/90 Analyst: MB Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene Isobutanol Methylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Det 1400 Not Det Not Det Trace Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det 22 Not Det Not Det Not Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CLJ/.J Ooooi I30 Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03425 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1,4-Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4-Dinitrotoluene 2,3,4,6-Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2,4-D 2,4,5-TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det Not Det 68 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Compc 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Compi .1 .1 Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 3.00 Component MDL . 005 . 01 CWH 000010131 Vista Chemical Company Page: 4 April 3, 1990 Sample I.D. AA03425 (continued) Data for TCLP Metals (continued) Component Name Cadmium, TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration Not Not Not Not . 02 Det Det Det .Det 02 Component MDL . 01 1 . 01 .2 .. 005 01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. Reviewed By: James W. Pinson, Ph.D. President From: American Laboratories and Research Services, Inc. P.0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Company P.0. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03433 Sample location: VISTA Vista Sample Loc. NP-5-2-3 Collected by: K. MCCALISTER Collection date: 03/22/90 Time: 14 Laboratory submittal date: 03/22/90 Time: 23:10 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 19:50 Parameter: TCLP Metals Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 08:00 Ed Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.35 Date started: 03/29/90 mmpy Time started: 19:05 Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP Date finished: 03/30/90 Analyst: BB CUN 000010133 Vista Chemical Company Page: 2 April 3, 1990 Sample I.D. AA03433 (continued) Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/02/90 Time started: 17:00 Ed Degrees F Date finished: Analyst: JKP 04/02/90 Parameter; Reactivity Method reference: SW846 3rd Result: see appended report Date started: 03/23/90 Time started: 01:00 Ed Date finished: 04/02/90 Analyst: BB Parameter: Oil and Grease Method reference: EPA 413.1 Result: 40000 mg/L Date started: 03/29/90 Time started: 12:30 MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA Parameter: Moisture content Method reference: SW-846 Result: 65.26 % Date started: 04/02/90 Time started: 14:30 MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene Isobutanol. Methylene Chloride Methyl Ethyl Ketone 1,1/1,2-Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Det 1900 11 Not Det Not Det Not Det Not Det Not Det Not Det 35 26 Not Det Not Det Not Det 30 Not Det Not Det Not Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CUN 0000.103 34 Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03433 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis (2-Chloroethyl) Ether 1,4-Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4-Dinitrotoluene 2,3,4,6-Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2,4-D 2,4,5-TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Component MDL .1 .1 Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 4.00 Component MDL . 005 . 01 CUIS-I 000010133 Vista Chemical Company Page: 4 April 3, 1990 Sample I.D. AA03433 (continued) Data for TCLP Metals (continued) Component Name Cadmium,TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration o to Not Not Not Det Det .2 Det .02 Component MDL . 01 l . 01 .2 . 005 . 01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. CWW 000010136 From: American Laboratories and Research Services, Inc. P.0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: vista Chemical Company P.O. BOX 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03470 Sample location: VISTA Vista Sample Loc. SL 5-8-8 Collected by: K MCCALISTER Collection date: 03/26/90 Time: 12:00 Laboratory submittal date: 03/27/90 Time: 21:45 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 10:11 Ed Date finished: 04/02/90 Analyst: RLH Parameter: TCLP Metals Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 08:00 Ed Date finished: 04/03/90 Analyst: JWP Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/03/90 Time started: 04:30 Ed Degrees F Date finished: Analyst: JKP 04/03/90 CUH 0000101.37 Vista Chemical Company Page: 2 April 3, 1990 Sample I.D. AA03470 (continued) Parameter: NACE Corrosivity- Method reference: TM-01-69 Result: less than 6.35 mmpy Date started: 03/29/90 Time started: 19:05 Parameter: Reactivity Method reference: SW846 3rd Result: see appended report Date started: 03/23/90 Time started: 01:00 Ed Parameter: Oil and Grease Method reference: EPA 413.1 Result: 22000 mg/L Date started: 03/29/90 Time started: 12:30 Parameter: Moisture content Method reference: SW-846 Result: 82.85 % Date started: 04/02/90 Time started: 14:30 Date finished: 03/30/90 Analyst: BB Date finished: 04/02/90 Analyst: BB MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene Isobutanol Methylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Det 16 