Document BvQQeO11MjkBXQQZ1RD5Xra3X

A R -o l lo EnviroSystems Study Number 90171-3 RESOURCE ANALYSTS, INCORPORATED ENVIROSYSTEMS DIVISION PRODUCT REGISTRATION LABORATORY AQUATIC TOXICOLOGY STUDY PROTOCOL Static Acute Toxicity Test With FM 3820 And The Daphnid, Daphaia aagna Sponsor 3M Conpany PO Box 33428 St. Paul, Minnesota 55133 Sponsor Approval of Protocol f' Testing F acility EnviroSystens Division Resource Analysts, Inc. 1 Lafayette Road Hanpton, NH 03842 BEST COPY AVAILABLE Estimated Test Initiation Date: October, 1990 Estimated Test Completion Date: December, 1990 Study Director: Timothy J. Vard Study Director Approval of Protocol j l j Pte -//ft t h i s is a c e r t i f i e d Page 1 of 6 Ip i poe^b R eu u c* Analysts. V c . ScP*Sary 0MUPORE 001624 EnviroSysteas Study Number 90171-3 1.0 TITLE Static. Acute.. Toxicity Test With FH 3820 And The Daphnid, Dapbaia aagna 2.0 PURPOSE To determine the 24 hour and 48 hour Median effective concentrations (EC50s) of the test substance to the daphnid, when exposed for 48 hoars under static conditions. 3.0 TEST MATERIAL 3.1 The test substance and related stability and purity data will be supplied by the sponsor. Test Material will be stored at room teaperature in the original shipping container unless alternate storage conditions are reguested by the sponsor. Handling of the test Material trill be in accordance with inforaation contained in the sponsor-supplied Material Safety Data Sheet and RAI Standard Operating Procedure 01-02-1106. A subsanple of test substance (approxinately 1 gran) will be renoved fron the original container and transferred to a glass vial for archiving. All unused test substance will be returned to the sponsor. 3.2 Calculations are based on noainal concentrations of the test substance. Test substance stock solutions are prepared in deionized or dilution water without the use of a solvent (carrier) if possible. If a solvent is required, dinethylforaanide, triethylene glycol, or acetone will be used. The concentration of solvent will be liaited to 100 ag/L. 4.0 TEST SPECIES 4.1 The selection of test species is deterained by the sponsor. Healthy juveniles (free fron known diseases) fron a single source will be used to initiate the test. They will be obtained fron an in-house culture with a known history and will be less than 24 hours old at the initiation of the test. The vet weight of control organises will be deterained at the end of the test. 4.2 Identification of the test aniaals shall be verified using appropriate taxononic keys. 5.0 PRETEST OBSERVATIONS AND PROCEDURES 5.1 Pretest observation data concerning the source, handling procedures, receipt date, disease treataent (if any), health, feeding, and Mortality of test aniaals will be recorded and reported. 'SEST COPY AVAILABLE Page 2 of 6 Poxxjc Inc. Sutwcfi'-y of MXlFOPt 00162S EnviroSystens Study Number 90171-3 ` 5.2 Daphnids will be maintained under static or replacement conditions prior to test initiation in the sane water and at the sane photoperiod and tenperature that will be used for testing. The aniwals will be fed at least once daily with a Mixture of yeast, trout chow, and cerophyl and/or freshwater algae. Daphnid cultures will be waintained in dilution water at test conditions (tenperature, hirdness, and photoperiod) for at least 14 days prior to testing. 6.0 EXPOSURE CONDITIONS 6.1 The test will be conducted under static conditions, and test nedia will be supplied only at the beginning of the test. 6.2 Dilution water will be natural ground water. It will be free of Measurable concentrations of pesticides. Rater will be passed through a <20 micron filter and cheaically characterized (at least twice yearly analysis at R1I) prior to use. 6.3 Rater temperature will be 20 1C. 6.4 Dissolved oxygen concentration should be above 70% saturation, but aeration will not be utilized. 6.5 Photoperiod will be automatically controlled and adjusted to 16 hours light and 8 hours dark. 6.6 The test vessels will be 250 ml beakers of that contain 200 ml of test media. The loading rate will be less than 0.5 g/L. 7.0 STUDY CONDUCT 7.1 The results of a range finding investigation and/or previous testing data will be used to select the concentration range for the definitive test. If a range finding test is conducted animals will be exposed to a series of concentrations of test substance plus a control and a solvent control (if required). 7.2 During the definitive test the animals will be exposed for 48 hours to at least five concentrations of test substance plus a control (dilution water without test substance) and a solvent control (if necessary) under static conditions. Test concentrations will be chosen to bracket the anticipated EC50. 7.3 At least 20 animals will be exposed to each treatment. The animals will be exposed in groups of 5 animals per vessel (4 replicates per concentration), each containing 200 al of solution. The animals will be assigned to randomly positioned test vessels (a random numbers table will be used to choose the position of each test vessel), and they will not be fed. 7.4 Animals will be added to test media after test substance has been added and aeration will not be enployed. b t' f EnviroSystems Study Humber 90171-3 7.5 The highest tested concentration will be 1,000 mg/L. 7.6 A toxicity -test shall also be conducted with a reference toxicant and the batch of daphnids used for the test. 7.7 Dissolved oxygen concentration, pH, temperature, and conductivity will be measured and recorded at the beginning of the test and daily thereafter in all test vessels, as long as living aniaals are present in those vessels. 7.8 Mortality and sublethal effects (immobilization) will be recorded at 24 hour intervals during the test. Dead aniaals will be reaoved. 7.9 Data Analysis and Statistical Methods 7.9.1 The EC50 values and their 95% confidence intervals will be calculated using mortality and/or immobilization data by the binomial, moving average or probit methods. 8.0 QUALITY ASSURANCE AND QUALITY CONTROL 8.1 The test will be repeated if any of the following conditions occur: 8.1.1 Control survival at the end of the test is less than 90%, or more than 10% of the control daphnids are stressed or immobilized, or any control animals are trapped at the surface. 8.1.2 Temperatare in any test vessel is outside of the range of 19 - 21C. 8.2 The test will be conducted according to OECD Good Laboratory Practice Standards. 8.3 The test will be audited by the Quality Assurance Unit. 8.4 The Study Director will be responsible for reviewing all data and for recording any changes to procedures outlined in this protocol in a protocol amendment. Protocol amendments will be approved by tbe sponsor. 8.5 Original data will be archived at Resource Analysts Inc. for at least 10 years or it will be transferred to the sponsor for archiving. Page 4 of 6 EST COPY AVAILABLE Pesomce Analysts. Inc, Sutc*ar,,'d MUJPORE 001627 EnviroSystems Study Number 90171-3 9.0 REPORT 9.1 An original report will be prepared after review of a draft report by the -sponsor. The final report will be signed by the Study Director and staff that conducted the study and prepared the report, and by the Quality Assurance Unit Representative. 