Document DM4XjR3nrO64de87aYbaee8nB
i b o r a t o r i e s
INowHoftni
P O 'B a x m a s . L w n t e r , P A 1780S - 342S
r L u - t1 6 3 ^X
3ontWa*h}:fitfconWorks
304-883-4476
EVthffl
WtehOB* Wumbsf
Wingl Routs 892 South Washington WV 25181
yAddrwi
veOpp
^
Fsdsml Exprs*
flrtiwBcrtwWtm
rmt^orterAdds*'
Btpres* Saver
g tsw n te
Jus.RtSSMANiWELL7/01
9W i P r o d w h a S i m c l
iovwrt) StmelHw
MftodcfSfaeino
Sb u L( BLLuUka I atj,>Mim
^E222*2sB S u 2 H s2 2 ! ^
7 DAYTAT; Confirm hit byQQMtS
3(1155040 IQ-- aMsBtiiisakK-
p* option. - c k u ssm a W P
M * rim * jStm pi /duro P n ta r/iih O w H y poB)s :
pVP* {)
p*
7ia a ? f
i W fbfiS"""
i. 6
FC4 J Kl
7O35$07O85-772OC
ProbaNBwibw
.. -
S U n q tM w d bv R
***** S M rtvto q s sta d ib v
'< - `6 r t f ) X > s.
o t m * '? - 4' V o ) r 5 '* - - - - - - - - - - - - - - - - - ^ u a x p f - - - - - - - - - - - D a t t n r k n f t t l
D t i t T i m 'tls L r S s 9 R e * f / J b v \
; D aU itT kiM ," x
' D tu fflm
X \
W o rtv alb V
^ * X _ 'n - D tlsfflm *
R sW fibd by \y P M h f A ^ i M em fflJZ ljhp
C o n d B o n o f S * n b * U o e n ir H v tlit R n tl tJ**ftT*tfon
< j k % < Z b T a n p .o f S trap ! * o n tatv * I
c
gwaurofUt
AR226-2498
EID143235
sauoH SV
.I
V IanrasterLaboratories
Wh^quaJty8asenc&
On 07/27/01, 1 tapie ate baitted to Lancaster baborttorict Belov tie listed our tapie ushers with your corresponding description and code.
Please refer to your Lancaster Laboratories client account nuaber hen subalttlng samples or corresponding with the laboratory. Account habiti 07033
ABQK MO SERVICES
-
tUtS - BIAHOH
B A K U * KILL. PLAXA BLDQ 37
L7WCASTEB 0 1 A SOOTS 141
KILKIWG7 pit 19005
phones 303-093-0595 PAX s 303-092-1533
BILL 70s
ABQM AP SHWICBS csfl-K i wjpowr os m s k w r s & co
amili HILL PLAZA BLi 2?
M w c A s n a p i a spots ii mUOBGTCtl PS 19B05_
Phones 302-992-6760
P.0. BOSKS: HK0-54337
COPIES T0< 1 BBS - Pisaonds . AD0M AP Services , ` B a rle y H ill P ia * , B ld g . 37
Lancaster Pike A (tonte 141 Wilmington DB 19005
RBL (TOMER; 18757
SPECIAL JOB DO:
BOOTS (TOMER: 135003 A
LAI So.