Det Det Det Det Det Det Det Det 11 Det Det Det 300 Det Det Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 00001.0138 CUH Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03470 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1.4-Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6-Trichlorophenol 2.4.5-Trichlorophenol 2.4-Dinitrotoluene 2.3.4.6-Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4-D 2.4.5-TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det Not Det Not Det Not Det Not Det Not Det Trace Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Component MDL .1 .1 Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 23.00 Component MDL .005 .01 CUH 000010139 Vista Chemical Company Page: 4 April 3, 1990 Sample I.D. AA03470 (continued) Data for TCLP Metals (continued) Component Name Cadmium, TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration . 02 Not Det .Not Det 2 Not Det . 04 Component MDL . 01 .1 01 .2 . 005 . 01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. Ricky L. Hatton, Ph.D. Vice President Reviewed By: James W. Pinson, Ph.D. President From: American Laboratories and Research Services, Inc. P.O. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Company P.O. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03471 Sample location: VISTA Vista Sample Loc. SL 8-2-8 Collected by: K MCCALISTER Collection date: 03/27/90 Time: 9 Laboratory submittal date: 03/27/90 Time: 21:45 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 10:50 Ed Date finished: 04/02/90 Analyst: RLH Parameter: TCLP Metals Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 08:00 Ed Date finished: 04/03/90 Analyst: JWP Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/03/90 Time started: 05:00 Ed Degrees F Date finished: Analyst: JKP 04/03/90 CUH 000010141 Vista Chemical Company Page: 2 April 3, 1990 Sample I.D. AA03471 (continued) Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.3 5 mmpy Date started: 03/29/90 Time started: 19:05 Parameter: Reactivity Method reference: SW846 3rd Result: see appended report Date started: 03/23/90 Time started: 01:00 Ed Parameter: Oil and Grease Method reference: EPA 413.1 Result: 34000 mg/L Date started: 03/29/90 Time started: 12:30 Parameter: Moisture content Method reference: SW-846 Result: 80.25 % Date started: 04/02/90 Time started: 14:30 Date finished: 03/30/90 Analyst: BB Date finished: 04/02/90 Analyst: BB MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene Isobutanol. Methylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Det Det Det Det Det Det Det Det Det Det Det Det Det Det 21 Det Det Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CUH 000010142 Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03471 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1.4- Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6- Trichlorophenol 2.4.5- Trichlorophenol 2.4- Dinitrotoluene 2.3.4.6- Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4- D 2.4.5- TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Component MDL .1 .1 Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 14.00 Component MDL . 005 . 01 CWH 000010143 Vista Chemical Company Page: 4 April 3, 1990 Sample I.D. AA03471 (continued) Data for TCLP Metals (continued) Component Name Cadmium,. TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration Not Not Not . 04 Det Det .2 Det . 04 Component MDL . 01 1 . 01 .2 . 005 . 01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. President CUN 000010144 From: American Laboratories and Research Services, Inc. P.O. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Company P.O. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03472 Sample location: VISTA Vista Sample Loc. SL 1-4-5 Collected by: K MCCALISTER Collection date: 03/27/90 Time: 11:00 Laboratory submittal date: 03/27/90 Time: 21:45 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 11:28 Ed Date finished: 04/02/90 Analyst: RLH Parameter: TCLP Metals Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 08:00 Ed Date finished: 04/03/90 Analyst: JWP Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/03/90 Time started: 06:05 Ed Degrees F Datefinished: Analyst: JKP 04/03/90 CWH 000010145 Vista Chemical Company Page: 2 April 3, 1990 Sample I.D. AA03472 (continued) Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.35 mmpy Date started: 03/29/90 Time started: 19:05 Parameter: Reactivity Method reference: SW846 3rd Result: see appended report Date started: 03/23/90 Time started: 01:00 Ed Parameter: Oil and Grease Method reference: EPA 413.1 Result: 26000 mg/L Date started: 03/29/90 Time started: 12:30 Parameter: Moisture content Method reference: SW-846 Result: 79.17 % Date started: 04/02/90 Time started: 14:30 Date finished: 03/30/90 Analyst: BB Date finished: 04/02/90 Analyst: BB MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene Isobutanol. Methylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Det Trace Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det 12 Not Det Not Det Not Det 200 Not Det Not Det Not Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CWH 000010.146 Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03472 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1.4- Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6- Trichlorophenol 2.4.5- Trichlorophenol 2.4- Dinitrotoluene 2.3.4.6- Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4- D 2.4.5- TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det Not Det Not Det Not Det Not Det Not Det 47 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Component MDL .1 .1 Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 20.00 Component MDL . 