Document ByQVvnEm93y6pRBxyXN4RJYb4

Waste Material Data Sheet no. 1 315Q7 fcj GENERAL INFORMATION ! CUSTOMER INF invoice Address Cert Address^ --GERALD L. PERRY ^ipinctnmar Mama PPG INDUSTRIES, INC. Arlrlraaa City Statn Phnno# USEPA ID# P.0. BOX 1000 LAKE CHARLES LOUISIANA 7ip 318-491-4370 LAD008086506 70602 N/AD SHIPPING FACILITY invoice Address] Cert Address N/AC Contact GINGER BUSBY ___________________ Facility Name. Address_____ City________ PPG INDUSTRIES, INC. P.0. BOX 1000 LAKE CHARLES State________ Phone#_____ USEPAID # . LOUISIANA 7ip 70602 318-491-4500 LAD008086506 Generator Name (it different). r'l-WASTE DESCRIPTION " NAME OF WASTE Classifier Sludge and Solids PROCESS GENERATING WASTE WTU Classifier GENERAL CHARACTERISTICS (at 70* F unless otherwise specified) COLOR Black UOUID 30 % FREE PHASES . ODOR Yea SOLID SINGLE LAYER NFPA HAZARD CODE HEALTH REACTIVE NONE Kl STRONG (3 SLUDGE 3 DOUBLE LAYER MILD POWDER MULTI-LAYER SPECIAL HANDUNG INSTRUCTIONS If special handling techniques are required, specify; Use ProPer protective equipment. Is a representative sample provided'' Yes No O Sample Purchase Order No. RCRA INFORMATION Is this a USEPA hazardous waste? X Please give USEPA hazardous waste codes: FQ24 ____ Mi D022 m SHIPPING INFORMATION DOT hazardous material PROPER SHIPPING NAME Waste Flammable liquid,n.o.s.* HAZMO CUSS in#UN1993 R/Q 1 lb. ANTICIPATED VOLUMEGAL. ________ YDS.. 100000 .LBS. D039 J2Q4P -BQ-29 ;ribe nature of reactivity if D003 waste: D009 ______DRUM(S). BULK X RAIL ONE TIME WK Type and size of container. WT PER CONTAINER____ MO fi YR 55 gallon drum 500 lbs X OTHER _ WT PER GALLON:_____________ 12 | bS SPECIFIC GRAVITY <0.8 0.8-1.0 n i n-i ? jr 1.2-1.4 1.4-1.7 a>1.7 n VISCOSITY (centipoiee) i-ioo n ii 100-1000 1000-10.000 >10.000 ASH<%WT) <0.1 0.1-1.0 1.0-5.0 nsn.9n n >20 TOTAL SUSPENDED SOLIDS (HWT) <0.5 05-2.0 n 2,,.,,0-5..0 5.0-20 S> 20 acajaJ PH <2 >12.5 1tl9.fi 6-8 n n.m mm, 10-12.5* OBSNkimt BTU's 1000/lbs. Jff<1 12-16 Kl-4 >16 nu 8-12 | FLASH P INT (closed cup) SULFUR (HWT) HALOGENS (H) METAL 3C TOTAL (PPM) EPA E P (mg/Li qcoooF a>200F <0 >5 100-140 F _________ 0.5-2.0 _____ 140-200 F 2-5 I kllMZARDOUS CHARACTERISTICS AND OTHER COMPONENTS ChlorfiiPd^luonne Bromine ^ Iodine. ^ Reactivity: C^fooe Exptoerve Pyrophoric Shock Sensitive Water Reactive Etioiogical Radioactive Acutely Hazardous Waste Areenic (As) Barium (Be) Cadmium (Cd). Chromium (Cr) Mercury (Hg) _ (Pb)-------- 114 23 44 Cyanides--LA*____ (ppm) PCB"* 50 Sulfides _ 11* (ppm) Phenolics LL-- (ppm) PemicirieaHD^ <P|trEB________ (ppm) VKSS&tfT Chromium-Hex (Cr+6) tfNnt- Toe t oii Selenium (Se)__ K Q-.3_(TCLP) CHEMICAL COMPOSITION (MUST TOTAL 100%) Wateri i2Q=5ft* Solids (carbon.i l5n25f% Chlorinated Hydrocarbon Mixture Ffhyl fhloride- -5=10% farhm Tgrra-HInr-iHe 0-1 