9.2 The final report will consist of at least the following information: 9.2.1 Title page, including the study title, data requirement. author, study completion date, testing facility, and sponsor. 9.2.2 Sponsor-supplied confidentiality claims. 9.2.3 Good Laboratory Practice Statement 9.2.4 Certification of Good Laboratory Practices. 9.2.5 Table of Contents. 9.2.6 Summary of test procedures and results. 9.2.7 Introduction. 9.2.8 Methods and Materials, including a description of test methods, organisms, dilution water, and statistical techniques. 9.2.9 Results, including all data from range-finding and definitive tests, and EC50 values. 9.2.10 References. 9.2.11 Appendices, including all water quality data. 10.0 REFERENCES OECD. 1984. OECD Guidelines for Testing of Chemicals. Section 2: Effects on Biotic Systems. Method 202, Daphnia sp.. Acute Immobilisation Test and Reproduction Test. Adopted 4 April 1984. U.S. EPA. 1986. 40 CFR Part 797. Toxic Substances Control Act Test Guidelines; Final Rules. Federal Register, Monday, January 6, 1986. Section 797.1300. U.S. EPA. 1987. 40 CFR Part 797. Toxic Substances Control Act Test Guidelines; Amendments. Federal Register, Wednesday, May 20, 1987. Section 797.1300. Page 5 of 6 Resuca Anotan,me. SubvctayocMUPORE 001628 EnviroSystems Study Number 90X71-3 ors o k m a r t test conditions Acceptable Species: Test Type: Test Duration: Flow Kate: Dilution Water: Age/Size of Test Organises: Acclimation Period: Temperature: Photoperiod: Light Intensity: Number of Concentrations: Dilution Factor: Nunber of Replicates: Number of Organisms/Replicate: Test Vessel Size: Test Vessel Volume: Solvent: Loading Rate: Feeding: Aeration: Effects Measured: Test Concentration Analysis: Water Quality Measurements: Acceptability Criteria: Dapbnia magna Static 48 Hours Rot Applicable Natural Ground Water Juveniles; Less Than 24 Hours Old Continuous 20 1C 16 Hours Light/8 Hours Dark Ambient Laboratory Lighting 5 or More; less than 1,000 mg/L Si.6 4 or More 5 250 ml or larger 200 ml or more Dimethylformamide, Acetone, or Triethylene Glycol. Less than or equal to 100 mg/L <0.5 g/L Rone During Exposure Rone Death; Immobilization Rone DO, pH, Temperature and Conductivity at 0, 24, and 48 Hours 10% Control Mortality, Stress, or Immobilization Acceptable Teaperature Range BEST COPY AVAILABLE Page 6 of 6 ResolveAnaiysfi.me.SubscSatyofMUJPOfii 001629 - T COPY AVAILABLE PRODUCT REGISTRATIOR LABORATORY SAMPLE RECEIVING LOG RAI Samnle Number Sponsor Name and Address >i J - 1eJa U * J - j r - S . * i 3 S j s L A/c. <f-- P * j l 1I Sponsor Saaple Identification . / V A/_____ f i S / O i ___________________ H ^ 3X30 Sample Container Label Data U m H -t F/viJXXo 7. Method of Shipment Shipped From Via 'S* . PftjI f^cJ-xr bJ c<- 8. Description of Shipping Container(s) (Number, Type, Size) 1 PU* H e V 9. Description of Sample Containers(s) (Number, Type, Size) 1 JLSO **. ^(ass b o ff-U . 10. Sample Storage Location and Required Storage Conditions )2ts**4*~p 11. Signature 'I C + i J i J d U l ___________________ Date I I - I L - 0 _______ 12. Notes 2.-5-V> 13. Date and Location of Archive Sample Removal and Storage Location ___________ )l7fc?o f t ? - r __________ ___________________________ HiS Ka CERTIFIED TRUE COPY. SIGNATURES DATE &i* 0 Oeiouce A n e w , m e. SuOujcn/ ct vn^PG' 001630 q o m -3 PRODUCT RSGXSTKA7XOK LABORATORY TEST SUBSTAXCE USAGE LOG RAI SAMPLE HUMBER TEST SUBSTAMCE IL L WEIGHTS U S MEASURED I> CRAMS DATE M '/M o Z H ITIA L CROSS WEICHT HS3.J * S/X-0at J rn Wo ELIGHcrToss ARMEMOOUVKETD D ISPO SITIO '/S X .l hO ^ tc U lv f is-*? J2- w z /-<> 4<>'7/-3_____ TrmR sl! ICSAOCPYERHF ED SJGi VTURE3ta. _DA75J|2Lfl3<ii BT f> * cT5 S ') X Saaple Description:_____ p<f. It& Jl d. Container Label Information: ______ H~ j t W ' t _______" t t > 0 Date Keceived: Date Of Return To _____________ Sponsor: BEST COPY AVAILABLE O*iou>c* Ancv.ri. m e. SuO K oy of MUiBO 001631 THIS IS ACERTIFIED TRUE COPY. SIGNATURESJrV--D A T E ' PRODUCT REGISTRATION LABORATORY ORGANISM ACCLIMATION LOG Species:. Day of Month f l l A a A J L - _____________ Lot No. / h Z S 9 t i l _____________ " -fi/SOU JdC * 1 0 7 4 6 / Nunber of Dead Food Feeding Fre quency c D.O. Sal. (ag/L) (ppt) Notes By/Date 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 o IX */? ua 29 30 O D V$ i% 3 .! tM i t . rT.f ^ _ A 31 L / es Ca CJ -'Io BEST COPY AVAILABLE PROCUREMENT DATA: Ag_e____.__l_*_/_h_r_. Con.di-t.ion a<9 W Pate n fsL g f o Source, Collection and/or Transportation Method j rt*jL*~A-L utfrLXXoD- JAsrnL. A tr . Number Procured: ___________ Motes I V U J t t ' i r x . Ct*o-a < ^n HATER QUALITY: D.O. pH Temp. Salinity Conductivity g/L ___ C ppt unho/cn At S h i p p i n g : _ .......................... ...... ............................ At Arrival: _________________________________ ACCLIMATION DATA:Vater Source n a S l / j a J c p v u j j j u ) hH j , U o ^ / 9 6 / X A f i ~ _____________________ Food and Lot * ) .. . `- i <w- j* rv l ^ ' avrarcavt? if-.s,gasmv<<aaujPOBE Note: Include any observation of drisease or abnornal behavior. Use additional sheets if necessary. 0016,, 3,, 2,, BBTCOPYAVM IE PRODUCT REGISTRATION LABORATORY ORGANISM ACCLIXATION LOG Specie: Day of Month _ Nunber of Dead Food 116*746_____________ Lot Ho. //J 2 & 4 6 I ____________ -/yf^C l i t / Feeding Fre quency C D.O. Sal. (ag/L) Cppt) Notes By/Date 1 jr^ /V XW 2A /X. f i r J>j> 3 a ij. r tf' --- t i e 4 0 j3. IX. S b .x do- e j U .-/-10 e t 0 .-3.-^ . S t /M-M e - t a-*-* 5 6 7 % n Jo K JXL. /* r t f iM Kr 7<J<> "___ k/ A - e t tt-L -ti (Vm lL7-T(6> 8n lx *1 tJ* {9 hr 3J-0 - fJA `p i t la-fYo 'pic**# 10 o uA 1* it* 11 A ft /> 12 fife lx. A j U ^ -- JtJrf k t a-*-Ik es P 1 la-ia-to 413 a 0*3 lx ___ rig 14 A lx a/J 15 f) u 7 Sr 2ft.^ ________ A)A- /a-n-to C /2-W^Ta 3riM/L-/y,?< 16 o 'M Kr M tfuilZ/C .qo 17 t> tf;-V iy ^___ U / `e t a-iT-e d18 A 19 IV ____ ^ iiO M0&/%>*9nTHi *i 20 21 7 NS is a rcRTmi n 22 7 lue n n p v 23 S GNAT! ine o l . 24 DATE-liguf, ' 25 26 27 28 29 30 31 * -fjSJJSrfiJUud PROCUREMENT DATA: Age__________ Condition_______________ Date. Source, Collection and/or Transportation Method:___________ Nunber Procured: Notes: WATER QUALITY: At Shipping: At Arrival: D.O. no/L pH Teap. C Salinity out Conductivity uaho/ca ACCLIMATION DATA:Vater Source Food and Lot Note: Include an/ observation of disease or additional sheets if necessary. abnoraal behavior. -- ^ o^toiy/itmiipnot Use 001633 fe. Li. ESr COPY AVAILABLE Resource Analyst, Inc./ EnviroSystens Division Product Registration Laboratory Raw Data Study Number Qu i T I - ^ Sample Number Test Substance f 'TM - S x . o Test Type: screen / definitive TEST CONDITIONiSs ojsjiiDate _____ Test Organism ~D . Recorded By maLot Number n f f r i 0 Test Duration 4K h fr Dilution Hater S V zfk A tS rio Rate Salinity/ Hardness J ti' U h ( L . </$Z>/XCjfJL Age and Size of Test O`rgaanniissmes ` -3*4 ________ JTest Organism Abnormalitiies. Illness. or Injuries: none* J _ some (note)___ Acclimation Period (length at test initiation in days) tSA_____________ <0 Temperature -- /_______________ Incubator Number / J - ______________ Photoperiod: time o n P h t/fi time off Light Intensity -G> uEin 15 Kinute Transition Period: Tes ____ No i X Number of Concentrations 'T - r / > s x . 