Document DGqm3K4QpX8KnvO5MokqraQwO
CODE YE-69S-D
M.
__7flT_P ( DATE t)
BLENDED BACK:
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< LOT )
( EST WT )
, pg 98, ,,b^L/^ri CG Gi
(CODE)
PROCESSES ( ) YE-69S-D <T)
APPROVE FWP 16/15/32
COMTYP JOB NAME: G1YE69SDMT
Tl o t )~ "
(POUNDS*)'
- EQUIP KENT
NAME: MOLYBDATE ORANGE
PREP 1
351 o
tg>i AA I
I---
I !
i-TA'IN SODIUM SULFATE FOR S-13 CALCULATE 6 SET ON BADGER METER FOR (NITRIC ACID WEAK) OBTAIN SODIUM CHLORIDE FOR S~33 OBTAIN SODA ASH FOR S~37 OBTAIN SODIUM SILICATE FOR S-39 ' OBTAIN SODA ASH FOR S-43 OBTAIN ANTIMONY TRIOXIDE FOR S-46
WEIGH SODIUM CHROMATE INTO V-3514
OPTR
M
...
OPTR
m
359 3
WEIGH IN SODIUM MOLYBDATE SOLUTION
S
OPTR
MK iST, T-3Zi?,
OPTR____ MK
USE LBS
84
| i ACC7 i N-CODE | LBS
j 108-A i
84
1 33-D I 60
734 i 4~A 1 734
146 1 3-A 1 146
237 |
Dj c | 237
350 ) 3-A i 350
70 j 711-B I 70
10-D i I !i So*! ----------- -- 1
423-D 1
1885 303
358 4
5
Iff'^URdN 10* (508 G) WATER INTO V-3S8
|
RUN V--359 INTO V-351 &PUMP IN V-351
i
ADJ TO 55" (2600 G)
!
M*J^SIFT IN N-10S-A FROM S1*3 &
!
i1fj^,STIR 5 MIN 4c RECORD: FIT jQj|,,<9.0-1 0.0?
j
115/f ADJ TO PH 9,8-9.9 6 RECORD: PH__SZT~
!
j 1 (CAUSTIC SODA SOLUTION)
ASSUME 50% I.
I jU.
ASSUME 66% 1,
H#j^ADD N-33-D FROM S 2 USING BADGER METER
|
T\*T\ ADJ TO 66* <3i2J G) AT 47*6 9*F I I RECORD: y.OL_iJfc* 6 ^JuLU~
! I
J'lV-r'STIR 5 MIN^fc RECORD: POU<7.4-7*6) 6 i 1 G/ML 'LLlflttU -.080-1 ,083)
i i
i I NOTE IF G/ML OUT OF LIMITS FILL GUT CHECK 1
i -I LIST l, ATTACH, TAKE 1 QT SAMPLE
II^TmJN 20 * <996 G > WATER INTO
!
i i RECORD N-4-1-D STORAGE TANK TO PUMP FROM, | L^tlftCLE ONE: 40:2 410 411 420 424 425 JCjS^T CHECK WITH CU SUFV: I I wSTORAGE TANK MUST CONTAIN AT LEAST 2376 i | GAL: 402=491 410=25* , 411=48*', 420=25*,
424=25 |S\ 425=31 " ?TORHCE TANK MUST HAVE STIRRED AT LEAST 2 MIN SINCE LAST ADDITION OR ADJUSTMENT ^STORAGE TANK MUST BE ISOLATED UNTIL ALL PUMPING FOR THIS BATCH IS COMPLETE SET METER FOR 300 G
j 1 i | |
7-D i______ _J 33-D |_____
iJ I!
DUP050103075
LOT; . EQUIP MENT | ...___ I. SV !J
CO HTTP .JOB NAME: Q1 YE698.BMT PAGE 2
DATE P.R J NT ED ; 1 0/ i 5/82 ! USE i N- |ACCT . LBS I CODE 1 LBS
AT APPROX 10 G WHILE CONTINUING TO PUMP,
CHECK PH & DENSITY. 'RECORD BELOW* IF NOT
IN RANGE,, STOP PUMPING A SEE SUPV* * PH:^a5_ <2.2-3*7)
JS>WSNSITY:
G/ML < 1 * 270-1 * 323)
TF 5-22 OK & WHEN 5-21 COMPLETE, RECORD
DENSITY Au3b& G/ML ON TRAPPED SAMPLE jSROM END OF S-21 PUMPING*
JSING DENSITY FROM 5-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21* CIRCLE DENSITY A SETTING IN TABLE BELOW*
*#** TABLE **'
""l
-----i
II II
SETTING 1 G/.ML
1673 ] 1 .291
1670 | 1 *292
1663 I 1 *293
i 656 | i .294
1649 | 1 ,295
1641
! 1*296
1634 | 1 .297
1627 | 1 *298
1620 | 1 .299
1614 | 1 .300
1.607 | 1*301
1600 I 1 .302
1593 f i.;
1586 t
1580 | 1*305
1573 | 1 *306
1566 J 1 *307
1566 I 1 .307
1559 i 1 .308
1553 I 1 *309
1546 ! 1 *310
1540 ! 1.311
SETTING 1534 1527 1521
1515 1509 1503 1497 1490 i 484 1478 1473 1467 1461 23sS>
SET METER & PUMP
(RECORD FROM TABLE)
FLUSH LINE WITH WATER.. INTO SV FOR APPROXIMATELY
SECONDS
V^-DV-rf
ADJ LEAD NITRATE T\76VT3625 G) AT 67-69*F
CORD: --*E 7T"
|
SJSRr5 MIN A RECORD PH:
(2.2-3*7)
|
F NECESSARY ADJ TOfi-l 3*0-3.1
ASSUME 66%!