005 .01 CUH (>0010J.4? Vista Chemical Company Page: 4 April 33, 1990 Sample I.D. AA03472 (continued) Data for TCLP Metals (continued) Component Name Cadmium,*TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration Not Not Not . 03 Det Det .3 Det . 04 Component MDL . 01 1 . 01 .2 . 005 . 01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. Ricky L. Hatton, Ph.D. Vice President Reviewed By: James W. Pinson, Ph.D. President CWH 00001014s From: American laboratories and Research Services, Inc. P-0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Company P.O. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03473 Sample location: VISTA Vista Sample Loc. NL 1-9-8 Collected by: K MCCALISTER Collection date: 03/27/90 Time: 14:30 Laboratory submittal date: 03/27/90 Time: 21:45 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 15:17 Ed Date finished: 04/02/90 Analyst: RLH Parameter: TCLP Metals Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 08:00 Ed Date finished: 04/03/90 Analyst: JWP Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/03/90 Time started: 07:00 Ed Degrees F Datefinished: Analyst: JKP 04/03/90 CUJH 000010149 Vista Chemical Company Page: 2 April 3, 1990 Sample I.D. AA03473 (continued) Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.35 mmpy Date started: 03/29/90 Time started: 19:05 Parameter: Reactivity Method reference: SW846 3rd Result: see appended report Date started: 03/23/90 Time started: 01:00 Ed Parameter: Oil and Grease Method reference: EPA 413.1 Result: 26000 mg/L Date started: 03/29/90 Time started: 12:30 Parameter: Moisture content Method reference: SW-846 Result: 79.14 % Date started: 04/02/90 Time started: 14:30 Date finished: 03/30/90 Analyst: BB Date finished: 04/02/90 Analyst: BB MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics % Recovery Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane lr1-Dichloroethene Isobutanol Methylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Det 1500 Not Det Not Det Not Det Not Det Not Det Not Det Not Det 18 Not Det Not Det Not Det Not Det 1100 Not Det Not Det Not Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CUH 00010.(5o Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03473 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1.4-Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6-Trichlorophenol 2.4.5-Trichlorophenol 2.4-Dinitrotoluene 2.3.4.6-Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4-D 2.4.5-TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Not Det Det 51 Det Det Det 60 Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Det Component MDL 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Component MDL .1 .1 Data for TCLP Metals % Recovery Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 2.00 Component MDL . 005 . 01 f-WH 0000.10151 Vista Chemical Company Page: 4 April 3, 1990 Sample I.D. AA03473 (continued) Data for TCLP Metals (continued) Component Name Cadmium,' TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration O to Not Not Not Det Det .2 Det . 02 Component . 01 1 . 01 .2 . 005 . 01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. oooo V<y.l52 c.uvi From: American Laboratories and Research Services, Inc. P.O. BOX 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Company P.O. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03483 Sample location: VISTA Vista Sample Loc. NL 9-5-9 Collected by: K MCCALISTER Collection date: 03/27/90 Time: 18:00 Laboratory submittal date: 03/29/90 Time: 0:48 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 22:05 Ed Parameter: TCLP Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 08:00 Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.35 mmpy Date started: 03/29/90 Time started: 19:05 Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP Date finished: 03/30/90 Analyst: BB OOiOi'53 Vista Chemical Company Page: 2 April 3, 1990 Sample I.D. AA03483 (continued) Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/02/90 Time started: 17:55 Ed Degrees F Datefinished: Analyst: JKP 04/02/90 Parameter: Reactivity Method reference: SW846 3rd Result: see appended report Date started: 03/23/90 Time started: 01:00 Ed Date finished: 04/02/90 Analyst: BB Parameter: Oil and Grease Method reference: EPA 413.1 Result: 44000 mg/L Date started: 03/29/90 Time started: 12:30 MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA Parameter: Moisture content Method reference: SW-846 Result: 81.3 % Date started: 04/02/90 Time started: 14:30 MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics % Recovery Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene IsobutanolMethylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Det 410 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Trace Not Det Not Det Not Det Not Det 180 Not Det Not Det Not Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CWH 000010154 Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03483 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1,4-Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4-Dinitrotoluene 2,3,4,6-Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2,4-D 2,4,5--TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Compc 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Compi .1 .1 Data for TCLP Metals % Recovery Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 11.00 Component MDL .. 