'f v L --------------------- Dilution Pactor ^ A ___________________________ ________ _ Number of Replicates L______________ __ _______________________ Number of Organisms per Replicate K ' ____________________ Test Vessel Size (L) . ________ Test Solution Volume (L) . XQ G Test Solution Depth (cm). Solvent and Solvent Concentration eh o/i/* Loading Rate /*>= -- 5 ^ y z Feeding Dissolved Oxygen Levels > l&'J* Effect (s) Measured jlM s#].* Test Concentration Analysis /m O t* Vater Quality Measurements 7 ^7 / / } # *.--S`t fUp n'w j jj tf* LJvg.'vt nr.sjeic-c* ii .wiimb f c t u e u M <u> x l i { * t EST COPY AVAILABLE onte X a t l/iU, Ine./ XaYiroSjstexz Siriiiea P r o d a e t Xag l s t r a t l o a U i o c a t o i j Xt* fiata Study XuaBr ___________ S s s r flm X<wl*r _ A r * ft-& .6 Test Suiituei f'G -ZA 4 ______ _ Test Tn*: * cre a d cfiaitiT * STOCX SOLCTIOX JXXPiXJlTIOif Perceat. actir iagredicat {% XI) J/ *fo Xoaioal Conceatratioa* corzeeted for % XX ? Tc* _ .no Balaaeed TXsed for Stoci Solution Preparatloa Pd-L -/____ L A hA & ^ / T ifil e . . / / j ^ d _ t)tUL tira to ti' UC& H Asi&nJ' u fi -fa /te O /ii uJL .r td iiS l jn l- J A j ,, ., i c W M j -- Z tjL --_________________________________ :_______________________ Y : fr .Q .L o d ili_______ ^ f s fr A p - k J A * i u f & h lM - / A Ck w o v o k \ x . S u e v c c r, a i K J t ' 001635 8EST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystems Division Product Registration Laboratory Raw Data Study Number 3 _________ Sample Number _________ Test Substance / V # ^fjU)______ Test Type: screen x / definitive GENERAL INFORMATION 001G36 SEST COPY AVAILABLE Study Wunber ..H h n ' J -- ------ aSaepple lluaber _52fe^/Z-- ---.--.-- -- Test Substance rcfn . f j ----- . TTeest Type- screen definitive -- DAPHHID SOLUBILITY Initiation Date ,,.S'ffiii. Test Organisa m y tb - Test Vessel I.D. Insoluble Raterial 0 hr 24 hr 48 hr Control I0 L0 00 0 0 5 0b S' . 0 - 0 0 o 0 Recorded by \q*J> fa (W Date: fe* / fr itti. UO ia If no insoluble Material is observed enter a zero in the appropriate box. If insoluble eaterial is observed enter a check nark in the appropriate box and describe the observation below. Notes: ----------------------------- - -------------------- 001L37 r$T COPY AVAILABLE Study Number RawResource Analysts, Inc./ EnviroSyste's Division Product Registration Laboratory Data 3________ Sample Number __________ Test Substance / y y ______ Test Type: screen j d e f i n i t i v e DAPHNID SURVIVAL AND SUBLETHAL EFFECTS Page 1 of 2 Initiation Date . 1 2 - 5 % ) _ Test Organism T> rh O jA M -^ Test Vessel I.D. Number of Live Daphnids Rep. 0 hr 24 hr 48 hr Sublethal effects 0 hr 24 hr 48 hr 1 *f 5 r n _ O 0 052 i T o _ O 1 / ( 2 5 DO o Qt f o A 3 i $ ! Xy 1 ?j... 2 ?1 ?2 ? ?2 1 2 I 1 9* LL_ S' 00 n yf O Hs 9*> $ r Oo 0 3S ' 5 -- 3o S' 40^ J? 0o 6 _-- i,-- - // / / X// / / Recorded by: Date: e*i /a-fc-Y P K . <f5 \ e* ili? If no subletha! effects are observed enter zero in the appropriate box. If sublethal . effects are observed enter the number effected in the appropriate box and describe the observation belo". fit a-7-fo jlUIillJ kt_ _ _ _ _ _fc Ano.s'v tec xav cf MtUJPORE 001638 Resource Analysts, Ine./ EnviroSystens Division Product Registration Laboratory Ra Data Study Humber Test Substance ^ ________ Sa*ple Quaker *3Jr4l*fc_________ ______ \STest Type: screen definitive _ DAPHNID DISSOLVED OXYGER COHCEMTRATION AND pH Rage 1 of 2 Initiation Date 12. * $ * ^ 0 ______ test Organisa ~ f . f A G x f l s Test I.D. Rep. Dissolved Oxygen (sg/L) 0 hr 24 hr 48 hr 0 hr pH 24 hr 48 hr Control 1 - .... J 1 2 1 2 1 2 1 2 1 *3 r1 2 1 12 Recorded by: Date: V nm X y 77 77 77 77 n m l-ic Up 7 3" 7 - S' fa fa 8 / 8 'le ft. ?x f-5- 7 . 0 ?. tf.? 83 83 r-C t r 1-0 fr ^.3- fa fa M 83 8 .3 83 83 83 8f 83 83 83 8q U fr-G f . r T-o 8 3 ? f ?.of i r fa / / '/ y /^ / 83 ? ..3 8 -5 83 r-t / '/ / fC b i/tfi P* *71 e-> b -5 * & U-7-fo 001639 BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystens Division Product Registration Laboratory Rav Data Study Muaber /jf/'f/' 3 Sanple Number Test Substance p/K, tfoJ) Test Type: screen 1/ definitive __ DAPHNID TEMPERATURE AMD CONDUCTIVITY Initiation Date IM * h > Test Organisa Page 1 of 2 'P.niUfAJf Test Vessel I.D. Rep. Temperature (C) Conductivity (uahos/ca) 0 hr 24 hr 48 br 0 br 24 br 48 br Control 1 2 1 / 2 1 JL 2 1 32 1 lL 2 7 s1 2 _1 s' 2 Recorded by: Date: 2G.1 ^6n ^ 00 ao-7 J.K JO'1 M / / /** /f-i- H 17-9 >?'5 |<r-7 /4 k > / O G t i f j4 * 0 /ltd . 2fid f3 > /3 j Oo oo lit \^ro l% 0-0 19-1? w.t /3 r d /3 i> /z * /2 * P B 0 30-X l U a o .lL lt-7 /Z t> /3 3 /3 fd j3 * b \?O I3J0 <2e ir Jo-<+ >c3.C >4-1 j3& /3 f /3 * d /3 * BOO CdO d o -? 3.O ft.) f t i ) /3 * /f * /3a Bao B0 y yy / / / / / / / 5 f * ??> &> jt u - - v * /2 < r* o V 7 - t Motes: Instrument Number: 5. PjuShtd./ l U U t fiCL - f Resource AroMfi. Inc. Sub*d--.y c*<*UJPOP 001640 BEST COPY AVAILABLE BESTiOPY AVAILABLE Resource Analysts, Inc./ EnviroSystems Division Product Registration Laboratory Raw Data Study Number 373^ Idt. ** Tent Substance I Sample lumber Test Type: screen definitive TEST CONDITIONS Date } ' ( Y * Q Test Organism ~T) 'W h r.Test Duration __ Dilution Water ____ Recorded By < ^ J n jU A c i~ ._ & /F96LLot Number _ _ Flow Rate C lfa fa Q s Salinity/ ,, Hardness J t o p &< * ^ 1 , Age and Size of Test Organisms _______ _________________ Test Organism Abnormalities, Illness, or Injuries: none ' / some (note). Acclimation Period (length at test initiation in days) i J A ___________ Temperature <2a ~ /______________ Incubator lumber 3-*____________ Photoperiod: tine on 6lfCfi time o f f Light Intensity 2^> uEin 15 Hinute Transition Period: Yes ____ lo Number of Concentrations _____ ___________________ Dilution Factor __________ _________ Number of Replicates Number of Organisms per Replicate 3 ______ _ ___________________ Test Vessel Size (L) > J < Test Solution Volume ( L ) _ i__ Test Solution Depth (cm). Solvent and Solvent Concentration /U0 Loading Rate ______ Feeding Dissolved Oxygen Levels > Yp ^ .SA & i-. Effect(s) Measured d a 't //H /H b th ' z d & S X ^ Test Concentration Analysis J U f t ___________ _____ Water Quality Measurements & dIvC.tMa Uu".^Jc-r r 'fO 2/v 3EST COPY AVAILABLE Resource Analysts, Inc./ KnviroSysteas Division Product Registration Laboratory Raw Data Study Nunbar ____________ Sample Rusher___ Test Substance ^ ^ ^ %7o/ Test Type: jcreei^_ definitive ^ RAMDOXIZATIOM IHFORKATIOM Initiation Date- ^ Test Organisa . Test Tessei I.D. Vessel Vessel Rep. Loca Rep. Loca tion tion 1 O tfii l 2 1 f2 1 JL 2 1 J2 1 A 72 1 fi 2 3M fie 4 3 u 3? 4 /? H3 /3 4 /V J- 3 3 4 to ? Jj 3 H4 -> 0 3 1 /? 