Document D3vEmojzdQzDM6a1NNxbMq9o
aCem Fntee
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ea elE
DuPcat Haskell Laboratory He. 2.2. 6/555
June23, 2000
U.S. Eaviroumental Protection Ageacy OfoffPi ollc utieon PreveanndtTioxoicns Chemical Control Division 401 M Stress NW, Room 403 `Washington, D.C. 20460
Eaclosed are two copiesof Hie summary sn Ammonium Perfluaroocmmoare.Onecopyis 2publiccopy andtheother copy zrivaieandmarked accordingly. Ifyou have any
questions. pieasecallmeon 202-366-5259.
Veryty yous.
pe2d fornsd2,, [/; hi
GeLr.Kaenledd y, Jr"
Director,Applied Toxicology
and Health
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DuPontHaskell Laboratory
S supe tm rao7nti3soa tnrmaarmyavesioe eet mim
June 23,2000
Or. ChaM.rAuelr, Deirecscor
C.S. EavironmentalProtection Ageacy
Office ofPollutionPreventionand Toxics
;
Chemical Control Division
W40a1 MsS hit nDgNr .WCt.,e o2R0on4oe 6,m04t 03
DearDr. Auer:
MAasyy1o,ur2e0q0u0e,satmeadcihnieydoiusrAapsruimlm1a9,ry2o0f00DluPeoaarta'nsdUd.uSr.iunsgeosuorfsAumbmseoqnuieunmtmeetingon.
|
Perfluoroocmoats (APFO,CAS# 3825-26-1)as afuoropolymer reaction idincluding
.
releases from DuPont site and the faze ofAPFOinfluaropolymerdispersionproducts, a
summaryofindustrialbygienedatacollectedatourU.S. flucropolymermanufacturing
site,and asummaryoftheemployeeblooddatafrom asitein the US. Asummaofrtyhe
"oxicalogyavailableto DuPontwassentunderseparatecovercu May26, 2000.
tisimportant eamphasize thefollowingpoints:
>DuPontdoes aotmanufacAaPFrOe.AllAPFO usedinourprocess25es3
*
reaction idispurchasedfromanoutsidesupplier.
> Mostof the APFOusedisremovedfromtheSucropolymerproductsbefore theyaresoldtooutsidecustomers. A relativelysmallamountof APFO
~~{pwroordladcwai.da, intheU.S.) leaves DuPout facilidesiafluoropolymerdispersion
> Of the APFOintheproductsSold.most(>97%)isdeszrovedduringcastcmer
procassing to a soa-~carboxylazedhydroftucrocarbon.
>AplotlenotfitahleaUr.eSc.onCcuePnotrnattoepderaactiooensltohcaattiuosne;WAaPsFkOinwgiwthaWsiogneikfiscianntWeaxsphoisnugroen, >z
WV.Therefore,mostofthe industrial hygienedazandbloodserumdara
resentedin hisdocument arefrom thatlocation.
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Dr.Cuacles M.Auer, Direcaor
Page2
C5. EavwoumentalProtection Agency
. > EAxPeFaOsisvaeoiwndauisrwbioarlneheyxgpioesnuerdeasttaocbolelseicgcneidfiocnanwtolrykbeerlsopwottehaetiAaCllGyIexHpToLseVdotfo si0gn.ifi0can1tlmysgbirn/,ceTtmWhAe'.coEnxvpeorssuironetlev1e0lsAoPfFpOlasnotfwuatrikoenfrsrhoamv2eddrryoppopwedde.r.
>inAsMpaarrtcohfatnhdeAognrgoiiongtshuirsvyeeilalranasceeroifewsoorfkbelrosopdostaeamtpilaellsyweexrpeostaekdentofrAoPmFO, workersinthe U.S.,The Netheriandsand Japant0beanalyzedforserum APFO concentration.DuPonthas aotrecsivedthe results from ourconmact Iaboratactisotrimye.DuPoot illsabi asummaryof the resultswhen theybecomeavailable.