i% Silver (Ag)______ ___________________ Copper (Cu) Nickel (Ni) _ toot Tested 110 FeCl-j.sand.etc)| ||% Chlorinated Hydrngrhnn ?f)wfin (mixture of C2-G^)i I1% ------------------------------- I I1% I I1% (Til nmfnrm Fthylene DirhlnriHe. Vinylidene rhlnriHc Trichloroethvlaie Perchloroethvlene -1=10% -1=5 1% 1=5 i% 10% I 10% Zinc (Zn)___ fclot Tested Thallium (Ti)__ -UQ- Other (Specify) I I1% .1 1% I HEREBY CERTIFV THAT AU. INFORMaWn SUSMlttED IN Thi6 AND au. attached documents is complete and accurate ano that all KNOWN on SUSPECTED HAZARDS HAVE been disclosed I1% I1% AUTHORBED SIGNATURE ENV.CTRL.SPEC. 4^3JL TTTLE PC / WSE ENSCO USE ONLY MMAECEHTOTCATION DATE SL 021438 From: American Laboratories and Research Services, Inc. P.0. BOX 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: February 6, 1991 To: Mr. Gerald L. Perry PPG Industries Chemicals Division p. o. Box 1000 Lake Charles, LA 70602 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I*D. AA07095 Sample location: 1002GP LabLog 1520 Classifier Solids collected by: GPP Collection date: 01/31/91 Time Laboratory submittal date: 01/31/91 Time: 15:57 Received by: RLH Validated by: RLH Parameter: TCLP Extraction Method reference: SW846-1311 Result: done Date started: 02/01/91 Time started: 16:00 Parameter: Mercury, TCLP Method reference: SW846-7470 Result: .009 mg/L Date started: 02/05/91 Time started: 08:30 Parameter: Mercury, Total Method reference: SW846-7470 Result: 1.25 mg/L Date started: 02/05/91 Time started: 08:30 Date finished: 02/02/9: Analyst: BLM MDL or sensitivity: .0 Date finished: 02/05/9 Analyst: BLM MDL or sensitivity: . c Dare finished: 02/05/: Analyst: BLM SL 021439 From: American Laboratories and Research Services, Inc. P.0. BOX 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: February 6, 1991 To: Mr. Gerald L. Perry PPG Industries Chemicals Division P. 0. Box 1000 Lake Charles, LA 70602 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA07095 Sample location: 1002GP LabLog 1520 Classifier Solids Collected by: GPP Collection date: 01/31/91 Time: 9:15 Laboratory submittal date: 01/31/91 Time: 15:57 Received by: RLH Validated by: RLH Parameter: TCLP Extraction Method reference: SW846-1311 Result: done Date started: 02/01/91 Time started: 16:00 Parameter: Mercury, TCLP Method reference: SW846-7470 Result: .009 mg/L Date started: 02/05/91 Time started: 08:30 Parameter: Mercury, Total Method reference: SW846-7470 Result: 1.25 mg/L Date started: 02/05/91 Time started: 08:30 Date finished: 02/02/91 Analyst: BLM MDL or sensitivity: .005 Date finished: 02/05/91 Analyst: BLM MDL or sensitivity: .005 Date finished: 02/05/91 Analyst: BLM Si 440 Mr. Gerald L. Perry Page: 2 February 6, 1991 Sample I.D. AAo/095 (continued) Comments: Refernece Lab Report No. R1905. If there are any