005 01 CUH OOOOlOiSb Vista Chemical Company Page: 4 April 3, 1990 Sample I.D. AA03483 (continued) Data for TCLP Metals (continued) Component Name Cadmium, - TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration Not Not Not . 02 Det Det ,2 Det 04 Component MDL . 01 1 . 01 .2 . 005 . 01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. Ricky L. Hatton Vice President Reviewed By: James w. Pirfson, Ph.D. President CU.IH 000010156 From: American Laboratories and Research Services, Inc. P.0.Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Vista Chemical Company P.O. Box 200135 Austin, TX 78720-0135 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03484 Sample location: VISTA Vista Sample Loc. NL 5-7-5 Collected by: K MCCALISTER Collection date: 03/28/90 Time: 8:30 Laboratory submittal date: 03/29/90 Time: 0:48 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 21:20 Parameter: TCLP Metals Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 08:00 Ed Parameter: NACE Corrosivity Method reference: TM-01-69 Result: less than 6.35 mmpy Date started: 03/29/90 Time started: 19:05 Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP Date finished: 03/30/90 Analyst: BB CWH 0000.10157 Vista Chemical Company Page: 2 April 3, 1990 Sample I.D. AA03484 (continued) Parameter: Ignitability Method reference: SW846 3rd Result: greater than 140 Date started: 04/03/90 Time started: 07:15 Ed Degrees F Date finished: Analyst: JKP 04/03/90 Parameter: Reactivity Method reference: SW846 3rd Ed Result: see appended report Date started: 03/23/90 Time started: 01:00 Date finished: 04/02/90 Analyst: BB Parameter: Oil and Grease Method reference: EPA 413.1 Result: 39000 mg/L Date started: 03/29/90 Time started: 12:30 MDL or sensitivity: 5 Date finished: 03/29/90 Analyst: KA Parameter: Moisture content Method reference: SW-846 Result: 73.56 % Date started: 04/02/90 Time started: 14:30 MDL or sensitivity: .1 Date finished: 04/02/90 Analyst: MB Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene Isobutanol Methylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Concentration Not Det 230 Not Det Not Det Trace Not Det Not Det Not Det Not Det 20 120 Not Det Not Det Not Det 95 Not Det Not Det Not Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 CUH 000010158 Vista Chemical Company Page: 3 April 3, 1990 Sample I.D. AA03484 (continued) Data for TCLP Organics (continued) Component Name Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1.4-Dichlorobenzene 1,2-Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6-Trichlorophenol 2.4.5-Trichlorophenol 2.4-Dinitrotoluene 2.3.4.6-Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4-D 2.4.5-TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det Not Det Trace Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 Data for Reactivity mg/L Component Name Cyanide Sulfide Water Concentration Not Det Not Det No Reaction Component MDL .1 .1 Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Concentration Not Det 5.00 Component MDL . 005 .01 CUI-I 000010159 Vista Chemical Company Page: 4 April 3, 1990 Sample I.D. AA03484 (continued) Data for TCLP Metals (continued) Component Name Cadmium,TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration Not Not Not .03 Det .Det 2 Det . 04 Component MDL . 01 1 .. 01 2 . 005 .01 Comments: Reference Lab Report No. R1100. All the appropriate EPA protocol including blanks, spikes, and duplicates were followed for these samples. If there are any questions regarding this data, please call. Reviewed By: James W. Pinson, Ph.D. President CWH 000010160 From: American Laboratories and Research Services, Inc. P.0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Blank Sample Analysis American Laboratories The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03434 Sample location: BLANK Method Blank Collected by: ALRS Collection date: 03/22/90 Time: 23:30 Laboratory submittal date: 03/22/90 Time: 23:30 Received by: RLH Validated by: RLH Parameter: TCLP Organics Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 16:00 Parameter: TCLP Metals Method reference: SW846 3rd Result: see appended report Date started: 04/01/90 Time started: 08:00 Ed Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP CWH 000010161 Blank Sample Analysis Page: 2 April 3 , 1990 Data for TCLP Organics ug/L Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene Isobutanol Methylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1.4- Dichlorobenzene 1.2- Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6- Trichlorophenol 2.4.5- Trichlorophenol 2.4- Dinitrotoluene 2.3.4.6- Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4- D 2.4.5- TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Sample I.D. AA03434 (continued) Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 200 10 10 10 10 10 10 10 200 10 10 10 10 10 10 10 10 10 10 100 10 10 10 10 10 10 10 10 10 50 10 50 10 50 100 10 10 2 1 1 1 10 20 CWH 000010162 Blank Sample Analysis Page: 3 April 3, 1990 Sample I.D. AA03434 (continued) Data for TCLP Metals mg/L Component Name Arsenic,. TCLP Barium, TCLP Cadmium, TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration Not Not Not Not Not Not Not Not Det Det Det Det Det Det Det Det Component . 