`Theformatofsheinformacionintheamachedis amodified UETPformat.Ifyouwish discusstheinformarioncontained ithearachment,pleasecontactRobertF. Pinchot a
(302)9994074ore-mailarRPobiernuFcior@usa.dour mpeaot(u30t2).36c6-5o25m9.
Verywulyyours,
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Voluagary CEIP. Ammonium Serisroocascum
Voluneary UseandExposure Information Profile Ammonium Perfluorooctanoate (APFO)
L CHEMICAL IDENTIFICATION
Chemical Name: CAS Number:
Ammonium Perflucrooczanoats 3825-26-1
o COMPANY IDENTIFICATION
Company Name: ELduPontdeNemoursandCompany
Site Locations:
Site whereAPFOisusedas areactionaid:
Washingwon Works RWaosuhtien8g9i2on, WV 26181
-
SairteepsrwohceesrseedA:PFOcontainingproducts ma arWad shine gton Works
Partin Plant Cheesequake Road Parlin, NJ 08859
5S4p0r1uaJnecfefePrlsaonnt Davis Hwy.
Richmond, VA 23234
Site which disposes of waste containing APFO:
:
Chambers Works
Ree. 130
Deegwater, NJ 08023
Technical Contact: (R3o0b2e)rt99F.94P0i7n4c.hot
CDhuePsotnuttFlRuuonroPplraozdaucss
>
Bldg. 7112210
:
CWaialrmeiBaoguileoDvnaE.r.d 19805-0711
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.
Voluuary UEP.AmmoaiunPefaaroosasces
OL DUPONT AND CUSTOMER ACTIVITIES NarradiveDescription of APFOUse
"The blockdiagramon theback page Ged"DuPont US APFO Balance"describesthe procasses discussedbelow.
aDnuPdotnectaufsieuosrAoePtFhOyalesne(arTeFacEt)iconoa-ipodliyntmehresp.rTodhuecptrioonceosfsputoillyitzeedwartaDfuiPuocarro'sethy(lPeTnFeE:)
Washington Works for making PTFEandco-polymers consists of polymerizing TFE
(andotherco-monomers if desired) inanaqueous mediawith asmall amount of APFO to 3idinthereaction.
Following thepolymerization step,thepolymer dispersion iseitherdriedtoremovewar andAPFOorconcentrated (removingsomeofthe APFO), stabilizedandsoldasan aqueousdispersion."Thedriedpolymer containsverylittle,ifany, APFO.
TheAPFOremovedfromthepolymeris recoveredforrecycle,capairedanddestroyed offsiteinanincinerator,capturedandsent toanoffsiteindustriallandfill,and/oremiced.
20airor waterazthe WashingWotroksn.
"Thestabilized polymerdispersions aresold byDuPont windustrial customers (both in. the USand cusside the US)fora variety of uses, internally Tansterredtothe DuPont `Spruance Plantfor theproductionofTeflonfibersandPTFEcoatedsyntheticfibers.or internally transferred totheDuPont ParlinPlantfortheproduction ofTeflonFinishes.
sAesnemraultleadmaotuWnatsohfinnognt-ohnaWzoarrdkosuiss weaastseedpiolnyamewra,swsawtaetre,rAwPeFaOmmaenadtotfahceirliatdyd2itDiuvPeosnt's
Chambers Works. Thismaterial iseitheremitted intheChambers Workswater discharge.
otcapaured on carbon andlandfilledin asecure landSIL.
Theinternal processattheDuPontSpurancePlanttoproducs Teflon bersinvolves.
fd orme osts obftyht tehperr foodlulco otw,ianyg"rsiee natcetrid ionng:"stepinwhichthe APFOconmainedintheproduct &
CFH(CFCOONEL" > CF(CEsCF:H + COz 43H
TEE Alii at. E pTrhoidsurcetacptrioocnegsoseedstaocDoumPpolnett'isoSnpartua3n5c0epClaanndtd0o.2e5sraeostigdeentscienttiemree.daAnsdmtahlulscaomnotuanitnos f
`smallamount of residAuPaFOl. These products are usedforindustrialpump, valveand
compressor packingmaterials.