4 'l s' 2 Recorded by: y / 3y 4/ Date: to v tlo Random Members* 8875S 35661 26335 626 954 83746 27998 82685 18386 18446 66027 5140) 27045 13094 92382 16215 09342 38148 23689 25407 25349 02322 15072 27002 66181 09779 10791 74833 17583 45601 60683 29956 91713 66^> 42832 3771 7470> 98896 47694 42562 3<g3 13862 13141 83052 75177 96779 62626 17725 62518 50809 14528 79oS> @97 37726 69456 77491 33261 31036 83316 01822 07706 55767 24038 46977 33112 81169 84235 33843 dfo 48J5> 56527 j|763 Qm 43 634q 2) 74625 <88 31842 47398 54309 73159 14Rg? 17752 49326 64727 03509 72382 73099 19693 56095 99219 85278 40386 45537 87481 31312 83701 39325 65995 18877 75296 * Draw a circle around the section of the randoa numbers table that is used to position the test vessels. Table of random numbers is from Steel,R.G.D and J.H.Torrie. (I960). Principles and Procedures of Statistics. McGraw-Hill Book Co. Mew York. Page 428. PMouceAncSywi.me.Sudkcoy d MlUfORE ui&wJL pJ ifafct 'PST CflPy AVAILABLE Xesource Analysts, Znc./ EnviroSystens Division Product Xegistration Laboratory Xav Data Study Number _ Test Substance /C+- / H i / Saaple Dumber Test Type: screen __ definitive stock solution pxepaxation Percent active ingredient i \ All //*t) *7o Noninal Concentrations corrected for % AI ? yes j / _ no Balanced Used for Stock Solution Preparation I_______ Preparation Botes: , / H )/x fj/ *-h>ab. a jL / xxu >L*. i o y. SS W /iMj LcL u zt, Ato-eJt: h SAH> sx-Ad o-cJ/iL____ /tid iA m r . * aT j , - fi& itL ta u W a ^a L < A & t M. W ? W i _______/a/s 3/xik h u m a i t uf) A> ^ j/ ____ _____________________ l _ ____________________________________ _ ___ L _____________________ - . * ______________________________ 5~_____________________ /_____________________________________________ /o _____________________ 2. _ ___________________ 5 001644 S Tm m iu B iE Resource JLnalysts, Ine./ ZnvlroSystens Division Product Registration Laboratory X** Bata Study Runber .57V)__________ Test Substanca _ __J_t_._f_t______/_ Supla Runber Test Type: screen_ definitive t// GENERAL. ZBTOmTZOR Rotes; ** T /j X /* a & tu z l* titu / o i t e t i d y j ____ ___- ^ fk & a u itb a , L M ^ ~ & 4 j U J /LLU > O ^ J iA a J b d P l - / j . _____________ g-s a <}*-<*. Q W u jlttf < ftfo l JL, 4 _____ ---- f a t r f __________ " -9& 7 A J lif rri,** , j n s i U s < ? A /n J LJM 1 S JL xA/do^Ji u jjJ L y EnvoSy*mi.I*..StXVCoy d MllUPC* 001645 ST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystess Division Product Registration Laboratory Raw Data Study Kunber S 'i) 5 ____________ Sample Number /C a Test Substance ____________________ .* Test Type: screen __ definitive Jtjf DAFBNID SOLUBILITY Initiation Date ' / & - 't? 0 Test Organism Test Vessel I.D. tetnf Insoluble Material 0 hr 24 hr 48 hr 0 0 D / 00 JL 0 3 00 s 00 r D0 /X Recorded by / Date: ii'lf-i 0 0 & If no insoluble material is observed enter a zero in the appropriate box. If insoluble material is observed enter a check nark in the appropriate box and describe the observation below. Notes: ---------------------------- 1 ------- -- -------------- :----------- 'FST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystems Division Product Registration Laboratory Saw Data Study Number _______ / C V /**?**> t Test Substance Sample Humber l)lV Test Type: screen __ definitive t / DAPHNID SURVIVAL AND STJBLETHAL EFFECTS Page 1 of 2 Initiation Date *7)./TUtAt--~/ ? ' 4 b ______ Test Organism Test I.D. `( f r r h t ( Rep. 1 2 3 4 1 2 3 4 Humber of Live Daphnids 0 hr 24 hr 48 hr 5 5 *r 5- 5 " *? 55 S ' V* 5*7 y 5* .5" 1 ? .r X 2 5- S f 5 53 ? 5 5* 4 jT 1 7 3 25 i- / s s' 53 6 4 ? r s Recorded by: Date: c f^ nm 5 Sublethal effects 0 hr 24 hr 48 hr 0O O 5 O <D O 0d c; 0 0 / 0 cl o G 0 0 0 00 00 U -L . >2-- o - tfw t-i /a--*-* P jjJ J L tM lf- ' j U J l / i f t t / B e W c e AnoN . SutAc-av o>MUPCOE 001647 BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystems Division Product Registration Laboratory Raw Data Study Number 5 7 ) ^ ______________ Sample Number ________ Jirc -tc Test Substance ____________________ Test Type: screen __ udefinitive DAPHNID SURVIVAL AND SUBLETHAL EFFECTS Page 2 of 2 If no subletbal effects are observed enter zero in tbe appropriate box. If sublethal effects are observed enter the number effected in the appropriate box and describe the observation below. Notes : n i t i - n -Gi j/r/nd'b/t t t c f ' ____________________ _____________ Ro>ce Anohin. Inc. S' s d o v c( MUJFORE 001G48 BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystess Division Product Registration Laboratory Raw Data Study Nuaber '-S**')*) /ct t* t Test Substance ___________ Saaple Nuaber Test Type: screen ydefinitive DAPHNID DISSOLVED OXYGEN CONCENTRATION AND pH Page 1 of 2 Initiation Date- _____ Test Organisa X /X0.4ASU TVeesstsel I.D. Rep. 1 2 fry^ 3 4 1 2 /3 4 1 2- 2 3 4 1 2 3 3 4 Recorded by: Date: Dissolved Oxygen (ag/L) _____ __________ 0 hr 24 hr 48 hr 0 hr 24 hr 48 hr sr- V? VI S-5 -0 t o 1? iT* %*> u 4 l i %b %-*> -0 t-h if-4 1-1 T'i 85 KL t* 1-7 T ? Tl i A V -7 KL- T? ?-3 3 "IP ** Vb Z-5 r-s 5 IX Sf) m -4? 9 V-.JL i i -l J y-H V ? f a H T-'/ V SB **> r o 1.1 T-o V i a %5 n a Zb 5 TO VK VJ i i t i Vfk-J 9*-' Qko 1\J 9 vj UR'% ix-m ntilo nr<-io iXfffiO lll buluw l f(U Oesouice ApoivjH v e . S te ic o v cf MUJPOR 001649 i, BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystees Division Product Registration Laboratory Raw Data Study Hueber J S V ? _______________ Sanple Number _____________________ tC -C /r t Test Substance ____________________ Test Type: screen __ definitive - DAPHNID DISSOLVED 0Z7CEN CONCENTRATION AND pH Page 2 of 2 InitiationDte^ ^ L ^ / ^ ? 0 ^ ^ ^ ^Tes^Organise^ ^ - ^ ^ ^ ^ ^ Test I.D. Rep. Dissolvi d Oxygen (ng/L) P A L -3 __________ 0 hr 24 hr 48 hr 0 hr 24 hr 48 hr d n ... r / / / / Recorded by: Date: 1 * 2 tx 3 fa 4 1 2... 3 n 4 TO 1 2 3 4 9^ m io in V r-3 Ta aroT b - fr-3 5 7 % -h fa T x-x o jk J iW ft M -t V m Ti ni 71777171 Qkj am S$ T 2, S T3 T* W Y -5 t-i T 5 ? r-5 ? * > y ic s M it Notes: /w / /- ^ Rmcuce Aoaiyjfi * < . SuOsOiaiy ct MIUFOPE 001650 BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSysteas Division Product Registration Laboratory Raw Data Study Nuaber J 5 D 5 Ait l2tf4o/ Test Substance Sa*pie Nuaber Test Type: screen definitive i S DAPHHID TEMPERATURE AND CONDUCTIVITY Page X of 2 Initiation Date / 2 S ' ^ _______ Test Organisa 2 > : fiM jffi-H . Test I.D. Rep. Teaperature (C) Conductivity (uahos/ca) 0 hr 24 hr 48 hr 0 hr 24 hr 48 hr 1 2 C ftihA 3 4 1 i 2-, 3 4 X a2 3 4 X 32 3 4 Recorded by: Date: 20 M zo-^r 209 J .f J .f ll u^o lio 13 0 0 'io o Il O fr i 0-9 ap Jon 0-9 o .9 AM xnfl Jo-*r M Tox 20A M 69 2% W.f o .f J o .f **>g J o .% o2C J .i Joj J? |XOO O ifoli ( * 0 O IM m m ioo tip tico m m m> H)c) li O IXCD \iD nao 1100 H fiO W jo ano lA D liDD fo 4/10 m dn ff otf % LM9d Mf JD D c. JiJ ~0 X f 20-K oJ O * C .^ IXfto. t r o 11(0 00 lino l \X L %iJLfl e*> (W o <'3c-*tc U-Kv U M m llo o 0K'j ll D < n Cfit-X vm> 5 R e ix jc e A n y tfi f<f.SjCh-Cio v o MaUPOG 001651 EST COPTAVAIIABIE Resource Analysts, Inc./ EnviroSysteas Division Product Registration Laboratory Ra Data Study Nuaber S D 5 ______________ Saaple Huaher pAr Test Substance f2JS7f Test Type: screen __ definitive ^ DAPHNID TEMPERATORR AMD COUDOCTIVITT Page 2 of 2 Initiation Data ^ "1 ______ Test Organisa 2 L 'XAA/-J*. Test Teaperature (C) Conductivity (uahos/ca) I.D. 0hr 24 hr 48 hr 0 hr 24 hr 48 hr 1 2 H3 4 I .. 2 *3 4 /1 /2 3 / / 4 Recorded by: Date: PiP -l? Jol M M-K At m .an.1 m Jn. 1 6 ao.y 1(1-1 J o L InK 0-7 JM 21.0 0-S <0.1 w u>.i 3 $ !