questions regarding this data, please call. SL 02l4Al 501-863-7173 ^nv*rw*nvntai vomoariv .AN UAk * :7, iyyi ''TiRncan 0,: Roaa ^ Box i ,:>57 D-.raao -'-Kansas r* '3' -1957 p?o INDUSTRIES, .NC. r.TTN: ^ERALD CLARK r.'J. =UX 1000 _,AKE CHARLES po # --------------------DATE RECEIVED-- Oi/14/yi LA /ObOC ~nMPL: -LASSIFIER SLUDOE AND lULIdS wAMPLE a ls oouisy/ TESTS BTU/LB i CHLORIDE t SULFATE FLASH POINT F RESULTS 3 = < > l, S7b.OO Dii . 00 1.00 140.00 PACE X'*' E. A. REDEN TECHNICAL MANAGER . UF SL 2l442 Gary Prejean DATE: l/jjLiW Analysis of Waste Characterization Samples Sample ID: Sample Date : LAB LOG s 1031 ^ COMPOUND PCB1 PCB2 PCB3 PCB4 PCB5 PCB6 PCB7 PCB8 PCB9 PCB10 TOTAL: EPA ADJUSTED TAL ppm PCB's: Wt. PPM 3.27 0.00 0.00 0.00 0.00 0.00 0.00 0.00 U .00 0.00 3.27 Analytical Method: PPG Method LD-2571 CC: H. Hoenes G. Perry/J. Wyche C. Parnell ANALYST: Anne Corbello APPROVED BY: '/ ^7 v _/^ ^ / SL 021443 'nj = TP"tCM .M l . :DU37=I JtSr.A'i'"'p '- E E -HAL : L I E f*n SAMPLE: WT5001: i'S r ei I i G Lt ^4v'3i j " 3iu '*1(4 T_ i ** iL- .'aiu ' l " r i n ' :-c*i i '.`r '.oTM s :"2ne - ~ ` - n i i_j r~ rt1 e ii n i~ <3 z n I oroethane rcz-thene vtracri 1 uroethans -t'." t-.c h l oroc- " nans '"thane . : ~ oen t c-n<= ~ 3 " t'jne tt'jtaaietie-- l . 7 " ICi ILC'F: "SC 3 TCE PEF.CHLGR 'JNSVM. rM PENTA ---DC!? HEX A HCED .*v I ' \m' * ` Ct j * 00 i\ m 7; ^ o. 44 1* I1 V> Oo * .-o < c3~ 1 SL 021444 -ASTE ANALYSIS REPORT Environmental Laboratory PPG Industries, Inc.. Laxe Charles. La. Sample: Location of Sample: Cleanout of solids from Classifier Separator at WTU. 10 - 12 arums oeme fillea at South Classifier Sample Collector: G. Pre.iean Sample Method/Device: Random grao/ scoop Date of Sampling 9-20-89 Date All Analyses Completed: 10-2-89 Report Submitted By: Date: Gary Prejean 10-3-89 ANALYSIS RESULTS_________________________________________________________________________ _ ____________Lao Log Sample No 1031 Test Parameters 1it ability___ L Standard N/A 1 140 o c i ' N/A I nch/vr Reactivity ..^n/A___________________ As EP Ba Toxicity Cd (mg/L) Cr ( 4 N/A Pb Hst Se A* _ i). 2 50 max 5.0 max 100.0 max 1.0 max 5,0 max 5.0 max 0.2 max 1.0 max 5.0 max i ! j 1 j Other Parameters lif needed ) ( ) N/A ND/none detected i1 .j 1 CHLORINATED HYDROCARBONS ( %) l Chloroeth^pe l VC ) ! PCBs N . D . DO' Chloroetnane (EC) | 22.63 Dichiormethane (_MeC_12 I Heat 1922.2 1.1-Dichioroethene ( VDC ) Value BTU/ 1 1.l_-Dichloroe thane (DCE) 0.18 1.2-Dichloroethene l cis/trans) Chlorine 14.52 Trichloromethane LCHC13 ) 1.2-Dichioroethane LEDC) 0.24 Water 48.30 wt 1.1.1 -Trichlo_roe thane LMC) Tetrachloromethane LC.C1.4 ) Density 1.291 a/m Trichloroethene (Trichlor i 1.1.2-Trichloroethane (TCE.) 0.25 Ash 24.96 wt 1.1.1.2-Tetrachloroethane (unsvm > 0.32 1.1.2.2-Te_trachloroethane svm) 0.44 Sodium <0.02 wt Tetrachloroethene !Perchlori Pentachloroethane (Penta) 0.28 Hexachloroethane (Hexa). 