>
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EID102809
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Valungry UEIP. AmmoniumPerucroocsous
`The process
operationof
formakingTeflon finishes at
fluoropolymer dispersions with
the DuPontParlin Plant igvolves 2
other additivesincludingsolvens,
blending
binders,
awnidsptisggmeeonartast.edTdhuersimnaglplroadmuocutncthaonfgAePovFeOrse.miSsosmioenosftothweaftueorrafproomltyhmiestfdaicslpceyrisisodnuies to
processed at contract facilitieswhere the material is driedat temperacures >350C hus
disernoycingothrientpAoPfFoinOiarschceaosprrtdoidneugcttdos.the reaction above.`Thisdriedmaterialisthen.
T(hesfi2n3aucloporckodwuachrtep)rvoidaucaed iusthtensspoorladytimongaopaptlriocltalteorrcesotshtaidtnag.pplEy mtheiprosdousfcAtiPtFo8Osfnurbossmtaiz
theseoperarionscousistof overspraythatiscithercapturedon flrsandlandfilled or iabsstohrebnetdyipinctaolwlayg"esrinrteesrueldt"iangtitnem3pewraatcearreemsiaspspiorno.acPhriondguSc0t0thFatriessualptpilnigeidatwtthheeresmuovbasloef theAPEOfromthesubstrateand subsequentdestructionaccording to thereactionabove.
`mCuossttomapeprlsiocaftdiionsspiearvsoilonvepraod"uscinttseursinegt"shtemeaptewrhiearle tfhoreaAvParFiOetiysodfeasprpolyiceadt.iTonhse.rHeoawreevaer,
smallnumber oftaaplplliocwatthieonAsPwFheOrteotshuebcluismteormeesurlhteiantgsitnhaeidriesmpiesrssiioonnsp.rTohdeurcesarealso 3 stmemaplelraamuumrbeesrtohafapplicationswherethe customer'sproductisaot beatedresultingin the
AiPFnOdsauyfiilnsegrwifiatbarhitclhse.product.`Theseapplicationsincludeindustrialpackings,and.
IV. SITERELEASEANDTRANSFERINFORMATIONFORTRICHEMICALS
`Notappl APFi O ic s aoa t lisb ted l oate heT- RI
V.SITERELEAASNED TRANSFER INFORMATION FOR NON-TRI CHEMICALS
A. Ou-AisrRieletasees.
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TWareEnsuwmoartked| ToPaaria | SRoelreaeses|s (C1bhsa.1m99b9e) nWoks
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Comments
liAmirietmeidsmseiaosnusraermeeenstismoaftesdpeucsiifnigcpeoxignitnseoeurrincgecsaciocnudluatcitoendsiaatndhejpudagements and
>
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Voiuasary CEP, AcmosiumPtoroocascu
B. On-site WaterReleases ee --------
ES
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. Foun: Source
i me Esta Ti oPaalm dAana n|ua Sat loRnee laeapsd ees|s(S[bCs.hm 1a99m9)beWror
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lWiamtietreedmmeisassiuornesmaernetessotfimsapteecdiufiscisnoguerncgeisnceoenrdiuncgtceadlicunltahteiopnassato.d judgements ind
.
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`WashingtonWorskiosnesmoicscsuiornfsoorcc10u-r1f0o0rdaapypsr/yorx.imRaetleealsye3s5o0fdaAyPs/FyOrtwhoitlheethOebio
othersites'emis RiverfromtheDuPont
Washington
WorksPlant
weremodeled
using
the
`Probabilistic Dilution Model(PDM BetaVersion 4.0Beta June11, 1999, US
EPA Office of PollutionPreventionand Toxics) and aconstructedMicrosoft
Emxocdeellsipnrgeeaxdesrvhieseetsm.odTehl.eAPPDFMOirnedilceaatseeddtahtaatfAoPr F1O99c6onwceeraetruaszeidoinnsbooft1h.0vgC-
W/Lwouldbeexceededabout50% of the timeduring the year. APFO
concsatrationsof in the riverwouldexceed 0.1 ug APFO/L 90% of the time
Curingtheyearand 10ug APFO/L about2.2% ofthetimeduring theyear.