People Code/PMCSiptiOn
SP3C55315 PHi-CKRiESKAiMCAP Pater Sample
c h r i s e k a h w e l l 7/oi
collected on 07/35/01 at 0915 by SO
'
Analysis (habarsiOlU 0495 1550 3003 3334 3325 4513
)"\ '
Washington Po;
Job Mo.: 7035-5074
* (jSTXKAXHD TOTAL
Tot Price Diacp`ijTd0;EEElmate
.*20uASi >`!&S8i.Wr 520.00
520.00
Siolb'o" 0.00 0 ,0 0
$520,00
AnalysiS^^ue 0141 3 OC Summary 0495 3 OC/KS Conili 1550 30 Lab Chronicle 3003 39 Rush Pax/Call 3334 34 PC-143 . 3335 34 Pesticide Alternate Pater Bxtr 4513 3s Piekette Deliverable
Total Analyst and Prep charge
LiC DlfcMAb 6X08
Qtt frle price Satinate
1 0,09 0.00 * 0.00
1 295.00 295.00
205.00
1 . 0.00
0*00
0*00
1 0.00 9.00
0.00
1 22S.0 235,00
335*00
0.00 0.00
0*00
1 0.00 0.00
0*00
520.00
SOB OIM^
520.00
Washington Ports ebriasman Sell - 7/01 Job 0.: 7035-5P79S'-773000
*** KS1HATEP TOTAL
$ 5 2 0 .0 0
Discount 0*00 o*oo 0*00 0*00 . 0.00 0.00 0,00
Pet Eatiwite 0.00
295.00 0.O O.0O
235.00 0.90
0.00
520.00
o.oo
520.00
$0 .0 0
$520.00
00 ..00 00
BILLIW3 ... All fee are charged or billed directly to the client. The billing ot a third party will not be accepted without a statement, signed by the third party, which acknowledges and accepts payment responslbllty.
The paperwork submitted with your Mples will be assumed to describe the testing protocol you desire. Any change# to this protocol
must be submitted to LLI in writing. 3t testing is already in
progress, you will be billed. (Our PAX number is 717-555-3501*
Send changes to: Client Services - BSSSHTI)
Lancaster Laboratories reserves the right to e n d this acknowledgement i the sample(a) a# received require additional preparation charges.
ASH011733
Lanca;ter
MEMBER
A C L
0fF 717 S S L
22(7 S o t 3 (5 )0
BIK143236
I ancasterLaboratories
Whernguaittyisasderm.
ANALYTICAL RESULTS
Prepared (on
CRO>BLDuPontde Nemours & Co BarfeyMill p lea , Bldg. 27 LancasterPike & Route 141 Wilmington DB 19805 302-992-6768
Prepared by:
Lancaster Laboratori 2425 New Holland Pike I ra ser, PA 17605-2425
S A f f llM
TUe samplegroup for ibis submitted is 771875..Saple3 arrived at ttw l^ w a to iy on Saturday, July 28,
200L T he PC# for (bis group LBIO-64237 and the release number LB748.
LTL-O-SJl Ussparerf Water Sample
LTL-G-SLTAP Water Sandle
LTLhO-SJ-TAP-DW? Water Sandle
Tannastcr Labs Number
3656026 3656027 3656028
MraBfitQY
.
The Specific methodologies used ia obtaining the enclosed analytical results are iodieated on foe laboratory
chronicles.
.
1CCJPY T
URS - Diamonds
Attn; AUQM AP Services-
Questions? Contact your Client Services Representative Nancy Bornholm at (717) 656-2300.
R espectfully Submitted,
Christine M. Dulaney Sr, Chemist '
ASHDW34
A atM E M B E R
UmcagtarUbontortaC toe.
25HewHollatllBi*
ronuttMZ Uncswe TA0605-2425 70-656-2300 FS3c 717-656-2SS1
2216 a*. 9/11/00
EID143237
'Andly0.RejDgrf
lancasterLaboratories
# f W h e r e qualityisa sdence.
T.iM!iu ilM t .l a b o r a t o r i w S l i p l i V O . W
Collectedt07/26/2001 14:00
by KM
Submitted: 07/28/2001 10:05
Reported: 08/22/2001 at 13:28 Discard; 05/22/2001 i/rL-a-siFl D n s p i k e d W a t e r S a m p l e STEVES JORDON WELLS 7/01
3S56026
Page 1 ofl
Account umber: 07032
'
CRG-E.I.DuPont de Hentours & Co Barley. M i l l P l a z a / Bldg' 27 Lancaster Pike 6 Route 141 Wilmington BE 15805
SJ001
ex* Mo. 029*4
SDG#: XXXOl-OlBKQ
As Received
M Sucairad
Settled
CM
suit
Dataction
I4lt
PC-143
9*35-26-1
0,085 J
0.028
The recovery <>t the surrogates m A end l l H - p m w e outside the
q c limits,
00495
The *6-143 recovery is outside the QC limit* ior the Ms/m s d . The Rp d between the Hs/HSD is outside the QC criteria. The PC-143 recovery net QC
criteria for the associated DCS. .