0.14 Hexachlorobutadiene oara-Dichlorobenzene (RCBD) (P-DCB) 0.47 SL 021445 Unknown C1HC 0.2,1 1 1 iota! C1HC i%J)25.16 | .TEST. PROCEDURE >1 PARAMETER 11 Ignitability ^J/A | corrosivity ( pH ) N/A LAB LOG NO. 1031 METHOD USED Pensxv-Martens Closed Cup Tester ASTM Standard D-93-79 Setaflash CIosm Cup Tester ASTM Standard D-3278- 78 Other (Specl: 5W-846 Method 9040 pH measurement Other (Specl: Corrosivity linch/yr) -'n/a ____ National Association of Corrosion Engineers Standard TM-01-69 Other (Speci: Reactivity /A t One affirmative answer will classify waste reactive I 1. Normally unstable without detonating? 2. Reacts violently with water? Forms potentially explosive mixture with water.' Cyanide or suifiae oearing waste wnicn can generate toxi gases, vapor or fumes under pH conaitions Detween 2 ana 12.5? 5. Capable of detonation or explosive reaction if subjected strong initiating source or if heated under confinement? 6. Readily capable of detonation or explosive decomposition reaction at standard temperature and pressure? 7. Forbidden Class A, or Class B explosive as defined in 49CFR 173.51, 173.53, and/or 173.88? SW 84 6 ------------------- 1 SW 846 SW 846 Parameter Method Parameter Method Parameter Method EP Toxicity SW-846 As 7060 As 7761 /PCB LD-257 Method 1319 Ba 7080 C1HC 5030 wCIHC LD-25b ^N/A -Cd 7131 '^Sodium 3050 . bOlO Heat Value LD-256 Cr 7190 L/pH 9040 Chlorine LD-2 5 6 TCLP* -Pb 7420 yWater LD-256 "'N/A H* 7470 */Ash LD-2 5 b & 7740 *Toxicity Characteristic Leaching Procedure LABORATORY IDENTIFICATION Laboratory:___ EEfi lake Charleslast Parameters Analyzed and Date Analyst Is): A. Corbello PCB's 9-22-89 E. Hider Sodium 10-2-89 B. Martin CLHC, BTU, CL2, H20. Density, Ph. Ash 10-- Si 02^6 PPG 'AST" .^.ALISIS REPORT 'ircnmenLaj. ,dDora:crv '.r.austriss, 2r.c . . _j.tie "r.anes . _______ \mVi e : ft,:, : Sample: S a lit n 2 lassi: ier Siuage. A'TS-ao l Drums at HVSA. nmoie ,iec:cr: A'. 'ooper ampie Methoa/Device: P.anaom srao - tipper m-, Time oSampling i~'i-90 5 : at) am 2a:e Ail Analyses Completed: 9-^-90 Report Submitted Bv: Date: Gary Prejean 9-24-90 - A aLVS 15 RESULTS.,. -^=r Parameters :nitaoiiltv ' 'orrosivitv >./a 1 N/A. 1 sM______ i i nch/vr Standard 140F 2-12.5 0.250 max | 1 | Lab Log Sample Ap 1351 i \ .... 1- i. i -i - ; Ii 1 eact :viv* ^i i As ! 1.0 max ! ND i iI i -:l? img/L) N/A ! Ba Cd Cc_.,, EJ2 n& Se 4S 100.u max ... 1 0 max 5.0 max 5.0 max 0.2 max 1.0 max o.0 max 1.70 0.30 1.10 0.40 0.30 ND 0.02 ! i .. ! i I i .. _ . 1 i I .i i ! iI n i jjrtvju.nKoUiNo \ ~o I 'I Chloroetnene ihlorpetnane (vc; !ec: PCBs the :* arameters if neeaed Dicniormetnane 1. 1 -Dichloroetliene 1. 