005 . 01 . 01 1 . 01 .2 . 005 . 01 Comments: Reference Lab Report No. R1100. If there are any questions regarding this data, please call. CUH 00001.0163 From: American Laboratories and Research Services, Inc. P.0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Sample Matrix Spike American Laboratories The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03522 Sample location: SPIKE TCLP Matrix Spike 1 Collected by: Collection date: Laboratory submittal date: 04/01/90 Time: Received by: RLH Validated by: RLH Time Parameter: TCLP Organics Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 09:16 Parameter: TCLP Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 08:00 Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP CWH 000010164 Sample Matrix Spike Page: 2 April 3, 1990 Sample I.D. AA03522 (continued) Data for TCLP Organics % Recovery Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform 1.2- Dichloroethane 1.1- Dichloroethene Isobutanol Methylene Chloride Methyl Ethyl Ketone 1.1.1.2- Tetrachloroethane 1.1.2.2- Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1.4- Dichlorobenzene 1.2- Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6- Trichlorophenol 2.4.5- Trichlorophenol 2.4- Dinitrotoluene 2.3.4.6- Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4- D 2.4.5- TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det 97.0 Not Det Not Det 97.0 96.0 98.0 Not Det Not Det Not Det Not Det Not Det Not Det Not Det 99.0 Not Det Not Det Not Det 82.0 Not Det 94.0 99.0 Not Det Not Det 90.0 Not Det -99.0 Not Det 105.0 Not Det Not Det Not Det Not Det Not Det Not Det 86.0 Not Det 121.0 88.0 Not Det 91.0 Not Det Not Det Component MDL .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 ,1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 CUH 000010165 Sample Matrix Spike Page: 3 April 3, 1990 Sample I.D. AA03522 (continued) Data for TCLP Metals % Recovery Component Name Arsenic, TCLP Barium, TCLP Cadmium, TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration 85.0 90.0 100.0 93.0 96.0 100.0 91.0 95.0 Component MDL .1 .1 .1 .1 .1 .1 .1 .1 Comments: Reference Lab Report No. R1100. If there are any questions regarding this data, please call. CWH 0000J.0.166 From: American Laboratories and Research Services, Inc. P.O.- Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: April 3, 1990 To: Sample Matrix Spike American Laboratories The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA03523 Sample location: SPIKE TCLP Matrix Spike 2 -Collected by: Collection date: Laboratory submittal date: 04/01/90 Time: Received by: RLH Validated by: RLH Time Parameter: TCLP Organics Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 10:00 Parameter: TCLP Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 04/01/90 Time started: 08:00 Date finished: 04/02/90 Analyst: RLH Date finished: 04/03/90 Analyst: JWP CWH 000010167 Sample Matrix Spike Page: 2 April 3, 1990 Sample I.D. AA03523 (continued) Data for TCLP Organics % Recovery Component Name Acrylonitrile Benzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroform l, 2-Dichloroethane 1.1- Dichloroethene Isobutanol Methylene Chloride Methyl Ethyl Ketone 1,1,1,2-Tetrachloroethane 1,1,2 r 2-Tetrachloroethane Tetrachloroethene Toluene 1.1.1- Trichloroethane 1.1.2- Trichloroethane Trichloroethene Vinyl Chloride Pyridine Phenol bis(2-Chloroethyl) Ether 1, 4-Dichlorobenzene 1.2- Dichlorobenzene Cresols, total Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4.6- Trichlorophenol 2.4.5- Trichlorophenol 2.4- Dinitrotoluene 2.3.4.6- Tetrachlorophenol Hexachlorobenzene Pentachlorophenol 2.4- D 2.4.5- TP(Silvex) Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Concentration Not Det 105.0 Not Det Not Det 109.0 99.0 102.0 Not Det Not Det Not Det Not Det Not Det Not Det Not Det 110.0 Not Det Not Det Not Det 91-0 Not Det 93.0 98.0 Not Det Not Det 91.0 Not Det 97.0 Not Det 108.0 Not Det Not Det Not Det Not Det Not Det Not Det 81.0 Not Det 122.0 103.0 Not Det 100.0 Not Det Not Det Component MDL .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 '.1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 .1 CUH 000010168 Sample Matrix Spike Page: 3 April 3, 1990 Sample I.D. AA03523 (continued) Data for TCLP Metals % Recovery Component Name Arsenic, TCLP Barium, TCLP Cadmium, TCLP Chromium, TCLP Mercury, TCLP Lead, TCLP Selenium, TCLP Silver, TCLP Concentration 88.0 92.0 97.0 89.0 93.0 101.0 92.0 97.0 Component MDL .1 .1 .1 .1 .1 .1 .1 .1 Comments: Reference Lab Report No. R1100. If there are any questions regarding this data, please call. 0 Reviewed By: James W. Pinson, Ph.D. President CUM 0000:10169