\ 0.1 Uno 1360 a IAfD Ilo iVr ito \lO liflD cp \%p lim l^(7D \ico ito? lW> (IfD l^iO &> I W a l i&J 0 { j 7 ^ G<> ii-m > M b <VL/ C/fas 9 ^ i m o tx fiw l-k-lu Notes: ---------------------- -------------------- Desoixce Andy*, me. SutxOcry d MUJPOff 001652 OPY AVAILABLE Resource Analysts, Inc./ EnviroSystens Division Product Registration Laboratory Rav Data I HARDNESS DETERHIHATIOK Date Water type al EDTA titrant ng CaCOe equivalent to 1.00 EDTA nls saaple - Hardness ag/1 as CaCCh B BEST COPY AVAILABLE Xesource Analysts, Zac./ EnviroSysteas Division Product Xegistratioa laboratory Xa* Data Study Nunhcr ________ Test Substance ^ccir Saaple Euaber f^P> Test type: screen_ definitive l/ BKXOX CODED 1. Misspelled 2. Mathematical Error 3. Prong Entry 4. Transposition or Sequencing Error (inverted or vrong order) 5. Transcription Change (copy error) 6. Procedural Change 7. Prong Conclusion X. Illegible Entry 9. Unnecessary Entry 10. Footnoted Explanation 11. Additional Consent 001654 I BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystems Division Product Registration Laboratory Raw Data Study Nunber q n n i - 3 Test Substance 0- Sample Xunber 2 ( J i L ( T Test Type: screen __ definitive TEST CONDITIONS Date /3 Recorded y f Test Organisa A - Lot Number SA/ / _________ Test Duration A f< _____ Tlow Rate Dilution Rater g g i l u ^ _ Hardness .HaQ'ftQ`y k M W .Age and Size of Test Organisms Test Organism Abnormalities, Illness, or Injuries: w o / ' some (note). Acclimation Period (length at test initiation in d a y s ) _ / M ____________ Temperature ____ Incubator Number I'Z-_______ Photoperiod: time oiCtfcCO time off Z-ZOD Light Intensity Z Ji uEin 15 Minute Transition Period: Yes ____ No Dilution Factor Number of Renlicates 5Number of Organisms per Replicate -2STest Vessel Size (L) T A st S o l u t i o n Volume (L) > 2 0 Test Solution Depth (cm) (p OASolvent and Solvent Concentration Loading Rate Feeding ____ *L" UO--'W^Hh* tifiT 'fe fv Dissolved Oxygen Levels y l h \ ( i o / i l Effect(s) Measured /jpgUi Tljh )jf Kill Test Concentration Analysis oft _______ M rr k /n/m>i eaM^K. Vater Quality Measurements IV`XWVg'iT<kr|l{Id<yuuOLuJ1-.V*uArl,*Chl41 BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystems Division Product Registration Laboratory Raw Data Study Dumber *%)/ 7 / - 3 _________ Sample Dumber __________ L. Test Substance r /X . ______ Test Type: screes __ definitive XADDOHIZATIOR IDFORKATIOD Initiation D a t e __ _____________ Test Organism ~I)- Test Tessei I.Q. Tessei Tessei Rep. Loca Rep. Loca tion tion 1 mini 2 1 f2 & > /u n 1. 3- o l 2 / 1 /s J2 3 1 lx . 'i 2 x f 513 2 A3 1 y y 2 y Recorded by: Date: 3 / 4 '7 3 /y 4H 3 ? 41 3 n 4 t 3 3JX 4 <z 3 4 b 3/ 4/ es b 'tt't Random Dumbers* S8758 35661 26335 60826 95044 83746 27998 82685 18386 21717 18446 66027 514g>> 2-KH5 13094 92382 16215 09342 38148 23689 25407 25349 02322 15072 27002 66181 09779 10791 74833 17583 45601 60683 29956 91713 66605 42832 03771 74718 98896 47694 42562 323H) 13862 13141 8^8 751/7 96779 62626 17725 62518 5@09 14528 79001 19997 37726 69456 77491 33261 31036 83316 oia@> 07706 55767 <3D38 46977 3320 81169 84235 33843 a^4o 46fiP 56527 13763 063 634 74625 3<@42 47398 54309 73159 143 17752 49326 64727 03509 72382 73099 <13693 56095 999 85278 40386 45537 87481 31302 833 39325 65995 18877 75296 f BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystess Division Product Registration Laboratory U Data Study Nuaber 4 O r t i -- 3 ___________ Sample Dunbar ____________ Test Substance f'S K JT JL -g _______ Teat Type: screen __ definitive t / STOCK SOLUTION PREPARATION Percent active ingredient (% AI) / j) *7e Noninal Concentrations corrected for % AI ? yes / no Balanced Used for Stock Solution Preparation _______________ Preparation Rotes: a , /~tH> /H tjte a A Jt, u* /to a d * < * 7 7 T! t a * * .,.- . b ----- Ul u H U jite t' bHLejLb etf? / m h Z2~>-- a b ti& n L , f i t e t u , It o j f i M - , / j L / ) u x j & L c i l i . H*L ' ________________________ <Pdl n j^/4 -' a A to flk L ie u 's*+ *a Jr M- ? ta g ________________ BevMee AraM Inc. SuUOioy ol MtiPODt 001657 tsr m m m i E lesource lulysti, Ine./ EaviroSystems Division Product Kegistratioa Daboratory U Data Study Number __________ Sample Number _____________ Test Substance ______ Test Type: s e r e e s __ definitive 1/ central unrowanoN Notes: /to a fjjjjc t,U > * jL /td d o c L __ ' f l t t M J A s tJ /X S IHAA id& d- A fc & t q, i H Q y ^ __________ /iA s tln M -L ______ __________ :--- g -j 'T u t A J L t e i l t i * M jL- *uA * u l J L 'f Z - . _______________________________________________________________ fe*> # J i ^ e a / n t /-//1?- kiM L. & L (Lj)q*1' JL /).6Stt jL < J 0 * i> o o 1 4 , & n t 4 ----------------- 2 ------ f tU * J U (k t 4 4 j* -d u i x c f d ^i -. ff-ta** ~ D .o & o t 1 i f l / l t P sulkjumJ -- L - p d j ^ - U ^ j E'wifoSfi'r ' i lc . z: V 'li:?C i 001658 BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystems Division Product Registration Laboratory Raw Data Study Kunber __________ Sanple Dumber ___________ Test Substance P n t- 3ft^Lc>______ Test Type: screen __ definitive / DAPHNID S0LDB1LITT Initiation Date- " ^ 0 ______ Test Organisn ~D- Test Insoluble Material Vessel - I.D. 0 hr 24 hr 48 hr Con 0 o / o 0D 0 3 0 0 .V 0 0 s 0b // Recorded by Date: // & /--* If no insoluble Material is observed enter a zero in the appropriate box. If insoluble material is observed enter a check mark in the appropriate box and describe the observation below. BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystens Division Product Registration Laboratory Raw Data Study Nunber 3 Sanple Nunber Test Substance 3 Test Type: screen definitive DAPHNID SURVIVAL AND SUBLETHAL EFFECTS Initiation Date / ' t f '* fO ________ y Page 1 of 2 Test Vessel I.D. Nunber of Live Dapbnids Rep. 0 hr 24 hr 48 hr Sublethal effects 0 hr 24 hr 48 hr 1 2. * *> 3 *7 4 *> 1 *5 2 / 3 5 4 1 *? 2 X 3 4 5 1 5 32 *> 3 r 4 *> Recorded by: Date: VfluJ iMn 5 ? *> 5y 55 M S' 5 5 ii-i-V y S' S' 5" S < 5" S 3 y * / s ft 00 6 0 O O 0o O 00 0S 0O 00 0 0 0 o 0 06 / 0d Q oc) o2_ 0 0 f 0 L3 ty n J ft U if- % J3 U-KW fiu U L O vl fU J l M * ! (Jesxrre AnotyOi mc.SubrrtorvdMy.>ocE 001660 8EST COPY AVAILABLE Resource Analysts, Inc./ EnviroSystems Division Product Registration Laboratory Raw Data Study Number -*_? Sample Number 4L, tr~ Test Substance / / t j y U d Test Type: screen __ definitive l / DAPHNID SURVIVAL AND SUBLETHAL EFFECTS Page 2 of 2 Initiation Date- *7_______ Test Organism ~2)- Test TfeitHikl I.D. 4 Jf Number of Live Daphnids Rep. 0 hr 24 hr 48 hr 1 `J 2 *9 3 *5 4 1 2 3 5 4 1 5 & fo *> 0 5Q JO 50 M0 H r> Sublethal effects 0 hr 24 hr 48 hr 0 00 0 O 0 n 0o o 00 o 0 0 0 , B5 2 3 4 Recorded by: Date: qfko et /Z'Ji.fi 7 ~ e*> W JC -f/j If no sublethal effects are observed enter zero in tbe appropriate box. If subletbal effects are observed enter the number effected in the appropriate box and describe the observation below. Mote*:___ 6 3 >*-'SK>~4d fitJUltUJt*/./ 1 & ifafaf Besouce Analyse Inc. Subndia dt MU.SOG 001661 BEST COPY AVAILABLE source Analysts, Inc./ EnviroSysteas Division Product Registration Laboratory Saw Data Study Nuaber __________ Sanple Jfunber oko*i(a E _________ Test Substance ('SX-3?Xi>______ Test Type: screen __ definitive lX'1' DAFHNID DISSOLVED OXYGEN CONCENTRATION AND pH Page 1 of 2 Initiation Date 4t>_______ Test Organisa D . /X A /h L ft_ Test Tm 1 I.D. Rep. Dissolve^Ox|gen (ag/L) 0 hr 24 br 48 br ~A 0 br 24 br 48 br /p cfivl .... / 3 Recorded by Date: 1 E'X' $5" 2 3 &$ 4 1[Sl y.'Sb fas )- r*? 3 r-3 f-l t* 4 V? ? t * 1 r/ yj 2 ra 3 s; Y^ 4 1 2 3 R 4 V *0 y-i -3 f a r-* *!