1-Dichioroethane 1.2-D.ichioroethene Trichloromethane 1.2-Dichloroethane 1.1.1-Trichloroethane Tetrachloromethane 1MeC12 ) ; vdc i LDCEJ I (cis/trans ) (CHC13) (fSEDcC1 ) (CCl4 ) 1 Heat Vai ..e Chlorine 1 Water .......... 1 Density / A Trichlor.oethene (Trichlorl 1 1.1.2-Trichloroethane (TCE ) l Tetrachlorethene (Perchior j 1.1.1.2-Tetracniorcethane unsvm) | Ash I iSodium i . none .el rC ~ ~Q 1.1,2.2-Tet racnioroethane Pentacnioroe thane aara-uichioroDenzene Rexacniqroetnane Eexacnio romi taa ione Unknown C1HC svm ) . Penta i (d-DCB! (HEXA) HCBD ' 1 i ct, 021447 1 onm i ETC / . b % wtX - */mi ^t5o -t% Total-^UiC lisDosai M tnoa Profile No ATS - 001 c o c -c n c c o ^ c n ^ c n s .s n s .s n s .s n s .s o s .s o s .s o s .s a s .s o s .s o s .s o s . Ji SGS*SGS*SGS*SGS*SGS*SGS*SGS*~~S*SGS*SGS*SGS*SGS*SGS*SGS*8G9aSG$*SGS*SG$*8GS*8G8*8GS*8GS ft SGS Environmental Lab ratories E9008-038 RESULTS - Sample ID*. 1251 Classifier Sludge SGS ID* E9008-38-17 TCLP Metals Date Extracted* 8/14/90 Date Analyzed* 8/17/90 Concentration in ppm (mg/L) in TCLP Extract C3 CO EPA HW CO w CO D004 CA to 0005 CA D006 > D007 a CO D008 CA D009 <3 CO D010 TCLP Metals Arsenic Barium Cadmium Chromium Lead Mercury Selenium (A D011 a <A Silver CA a CO Total petals Result ND 1.7 0.3 1.1 0.4 0.3 ND 0.02 Blapk ND ND ND ND ND ND ND ND Method Detection Limn-. 0.5* 0.02 0.03 0.04 0.1 0.0002 0.3 0.02 Date Analyzed* 8/20/90 Concentration in ppm (mg/Kg) in sample Antimony Arsenic Barium Beryllium Cadmium Chromium Lead Mercury Nickel Silver Thallium Result Blank Method Detection Limit * High MDL due to spectral interferences. ND denotes Not Detected at a level above the method detection limit. SL 021448 ^03*MiMO*iai*aMai*iaa*ia*as*tQMatiaaiai*iaiiai<Q*ioiaQSttaa*MitQ<iQij o) 8Q8 Environmental Laboratory C9008-038 RESULTS - TCLP TOIICITT VOLATILES SG8 IQ> S90O8-O38-17 PPG IDi 1351 Classifier Sludge Date Extractedt 8/27/90 Date Anaiyzedi 8/29/90 Concentration in ppb (ug/L) in TCLP Extract Method 1351 Cleeeifiier Detection ___ Slndfla____ _Limit Benzene 400 250 carbon Tetrachloride 2,150 250 Chlorobenxene 325 280 Chloroform 33,100 250 1,4-Dichlorobenxene ID 250 1,2*Dlehloroethane 13,000 250 1,l-Dichloroethylene 8,950 250 Methylethylketone 7,200 500 Tetrachloroethylene 0,550 250 Trichloroethylene 35,050 250 vinyl Chloride ID 500 TCLP Blink ID ID ID ID ID ID ID ID ID ID ID Blank Dataotlon Limit 5.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 5.0 5.0 10.0 Surrogate Standard Percent Recovery (at a.050 ao/Ll 1,2-Dichloroethane-d4 Toluene-dS 4-Broxofluorobenxene 1351 Clsaeitler flladot Mart SL 021449 8 XD den tee Sot Detected at a lev 1 above the a thod date tlon Halt. ><Vmbr of th* aoa Qreue i FiO0i0O>0O>0Oi<0OaiQ--fl--SOS--O8*SQf0QI ft MOKiaitMliMItiaMQIiMtHQttMliMlf SQt Eiwtrenmontol Uboratortoo RMBOLTS - TCLP TOIICITT 8MMXV0LATXLM8 89000-038 308 XOi 