6 RECORD PH:
ASSUME 50% |
--------- DILUTE N-Y-D 10:1 WITH WATER BEFORE ADDING j RECORD: JlL^rSi G/ML (1.143-1 *144) IF OUT OF SPEC I
^LL OUT CHECK LIST 6 ATTACH*
.
\
STIR AT 67-69-k F FOR S-31 . TAKE 1 QT SAMPLE-
i
41 -D 57-A
5110
33-D 7-D'
DUP050103076
i.LOTf ,
^Egiifp ,HENT{
CQNT 1
CDKTYF JOB NAME : 1YE698DMT PACE 03
DATE PRINTED1 445/82
I USE I N- |ACCT
I LBS 1 CODE I LBS
______________________________________ _____________________IiI
'i OBTAIN 1 QTSAMPLES OF S-18 6 S-3 SOLUTIONS I
j|
i & TITRATE TWICE I NOTIFY SUPV IF ML N-10-D IS NOT IN
II!
RANGE I
II
I 7*1-7.4 OR IF THE TWO TITRATIONS DIFFER BY
I
1|
I MORE THAN 0,1 ML N~i~D (IF YES, FLUSH ALL I EQUIPMENT & REPEAT TITRATIONS). DO NOT
i |
|| ||
iPROCEED IF
N-10-D TITRATION IS OUT OF RANGE I
S|
1 ADJUST V-358 FOR A TITRATION PH OF2.1 TO 2.2!! 33-D !
| FROM FINAL IN-LINE TITRATION, RECORD LOWEST I __ | PH ______ _ 6 HL N-10-D____
-d i La
I
WHEN S-31 TITRATION OK , STRIKE V-358 THRU
BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
I 16-16 MIN RECORD: START
, TOTAL
____
NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
't BUBBLES APPEAR IN SIGHT GLASSES
IMMEDIATELY DUMP IN N-4-A FROM S 3 6 SET TIMER
OR 15 MINUTES DURING S 33, WASH IN V-358 STIR 2 MIN N RECORD PKj&LaLn .8-2.5)
^'BXS ,
( MUST BE + )
STIR TOTAL OF 15 MIN FROM S-33 & RECORD; TEMP,,_jt4t_F (67-73i*F>
IMP N-3-A FROM S-4
"IR 3 MIN Tn H-32-D FROM S-5
IR 2 MIN
IN LIQUID ALUM USING BADGER METER MIN & FLUSH ALUM LINE WITH WATER
IP IN N-3 FROM S-6
STIR 4 MIN FOR S-48
?34 115-Di 367
fie *7
IN HYDROCHLORIC ACID USING WEIGHT & FLOW
I CONTROL PANEL
MK , 3l>
MK
DURING S--44 SIFT N-711-B FROM S-7 INTO V-39Q
WITH AGITATOR ON IN 1-2 MIN
STIR 1-2 MIN TO MILKY SOLUTION '
/,, t
28--D 28-D
1 5
WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N--711-B
SOLUTION GRADUALLY OVER 5-MIN PERIOD INTO SV i i WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
K"UNTIL FOAM SUBSIDES.
//O
UMP IN BLANC FIXE N
I -33r
WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON l
1 TOP' OF PAGE 1 .L^RECORD: CODE
LOT
-SU&LJi
STIR 2 MIN
5^>,REC0RD : PH
(5.8-6. >
&r\ IF NECESSARY, ADJ TO PH 5J5-6.
ASSUME 5%
U RECORD: PH-_____ASSUME 66% FLOOD TO 153" (7228 G) 6 STOP AGITATOR
/fO 128-A! 330
7-D 33-D
FINISH^
2P.TR
DUP050103077