A`vMiecrraogsoefatnuEaxlceAlPsFprOecaodnscheenettrwaatiso0n.s4i2n3tjhiegOAhPiFoOR/iLv.erMcoadleclueladtAedFbyPuOsing a
concentrations intheriver rangedfrom a lowof0.199jig APFO/LinMarch 02
rhiivgehrfolfo0w.s9,65rejsipgecAtPiFveOlCy-. 3A/vLeriangeSeOphtieomRbierv,ewrhfilcohwscaornrdevsopolnudmteodhaiagchaalncdullatoewd.
from theUSGeologicalThSeurBveelylwevaisllceolDlaecmtiesdaotntthheeOBbeliloevRiilvleeDra1m3mi0ldeussedia
the spreadsheetmodel. downstream ofthe Washington Works
Plant.This riverflowdataistheclosest
locariondownstream from theplantwherethis type ofinformationis available.
i 1iamm1e9d9i9ataedlryidnokwinngswtarteearmsoanmptlheeoObhaiiooReivdefrrformoGmDEupPiaosstticWsa,WsahsiknigntgownoWaoWrVks,
sowed0.552ugll APFO.
LIunbadedciktiPounbslaimcSpelrevsiocebDiinsetrdiicta,Jdaonwunasrtyre2a0m0o0froWmasthhirnegsidiofnfWeorrenktswcelaltshaetOtbheio
River,showed0.8ug/l, 0.44ug/! and 0.313 ug/l.APFO.
2
TLSart.Modeling releasesof ammonium perzucrooctasous(uothe Olio River, DuPoutIasmrmal Report EMSES40.
:
EID102811
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C. On-LaSndiRelteasees | CEhsgaimnbeesrrisngWocarlkcsutlraetaitosnsAaPnFdOmecaosnutraeimneinngtswaisntdeiicaate3tWhaastteawppartoexriTmeaatemlmyen3t0s%yosfte.
lheaAnPdFfOioilnnlstiheteed.wTahsteeswealtaenrdTreealteeadsiessaabrseoersbteidma0tedtotoabcear3b9o0n0m1ebdiia1t9h9a9t.is Prioroperationshave resultedinmeasurableAPFOconcentrationsin three sluarnfdfaiclelwsaotpeerramteeadsbuyrtehmeenWtassihnin1g9t9o9naWnodr2k0s0i0nytWdersatnVgiergfirnoima2.A23suLegtlart'landfill t3h2e4s0aumg/eltwiimteh paenraiovdearLaeogaefrt13l9an2d0fgi/lll.rGarnogeufnrdowmat60e.r3muega/slturoe1m7e4n0s0tuaglklewnidtuhri=ng aveorf25a37gug/eL.Atthe "locallandfill"thegroundwaterconcentratiroangse fhreom"lo0c.a0l4l6angd/flitlol"3r9aungg/elfwromi0a.n5a4tvuegr/halge0of7u8g./8l3uwgi/tl.haSnuarvfearceagweatoefrs1a8m.p5luegs:atAx Dry Runlandfillterearelimitedmeasurements ofgroundwater and surface waterwithmaximumconcentrationsingroundwaterof 15gandthe maximum concentration in thepermittzdoutfall bas been 33g. In 1999 3 RCRAFacilitylavestigacionwascompletedforWashington Worksand wFaosunsduwbamtietrecdotncoeEntPrAatRieognisoonf AIPiFnOJuanteWa1s99h9i"n.gTtohnerWeoprokrst.contadairanosn. D. Tratno Ofsf-sfiteeLocratisons Washington Works:
| {Tacieration [Waswwatar seament
castes Ob, 1999
]
16000
T
13400
| HazardousWaste Landfill Other landfill
T T
o=
(1 Recveleoerecovery
IV. ON-SITEWORKPLACEEXPOSURE
-
A Informationonthe Number of EmployeesPowatiallyExposed
.