89008-038*17 PPG IDi 13S1 Claaaifiar Bludga Data Extractadi 8/31/90 Data Aaalycadt 9/08/90 Concantration In ppb (ug/L) in TCLP Extract o-eraaal a-craaol p-craool Craaol 1391 Claaaifiar Sludca XD MO MD XD Bl|pk XD MD MD ND Mathod Dataatian Llnit 10.0 10.0 10.0 10.0 2,4-Dlnitrotoluana XD XD 10.0 Haxaohlorobanxana XD MD 10.0 Haxachlorobtttadiana MD MD 10.0 Haxacbloroathana XD MD 10.0 Mltrobansana ND XD 10.0 Pantachlorophanol XD MD 50 pyridina MD MD 10.9 2 , 415-Trichlorophanol MD MD 50 2,4#6-Trichlorophanol XD MD 50 lat 0.200 aa/Ll 1381 Claaaifiar moat aionfr Z-fluorophanol Pbanol-dS 2,4,6-Trlbromopbenol Mltrobanaana-dl 2-Fluoreblphenyl Tarphanyl-dl4 10 % 19 14 % 25 % 17 1 48 % 17 % 18 % 32 % 33 \ 38 % 41 St 2KhSoqn ND danotaa 1 t Dataotad at a laval ab va tha nath d dataati n 11b i i i m 8 iooooo*oooooo % Waste Material Data Sheet CT GENERAL INFORMATION ENSCO CLIENT Invoice Address Cert Address N/AQ SHIPPING FACILITY No. ' Regional Office Invoice Address Cert Address N / A C .Contact. ^^^ustomer Name IK!":!*:: Address________ a::s: w.h. cooper too City____________ State Phone # 452 USEPA ID#___ Zip. .-4250 LAD008086506 |=| WASTE DESCRIPTION NAME OF WASTE PROCESS GENERATING WASTE Contact_____________ Facility Name Address_____ GINGER BUSBY City________ State_______ Phone# ___ 2ip_I^602_ -Li.- 4526. USEPA ID # I-!??:?:::?-: . y. ' r GENERAL CHARACTERISTICS (at 70s F unless otherwise specified) color Brown-BLack rli loum 99+ % phases Q NFPA HAZARD CODE Enclose copies of safety data ODOR yes SOLID% SINGLE LAYER sheets applicable to waste. Include NONE 5 STRONG SLUDGE% B DOUBLE LAYER data constituents of waste and MILDn POWDER % MULTI-LAYER materials used in process. a- SPECIAL HAHDUNG INSTRUCTIONS If special handling techniques are required, specify:. __________________ Use proper OSHA protective equipment HEALTH REACTIVE i RCRA INF RMATION V Is this a USEPA hazardous waste? -- Please give USEPA hazardous waste codes: Do not include state waste codes in this section. F024 D001 D019 D022 D029 D039 D040 Describe nature of reactivity if D003 waste: D043 b SHIPPING INFORMATION DOT hazardous material ePJiQEeasHiBeiNIGNAME Waste Flammable Liquid, n.o^s.. (Etr?^Lenei:"Ji(chloride, ethvl chloride)_______________ HAZARD CLASsflammable___,Q 4 TIN19Q3 r/q 1 lb. ANTICIPATED SHIPPlwWAfME _GAI ------ X----- DRUM(S), BULK % ' N TANK TRUCK ONETIME WK MO RJYR YDS. 'RAIL OTHER. LBS. Type and size of container___ SS gal rtmmc_____________ WT PER CONTAINER___ 60Q . WT PER GALLON: 12 lbs. SPECIFIC GRAVITY <0.8 0.8-1.0 1.0-1.2 1.2-1 4 Si.4-1.7 >1.7 1.39. actual VISCOSITY ASH (%WT) (centipoise) Si-ioo n 13_ ICtUBl 100-1000 1000-10,000 > 10,000 <0.1 0.1-1.0 1.0-5.0 n s n.7n n UNK _^ acrual >20 TOTAL SUSPENDED SOLIDS (%WT) <0.5 n os-do __. _. 