GC/MS Confirm of PC-143
3825-26-1
M.D.
0.090
The recovery of PC-143 m outside of QC limit to the MS -associated,
with this sample. The relative percent difference .for PC-143 between the
m s /MSS was also outside of QC limits. The recovery ms within QC limits
in the tcs.
U nits 9 /1
g/1
Dilution factor
1
CIS Mo. 02324
00495 02325
analysis Marne PC-143
GC/MS Confirm of PC-143 Pesticide Alternate Mater
Laboratory Chronicle
Analysis
fethnd
Trial* Date and Tim*
PC-149 by GC/BCD*
1 08/06/2061 10:01
LO/91 PC-149 by GC/MS
PC-149 10/91
1 08/15/2001 11:45 1 08/01/2001 08:09
Dilution
Analyst
vector
Michelle J.
1
Kolodsiejski
Timothy Trees
.1 .
Deborah M. zimmenaui 1. .
ASH011735
AC
lancasttfLaboratories.Me.
n 2*25 Now HcSandPOce PO fcm12*25 D w K e ttti* 17605-2425
MV-SW--JWI
2216 8**. 9/11/00
EID143238
Lancaster labocatoria*.Swnjplo Ho* Hit 3656027
Collected*07/26/2001 15 M S
by KM
Submitted: 07/28/2001 10:05 Reported: 08/22/2001,at 13:28 Placard: 09/22/2001 Mb-a-Stf-TAP Hater sample STHVBN JQRDOB HBLLS 7/01
Page 1of1
Account Humbert 07032 GRG-B.I.DuPont de Nemours & Co Barley Mill Plaza, Bldg. 27 Lancaster Pike & Route 141 Wilmington DB 1980S
,SJTAP
err no.
02324
U Received
Analysis Marne
CAS Humber
AS Received M nU t*
Method
D etection L ia it
re_143
.
3B2S-26-1
0.046 a
0,029
M, recovery of the surrogates S T O A aad HS-PTOA are outside the.
C Halts.
m e PC-143 recovery is outside Hie QC H a l t s tor the HS/HSD. The SIB between the M5/H5D is outside the QC criteria. She PC-143 recovery t .QC
I 00495
criteria tor the associated DCS.
BC/H3 Confirm o FC-143
3925-26-1
H-U-
>**1**^* .
m e recovery o PC-143 was outside of QC Halts in the MS associated
with this simple. She relative percent difference .tor FC-143 between the
MS/MSP was also outside o QC limits. She recovery as* within QC limits
in the hCS.
'
,
units
ug/i
ug/l
Dilution Paster l
1
CM He. 02324
. 00495 02325
analysis Hama PC-143 1
G/H3 Contira ofPC-143
Pesticide AlternateHatir
Extr
*Laboratory Chronicle
`Analysis
Msthod ' FC-143 by GC/xCD
Trial# Date and Time 1 09/06/2001 12rl0
10/91.
-
FC-143 by GC/MS
PC-143 10/91
1 08/1^/2001 15:14 1' 08/01/2001 08:00
Analyst
Michelle J. Kolodsiejshi Timothy Trees Deborah H. m e u M U
Dilution Pactor
1
1 1
ASH011736
MEMBER
lanoHtertahontortM*tot-
2425 Nee Holland Pike
?Q *0x12425
U n c u t ; M WOiXe.Ivnn
72-.6.0.5--T2.472c5eeOK*.
w 4m 9/il/OO
BIJ3143239
L a a e a i b t r L a b o r a t o r i e s S a m p le H o . M r 3858028
C0llectedsO7/26/2OOl 1S;4S by KM
Submitted: 07/28/2001 10:05 Reported: 08/22/2001 at 13:28 Discard: 00/22/2001 ML-G-SJ-TAP*DOP Hater Sample STEVEN JORDON WELDS 7/01
'
Page1ofI
Account Number; 07032 CRG-B.I.DuPont de Nemours & Co Barley Mill Plaza, Bldg. 27 Lancaster Pike s Route 141 Wilmington DE 19805
, TAPDP
-p w Ha,
0332 .
as Received
A* X H a l w l
Method
Analysi* Man*
CAa Mm-bar
***ult
Detection biait -
FC-143
3825-36*1
0,053 J
0.026
The recovery of the mirrogates PFPPA and UB-PFPA are outside the
QC iiaits,
.