> T V Of tl-ft-le o-no Tf %x n <(.X % ?x % K-X IK R 7-r XX fa4 ir-iv r-ie n !T-k ST-Ce n TV SJL fai, 1 4 f-Cr ri ro K'h v% <1 7-K u t(a f a K-l* 7X w u 7-f f a u 1% * k u Qv^> O/M < V u-ijHi1UfiflO ly^c fa jjtu * - lW x (z(< u Rm o u c b Analysts !nc. SubsOov at MUliPOfiE 001662 1S T COPY AVAILABLE Resource Analysts, Inc./ EnviroSysteas Division Product Registration Laboratory Rav Data Study Nuaber *3 Sanple Number Test Substance f / X 3 S a -& Test Type: screen __ definitive \ / DAPHNID DISSOLVED OXYGEN CONCENTRATION AND pH Page 2 of 2 Initiation Date ) ' / _______ Test Organisa 7?. n t Q A A ^ Test Vessel I.D. Rep. 1 42 $ .3 4 1 ....2. . 5 3 4 / / / / 1 2 3 4 Recorded by: Date: D i s s o l v ^ O x y g e n (ag/L) ________ p r _________ 0 hr 24 hr 48 hr 0 hr 24 hr 48 hr VX fr'3x U Pr-i Vb r-i n %> f-*7 n u t* uV-1 <5 7n k I17K*-r 7f Sv| Vw* r* Sx ffi'k, r-fc 1OijlmMj % Jim . V Notes: Qjjjju xjlq L j l U Resource Anovsti me. Sucsocr, oi vnuiPCRE 001663 B is u m m u m Resource Analysts, Inc./ EnviroSystems Division Product Registration Laboratory Raw Data Study Humber Test Substance ' 3 ____________ Sample Humber =2/^1t . t r '_________ 3 S a * e ________ Test Type: s c reen definitive\ J DAPHHID TEMPERATURE AHD COHDOCTITITT Page 1 of 2 Initiation Date J '/ f t _______ Test I.D. Temperature (C) Conductivity (umhos/cm) _____ fX L -S ____________ . 0 hr 24 hr 48 hr 0 hr 24 hr 48 hr 1 2 Oficfal 3 4 1 /2 3 4 1 2 3 4 1 32 3 4 Recorded by: Date: Mm J U o I J 8 0 } } o o \* o c M IXPMO 3J- \ m llo lo x an 3 Jto^ of Jo-1 \}0 0 Jno UO y * \W 0 ^00 l^ t O 15 o m lO l mi 204 2o r m JJ- JJo Jo (Mo JM iq IU T) \ \ 0Q i w iyt> IOO liO O IOV 2& \ J o .i m Ifto \lo o M % 2 0 % 7c. L UOD llC D IjOO JM 2 S ) 'l MM MS A lW o M } i 22c U MX M M Xi 0 .1 J 6.y 2 o. *i m Af %U-I-Il />^'A Q C t? BCO I2M ISO U no m X O b \ior> rlO \W O OO !UJQ OfkS % ll-Rfy 600 W ju WD *3o d _ wp 6 \) fj, W<> / 7^ Resource Anotytfv <nc SuOSCov ol MUFORf BEST COPY AVAILABLE Resource Analysts, Ine./ EnviroSysteas Division Product Registration Laboratory Raw Data Study Nuaber 3 Saaple Nuaber Test Substance /7K Test Type: s c r e e n __ definitive j / DAPBNID TEMPERATURE AND CONDUCTIVITY Page 2 of 2 Initiation Date ' / # ' ________ Test Organisa ))-i Test I.D. ii r y Rep. 1 2 3 4 1 2 3 4 1 Teaperature (C) Conductivity^(uahos/ca) 0 hr M M M M ft 3 I7 6i 24 hr M -% 30 r 0 .1 iofl 48 hr J J .fi JoM Jo Z io J0.f M Jo-*/ 0 hr 24 hr \}C D l $ > f?e0_ H f O 10 0 tw o OD HftD Ken ibC D ll D 110 0 JL W m io ifo) 48 hr l?W 1bCP 1400 tm m 10 Ity o 2 3 4 Recorded by: Date: C fb -s & l* 7 \x .fM o b x s 'r ,. Q J I H M * XA0 Notes: fijU L tU L t/.! i t i Reloue Artivi. Inc. Sutr-aioiy of MUJFORE 001665 BEST COPY AVAILABLE Resource Analysts, Inc./ EnviroSysteas Division Product Registration Laboratory Rav Data HARDNESS DETERMINATION Date Vater type al EDTA titrant ag CaCOs equivalent to 1.00 EDTA als saaple Hardness ag/1 as CaCOs By 001666 M w rm tifevre* Analysts, Zac./ EnviroSysteas Division Product Registration Laboratory Kaw Data Study Nuabar ~7 I ' -3__________ Saapla Muabar 6~---------- Test Substaace /> 3 g a a ________ Test Type: s c r e e n __ definitive itn i ERROR CODES I. Misspelled .2. Katbeaatical Error 3. Prong Entry 4. Transposition or Sequencing Error (inverted or wrong order) 5. Transcription Change (copy error) 6. Procedural Change 7. Prong Conclusion 8. Illegible Entry 9. Unnecessary Entry 10. Footnoted Explanation II. Additional Consent Env*roS>Vemt. !it "0016G7 *****************c**t******(****t***t** LC VALUES IT IS IMPORTANT THAT ALL RESULTS BE COMPARED WITH THE p h 2> ORIGINAL DATA TO SEE- IF THE RESULTS SEEM REASONABLE. MOST. IF NOT ALL. METHODS FOR CALCULATING LC50 VALUES PERFORM POORLY WITH SOME SETS OF DATA. ALTHOUGH MANY S PRECAUTIONS HAVE BEEN INCORPORATED INTO THIS PROGRAM, SOME QUESTIONABLE RESULTS MAY BE PRINTED WITHOUT A 4 f # - C LSD CAUTIONARY STATEMENT. -fio ******************************************************************* ' ******************************************************************* --BINOMIAL TEST- CONC. NUMBER NUMBER EXPOSED DEAD 50 20 20 25 20 10 10 20 3 5 20 3 1 20 4 THE BINOMIAL TEST SHOWS THAT 10 AND PERCENT DEAD 10O 50 15 15 20 50 CAN BE BINOMIAL PROB.(PERCENT) LESS THAN 0.001 58.8098 .1288413 .1288413 .5908963 USED AS STATISTICALLY SOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS BECAUSE THE ACTUAL CONFIDENCE LEVEL ASSOCIATED WITH THESE LIMITS IS GREATER THAN 95 PERCENT 25 CAN BE USED AS AN APPROXIMATE LC50 FOR THIS DATA SET ''T COPY AVAILABLi -------- RESULTS CALCULATED USING THE MOVING AVERAGE METHOD C *o Q ih (9 ( SPAN G -fcCSO 95 PERCENT CONFIDENCE LIMITS 4 7.809S02E-02 15.58225 10.89568 23.84768 3 8.009978E-02 17.89105 13.92568 23.48557 2 .0864314- 20.97725 16.68199 25.78795 1 .7002976 25 16.9624 313.4993 AN LC50 CALCULATED USING THE MOVING AVERAGE METHOD MAY NOT BE A VERY GOOD ESTIMATE IF THE SPAN IS MUCH LESS THAN THE NUMBER OF CONCENTRATIONS. IF ANY HIGHER CONCENTRATION PRODUCES A LOWER PERCENT DEAD THAN A LOWER CONCENTRATION, THE CONFIDENCE LIMIT AS OBTAINED BY THE MOVING AVERAGE METHOD WILL PROBABLY BE TOO CLOSE. -------- RESULTS CALCULATED USING THE PROBIT METHOD------------- ITERATIONS G H CHI-SQUARE PROBABILITY 4 3.296692 7.061959 21.18588 LESS THAN 0.001 BECAUSE THE PROBABILITY IS LESS THAN 0.05. RESULTS CALCULATED USING THE PROBIT METHOD PROBABLY SHOULD NOT BE USED. SLOPE 1.295843 95 PERCENT CONFIDENCE LIMITS ** -1.056992 AND 3.648677 POINT CONC LOWER UPPER 95i: CONFIDENCE L '-IITS 001668 BEST COPY AVAILABLE <**************************************, ------------------ --- LC VALUES-------------------- t o m - 2> r IS IMPORTANT THAT ALL RESULTS BE COMPARED WITH THE 4grtc.eT> RIGINAL DATA TO SEE IF THE RESULTS SEEM REASONABLE. OST, IF NOT ALL. METHODS FOR CALCULATING LC50 VALUES SRFORM POORLY WITH SOME SETS OF DATA, ALTHOUGH MANY RECAUTIONS HAVE BEEN INCORPORATED INTO THIS PROGRAM, OME QUESTIONABLE RESULTS MAY BE PRINTED WITHOUT A AUTIONARY STATEMENT. jw */*// t***************************************************************** ****************************************************************** BINOMIAL TEST- ONC. NUMBER NUMBER PERCENT BINOMIAL EXPOSED DEAD DEAD PROB.(PERCENT) 150 20 20 lOO LESS THAN 0.001 100 20 20 100 LESS THAN 0.001 60 20 14 70 5.765907 40 20 6 30 5.765907 25 20 0 0 LESS THAN 0.001 HE BINOMIAL TEST SHOWS THAT 25 AND 100 CAN BE iSED AS STATISTICALLY SOUND CONSERVATIVE 95 PERCENT 'ONFIDENCE LIMITS BECAUSE THE ACTUAL CONFIDENCE LEVEL ASSOCIATED WITH THESE LIMITS IS GREATER THAN 95 PERCENT AN APPROXIMATE LC50 OF 48.98977 IS OBTAINED BY IONLINEAR INTERPOLATION BETWEEN 40 AND 60 -RESULTS. CALCULATED USING THE MOVING AVERAGE METHOD---- PAN G LC50 95 PERCENT CONFIDENCE L A .042276.6 50.3058 43.4101B 57.25496 3 5.480177E--02 49.29081 43.61243 55.76042 *!