2.0-5.0 5.0-20 0 > 20 itvk acwai <2 pop-R > 20 fi.n 6-8 na-io rrirmiiuwii 10-12.5 g] BTU'a 1000/lb. <1 012-16 1-4 D>16 4-6 6297 J4fe- -e actual 8-12 | FLASHPOINT (closed cup)| SULFUR (HWT) HALOGENS (%) ARE METAL OBJECTS <100 F >200" F g <0.5 >5 Qt 100-140 F 140 0.5-2.0 _____ 140-200 F *CIU*' 2-5 XT HAZARDOUS CHARACTERISTICS AND OTHER COMPONENTS Clorin45nl5ZFIuorine Bromine _Q__Iodine _Q PRESENT IN THE WASTE? YD MB IF YES. DESCRIBE IN SECITONI Reactivity: CZNone Explosive Pyrophoric Shock Sensitive Fuming/Smoking Waste Water Reactive Air Reactive Radioactive Biological Asbestos Cyanides------ 9------- (ppm) PCS'*-------19_______ (ppm) Acutely Hazardous Waste Sulfides___ 19_____ (ppm) Phenolics 9_______ (oom) Dioxins & Furans unknown r CHEMICAL COMPOSITION (If actual percentages are not known use ranges) Total should be at least 100% chlorinated water Actual __ ____% Range % hydrocarbon mixture------------- Solids __ ____% % rhlnrnefhane__ (carbons. etc.I % % chloroform Chlorinated Hvdrm<- ___ --____ % EDC I ^3carbons (mixtures % VDCM ...w - Ce 4-- -------- % ____ ____ % % Trichlor % Perchlor ____ ____% % TCE Actual % % % % % % % % ____ ____% % VC % ____ ____% % % i icheit centr that a HAIAADi HOICK T L leoataimi xwtrrB) t n ak> au arraoo DOOMarti cowun ate acowim no that au newt at Mrccrtc i or metal OAXcti as a coawnruetr or tw wwtl haw Range ----- ----- % 1 .--_5 % _1 -- _5 % l -_i_% _1_ - 5_% 1 - 5 QA. 0 -- 1 , -% H. COOPER ENV. CONTROL SPEC. 11-20-9 yt] METAL RTOTAL (PPM) DTCLP(mg/L) Antimony (Sb) < 30 Arsenic (As)__ <0.-1 Barium (Ba)___ 5.7 (TCLP) Beryllium (Be) <30 Cadmium (Cd) <1 Chromium (Cr) 132 Lead (Pb)____ 24 Mercury (Hg) .009(TCLP) Selenium (Se)... ^ 1__________ Silver (Ag) _ <5 Thallium (Th)__ ^ 20 Other (Specify) Zn 98 r.n 47 7 AH BWnkt Mutt Bt ComoMWd H mtUHal s/wt not nr--it inoictw "None --wi-n uSE ONLY SL 02145! From: American Laboratories and Research Services, Inc. P.0. BOX 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: February 6, 1991 To: Mr. Gerald L. Perry PPG Industries Chemicals Division P. 0. Box 1000 Lake Charles, LA 70602 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I*D. AA07095 Sample location: 1002GP LabLog 1520 Classifier Solids uoxlected by: GPP Collection date: 01/31/91 Time Laboratory submittal date: 01/31/91 Time: 15:57 Received by: RLH Validated by: RLH Parameter: TCLP Extraction Method reference: SW846-1311 Result: done Date started: 02/01/91 Time started: 16:00 Parameter: Mercury, TCLP Method reference: SW846-7470 Result: .009 mg/L Date started: 02/05/91 Time started: 08:30 Parameter: Mercury, Total Method reference: SW846-7470 Result: 1.25 mg/L Date started: 02/05/91 Time started: 08:30 Date finished: 02/02/9 Analyst: BLM MDL or sensitivity: .c Date finished: 02/05/s Analyst: BLM MDL or sensitivity: . Date finished: 02/05; Analyst: BLM SL 21452