Document DMEZKr03wjoXg940aQyQRpGOQ
CO 50 < DFfTE )
CpDE YmTyJj*lj'dDn PKG
SxS&ZZOrJ (LOT NUMBER)
EST, WT * 2525* LBS-
PREPARATION NOTES:
PROCESSES < ) YT-562--D <F')
APPROVED BY: EWK 12/23/01
CQMTYP JOB NAME: 5GYT562DMP
STANDARD HRS- __
j TMT2j
i/4
NAME' GREEN GOLD
STAIN 2,4 DIHYDROXY GUINULINE FOR S OBTAIN P..OHLORO ANILINE FOR S 9
RUN 39" (2037 G > WATER INTO ^EAT TO 85-90 DEG F DUMP A RINSE IN 2,4-DIHYDROXY QUINOLINE
NOTE : WEIGH AND RECORD ALL N-44-C
HSZ 44-C | 44-86r
IIMP IN SODIUM CARBONATE ADJ TO 54" (2836G)1 AT 85-90F 6 STI
A | 408
(595 G) WATER INTO V-
HYDROCHLORIC ACID FROjJ 324,
TO 68-72 DEG F & DUMP~IN FROM MOTE (13 THE RESOURCE CONSERVATION
;>
|/f/J X
! Inl .
RECOVERY BILL HAS CLASSIFIED PARA-
CHLORANILINE (N-&13-C) A HAZARDOUS
WASTE MATERIAL, THIS REQUIRES
EMPTY N613C CONTAINERS TO BE GIVEN 3 WATER I
RINSES WITH 135-145* F WATER FROM HOT WATER!
MIXER INTO DV BEFORE DISPOSING. NOTE (2) N-613-C IS EXTREMELY TOXIC DESTROY
j L^rRUMS PER STANDARD PRACTICE
\\Hr \ STIR 30 MIN OR LONGER TO DISSOLVE FOR S J 3
r1
RECORD:. ST ART
1I
2S-D i
I 613-C i
616 876
ft
T --"T--....... .............
.........MAKING INSTRUCTIONS: BATCH UNIT
EQUIP HENT
PAGE 2 OF 3 CG 5 CODE YT-562-D
1 USE (P) 1 LBS
"WHEN S 1 STIR COMPLETE/ ADJ TO 58" (20G>! *)
I
AT 56-60 DEG F* ICE
I /X'330 i
SIPHON IN IN 10-12 MIN* SODTIUM NrITRR1ITT$*MrW^,
TIR 5 MIN & RECORD: KI_jm__., MUST BE +
TIR 3 MIN AT 60-72 DEG F MAI NT AININ G, ^ >J.
, +CR , +KI FOR S 20. RECORD: TIME START/jZZ^I
J- CR__4z____< + > KI,,rfT______ :< + )
I
j NOTE: (1) IF CR-, KI-, ADD 20# "AS IS"
1
i INCREMENTS HYDROCHLORIC ACID
ASSUME 32% ]
! RECORD: CR_.,,__,,_(+ >, KI________( + >
|
I (.2) IF CR+, KI-, ADD 20# "AS IS* INCREMENTS I
j SODIUM NITRITE
ASSUME 33% i
i RECORD; CR________( + ) KI__________(+)
|
283 1JWT | RUN 15" (760 G) WATER INTO V 283 & HEAT TO
i >1o6-3S DEG F
HB l^tmp IN NICKEL SULFATE 6 STIR TO DISSOLVE 1 1@33
SIPHON IN IN i 0-*f2 MIN & STIR FOR S 29
l 561
AMMONIUM HYDROXIDE
WHEN S 16 STIR COMPLETE., TEST DV & RECORD: |
I CR^nZ(-t), KI,,_Jr,,( + >, TEMP___ ___<60-72*F> ]___
1 NOTE: (1) IF CR-. KI-. ADD 20# "AS IS"
j
i INCREMENTS HYDROCHLORIC ACID
ASSUME 32%!___
I. RECORD : CR________ t + ) KI________< + >
!
j (2) IF CR+-, KI-, ADD 20# "AS IS" INCREMENTS!
i SODIUM NITRITE
.' ,
ASSUME 33%I
CORD: CR________( + > l< I________( + )
i
SETTLE 15-3 MIN FOR S 23
-j
RECORD; ___________ " DV,. START___ _
|
ADO CV TO 82-8S^DEG F AT 42" <4?4 G)
|
CORD: HT,,J5C___F & REC_o 3Z__F
|
, WHEN S 21 SETTLING COMPLETE, COUPLE DV ! UNDERSURFACE IN 6-7/klN
j J
! | RECORD: ST ART
z TOTAL MIN 2I
_J^rT DRAIN IN DV 5 MIN & WASH IN LINE ONLY
|
i^TT STIR 3 MIN. 6 DISCONNECT TRANSFER LINE AT I
f L_CV IMMEDIATELY
I
RECORD: DIAZO__,,*r_-.<-) / BASE_.__.irL_. < + > , j- PH____5Lj-_< 829-9.0)
I I
1<1) IF DIAZO , BASE
& PH BELOW S.G
J
i (A) ADJ TO PH 8.0-9.^SODIUM CARBONATE |_
j (B) RECORD: PH
i
|(2) IF DIAZO+, BASE-/ 6 PH 8. OR ABOVE
1
:| (A) ADD 10# 1 0% N-44-C TO A 55 G DRUM i
j 2,4-DIHYDROXY QUINOLINE
i (B) ADJ WITH WATER TO (+,-> 25 G
1 (C) STIR TO DISSOLVE
! (D> POUR INTO CV
J^T *
1 (E> STIR 10 MIN
1(3) REPEAT (1) 6 (2) ABOVE AS NECESSARY
I TO - DIAZO, + BASE
80
.....
725-A
707-B 1 22-D
1033 561
57-A 2S-D
725-A
-a i__r:
44-C
36
DUP050103906
EQUIP. M&T
CV ' *s ' CON!' T`
HA'KISUnKSTRUCTXOHS : BATCH UNIT
i USE PAGE 3 OF 3 CG 50 CODE YT-562--D (P) | LBS
N-CODE
ACCT LBS
HEAT TO 148-152 DEG F IN 32-33 MIN
I
STIR 20-25 MIN AT 148-152 DEG F. DURING i
TIP WASH DV TO SEWER
1
RUN IN V 283 IN 20-25 MIN MAINTAINING
]
3-152 DEG F
a0
STIR 5 MIN & RECORD : PH___fLJL (7,8-8* B'j
| !
UMP IN BARIUM SULFATE
|
STIR 60 MIN AT 148-152 DEG F
!
RECORD: S T A RT_
I
FLOOD TO
I
STOP AGITATOR TAKE 1 QT SAMPLE
i
S 33
V-105
V-106
V-1 00
V-1 32
GAL
94" <9174G)
96* < 9322G)
33" (8250G)
84* < 8300G)
7 ~
START
__3jJi.0_*X
FINISH
/ 2^o OPTR
250
85-A
250
SUPERVISOR NOTE: <1) IF BXAZQ + AFTER INITAL COUPLING <S26)
ADVISE PROCESSING Tp: I (A) LOAD IN DRUMS @"325=1 NET AS PRESSGAKE
TAKE 1 QT SAMPLE, DO NOT DRY. <B> HIGH PRESSURE HOSE PRESS AND BOX (AFTER
DROPPING BEFORE FILLING NEXT BATCH,
SUPERVISO R__.____________ ______ .___________ -____ DATE______ ______ ________.______ _____
DUP050103907