> .1234816 48.98979 39.82044 56.50342 n .1234816 48.98979 42.74617 59.71668 4 4 .6117131 48.98977 37.98345 63.18534 AN LC50 CALCULATED USING THE MOVING AVERAGE METHOD MAY NOT BE A VERY GOOD ESTIMATE IF THE SPAN IS MUCH LESS THAN THE NUMBER OF CONCENTRATIONS. RESULTS CALCULATED USING THE PROBIT METHOD------------- ITERATIONS-' G H CHI-SQUARE PROBABILITY 5 .1496121 1 1.004782 .8000948 SLOPE = 7.77544 95 PERCENT CONFIDENCE LIMITS - 4.767922 AND 10.78296 P01 (rtu 50 CONC 4.0 3 6 6 4 LOWER UPPER 95*/. CONFIDENCE LIMITS 43.25647- 55.85722 001669 'i - n M i n kMU M r c i f PRODUCT CODE: F-7082C M-382 F -7460 KA*jfc I OF 2 91.0604 MATERIAL DESIGNATION: ISSUE OATE: 9/17/1987 SUPERSEDES: 05/28/86 FLUOROCHEMICAL SALT 3M 1.0. NUMBER: 41-2600-7082-0; 41-2700-3820-5: 41-2600-7460-8 NFPA DIAMOND CODE: HEALTH: 1 FIRE: 2 REACTIVITY: 0 OTHER: NO FOR 24-HOUR EMERGENCY INFORMATION ON HEALTH EFFECTS CALL: (612J733-2882 1. INGREDIENTS CAS NUMBER * T L V ( R )tUNIT) OIETHYLENE GLYCOL MONOBUTYL ETHER* WATER FLUOROCHEMICAL SALT 112-34-5 CA 36 7732-18-5 CA 36 2795-39-3 28 NONE NONE NONE BEST COPY AVAILABLE SUBJECT TO SECTION 313 SARA TITLE III 2. PHYSICAL DATA BOILING POINT: >212 DEG F SOLUBILITY IN WATER: SOLUBLE VAPOR PRESSURE: <18NM@RT SPECIFIC GRAVITY(H20=1): 1.08 VAPOR DENSITY!AIR=1) NO PERCENT VOLATILE: 72% EVAPORATION RATE: NO VISCOSITY: <100 CPS PH: 10-10.5 APPEARANCE ANO OOOR: SLIGHT TINTED LIQUID; BUTYL CARBITOL ODOR 3. FIRE AND EXPLOSION HAZARD DATA FLASH POINT!TEST METHOD): 172 DEG F. MIN.(CC)(EST.) FLA.LMT. LEL:NO UEL:ND EXTINGUISHING MEDIA: FOAM, DRY CHEMICAL, C02, WATER FOG. SPECIAL FIRE FIGHTING. PROCEDURES: NONE UNUSUAL FIRE AND EXPLOSION HAZARDS: NONE EXPECTED. BUT SEE ALSO SECTION 7. 4. PRECAUTIONARY INFORMATION WEAR FULL FACE SHIELD. WEAR IMPERVIOUS GLOVES. PRODUCT CODE: F-7082 FM-3820 F-7460 PAGE 2 OF 2. 5. HEALTH HAZARD DATA ! EYE CONTACT: CAUSES IRRITATION ON CONTACT. SKIN CONTACT: MAY CAUSE IRRITATION. DRYING AND CRACKING ONPROLONGED OR i REPEATED CONTACT. MAY BE A8S0RBED THROUGH THE SKIN. INHALATION: *== 1 INGESTION: MODERATELY TOXIC ON INGESTION. ; i SUGGESTED FIRST AID ; E YE C O N T A C T : I M M E D I AT E L Y FL U S H WITH LARGE AMOUNTS OF WATER FOR AT LEAST TEN t MI NUTES AND G E T MEC ICAL ATTENTION. i -! SKIN CONTACT; REMOVE CONTAMINATED CLOTHING. LAUNDER BEFORE RE-USE. WASH A F F E C T E D s k i n a r e a WITH SOAP AND WATER.DISCARD `NTAMINATED ! i INHai. 7 ION : [ N O S ' 7 TON : SHOE : VND G L O V E S . GIVE WATER OR Mfl.S * 0 G E T ME D I C A L * " E r l T I-Vrl IMm ED I A 7 El. ' . 001070 | BEST m AVAILABLE SPILL RESPONSE: OBSERVE PRECAUTIONS FROM OTHER SECTIONS. USE APPROPRIATE ABSORBENT MATERIAL AS NEEDED IN CLEANUP PROCEDURE. COLLECT SPILLED MATERIAL. CLEAN UP RESIDUES WITH WATER. PLACE IN AN APPROVED METAL CONTAINER AND SEAL. RECOMMENDED DISPOSAL: SEND TO 3M CHEMOLITE PLANT - BLDG. k 7 , OR TO A 3M APPROVED CHEMICAL WASTE DISPOSAL FACILITY FOR DISPOSAL. ENVIRONMENTAL DATA: SEE 1NON-REGULATED CHEMICALS* IN 3M WASTE DISPOSAL PROCEDURES MANUAL FOR LABELING/MARKING/PACKAGING/SHIPPING DATA. HAZARDOUS WASTE NUMBER/COOE: NONE 7. REACTIVITY OATA STABILITY: STABLE (CONDITIONS TO AVOID): NO INCOMPATIBILITY: === (MATERIALS TO AVOID): NO HAZARDOUS POLYMERIZATION: WON'T OCCUR (CONDITIONS TO AVOID): NA HAZARDOUS DECOMPOSITION PRODUCTS: HF. INFORMATION ON THIS DATA SHEET REPRESENTS OUR CURRENT DATA AND BEST JUDGEMENT AS TO THE PROPER USE AND HANDLING OF THIS PRODUCT UNDER NORMAL CONDITIONS. 001671 BEST COPY AVAILABLE W l -3 PRODUCT REGISTRATIMI LABORATORY EQUIPHEBT IRSPECTIO LOC nth 7 \ P /x J > L L ^ __________ Tear 1 * * 0 ------------- - Check ii Operation normal Say of Air Em. Has. Booth Bl. Gen. PH HVAC L&T T.S. Deionizer Lit Repl Rotes 1 z Z _ z tZ z 2 IZ z 3 Z z: ZZ 4 z. z (X 5 6 7 z Zz z x/ i/ z z -Z z z Z 1z y ^y . y /2|2-7-1, S V/ \ Z t Z w'' zz 9 c. -- O' z 10 <z z . v/ y Z 11 j Z Z z z zz 12 I Z .Z ^Caii'ie-*r- 13 Z t-/ z z tZ Z ' 14 15 Z z Z V v< S' Zz z i x ,/ z ,z 16 z </ Z z 17 18 z z z z z z zz z Z' y19 z Z l/ 20 z /z zz 21 22 23 24 jZ u z _ z -- _. -- w- tZ , / , z z Vz- Z __ __-_ ./ y ' 25 z z z z ~ls 26 27 28 29 30 z zz _z ' <-- iz" U-' _z zz __ iz z fa' z z y y --- t---- 31 hZ v/ z z z By/Date 63 IJL-I-^O g-> g a /j-6 -To S' g-s /*--* iz-n-V__ u-z-tv A />-Mm___ ^3 n - n t- h , S' __ 'g-*> rx-oc-'TO arfc. /-A/-Ve fo-A Pj 6 i Tt /g-Jyr-^O g-a 11.1-10 y^fX-Jg^o 'aw fw.tr-to /t/a> fio 63 zquipkent codes THIS ISA CERTIFIED TRUE COPY- Air Bl. - Air Blower SIGNATURE <a .DATE_uB<jj I*. Gen. - Emergency Generator L et me Lights and Timers VMft Heating, Ventilating and Air Conditioning Systen PH Pune Hood 'fas. T.S. - Vaste Treatment System Deionizer - Check "Lit" if both lights are illuminated, and check "Repl" if the unit was replaced ReioweeAndys,me.Suwoov OMUFOOE 001672 mum mum Month PRODUCT REGISTRATION LABORATORY EQUIPMENT INSPECTION LOG D lP /.m J jU -____________ Tear_______________________________ EQUIPMENT CODES CR culture roon flesouce Anoiysfi me. SubsOiay of MUJPOK 001673 BEST COPY AVAILABLE PRODUCT REGISTRATION LABORATORT EQUIPMENT CALIBRATION LOG Month '~ 7 \r S ,n < n s ^ Year /a d o Ilissolved pE Condtict- Salinity Refract- Day Oxygen of 1leter: irit:y ometer met:er: - V meter: Pi(l -9 meter:___ no.: fCt-L Mo. c Theo Act pS 4 pH 7 pHIO Theo Act Theo Act Theo Act By ! *- /S'" d /V' it, - w *\ 6j (</ n TS 4 //> 7-0 it \\ |2- i*r 1? c> ( f /? Iff k 1 I f nr 1$ n I 41 /f 2) M ??- K? A?> S o *a V i O If Zfr I f if it K /4 30 19 JLL. if3 q .< 4 .! f & <? %3 ?-3 Vt 4.1 <?.!> ?.? Ti *;.=; 4-1 *.*r *5 T.-r fS 46 n 9.3 * ./ 9A 1*7 4-7 7-7 <f7 TT fr 95 r> r-r 4- f- <?.*> 4.3 46 Qt 7 f *r ?,< Tb T- 4.5 4. #e f ^ x - Vi.pL J .tt4 s ' n?6 Lh -A/ **< V0 1b.A1 iff * f.M *n V a A siJ X Lxr /A on V-flO 1.0 5 IfTXJ* Innfi / rtr J _^ -24 -Uf> JO *4 2a Za 7-flO /rt-03 I.UO IDOL) '___ 7 0 2 0 0-<7 lsr> '-ono 1 .0 0 0 *f-OJ 7.82 l*.T V ^ o 7>k 1.9O* S ' f-o>0 s s f a 2d X. W V.*>* Li** /./an e*n v<*> l o t /05 U * n .0 0 0 __ 70 7d 4.00 n jti- 1-n n u \-O C V ^__ 7 0 2 t7 9-t/l/ lo o ln # f I<XXj u n c o ___ 2n z</ Vjo f** l . i f o l.bD t) J l> 02X1 7-00 ttjsrt UlCi /- a u . s s 3d 'if 4 0 J Tflf r ttfi HMD s' / 4n6 7.8^ ttM . f.wtm /Mf% / s 7VA In n a t.r m s 7n 2e) A\ 0 2 0 2er fjbO >01 W /.OOP lo u o s ' 70 9 9-60 Iff'- lo - fj i-OO /i/6 l.a n n until s t-O bO ' 2 0 2b s ' 70 UJX> "7.01 root lo r e sr> dO Hco 7-cy .ot lar ff9 ? D t.tid T-gT O-oJ 1-trfO l-tm , s f S ' JO f.tb f.HT l-eeo /Ova J o -Vv 9. nil 7 -Z1 V la-61, 1.01)0 ISXJis Tel ai. J .fn /4>Ut> s ' 2U Jo tw o Ttfl 1.909 1-000 ____ ^ 2 0 l<3 it* 7*r (<xz> (.OB/ Y.e* 7a} l**T f.eoc ( 0 0 0 / T4 zj / z*c 70 ./1 1-10 AM j ia w c s ' -2c g C g6 cL , _ d ___ p< pt^ --. .^3 <. *fH y~ C fu s 4* Ob e-i Q ns k*> OflAS ltd iu ) Theo theoretical 7alue Act * actual value measured by the instrument Thermometer calibration: Measured value (C) thermometer no.: HBST>cia n M U K - 1411 ItIS 72lS 7.UI U U n X 7 h t temperature 1JJ_5_ temperature 2 ' ih5_ JiiL H i ILL 25L Zt-.l US L. ILL L M \A L l_ 1 3 _ M _ lS _ J j_ JL_ 1 _ J S.t+41' 1 -vp- > O' ivjy : izi 2lt6 ^1 5 at.'S l-i ; t 1.4 Of ^ *-* ff BmoiKeAnolylflinc.SuCiieoyolMUIPORE 001674 iJUiiiiimuiw m iJ U i BEST COPY AVAILABLE PRODUCT REGISTRATION LABORATORY EQUIPHENT INSPECTION LOG Month-- ~]y/'i'.iyJ)ZA__________ T e * r _ _ Z l l _________________ w lji. w w ^w ^ii.W Jimn im aiihmh/hlji Iiiup u ,. EQUIPMENT CODES RT * room temperature sample storage area CR culture room FR freezer g)pe aivtt On u-lHi J* VjUwdi M><.t A t Wfc d'.ttT i<tr t. wk. jt in lao.VC.ff> U - J cW*oyJ. prwt *vt stujet-r tz tjt* M-t \oW a* *fUr *-jt** l.) fuarilti.. <l/M irnstkr N $W***T art ft'rt-H f t e : TQ-u-Vb TH'S 3A CERTIFIED TRUE COPY. SIGNATURES^ DATE0)03^I U lR illU U I)JI|p il!.p B |lli|||, I|i i J ! W i l j p p y R 8 ^ p |i p ^ ||p ||^ |g |i ||^ j p p |||p p p |p p || RAI BEST copy AVAILABLE Tall'J SufcScsyeiMUVCIE ?.0 .8 c 7 7 8 .0 w to B>m feed Msras=e<vNJ.C3H2 C3J 926-7777 Mr. Timothy Ward EnviroSysterns, Incorporated P.O. Box 778 Hampton. NH ' 03842 P.O. Number! 