' 00*95 .
*
she FC-143 recovery ia outside the QC Un i t s for the h s /m Sd . She RK)
between the MS/H3D is outside the QC criteria. The FC-143 recovery set QC
criteria for the associated LC3,
CC/H3 Confirm Of FC-143
, 3825-26-1
N.D.
0.090
The recovery of FC-143 v*s outside it QC limits in the MS associated
with this sample. The relative percent difference for FC-143 between the
KS/HS&.vas also outside of QC linden. The recovery was within q c limit*
in the LCS.
Delta ug/l
'
ug/1 .
Dilution rector l
1
CAT IfQo 02324
00495 02335
Analysis m m FC-143
.
GC/M3 Confine Of FC-143 Pesticide Alternate Mater B*tr
Laboratory Chronicle
Analysis
Method
Trial# bate and Tim*
PC-143 by GC/BCD 10/91
1 08/06/2001 12:42
FC-143 by GC/MS
1 09/1^/2001 15:53
FC-143 10/91
1 08/01/2001 08:00
Dilution
Analyst
Factor
Michelle a.
1
Kblodzlejski
Tinotby Trees
1
Deborah M. Stisseisan i
ASHOU'737
LancasterLaboratories b>c.
M E M B E R 3425 Hofendffk
PO.ox1242$
imeetetpa m & S & m
'*HI. iron -.-wire
EID143240
Analysis R
,tsasaence.
ty Control Summary
Page 1 o f2
C l i e n t Barnet C R G - E - I . D u P o n t d e H e m o u r e 6 C o
G r o u p H umber? 771875
Re p o r t e d * 08/22/01 a t Olt28 P M
...
. , Laboratory Compliance Quality Control
knalyMla, K m --
Batch masber: 012120009A
PC-143
'
Batch number; O1 2 1 2 WAX026 CC/k s Confirm of PC-143
Blank wife
Blank >55
Report tt*3 goltw S
gupple oUnb4f(i) s 36$$026"3656028
0.076 J *03
tog/1
**
$aopl6 ambr(ff) t 365fi026"3656028
11.D*
.1
ug/X
45
EsC8J? %RgC
Xpca/ifCSD LildlEt
3-55
3-55
RPD XPD K M
inalvala 1 M M
suaiber: 01212Q009AjPC-143
Batch nimbexi 01213WBX026
m / M S Confirm bf PC-143
Sample Matrix Quality Control
M3 %BBC
M3D %MC
M3/M3D Unltf
BPB bko RPD wax C6Qc
DUP Cone
Sample noaberta)i 3656026-3656028
25* 21
50r-100
32* 30 ,
Sample siU^berC) * 3656026-3656028
37* .57
50-100
45* 30
POP RPI>
BPP Mast
*
Surrogate Quality Control
toalyaia M>a*> PC-i*3 1" Water
Data sptbet: 01212oooyh
p$m
IXU-pfUa
3656036
3656027
6
3556028
9
Blank
12
.
LCS
`16 .
.
MS ' 14
K5D 21
2* . 1* 3* * 2* a*
2* 0
Limit*; 1*50
13-88
Analyoia HaMsei C O B Confix of PC-143 / Water Batch number; 01212HAX026
S'FNA
3656026 3656027 3656028 Blank
ICS-
HS MSB `
33 28 45 .
14 19 17 37
pfbba
is*
5* . 17* 11* 14' 14* 20*
50-150
-O utside o f specification
(1) The result for one or tfcfo detHimnatioiB was less than five times theLOQ.
The background result was mote than four times the spike added.