>
Z
+WRoappaerovfahsesu2amdieldloc@acMdoanrsc2a.dTs.aKcoifcihca.oRaeicroiinlgPlrocoagiroasmsViaandargeeerl.sEPrAeRsevgeilloanblIew.Poiulraecqeueispti.. This 3 he amemateri hak vas describedaboveiaparagraph |ofseconV.D.
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Volamory UEIP. Ammcsiem Perdosroocasous
tThheeirbnloersmablewloorwkdeascctirviibteietshfeorazuamcbeorfotfhweotrhkreeressittheastwmhaeyrbeeAePxFpOoseisduto AsoPrFeAOdPudFrOing containing productisprocessed.
. [HounDay |
Washington Works Day
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100-250 om
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Routineworkeractivities that have potentialforexposure:
> >
HHaannddlliinngg rraaww dmiastpeerrisailoAnsPcFoOnning APFO
> >
PMaiontelnadnrycyeeromofppeeorlaytmrieorniznadtiomnairnetacetniaonncseystems
> >
POapcekroautitoonfaPnTdFmEaaiantdecnoa-npcoeloyfmAerPdFisOperrescioovnepryrosdyucstesms
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ParlinPlant
Dayshe
7110-100
|7 100-250
18.
1
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Routine workeractivities thathavepotentialfor exposure:
> Handling of PTFEand Co-polymerdispersionproducts > Operationandmaintofebieandiang nfacicliteies
> Paoc ffik niso hedpu rodt uct
`NwohtereetthahteaAtPgEotOicmoeuilsdtshuebmlaitmeer.iTahlbearnedfloerdeatthetrheeiPsalriltitnlePploatnetnatitaalnfeolreevxaptoesduwrmepteoramre ha andliingr AoPfb FthOeapotolchyrimsefarncdiilsie pteyr.sAilonlmeaxtpeorsiuarlespaolteontfiwahliischtchornotuagihsnk<i1n%coAnPtaFcOtwdiurtihnmg:ost containing<0.25% APFO.
THowDry |
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`Routineworkeractivities thathavepotential forexposure:
>> O`HpaenrdaltiinognoafnPdTmFaEiannsednCnoe-epooflySmheerrdciosupteirnsgfiaocniplriotideusct
> Operationsnd maintoef snintaerinngcrolels
> Pacofk nooa -sing teri edprn odug ct.
`Notethatthe PTFEand co-polymer dispersionproductsused at she Sprucesite conua
0.9% APFOwithmostcontainingapproximately 0.3%APFO.
B. InformasionontheExposureLevels ofWashington Works Employees
i`hnSytigneicreemnmeedodisaatctoaeifsst0hcedopprrnoocdcauscestinsnigisaddrsoovotaeheacitsaseitttWhdeae.sTUhhiSenwgilwitomhniWtAeoPdrmFkOsea,naDdusPAoPauFt'rOsocseofinartaibaroisbnmoiereningnedaAustPtrFsiOal
>3
`cmonuccehnltomawseiolnesvealsthe(moobstelyrnsiotesnwh-eree cAPeFlOeccvoeanlstboaifnlAiPnegFgO)r.odTuhcetdartsaisnetdhehabviesehbeolwosw
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arrefele3cctommobniintaotriionngodfocvheeomviecratlhoeplearsattoryaenardsmaait nWtaesnhainncgetwoonrWkoerrkpse.rTshonealsasmampplleerse.sults
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t`hPaatrhcaalssbhiefetnapirrseatrmepalteesdwairtethaskoedniautmtbhyedrroaxeiodfel2e0t0hymlleomeigniyucsoilnigmeathTaennoalx.cTolhleecAtPioFnOaibse ddesoerbredfirovrmetaahgeenttc,uciboenszuvseriitnignnmgetgthheaAnoPlFichtyodritosgmeentchhylloersitdeer,.wAhficehrawlsoosrervltehsaeamsuetaphy,l eTshteemreistqhuyalnecsitfeireodufspienrgflaugoarosdcehcraonmoaitcoagcriadpih ueqsueidpapsedanwiintthearnnaellsenctdraorndca,paanudreatdleeteacsttor. Ptrherceiesciaolnibirsaetsitoinsmaatmepdlteosbaere+p/-re1p0a%rerdetlaotciovve.erthe concentration rangeofinterest.