2537 Date Received: 08/29/90 (1320) Lab Number: 23.394 Date Reported: 10/10/90 Attached please find test results for ammonia, total organic carbon, aluminum, arsenic, boron, cadmium, chromium, cobalt, copper, iron, lead, mercury, nickel, silver, zinc, fluoride, total suspended solids, pesticides/PCBas . Samples were received in acceptable condition. All samples were prepared and analyzed within the holding times specified in the referenced methods. \ Instrumentation used for analysis was calibrated and/or tuned with the appropriate frequency and to the appropriate specifications required by the referenced methods. Blank contamination was not observed at levels affecting the analytical results. Matrix effects, as monitored by matrix spike recovery, unusual physical properties and/or surrogate analyte recovery, were not apparent. Accuracy and precision, as monitored by laboratory control sample analyses, were within laboratory acceptance limits. RESOURCE ANALYSTS. INCORPORATED (M U i, Authorized Signature^^ THiStS A CERTIFIED TRUE COPY.,, SIGNATURE ___ . DATE i> D in /io /C O Date 001676 Field Identification: 2597-7 Laboratory Number: 23394-7 Parameter Total Suspended Solids (mg/L) ConcernIration <10 .. Matrix: Vater Date Analysed 08/30/90 Method/Ref. 160.2/1 Field Identification: 2597-8 Laboratory Number: 23394-8 Parameter Ammonia (mg/L as N) Concentration <0.2 Matrix: Water Date Analysed 09/04/90 Method/Ref. 350.2/1 Field Identification: 2597-9 Laboratory Number: 23394-9 Parameter Total Organic Carbon (mg/L) Concentration <1.0 Matrix: Water Date Analysed 08/30/90 Method/Ref. 415.1/1 Field Identification: 2597-10 Laboratory Number: 23394-10 Parameter Aluminum, total (ng/L) Arsenic, total (mg/L) Boron, total (mg/L) Cadmium, total (mg/L) Chromium, total (mg/L) Cobalt, total (mg/L) Copper, total (mg/L) Iron, total (mg/L) Lead, total (mg/L) Mercury, total (mg/L) nickel, total (mg/L) silver, total (mg/L) Zinc, total (mg/L) Concentration 0.04 <0.002 0 .1 0^0005 <0.002 <0.008 <0.005 0.03 0.003 0.0002 <0.008 <0.0005 <0.005 Matrix: Water Date Analysed 09/07/90 09/03/90 09/07/90 09/29/90 09/07/90 09/07/90 09/07/90 09/07/90 09/03/90 08/31/90 09/07/90 09/28/90 09/07/90 Method/Ref. 3010,6010/2 7060/2 3010,6010/2 3010,6010/2 3010,6010/2 3010,6010/2 3010,6010/2 3010,6010/2 3020,7421/2 7470/2 3010.6010/2 3010,6010/2 3010,6010/2 Beiouice Ap o w . inc. S t n eo y oi MUJSE 001677 ^ C B P Y A V fiiu m iE Field Identification: 2597-11 Laboratory Number: 23394-11 Parameter Fluoride (mg/L) Concentration o .io Matrix: Watar Date Analyzed 08/30/90 Method/Kef. 340.2/1 Field Identification: 2597-14 Laboratory Number: 23394-14 Parameter Total Suspended Solids (mg/L) Concentration <10 Matrix: Water Date Analrzed Method/Ref. 08/30/90 - 160.2/1 Field. Identifications- 2597-15 Laboratory Number: 23394-15 Parameter Ammonia (mg/L as N) Concerntration <0.2 Matrix: Water Date Analyzed 09/04/90 Method/Ref. 350.2/1 Field Identification: 2597-16 Laboratory Number: 23394-16 Parameter Total Organic Carbon (mg/L) Concentration <2.0 Matrix: Water Date Analrzed 08/30/90 Method/Ref. 415.1/1 DcxuaArCiAinc.SuMioyolMUfOK 00167S BEST COPKAVAILABLE Laboratory-number: 23394 -012 Sample Designation: 2597-12 Date Analyzed: 09/08/90 Matrix: HATER PESTICIDES/PCB'S ALDRIN ALPHA-BHC BETA-BHC GAMMA-BHC DELTA-BHC CHLORDANE 4,4'-DDT 4,4'-DDE 4,4'--DDD DIELDRXN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN ENDRIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOXIDE PCB--1242 PCB--1254 PCB--1221 PCB--1232 PCB--1248 PCB--1260 PCB--1016 TOXAPHENE ENDRIN KETONE METHOXYCHLOR CONCENTRATION (ug/L) BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL DETECTION LIMIT (ug/L) 0.06 0.06 0.06 0.06 0.06 .6 .1 0.06 .1 0.06 0.06 .1 .1 0.06 .1 0.06 0.06 .6 .6 .6 .6 .6 .6 .6 2 .1 .6 METHOD REFERENCE: 40 CFR PART 136, FRIDAY, OCTOBER 26, 1984 METHOD 608 BDL - Below detection U n i t n o u e* Arevsn k>c. SubnOoy of MUS0OE BEST COPY AVAILABLE Laboratory Nuabar: Saapla Daaignatloa: Dato Extractad: Data Analyzad: Matrix: 23394-13 2597-13 09/11/90 10/04/90 WATER PESTICIDES CONCENTRATION (ag/L) AZINPHOS METHYL"' BOLSTAR CHLORFYRIFOS COUMAPHOS DEMETON-O DBMBTON-S DIAZINON DICHLORVOS DISOLFOTON ETHOPROP FENSOLFOTHION FENTHION MERPHOS MEVINPHOS NALED PARATHION METHYL PHORATB RONNEL STIROPBOS (TETRACHLORVINPBOS) TOKUTHION (PROTHIOFOS) TRICHLORONATE BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL u DETECTION LIMIT (ug/L) 1.5 0.15 0.3 1.5 0.25 0.25 0.5 0.1 0.20 0.25 1.5 0.10 0.25 0.3 0.1 0.03 0.15 0.3 5.0 0.5 0.15 BDL - BELOW DETECTION LIMIT METHOD REFERENCE OS SPA METHOD 8140 taounM m incSuM itforircIM U IO it 001680 KSTm m m E X u e s m tolysti, Zac / ZnviroSyste** Virisia* Prodect Regi*tration hlortUr; " c n n o r cos to pt r o t i 'S t e d y H u n b cr: D a ta S a p le d : 2sv ? la u S a n p le d * 1! fk t J c C r dhjt^Gi-y N o te s : Gct\c*cX+.-c*X. f i d k c f n j v i ^ V v .+5 S u p le * Id e n tific a tio n N oeber and S lz e o f C o n ta in e ra te n a ri* tu S u p le R om bar 2 M '7 * ** <a * * m -1 -1 -3 -L -7 -s ~T ~(o 'il --IHn | 0*4 W | yaf 1 Se** P * J 5; * < p u i v i TO C kW J F o * * - ' ! * JH 1 II jK * p M PcBS I lf~i fki**. t 5 > 1 ja s * ,i jM l / U o o u a | <^k$5 T O C | f p u K t p * .fc js | - t fim i | . I L 5U S 5 Plurali t f r t t w d cA^AV < # 1P e s i - * pc< J* 1 U * * > p O 'i - S n r-` T 55 U/ i l 2 3 ^ k jc (( <s 2 3 r 7 8 r p n IZ. >S IH,JHW.W ..limiw m w i i un.WIPW WMPM!MIeBUiwe ni>8WnS MBWB P i e B M i g l ^ ^ R e lin a u is b e d by R e lin a u isb e d bv D a te D a te T ie e R e c e iv e d b v D a te T ie e T ie e R e c e iv e d b v 8 <H4o D a te J320 T ie e Dm c k c * ----------- T W O IO A O C n T I P I E P W i . SuOvCo y oW' . -- -- 31 2S I G N A T U R E J & . D A T E J J P ^ BEST COPY AVAILABLE l PRODUCT RXGISTRATIOIf LABORATORY SAMPLE RSCEZTZR6 LOO 1. - RAI Saaple Number - 2 { 2. Sponsor Naae and Address 3/YV Vu/- Ift.6 &l.<*. 2-3C-O S 935" -<SSL AJc. -- ' ... '911fr-- 1P 3. Sponsor Sample Identification . M N _____S S t Q i _________________ M HMi-6 F M 3X30 4. Sample Container Label Data U F/*J1XO S. Date Received- l^-tlS.-fo 6. Date Photographed 1. Method of Shipment Shipped From S* . PftJ 1 /V\/0 Yia P^J.xr vJe<kcC*.v 8. Description of Shipping Container(s) (Nuaber, Type, Size) 1 plA,i tn i r _________ 9. Description of Sample Containers(s) (Number, Type, Size) 1 JLSO jlfcS5 boffu. 10. Staple Storage Location and Required Storage Conditions p a.1 - >5~ *j**U~p 11. Signature . _________________ Date i H L - l a 12. Notes 13. Date and Location of Archive Staple Renoval and Storage Location. ___________ )176-90 _______________________________________ THISISA CERTIFIED TRUE COPY. SIGNATURE DATE 3iV 0 0 1 6 S 2Oesouice Aoctyin. >nc. Sufcjocr# e-vnUPOC BESTCOPY AVAILABLE !ha>*iVPC/ Tk phfffctcyJr* jfor. p jf djfa* /YSld- fa JU o f f e f ft*L /S H fk fa h k W iJ - -po lim b o 7 -y>~W Ir u vunfrlED TSIRGUNEACTOUPRYE.^ a D A T E O ^ ^ ; Btsouc Ano* nc. S u tad o y et MUPOBE 001683 BEST COPY AVAILABLE o sa a fti-a v i H Z W 4-4 F 3S20 iHiSISACEOTlFlED. T . ... TRUE COPY... SIGNATURE_QjA^DATE^36fdf Ul p Q . ^ M TF.SIS A CERTIFIED TRUE COP"/. SIGNATUREbf&vi DATEQTPPC) 001654