LancasterLaboratories,,JpC
MEMBER
242SNewHo9andPiM
p o go* 1345$
l^ancahei; 17SOW4i5
EXD143241
8SinOHSY
Analysis Report'
#LancasterLaboratories " T S a S & ' S B B o i Sujamary
Page 2 o f2
Client awe: CRG-B.I.DuPont de Nemours & Co
Group Number: 771875
Reportedt 08/22/01 at 01:28 PH
,. ,, Surrogate Quality Control
timita:
I'SO
ASH031739
- Outside o f specification
.
(1 ) The result for one or both deternnnatioiis was less than five tiroes the LOQ.
m The background result was more than four tiroes the spike added.
L>txtei laboratories,ktc. M 25 8 *w rtottend rtt* POBMU4K
~rw^t `-..i.--
EID143242
ici. 4orgtortes '
151663
NewHolajK K) Bex12425. UflMetr PA17808-34i' d l t Z j & & s l . J -- & B rtL 3 Ssyia..
ontWashington Works tV-Naroe ______
1X84000000 Tejeslwnttefeer
WtialBepress
ftsrwaortwMtnw..
T efet^e Number,
* 6 9 2 South Washington WV 26161
tyAddrtt*
_________
THntportwMtinrt*
>OppiAlison Crane
Express Savtr
VSUMWtef '
Methode?Shfocine
WT WPMtfc-aOM- SCBJ&J JogPAM KigULS T|ot
H t Predutfoa Smete
Sottili SMgphe tnttnwttow
/ C c *?*'
iv i.y
3QMS; SPME procdure
vwW Smeteo
*mr *
7035-507095*772l
Iprot^ Number-----------
Emotoveeete)HtndSrtg
________
.-
'
........ .......
...
1 ..--
pUoa
Deti limr Sample Vdume PreureaSv* Quantity goffi typ* W.
=0-1
5*aK / . *ms 3-3 4 -MSD
T ** ' 7 *'
sy*~ w r S6T" / Ww 1000'
isy*>
/*6a
?*** /S\r TTS7
TTC
Notte A < /V ii<
'S s 2B T " fi "T " f i
fi
x
* *r
r y
Ii
iI :
i
tUWInaJihedtwr
x ;uithadbv
XOtttfrsntiistr-oi ttQ BcaietftecoNtdfe/\
Oite/ttwe 2
ReeeNedbv
Ottima*
Reeelwdby
XDtt/11roe/N\
DtUfflim
I XOttt/Tlm*
GfindMannfSegete POftM W t FftlttOwtlnHteB..
sJSSE Stfsk*
uMtadbv
X Patema
X
ReaeNedby
iQttt/nmi
Pb
.s > */*/$
E ID 143243
i
GWIIOHSV
ASHQ1741
e
ui
o o
so
o o o
ow
a
*
Ig
I I 10
s*
$
i
lU")
S
K
8.
&
E ID 43244
ACCOHT 9 0 : 07033 a d q k a p sravicis
TOS - DIMfQtBS NWUEX HITO. P1-A2A BLCG 37 l a s c a s w P i r e o rootij u ta u m m a i tm u s o s
Pago 3
.
.
jrob o.; 7035-507005-773000 tstrek x sfi totai,
$15SO.fiO
$ 0 .0 9
hM0 . 0au0MPB
$1560.00
BXt&XMS ... M X ce ato charged or billed directly t the clienbrThe b illin g o f a third p arty * U l not be accepted without a ttttaait/PljMd by the third party, which acknowledge and accept payment reaponeibilty.
the paperwork mTOitte) with y e w Maplea will be iaauned to
-
describe the teating protOcoX yow dsalre. Any change* to thia protocol
nat be aubaitted to LLZ i t writing. I f teating la already in
pxogreaa, yon will be billed. (Our not
in 717-IM-2SII;
Send change# to t C lien t S ervice* - m f m U l )
'
ASH011742
bancaatcr l a b o n t w l e e reserve the right to amend thia acknowledgement if the ennpXe(a) a* received reguire additional preparation charge.
POR UTO BSe 771075 011 P 0 30 07/3 0 /0 1 1005 ASR000 3S1 034 So 00.00 C
u n t te; Laboratorio Inc. *2425 New Holland Pike, POBox 12425, UfKastef, WU7605-2425 #717^56-2300 Fax: 717^56-2681
A C ILMBM9BW
EID143245