oTnhleydaavrearaybofveewsshaomwplaevseraabgoevsectohnesiTsLtYen.tlWyhbeelroewretshueltAsGarCeHaIboTvLeVoor fae0a.r0t1omtgh/emT'LwVi,tsthe eevnegianteiesriinnvgecsotnitgraozlesd)atnodcroerdrueccettihveeeaxcptoiosnur(ealdedivteilosniaslpuenrdseorntaalkepnr.oceOctilvedeaqcduaifpremoemntrthoer: 1f9r8o0m'rsescehiovwinhgigthheerAlePvFeOls1osfe3xppoowsduerre.to1raectehieevainrgliyt1199a0n'asqWueaousssohlutiWioonnr.kTsghsitwsictohcahnnegde swhaosudlodnbeegtooreedducchaetthinetpohteen1t9i9a7lifmoreexppeorisoudr.etdhuersiintgswbaansdstiantgionfguthpednreywpAowPdFeOrr.ecIat very ffaacciilliittiieess.mOapyerhaatviencgoanntdibmauiznztdetnoatnhceehidigfhfeircullteiveeslsasosfoAciPaFzeOdiwnitthhethpeerstsaornta-luspaomfptlheesse curingthatyear.
nTtasiknsdpieccaitfiivce omofneimtpolroinygedsaetxapaonsudrweiupnedmaorneitaoortipnrgedsaernateedxihsetr.e.HThoesewsatemhepslveedsaaesraearreen 0identifyareaswhereadditioualexposurecoamrolsmaybenecassary.
Engineeringcontrolstoreduceexposureconsisto thefollowing:
>Reactionsystems areclosedsystemswithcoatinuousambient moaitoringfor
2
>`Vmeonnloamteirocnosoycsetaetmrassairoenisnstalledw: hereairborneconceamrationsaresiguificant >Thepolymerdryersoperateunderaegacivepressureto coazainAPFOand
g2 g
other mamerials.
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>Recoverysystemsareiaplacetoreduce airborneemissions.
Personal grotecrive equipmetnhatt workers regularlywearconsistofthe following:
>>SaIfmpeerryvsihoouessgalnodvessidwehsehnibealnddslafienrgyAgPlaFsOsessoilauatliolnasroerasa.queousdispersion > Cphreomduicctas.lprotectivecoveralls andgoggtesor faceshieldswhenthepossibility >oAifrslpilnaesrheesspiorfatAoPrsFoOrccoanrtwaiidngienrgessopliurtaitoonrssiwshperreesemnotn.itoringbasshown to have high exposurepotential.
APtrioWrasmheiansgatroenmeWnotrskosf,bbilooooddfsleuroruimdelelveevlesloshfaAvPeFbeOebaavtaekbeenpenrmieoasrur1e9d8s1ibnuctear1e9o81f. lidiemnittiefdiveadlAuePiFnOasesxepsossiunrgeepxoptoesatuiraelttoheAP1F99O5., 1A9s89u-m9m0,ar1y9o85f,r3e0sdul1t9s8o4fevomlupntleoeryewietsh dsuarmipnlgitnhgiesvpeernisodiosfinttihmee,taballeybseilsoowf. rDeuadestoofsdiagcniafaircaendtifjfoibcualsts.iTghumeednatrmaionvtehmeetaatble bceolmopwaprrisioonrstoof1r9e9l3aatirveefolerveelmspolfoyAePeFsOinicnlbuldoeoddisnetrhuem19c9an5sbaemcpolmipnagrdeadt.aTshoetehnattire daa setofblood concentraistaivaoinlasble uponrequest.
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